B.08 GFI SJAFB RW502 Raw Lab Data_Jan 2023.pdf

02/06/23

Technical Report for

AECOM, INC.

Seymour Johnson AFB RW502; Goldsboro, NC

60417848

SGS Job Number: FC1821

Sampling Date: 01/06/23

Report to:

AECOM, INC.

12120 Shamrock Plaza Suite 100 Omaha, NE 68154 jeff.aust@aecom.com; jared.desadier@aecom.com;

paul.m.wilson@aecom.com ATTN: Paul Wilson

Total number of pages in report:

Certifications: FL(E83510), LA(03051), KS(E-10327), NC(573), NJ(FL002), NY(12022), SC(96038001)

DoD ELAP(ANAB L2229), AZ(AZ0806), CA(2937), TX(T104704404), PA(68-03573), VA(460177), AL, AK, AR, CT, IA, KY, MA, MI. MS, ND, NH, NV, OK, OR, IL, UT, VT, WA, WI, WV

This report shall not be reproduced, except in its entirety, without the written approval of SGS.

Test results relate only to samples analyzed.

SGS North America Inc. • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: 407-425-6700 • fax: 407-425-0707

Test results contained within this data package meet the requirements of the National Environmental Laboratory Accreditation Program and/or state specific certification programs as applicable.

Client Service contact: Muna Mohammed 407-425-6700

Norm Farmer Technical Director

Orlando, FL 02/06/23 e-Hardcopy 2.0 Automated Report

SGS is the sole authority for authorizing edits or modifications to this document.

Unauthorized modification of this report is strictly prohibited.

Review standard terms at: http://www.sgs.com/en/terms-and-conditions

The results set forth herein are provided by SGS North America Inc.

Please share your ideas about how we can serve you better at:

EHS.US.CustomerCare@sgs.com

FC1821

mailto:EHS.US.CustomerCare@sgs.com?subject=Customer care improvement idea (report FC1821)

Table of Contents -1-

Sections:

Section 1: Sample Summary Section 2: Summary of Hits Section 3: Sample Results

3.1: FC1821-1: IW-3-0123

3.2: FC1821-2: TW-1-0123

3.3: FC1821-3: DUP-1-0123

Section 4: Subcontract Lab Data Section 5: Misc. Forms

5.1: Certification Exceptions (DOD) 5.2: Chain of Custody

SGS North America Inc.

Sample Summary

AECOM, INC.

Job No: FC1821

Seymour Johnson AFB RW502; Goldsboro, NC Project No: 60417848

Sample Collected Matrix Client Number Date Time By Received Code Type Sample ID

FC1821-1 01/06/23 09:59 TB 01/11/23 AQ Ground Water IW-3-0123

FC1821-2 01/06/23 12:35 TB 01/11/23 AQ Ground Water TW-1-0123

FC1821-3 01/06/23 08:00 TB 01/11/23 AQ Ground Water DUP-1-0123

FC1821-4 01/06/23 00:00 TB 01/11/23 AQ Trip Blank Water TRIP BLANK

Summary of Hits Page 1 of 1 Job Number: FC1821 Account: AECOM, INC.

Project: Seymour Johnson AFB RW502; Goldsboro, NC Collected: 01/06/23

Lab Sample ID Client Sample ID Result/ Analyte Qual LOQ LOD Units Method

FC1821-1 IW-3-0123

Benzene 1.1 1.0 0.50 ug/l SW846 8260D Naphthalene 2.1 J 5.0 2.0 ug/l SW846 8260D C9-C18 Aliphatics 129 J 190 97 ug/l MADEP EPH REV 2.1

FC1821-2 TW-1-0123

C11-C22 Aromatics (Unadj.) 98.1 J 190 97 ug/l MADEP EPH REV 2.1 C9-C18 Aliphatics 107 J 190 97 ug/l MADEP EPH REV 2.1

FC1821-3 DUP-1-0123

Benzene 1.1 1.0 0.50 ug/l SW846 8260D Naphthalene 1.8 J 5.0 2.0 ug/l SW846 8260D C11-C22 Aromatics (Unadj.) 78.1 J 190 97 ug/l MADEP EPH REV 2.1 C9-C18 Aliphatics 112 J 190 97 ug/l MADEP EPH REV 2.1

Sample Results

Report of Analysis

Orlando, FL Section 3

Report of Analysis Page 1 of 1

Client Sample ID: IW-3-0123

Lab Sample ID: FC1821-1 Date Sampled: 01/06/23

Matrix: AQ - Ground Water Date Received: 01/11/23

Method: SW846 8260D Percent Solids: n/a

Project: Seymour Johnson AFB RW502; Goldsboro, NC

File ID DF Analyzed By Prep Date Prep Batch Analytical Batch

Run #1 1A42654.D 1 01/12/23 17:41 KG n/a n/a V1A1711

Run #2

Purge Volume

Run #1 5.0 ml

Run #2

CAS No. Compound Result LOQ LOD DL Units Q

71-43-2 Benzene 1.1 1.0 0.50 0.31 ug/l

91-20-3 Naphthalene 2.1 5.0 2.0 1.0 ug/l J

CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits

1868-53-7 Dibromofluoromethane 100% 83-118%

17060-07-0 1,2-Dichloroethane-D4 94% 79-125%

2037-26-5 Toluene-D8 104% 85-112%

460-00-4 4-Bromofluorobenzene 95% 83-118%

U = Not detected LOD = Limit of Detection J = Indicates an estimated value

LOQ = Limit of Quantitation DL = Detection Limit B = Indicates analyte found in associated method blank

E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound

FC1821

3.1

Client Sample ID: IW-3-0123

Lab Sample ID: FC1821-1 Date Sampled: 01/06/23

Matrix: AQ - Ground Water Date Received: 01/11/23

Method: MADEP EPH REV 2.1 SW846 3510C Percent Solids: n/a

Project: Seymour Johnson AFB RW502; Goldsboro, NC

File ID DF Analyzed By Prep Date Prep Batch Analytical Batch

Run #1 NN041090.D 1 01/14/23 14:13 AF 01/12/23 06:10 OP94954 GNN1891

Run #2

Initial Volume Final Volume

Run #1 1030 ml 2.0 ml

Run #2

MAEPH List

CAS No. Compound Result LOQ LOD DL Units Q

83-32-9 Acenaphthene 1.9 U 3.9 1.9 1.9 ug/l

208-96-8 Acenaphthylene 1.9 U 3.9 1.9 1.9 ug/l

120-12-7 Anthracene 1.9 U 3.9 1.9 1.9 ug/l

56-55-3 Benzo(a)anthracene 1.9 U 3.9 1.9 1.9 ug/l

50-32-8 Benzo(a)pyrene 1.9 U 3.9 1.9 1.9 ug/l

205-99-2 Benzo(b)fluoranthene 1.9 U 3.9 1.9 1.9 ug/l

191-24-2 Benzo(g,h,i)perylene 1.9 U 3.9 1.9 1.9 ug/l

207-08-9 Benzo(k)fluoranthene 1.9 U 3.9 1.9 1.9 ug/l

218-01-9 Chrysene 1.9 U 3.9 1.9 1.9 ug/l

53-70-3 Dibenzo(a,h)anthracene 1.9 U 3.9 1.9 1.9 ug/l

206-44-0 Fluoranthene 1.9 U 3.9 1.9 1.9 ug/l

86-73-7 Fluorene 1.9 U 3.9 1.9 1.9 ug/l

193-39-5 Indeno(1,2,3-cd)pyrene 1.9 U 3.9 1.9 1.9 ug/l

91-57-6 2-Methylnaphthalene 1.9 U 3.9 1.9 1.9 ug/l

91-20-3 Naphthalene 1.9 U 3.9 1.9 1.9 ug/l

85-01-8 Phenanthrene 1.9 U 3.9 1.9 1.9 ug/l

129-00-0 Pyrene 1.9 U 3.9 1.9 1.9 ug/l

C11-C22 Aromatics (Unadj.) 97 U 190 97 78 ug/l

C9-C18 Aliphatics 129 190 97 49 ug/l J

C19-C36 Aliphatics 97 U 190 97 49 ug/l

CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits

3386-33-2 1-Chlorooctadecane 60% 40-140%

580-13-2 2-Bromonaphthalene 91% 40-140%

84-15-1 o-Terphenyl 78% 40-140%

321-60-8 2-Fluorobiphenyl 84% 40-140%

U = Not detected LOD = Limit of Detection J = Indicates an estimated value

LOQ = Limit of Quantitation DL = Detection Limit B = Indicates analyte found in associated method blank

E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound

FC1821

3.1

Client Sample ID: TW-1-0123

Lab Sample ID: FC1821-2 Date Sampled: 01/06/23

Matrix: AQ - Ground Water Date Received: 01/11/23

Method: SW846 8260D Percent Solids: n/a

Project: Seymour Johnson AFB RW502; Goldsboro, NC

File ID DF Analyzed By Prep Date Prep Batch Analytical Batch

Run #1 1A42656.D 1 01/12/23 18:15 KG n/a n/a V1A1711

Run #2

Purge Volume

Run #1 5.0 ml

Run #2

CAS No. Compound Result LOQ LOD DL Units Q

71-43-2 Benzene 0.50 U 1.0 0.50 0.31 ug/l

91-20-3 Naphthalene 2.0 U 5.0 2.0 1.0 ug/l

CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits

1868-53-7 Dibromofluoromethane 99% 83-118%

17060-07-0 1,2-Dichloroethane-D4 93% 79-125%

2037-26-5 Toluene-D8 103% 85-112%

460-00-4 4-Bromofluorobenzene 93% 83-118%

U = Not detected LOD = Limit of Detection J = Indicates an estimated value

LOQ = Limit of Quantitation DL = Detection Limit B = Indicates analyte found in associated method blank

E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound

FC1821

3.2

Client Sample ID: TW-1-0123

Lab Sample ID: FC1821-2 Date Sampled: 01/06/23

Matrix: AQ - Ground Water Date Received: 01/11/23

Method: MADEP EPH REV 2.1 SW846 3510C Percent Solids: n/a

Project: Seymour Johnson AFB RW502; Goldsboro, NC

File ID DF Analyzed By Prep Date Prep Batch Analytical Batch

Run #1 NN041091.D 1 01/14/23 14:42 AF 01/12/23 06:10 OP94954 GNN1891

Run #2

Initial Volume Final Volume

Run #1 1030 ml 2.0 ml

Run #2

MAEPH List

CAS No. Compound Result LOQ LOD DL Units Q

83-32-9 Acenaphthene 1.9 U 3.9 1.9 1.9 ug/l

208-96-8 Acenaphthylene 1.9 U 3.9 1.9 1.9 ug/l

120-12-7 Anthracene 1.9 U 3.9 1.9 1.9 ug/l

56-55-3 Benzo(a)anthracene 1.9 U 3.9 1.9 1.9 ug/l

50-32-8 Benzo(a)pyrene 1.9 U 3.9 1.9 1.9 ug/l

205-99-2 Benzo(b)fluoranthene 1.9 U 3.9 1.9 1.9 ug/l

191-24-2 Benzo(g,h,i)perylene 1.9 U 3.9 1.9 1.9 ug/l

207-08-9 Benzo(k)fluoranthene 1.9 U 3.9 1.9 1.9 ug/l

218-01-9 Chrysene 1.9 U 3.9 1.9 1.9 ug/l

53-70-3 Dibenzo(a,h)anthracene 1.9 U 3.9 1.9 1.9 ug/l

206-44-0 Fluoranthene 1.9 U 3.9 1.9 1.9 ug/l

86-73-7 Fluorene 1.9 U 3.9 1.9 1.9 ug/l

193-39-5 Indeno(1,2,3-cd)pyrene 1.9 U 3.9 1.9 1.9 ug/l

91-57-6 2-Methylnaphthalene 1.9 U 3.9 1.9 1.9 ug/l

91-20-3 Naphthalene 1.9 U 3.9 1.9 1.9 ug/l

85-01-8 Phenanthrene 1.9 U 3.9 1.9 1.9 ug/l

129-00-0 Pyrene 1.9 U 3.9 1.9 1.9 ug/l

C11-C22 Aromatics (Unadj.) 98.1 190 97 78 ug/l J

C9-C18 Aliphatics 107 190 97 49 ug/l J

C19-C36 Aliphatics 97 U 190 97 49 ug/l

CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits

3386-33-2 1-Chlorooctadecane 51% 40-140%

580-13-2 2-Bromonaphthalene 88% 40-140%

84-15-1 o-Terphenyl 76% 40-140%

321-60-8 2-Fluorobiphenyl 85% 40-140%

U = Not detected LOD = Limit of Detection J = Indicates an estimated value

LOQ = Limit of Quantitation DL = Detection Limit B = Indicates analyte found in associated method blank

E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound

FC1821

3.2

Client Sample ID: DUP-1-0123

Lab Sample ID: FC1821-3 Date Sampled: 01/06/23

Matrix: AQ - Ground Water Date Received: 01/11/23

Method: SW846 8260D Percent Solids: n/a

Project: Seymour Johnson AFB RW502; Goldsboro, NC

File ID DF Analyzed By Prep Date Prep Batch Analytical Batch

Run #1 1A42658.D 1 01/12/23 18:49 KG n/a n/a V1A1711

Run #2

Purge Volume

Run #1 5.0 ml

Run #2

CAS No. Compound Result LOQ LOD DL Units Q

71-43-2 Benzene 1.1 1.0 0.50 0.31 ug/l

91-20-3 Naphthalene 1.8 5.0 2.0 1.0 ug/l J

CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits

1868-53-7 Dibromofluoromethane 99% 83-118%

17060-07-0 1,2-Dichloroethane-D4 92% 79-125%

2037-26-5 Toluene-D8 104% 85-112%

460-00-4 4-Bromofluorobenzene 94% 83-118%

U = Not detected LOD = Limit of Detection J = Indicates an estimated value

LOQ = Limit of Quantitation DL = Detection Limit B = Indicates analyte found in associated method blank

E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound

FC1821

3.3

Client Sample ID: DUP-1-0123

Lab Sample ID: FC1821-3 Date Sampled: 01/06/23

Matrix: AQ - Ground Water Date Received: 01/11/23

Method: MADEP EPH REV 2.1 SW846 3510C Percent Solids: n/a

Project: Seymour Johnson AFB RW502; Goldsboro, NC

File ID DF Analyzed By Prep Date Prep Batch Analytical Batch

Run #1 NN041092.D 1 01/14/23 15:11 AF 01/12/23 06:10 OP94954 GNN1891

Run #2

Initial Volume Final Volume

Run #1 1030 ml 2.0 ml

Run #2

MAEPH List

CAS No. Compound Result LOQ LOD DL Units Q

83-32-9 Acenaphthene 1.9 U 3.9 1.9 1.9 ug/l

208-96-8 Acenaphthylene 1.9 U 3.9 1.9 1.9 ug/l

120-12-7 Anthracene 1.9 U 3.9 1.9 1.9 ug/l

56-55-3 Benzo(a)anthracene 1.9 U 3.9 1.9 1.9 ug/l

50-32-8 Benzo(a)pyrene 1.9 U 3.9 1.9 1.9 ug/l

205-99-2 Benzo(b)fluoranthene 1.9 U 3.9 1.9 1.9 ug/l

191-24-2 Benzo(g,h,i)perylene 1.9 U 3.9 1.9 1.9 ug/l

207-08-9 Benzo(k)fluoranthene 1.9 U 3.9 1.9 1.9 ug/l

218-01-9 Chrysene 1.9 U 3.9 1.9 1.9 ug/l

53-70-3 Dibenzo(a,h)anthracene 1.9 U 3.9 1.9 1.9 ug/l

206-44-0 Fluoranthene 1.9 U 3.9 1.9 1.9 ug/l

86-73-7 Fluorene 1.9 U 3.9 1.9 1.9 ug/l

193-39-5 Indeno(1,2,3-cd)pyrene 1.9 U 3.9 1.9 1.9 ug/l

91-57-6 2-Methylnaphthalene 1.9 U 3.9 1.9 1.9 ug/l

91-20-3 Naphthalene 1.9 U 3.9 1.9 1.9 ug/l

85-01-8 Phenanthrene 1.9 U 3.9 1.9 1.9 ug/l

129-00-0 Pyrene 1.9 U 3.9 1.9 1.9 ug/l

C11-C22 Aromatics (Unadj.) 78.1 190 97 78 ug/l J

C9-C18 Aliphatics 112 190 97 49 ug/l J

C19-C36 Aliphatics 97 U 190 97 49 ug/l

CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits

3386-33-2 1-Chlorooctadecane 48% 40-140%

580-13-2 2-Bromonaphthalene 77% 40-140%

84-15-1 o-Terphenyl 65% 40-140%

321-60-8 2-Fluorobiphenyl 76% 40-140%

U = Not detected LOD = Limit of Detection J = Indicates an estimated value

LOQ = Limit of Quantitation DL = Detection Limit B = Indicates analyte found in associated method blank

E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound

FC1821

3.3

Subcontract Lab Data

Report of Analysis

Orlando, FL Section 4

ANALYTICAL REPORT

January 20, 2023

SGS North America Inc. - Orlando, FL

Sample Delivery Group: L1576330

Samples Received: 01/14/2023

Project Number: 457005

Description: Seymour Johnson AFB RW502; Goldsboro, NC

Report To: Muna Mohammed

4405 Vineland Rd

Suite C-15

Orlando, FL 32811

Entire Report Reviewed By:

January 20, 2023

[Preliminary Report]

Jeff Carr Pro ject Manager

Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided, and as the samples are received.

Pace Analytical National 12065 Lebanon Rd Mount Ju l ie t , TN 37122 615 -758-5858 800-767-5859 www.pacenat iona l . com

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January 20, 2023

Jeff Carr Pro ject Manager

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TABLE OF CONTENTSTABLE OF CONTENTS

Cp: Cover Page 1

Tc: Table of Contents 2

Ss: Sample Summary 4

Cn: Case Narrative 5

Su: Summary Results 6

MADEPV Volatile Petroleum Hydrocarbons 6

Surrogate Recovery 7

GW Surrogate Summary 7

Laboratory Control Sample / Duplicate 8

WG1990341 LCS(R3882836-1) LCSD(R3882836-2) 8

Method Blank 9

WG1990341 R3882836-3 VOCGC2 01/19/23 02:52 9

Sample Result Summary Organic Analysis Data Sheet 10

L1576330-01 01/19/23 04:32 VOCGC2 10

Raw Data - 0119_09 11

L1576330-02 01/19/23 05:05 VOCGC2 13

Raw Data - 0119_10 14

L1576330-03 01/19/23 05:38 VOCGC2 16

Raw Data - 0119_11 17

Retention Time of Single Component Analytes 19

VOCGC2 01/14/23 11:28 19

Calibration Factor of Single Component Analytes 20

VOCGC2 01/14/23 11:28 20

Calibration Plots 22

Unadjusted C9-C10 Aromatics 22

Calibration Summary 23

Raw Data 24

0114_07 24

0114_08 38

0114_09 48

0114_10 52

0114_11 54

0114_12 56

0114_13 58

0114_14 60

Calibration Verification Single Component Analytes 62

VOCGC2 01/14/23 17:30 62

VOCGC2 - 011423 63

VOCGC2 01/19/23 00:07 65

VOCGC2 - 011923 66

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VOCGC2 01/19/23 07:49 68

VOCGC2 - 011923 69

Analytical Sequence 71

VOCGC2 01/14/23 11:28 71

Detection Limit Summary 72

MADEPV - GW 72

QC Result Summary Organic Analysis Data Sheet 73

BLANK(R3882836-3) WG1990341 01/19/23 02:52 VOCGC2 73

Raw Data - 0119_06 74

LCS(R3882836-1) WG1990341 01/19/23 00:40 VOCGC2 76

Raw Data - 0119_02 77

LCSD(R3882836-2) WG1990341 01/19/23 01:13 VOCGC2 79

Raw Data - 0119_03 80

Preparation Logs 82

WG1990341 82

Gl: Glossary of Terms 83

Al: Accreditations & Locations 85

Sc: Sample Chain of Custody 86

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SAMPLE SUMMARY

Collected by Collected date/time Received date/time

IW-3-0123 L1576330-01 GW TB 01/06/23 09:59 01/14/23 08:45

Method Batch Dilution Preparation Analysis Analyst Location date/time date/time

Volatile Petroleum Hydrocarbons by Method MADEPV WG1990341 1 01/19/23 04:32 01/19/23 04:32 ADM Mt. Juliet, TN

Collected by Collected date/time Received date/time

TW-1-0123 L1576330-02 GW TB 01/06/23 12:35 01/14/23 08:45

Method Batch Dilution Preparation Analysis Analyst Location date/time date/time

Volatile Petroleum Hydrocarbons by Method MADEPV WG1990341 1 01/19/23 05:05 01/19/23 05:05 ADM Mt. Juliet, TN

Collected by Collected date/time Received date/time

DUP-1-0123 L1576330-03 GW TB 01/06/23 08:00 01/14/23 08:45

Method Batch Dilution Preparation Analysis Analyst Location date/time date/time

Volatile Petroleum Hydrocarbons by Method MADEPV WG1990341 1 01/19/23 05:38 01/19/23 05:38 ADM Mt. Juliet, TN

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CASE NARRATIVE

All sample aliquots were received at the correct temperature, in the proper containers, with the appropriate preservatives, and within method specified holding times, unless qualified or notated within the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control are within established criteria except where addressed in this case narrative, a non-conformance form or properly qualified within the sample results. By my digital signature below, I affirm to the best of my knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the quality of the data have been identified by the laboratory, and no information or data have been knowingly withheld that would affect the quality of the data.

[Preliminary Report]

Jef f Carr Pro jec t Manager

Report Revision History

Level II Report - Version 1: 01/20/23 10:26

Project Narrat ive

Due to multiple preparation procedures, calculated analytes are not reported in the quality control samples for EPH and VPH Methods.

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Jef f Carr Pro jec t Manager

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MADEPV Volatile Petroleum Hydrocarbons

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2A-OR SURROGATE RECOVERY

Analytical Method: MADEPV SDG: L1576330

Matrix: GW

Sample ID Lab Sample ID Instrument File ID DMC-1 DMC-2 TOT Out

% Rec. % Rec.

IW-3-0123 L1576330-01 VOCGC2 0119_09 104 101 0

TW-1-0123 L1576330-02 VOCGC2 0119_10 110 105 0

DUP-1-0123 L1576330-03 VOCGC2 0119_11 108 106 0

BLANK R3882836-3 VOCGC2 0119_06 103 103 0

LCS R3882836-1 VOCGC2 0119_02 95.7 96.6 0

LCSD R3882836-2 VOCGC2 0119_03 98.8 99.9 0

Parm Abbreviation Parameter QC LIMITS

DMC-1 2,5-Dibromotoluene(FID) 70.0 - 130

DMC-2 2,5-Dibromotoluene(PID) 70.0 - 130

*: Value outside the established quality control limits.

D: Surrogate recovery cannot be used for control limit evaluation due to dilution.

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3B-OR LABORATORY CONTROL SAMPLE SAMPLE NO.:

LABORATORY CONTROL SAMPLE DUPLICATE R3882836-1

RECOVERY R3882836-2

L1576330-01,02,03

LCS Sample / File ID: R3882836-1 / 0119_02 SDG: L1576330

LCSD Sample / File ID: R3882836-2 / 0119_03 Analytical Batch: WG1990341

Instrument ID: VOCGC2 Dilution Factor: 1

Analytical Method: MADEPV Matrix: GW

Analyte Spike Amount

LCS

Result

LCSD

Result LCS Rec. LCSD Rec. Rec. Limits RPD

RPD

Limit mg/l mg/l mg/l % % % % %

Unadjusted C5-C8 Aliphatics 1.20 1.23 1.12 103 93.3 70.0 - 130 9.36 50

Unadjusted C9-C12 Aliphatics 1.40 1.40 1.26 100 90.0 70.0 - 130 10.5 50

Unadjusted C9-C10 Aromatics 0.200 0.213 0.193 106 96.5 70.0 - 130 9.85 50

Total VPH 2.80 2.84 2.57 101 91.8 70.0 - 130 9.98 50

Total Purgeable Hydrocarbons C5-C12

2.80 2.87 2.62 103 93.6 70.0 - 130 9.11 50

Benzene 0.200 0.176 0.168 88.0 84.0 70.0 - 130 4.65 50

Toluene 0.200 0.176 0.167 88.0 83.5 70.0 - 130 5.25 50

Ethylbenzene 0.200 0.180 0.167 90.0 83.5 70.0 - 130 7.49 50 m&p-Xylenes 0.400 0.376 0.348 94.0 87.0 70.0 - 130 7.73 50 o-Xylene 0.200 0.183 0.171 91.5 85.5 70.0 - 130 6.78 50

Methyl tert-butyl ether 0.200 0.197 0.193 98.5 96.5 70.0 - 130 2.05 50

Naphthalene 0.200 0.178 0.178 89.0 89.0 70.0 - 130 0.000 50

*: Value outside the established quality control limits.

D: Surrogate recovery cannot be used for control limit evaluation due to dilution.

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:

SGS North America Inc. - Orlando, FL 457005 L1576330 01/20/23 10:26 8 of 86

4A-OR METHOD BLANK SAMPLE NO.:

R3882836-3

Lab Sample ID: R3882836-3 SDG: L1576330

Lab File ID: 0119_06 Preparation Date/Time: 01/19/23 02:52

Instrument ID: VOCGC2 Analysis Date/Time: 01/19/23 02:52

Analytical Batch: WG1990341 Dilution Factor: 1

Analytical Method: MADEPV Matrix: GW

Sample ID Lab Sample ID Instrument File ID Analysis date/time

LCS R3882836-1 VOCGC2 0119_02 01/19/23 00:40

LCSD R3882836-2 VOCGC2 0119_03 01/19/23 01:13

IW-3-0123 L1576330-01 VOCGC2 0119_09 01/19/23 04:32

TW-1-0123 L1576330-02 VOCGC2 0119_10 01/19/23 05:05

DUP-1-0123 L1576330-03 VOCGC2 0119_11 01/19/23 05:38

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:

SGS North America Inc. - Orlando, FL 457005 L1576330 01/20/23 10:26 9 of 86

1A-OR SAMPLE RESULT SUMMARY SAMPLE NO.:

ORGANIC ANALYSIS DATA SHEET IW-3-0123

Lab Sample ID: L1576330-01 SDG: L1576330

Client Sample ID: IW-3-0123 Collected Date/Time: 01/06/23 09:59

Lab File ID: 0119_09 Received Date/Time: 01/14/23 08:45

Instrument ID: VOCGC2 Preparation Date/Time: 01/19/23 04:32

Analytical Batch: WG1990341 Analysis Date/Time: 01/19/23 04:32

Dilution Factor: 1 Prep Method: MADEPV

Analytical Method: MADEPV Sample Vol Used: 5 mL

Matrix: GW Initial Wt/Vol: _______________

Total Solids (%): _______________ Final Wt/Vol: 5 mL

Analyte CAS RT Result Qualifier DL LOD LOQ mg/l mg/l mg/l mg/l

Unadjusted C5-C8 Aliphatics C5-C8 ALI UNADJ 11 0.358 0.0333 0.0670 0.100

Unadjusted C9-C12 Aliphatics C9-C12 ALI UNADJ 20 0.147 0.0333 0.0670 0.134

Unadjusted C9-C10 Aromatics C9-C10 ARO UNADJ 22 0.119 0.0333 0.0670 0.100

Adjusted C5-C8 Aliphatics C5-C8 ALI ADJ 11 0.352 0.0333 0.0500 0.100

Adjusted C9-C12 Aliphatics C9-C12 ALI ADJ 20 0.117 0.0333 0.0500 0.100

Total VPH VPH 20 0.624 0.0667 0.150 0.300

Total Purgeable Hydrocarbons C5-C12

15 0.649 0.0667 0.150 0.300

Benzene 71-43-2 10.24 0.00500 U 0.00167 0.00500 0.0100

Toluene 108-88-3 13.74 0.00381 J 0.00167 0.00500 0.0100

Ethylbenzene 100-41-4 17.87 0.00757 J 0.00167 0.00500 0.0100 m&p-Xylenes 1330-20-7 18.02 0.0167 0.00333 0.00750 0.0150 o-Xylene 95-47-6 18.79 0.00585 J 0.00167 0.00500 0.0100

Methyl tert-butyl ether 1634-04-4 7.17 0.00224 J 0.00167 0.00500 0.0100

Naphthalene 91-20-3 23.70 0.00545 B J 0.00167 0.00500 0.0100

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:

SGS North America Inc. - Orlando, FL 457005 L1576330 01/20/23 10:26 10 of 86

SGS North America Inc. - Orlando, FL 457005 L1576330 01/20/23 10:26 11 of 86

Quantitation Report (QT Reviewed)

Data Path : C:\msdchem\1\data\011923\ Data File : 0119_09.d Signal(s) : Signal #1: FID1A.CH Signal #2: ELC2B.CH Acq On : 19 Jan 2023 4:32 am Operator : 859 Sample : L1576330-01 1x WG1990341 Misc : water ALS Vial : 9 (Sig #1); 0 (Sig #2) Sample Multiplier: 1

Integration File signal 1: EVENTS.E Integration File signal 2: EVENTS2.E Quant Time: Jan 20 06:16:39 2023 Quant Method : C:\msdchem\1\methods\VP02A14W.M Quant Title : Volatile Organics by GC/FID/PID QLast Update : Sun Jan 15 09:18:27 2023 Response via : Initial Calibration Integrator: ChemStation 6890 Scale Mode: Large solvent peaks clipped

Volume Inj. :

Signal #1 Phase : Signal #2 Phase:

Signal #1 Info : Signal #2 Info :

Compound R.T. Response Conc Units

System Monitoring Compounds

13) S 2,5-Dibromotoluene(FID) 25.35 80303450 103.6302923 ppb Spiked Amount 100.0000 Range 70 - 130 Recovery = 103.63%

15) S 2,5-Dibromotoluene(PID) 25.35 745346462 101.4222141 ppb Spiked Amount 100.0000 Range 70 - 130 Recovery = 101.42%

Target Compounds

1) H Unadjusted C5-C8 Alip... 11.00 432219500 0.3577332 ppm

2) H C9 - C12 Aliphatics 20.00 403753122 0.2663328 ppm

3) H TPH C5-C12 15.00 928501638 0.6487075 ppm

4) H LRH (C5-C8) 11.00 432219500 0.3577332 ppm

5) H C6-C8 Aliphatics 10.00 371172721 0.3457258 ppm

6) H C8-C10 Aliphatics 17.00 160277220 0.1105498 ppm

7) T Pentane 0.00 0 N.D. ppb

8) T 2-Methylpentane 6.82 11312907 NoCal ppb

9) T 2,2,4-trimethylpentane 9.65 36965688 NoCal ppb

10) T Nonane 0.00 0 N.D. ppb

11) T n-Decane 0.00 0 N.D. ppb

12) T Butylcyclohexane 20.72f 3556626 NoCal ppb

16) H Unadjusted C9-C10 Aro... 22.00 1188694619 0.1187385 ppm

17) H C8-C10 Aromatics 17.00 563910292 0.0818564 ppm

18) T,M Methyl tert-butyl ether 7.17 5197567 2.2396746 ppb

19) T,M Benzene 10.24 10552403 1.4541808 ppb

20) T,M Toluene 13.74 25855797 3.8070579 ppb

21) T,M Ethylbenzene 17.87 46627208 7.5703005 ppb

22) T,M m&p-Xylene 18.02 111527936 16.6626759 ppb

23) T,M o-Xylene 18.79 37640809 5.8531187 ppb

24) T,M 1,2,4-Trimethylbenzene 20.52 70071231 10.3480585 ppb

25) T,M Naphthalene 23.70 22760660 5.4455362 ppb

(f)=RT Delta > 1/2 Window (m)=manual int.

VP02A14W.M Fri Jan 20 09:18:25 2023 Page: 1

SGS North America Inc. - Orlando, FL 457005 L1576330 01/20/23 10:26 12 of 86

Quantitation Report (QT Reviewed)

Data Path : C:\msdchem\1\data\011923\ Data File : 0119_09.d Signal(s) : Signal #1: FID1A.CH Signal #2: ELC2B.CH Acq On : 19 Jan 2023 4:32 am Operator : 859 Sample : L1576330-01 1x WG1990341 Misc : water ALS Vial : 9 (Sig #1); 0 (Sig #2) Sample Multiplier: 1

Integration File signal 1: EVENTS.E Integration File signal 2: EVENTS2.E Quant Time: Jan 20 06:16:39 2023 Quant Method : C:\msdchem\1\methods\VP02A14W.M Quant Title : Volatile Organics by GC/FID/PID QLast Update : Sun Jan 15 09:18:27 2023 Response via : Initial Calibration Integrator: ChemStation 6890 Scale Mode: Large solvent peaks clipped

Volume Inj. :

Signal #1 Phase : Signal #2 Phase:

Signal #1 Info : Signal #2 Info :

2.00 4.00 6.00 8.00 10.00 12.00 14.00 16.00 18.00 20.00 22.00 24.00 26.00

5000000

1e+07

1.5e+07

2e+07

2.5e+07

3e+07

3.5e+07

Time

Response_ Signal: 0119_09.d\FID1A.CH

,5

-D ib ro m

C

C A

C -C

A li

T P

H C

-C

L R

H

C -C

C -C

A lip

U n a d ju s te d

2.00 4.00 6.00 8.00 10.00 12.00 14.00 16.00 18.00 20.00 22.00 24.00 26.00

2000000

4000000

6000000

8000000

1e+07

1.2e+07

1.4e+07

1.6e+07

1.8e+07

2e+07

2.2e+07

Time

Response_ Signal: 0119_09.d\ELC2B.CH

,5

-D ib ro m

N a p h th a le n

,2

,4 -T ri m o -X y le n e m p -X y le n e

E th y lb e n z e

C -C

A ro

T o lu e n e

B e n z e n e

M e th y l te r

U n a d ju s te d

VP02A14W.M Fri Jan 20 09:18:26 2023 Page: 2

ORGANIC ANALYSIS DATA SHEET TW-1-0123

Lab Sample ID: L1576330-02 SDG: L1576330

Client Sample ID: TW-1-0123 Collected Date/Time: 01/06/23 12:35

Lab File ID: 0119_10 Received Date/Time: 01/14/23 08:45

Instrument ID: VOCGC2 Preparation Date/Time: 01/19/23 05:05

Analytical Batch: WG1990341 Analysis Date/Time: 01/19/23 05:05

Dilution Factor: 1 Prep Method: MADEPV

Analytical Method: MADEPV Sample Vol Used: 5 mL

Matrix: GW Initial Wt/Vol: _______________

Total Solids (%): _______________ Final Wt/Vol: 5 mL

Analyte CAS RT Result Qualifier DL LOD LOQ mg/l mg/l mg/l mg/l

Unadjusted C5-C8 Aliphatics C5-C8 ALI UNADJ 11 0.0715 J 0.0333 0.0670 0.100

Unadjusted C9-C12 Aliphatics C9-C12 ALI UNADJ 20 0.104 J 0.0333 0.0670 0.134

Unadjusted C9-C10 Aromatics C9-C10 ARO UNADJ 22 0.122 0.0333 0.0670 0.100

Adjusted C5-C8 Aliphatics C5-C8 ALI ADJ 11 0.0715 J 0.0333 0.0500 0.100

Adjusted C9-C12 Aliphatics C9-C12 ALI ADJ 20 0.104 0.0333 0.0500 0.100

Total VPH VPH 20 0.297 J 0.0667 0.150 0.300

Total Purgeable Hydrocarbons C5-C12

15 0.382 0.0667 0.150 0.300

Benzene 71-43-2 10.25 0.00500 U 0.00167 0.00500 0.0100

Toluene 108-88-3 13.74 0.00500 U 0.00167 0.00500 0.0100

Ethylbenzene 100-41-4 17.80 0.00500 U 0.00167 0.00500 0.0100 m&p-Xylenes 1330-20-7 18.02 0.00750 U 0.00333 0.00750 0.0150 o-Xylene 95-47-6 18.79 0.00500 U 0.00167 0.00500 0.0100

Methyl tert-butyl ether 1634-04-4 7.28 0.00500 U 0.00167 0.00500 0.0100

Naphthalene 91-20-3 23.70 0.00627 B J 0.00167 0.00500 0.0100

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:

SGS North America Inc. - Orlando, FL 457005 L1576330 01/20/23 10:26 13 of 86

SGS North America Inc. - Orlando, FL 457005 L1576330 01/20/23 10:26 14 of 86

Quantitation Report (QT Reviewed)

Data Path : C:\msdchem\1\data\011923\ Data File : 0119_10.d Signal(s) : Signal #1: FID1A.CH Signal #2: ELC2B.CH Acq On : 19 Jan 2023 5:05 am Operator : 859 Sample : L1576330-02 1x WG1990341 Misc : water ALS Vial : 10 (Sig #1); 0 (Sig #2) Sample Multiplier: 1

Integration File signal 1: EVENTS.E Integration File signal 2: EVENTS2.E Quant Time: Jan 20 06:16:44 2023 Quant Method : C:\msdchem\1\methods\VP02A14W.M Quant Title : Volatile Organics by GC/FID/PID QLast Update : Sun Jan 15 09:18:27 2023 Response via : Initial Calibration Integrator: ChemStation 6890 Scale Mode: Large solvent peaks clipped

Volume Inj. :

Signal #1 Phase : Signal #2 Phase:

Signal #1 Info : Signal #2 Info :

Compound R.T. Response Conc Units

System Monitoring Compounds

13) S 2,5-Dibromotoluene(FID) 25.35 84934903 109.6071075 ppb Spiked Amount 100.0000 Range 70 - 130 Recovery = 109.61%

15) S 2,5-Dibromotoluene(PID) 25.35 768637389 104.5915018 ppb Spiked Amount 100.0000 Range 70 - 130 Recovery = 104.59%

Target Compounds

1) H Unadjusted C5-C8 Alip... 11.00 86354554 0.0714727 ppm

2) H C9 - C12 Aliphatics 20.00 341831095 0.2254864 ppm

3) H TPH C5-C12 15.00 547023369 0.3821837 ppm

4) H LRH (C5-C8) 11.00 86354554 0.0714727 ppm

5) H C6-C8 Aliphatics 10.00 63833001 0.0594567 ppm

6) H C8-C10 Aliphatics 17.00 50010956 0.0344946 ppm

7) T Pentane 0.00 0 N.D. ppb

8) T 2-Methylpentane 0.00 0 N.D. ppb

9) T 2,2,4-trimethylpentane 9.66 7269948 NoCal ppb

10) T Nonane 0.00 0 N.D. ppb

11) T n-Decane 0.00 0 N.D. ppb

12) T Butylcyclohexane 20.64 3683472 NoCal ppb

16) H Unadjusted C9-C10 Aro... 22.00 1212746205 0.1219695 ppm

17) H C8-C10 Aromatics 17.00 149613599 0.0217177 ppm

18) T,M Methyl tert-butyl ether 7.28 59947 0.0258315 ppb

19) T,M Benzene 10.25 113382 0.0156247 ppb

20) T,M Toluene 13.74 1972370 0.2904157 ppb

21) T,M Ethylbenzene 17.80 6377275 1.0354016 ppb

22) T,M m&p-Xylene 18.02 681692 0.1018472 ppb

23) T,M o-Xylene 18.79 693126 0.1077806 ppb

24) T,M 1,2,4-Trimethylbenzene 20.48 14969727 2.2107162 ppb

25) T,M Naphthalene 23.70 26220646 6.2733451 ppb

(f)=RT Delta > 1/2 Window (m)=manual int.

VP02A14W.M Fri Jan 20 09:27:20 2023 Page: 1

SGS North America Inc. - Orlando, FL 457005 L1576330 01/20/23 10:26 15 of 86

Quantitation Report (QT Reviewed)

Data Path : C:\msdchem\1\data\011923\ Data File : 0119_10.d Signal(s) : Signal #1: FID1A.CH Signal #2: ELC2B.CH Acq On : 19 Jan 2023 5:05 am Operator : 859 Sample : L1576330-02 1x WG1990341 Misc : water ALS Vial : 10 (Sig #1); 0 (Sig #2) Sample Multiplier: 1

Integration File signal 1: EVENTS.E Integration File signal 2: EVENTS2.E Quant Time: Jan 20 06:16:44 2023 Quant Method : C:\msdchem\1\methods\VP02A14W.M Quant Title : Volatile Organics by GC/FID/PID QLast Update : Sun Jan 15 09:18:27 2023 Response via : Initial Calibration Integrator: ChemStation 6890 Scale Mode: Large solvent peaks clipped

Volume Inj. :

Signal #1 Phase : Signal #2 Phase:

Signal #1 Info : Signal #2 Info :

2.00 4.00 6.00 8.00 10.00 12.00 14.00 16.00 18.00 20.00 22.00 24.00 26.00

5000000

1e+07

1.5e+07

2e+07

2.5e+07

3e+07

3.5e+07

Time

Response_ Signal: 0119_10.d\FID1A.CH

,5

-D ib ro m

C

C A

C -C

A li

T P

H C

-C

L R

H

C -C

C -C

A lip

U n a d ju s te d

2.00 4.00 6.00 8.00 10.00 12.00 14.00 16.00 18.00 20.00 22.00 24.00 26.00

2000000

4000000

6000000

8000000

1e+07

1.2e+07

1.4e+07

1.6e+07

1.8e+07

2e+07

2.2e+07

Time

Response_ Signal: 0119_10.d\ELC2B.CH

,5

-D ib ro m

N a p h th a le n

,2

,4 -T ri m o -X y le n e m p -X y le n e

E th y lb e n z e

C -C

A ro

T o lu e n e

B e n z e n e

M e th y l te r

U n a d ju s te d

VP02A14W.M Fri Jan 20 09:27:20 2023 Page: 2

ORGANIC ANALYSIS DATA SHEET DUP-1-0123

Lab Sample ID: L1576330-03 SDG: L1576330

Client Sample ID: DUP-1-0123 Collected Date/Time: 01/06/23 08:00

Lab File ID: 0119_11 Received Date/Time: 01/14/23 08:45

Instrument ID: VOCGC2 Preparation Date/Time: 01/19/23 05:38

Analytical Batch: WG1990341 Analysis Date/Time: 01/19/23 05:38

Dilution Factor: 1 Prep Method: MADEPV

Analytical Method: MADEPV Sample Vol Used: 5 mL

Matrix: GW Initial Wt/Vol: _______________

Total Solids (%): _______________ Final Wt/Vol: 5 mL

Analyte CAS RT Result Qualifier DL LOD LOQ mg/l mg/l mg/l mg/l

Unadjusted C5-C8 Aliphatics C5-C8 ALI UNADJ 11 0.406 0.0333 0.0670 0.100

Unadjusted C9-C12 Aliphatics C9-C12 ALI UNADJ 20 0.159 0.0333 0.0670 0.134

Unadjusted C9-C10 Aromatics C9-C10 ARO UNADJ 22 0.125 0.0333 0.0670 0.100

Adjusted C5-C8 Aliphatics C5-C8 ALI ADJ 11 0.399 0.0333 0.0500 0.100

Adjusted C9-C12 Aliphatics C9-C12 ALI ADJ 20 0.127 0.0333 0.0500 0.100

Total VPH VPH 20 0.690 0.0667 0.150 0.300

Total Purgeable Hydrocarbons C5-C12

15 0.714 0.0667 0.150 0.300

Benzene 71-43-2 10.24 0.00500 U 0.00167 0.00500 0.0100

Toluene 108-88-3 13.74 0.00393 J 0.00167 0.00500 0.0100

Ethylbenzene 100-41-4 17.87 0.00815 J 0.00167 0.00500 0.0100 m&p-Xylenes 1330-20-7 18.02 0.0181 0.00333 0.00750 0.0150 o-Xylene 95-47-6 18.79 0.00572 J 0.00167 0.00500 0.0100

Methyl tert-butyl ether 1634-04-4 7.17 0.00266 J 0.00167 0.00500 0.0100

Naphthalene 91-20-3 23.70 0.00577 B J 0.00167 0.00500 0.0100

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:

SGS North America Inc. - Orlando, FL 457005 L1576330 01/20/23 10:26 16 of 86

SGS North America Inc. - Orlando, FL 457005 L1576330 01/20/23 10:26 17 of 86

Quantitation Report (QT Reviewed)

Data Path : C:\msdchem\1\data\011923\ Data File : 0119_11.d Signal(s) : Signal #1: FID1A.CH Signal #2: ELC2B.CH Acq On : 19 Jan 2023 5:38 am Operator : 859 Sample : L1576330-03 1x WG1990341 Misc : water ALS Vial : 11 (Sig #1); 0 (Sig #2) Sample Multiplier: 1

Integration File signal 1: EVENTS.E Integration File signal 2: EVENTS2.E Quant Time: Jan 20 06:16:49 2023 Quant Method : C:\msdchem\1\methods\VP02A14W.M Quant Title : Volatile Organics by GC/FID/PID QLast Update : Sun Jan 15 09:18:27 2023 Response via : Initial Calibration Integrator: ChemStation 6890 Scale Mode: Large solvent peaks clipped

Volume Inj. :

Signal #1 Phase : Signal #2 Phase:

Signal #1 Info : Signal #2 Info :

Compound R.T. Response Conc Units

System Monitoring Compounds

13) S 2,5-Dibromotoluene(FID) 25.35 83641223 107.9376344 ppb Spiked Amount 100.0000 Range 70 - 130 Recovery = 107.94%

15) S 2,5-Dibromotoluene(PID) 25.35 775341420 105.5037457 ppb Spiked Amount 100.0000 Range 70 - 130 Recovery = 105.50%

Target Compounds

1) H Unadjusted C5-C8 Alip... 11.00 490295322 0.4058006 ppm

2) H C9 - C12 Aliphatics 20.00 430025857 0.2836634 ppm

3) H TPH C5-C12 15.00 1021693637 0.7138171 ppm

4) H LRH (C5-C8) 11.00 490295322 0.4058006 ppm

5) H C6-C8 Aliphatics 10.00 423947023 0.3948820 ppm

6) H C8-C10 Aliphatics 17.00 175994465 0.1213906 ppm

7) T Pentane 0.00 0 N.D. ppb

8) T 2-Methylpentane 6.81 13408417 NoCal ppb

9) T 2,2,4-trimethylpentane 9.65 41477103 NoCal ppb

10) T Nonane 0.00 0 N.D. ppb

11) T n-Decane 0.00 0 N.D. ppb

12) T Butylcyclohexane 20.72f 3923475 NoCal ppb

16) H Unadjusted C9-C10 Aro... 22.00 1231555665 0.1244962 ppm

17) H C8-C10 Aromatics 17.00 629798222 0.0914206 ppm

18) T,M Methyl tert-butyl ether 7.17 6171587 2.6593878 ppb

19) T,M Benzene 10.24 10901426 1.5022781 ppb

20) T,M Toluene 13.74 26675219 3.9277113 ppb

21) T,M Ethylbenzene 17.87 50172091 8.1458407 ppb

22) T,M m&p-Xylene 18.02 121364229 18.1322536 ppb

23) T,M o-Xylene 18.79 36774955 5.7184790 ppb

24) T,M 1,2,4-Trimethylbenzene 20.52 75041337 11.0820394 ppb

25) T,M Naphthalene 23.70 24127153 5.7724726 ppb

(f)=RT Delta > 1/2 Window (m)=manual int.

VP02A14W.M Fri Jan 20 09:27:30 2023 Page: 1

SGS North America Inc. - Orlando, FL 457005 L1576330 01/20/23 10:26 18 of 86

Quantitation Report (QT Reviewed)

Data Path : C:\msdchem\1\data\011923\ Data File : 0119_11.d Signal(s) : Signal #1: FID1A.CH Signal #2: ELC2B.CH Acq On : 19 Jan 2023 5:38 am Operator : 859 Sample : L1576330-03 1x WG1990341 Misc : water ALS Vial : 11 (Sig #1); 0 (Sig #2) Sample Multiplier: 1

Integration File signal 1: EVENTS.E Integration File signal 2: EVENTS2.E Quant Time: Jan 20 06:16:49 2023 Quant Method : C:\msdchem\1\methods\VP02A14W.M Quant Title : Volatile Organics by GC/FID/PID QLast Update : Sun Jan 15 09:18:27 2023 Response via : Initial Calibration Integrator: ChemStation 6890 Scale Mode: Large solvent peaks clipped

Volume Inj. :

Signal #1 Phase : Signal #2 Phase:

Signal #1 Info : Signal #2 Info :

2.00 4.00 6.00 8.00 10.00 12.00 14.00 16.00 18.00 20.00 22.00 24.00 26.00

5000000

1e+07

1.5e+07

2e+07

2.5e+07

3e+07

3.5e+07

4e+07

Time

Response_ Signal: 0119_11.d\FID1A.CH

,5

-D ib ro m

C

C A

C -C

A li

T P

H C

-C

L R

H

C -C

C -C

A lip

U n a d ju s te d

2.00 4.00 6.00 8.00 10.00 12.00 14.00 16.00 18.00 20.00 22.00 24.00 26.00

2000000

4000000

6000000

8000000

1e+07

1.2e+07

1.4e+07

1.6e+07

1.8e+07

2e+07

2.2e+07

Time

Response_ Signal: 0119_11.d\ELC2B.CH

,5

-D ib ro m

N a p h th a le n

,2

,4 -T ri m o -X y le n e m p -X y le n e

E th y lb e n z e

C -C

A ro

T o lu e n e

B e n z e n e

M e th y l te r

U n a d ju s te d

VP02A14W.M Fri Jan 20 09:27:31 2023 Page: 2

6B-OR RETENTION TIME

INITIAL CALIBRATION OF

SINGLE COMPONENT ANALYTES

SDG: L1576330 Calibration (begin) date/time: 01/14/23 11:28

Instrument ID: VOCGC2 Calibration (end) date/time: 01/14/23 15:18

Analytical Method: MADEPV

Analyte CS: 2.5 CS: 5 CS: 10 CS: 25 CS: 100 CS: 250 CS: 500 CS: 1000

UNADJUSTED C5-C8 ALIPHATICS 11 11 11 11 11 11 11 11

C9 - C12 ALIPHATICS 20 20 20 20 20 20 20 20

TPH C5-C12 15 15 15 15 15 15 15 15

2,5-DIBROMOTOLUENE(FID) 25.34 25.34 25.34 25.34 25.34 25.34 25.34 25.34

METHYL TERT-BUTYL ETHER 7.23 7.23 7.23 7.23 7.22 7.23 7.23 7.23

BENZENE 10.24 10.24 10.24 10.23 10.24 10.24 10.24 10.24

TOLUENE 13.73 13.73 13.73 13.73 13.73 13.73 13.74 13.74

ETHYLBENZENE 17.86 17.86 17.86 17.86 17.86 17.87 17.87 17.88

M&P-XYLENE 18.01 18.01 18.01 18.01 18.01 18.02 18.02 18.04

O-XYLENE 18.78 18.78 18.78 18.78 18.78 18.78 18.79 18.79

NAPHTHALENE 23.69 23.69 23.69 23.69 23.69 23.69 23.69 23.69

2,5-DIBROMOTOLUENE(PID) 25.34 25.34 25.34 25.34 25.34 25.34 25.34 25.34

UNADJUSTED C9-C10 AROMATICS 22 22 22 22 22

File ID: 0114_07 0114_08 0114_09 0114_10 0114_11 0114_12 0114_13 0114_14

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:

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6C-OR CALIBRATION FACTOR

SINGLE COMPONENT ANALYTES

SDG: L1576330 Calibration (begin) date/time: 01/14/23 11:28

Instrument ID: VOCGC2 Calibration (end) date/time: 01/14/23 15:18

Analytical Method: MADEPV

Analyte RRF: 2.5 RRF: 5 RRF: 10 RRF: 25 RRF: 100 RRF: 250 RRF: 500 RRF: 1000

UNADJUSTED C5-C8 ALIPHATICS 1219000000 1205000000 1057000000 1296000000 1275000000 1207000000 1205000000 1201000000

C9 - C12 ALIPHATICS 1855000000 1527000000 1295000000 1435000000 1399000000 1454000000 1544000000 1620000000

TPH C5-C12 1943000000 1482000000 1223000000 1371000000 1325000000 1326000000 1371000000 1409000000

2,5-DIBROMOTOLUENE(FID) 696400 698900 650900 826900 821700 847999.90 833200 823300

METHYL TERT-BUTYL ETHER 2770000 2682000 2400000 2672000 2436000 2037000 1866000 1703000

BENZENE 8183000 8221000 7525000 7985000 6928000 6611000 6525000 6073000

TOLUENE 7359000 7568000 6852000 7534000 6470000 6170000 6200000 6180000

ETHYLBENZENE 6669000 6816000 6209000 6556000 5893000 5784000 5968000 5380000

M&P-XYLENE 8075000 8125000 7210000 6875000 6704000 6597000 5735000 4225000

O-XYLENE 7529000 7381000 6722000 6743000 6161000 6052000 5992000 4868000

NAPHTHALENE 4324000 4165000 3596000 4797000 4342000 4365000 4224000 3626000

2,5-DIBROMOTOLUENE(PID) 6992000 7027000 6655000 8204000 8108000 7755000 7301000 6750000

UNADJUSTED C9-C10 AROMATICS

1762800000 0 13130000000 9200000000 8380000000 7661000000

File ID: 0114_07 0114_08 0114_09 0114_10 0114_11 0114_12 0114_13 0114_14

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:

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6C-OR CALIBRATION FACTOR

SINGLE COMPONENT ANALYTES

SDG: L1576330 Calibration (begin) date/time: 01/14/23 11:28

Instrument ID: VOCGC2 Calibration (end) date/time: 01/14/23 15:18

Analytical Method: MADEPV

Analyte RRF. Avg %RSD COD

UNADJUSTED C5-C8 ALIPHATICS 1208217000 5.86

C9 - C12 ALIPHATICS 1515972000 11.15

TPH C5-C12 1431310000 15.36

2,5-DIBROMOTOLUENE(FID) 774903.2 10.15

METHYL TERT-BUTYL ETHER 2320679 17.42

BENZENE 7256596 11.47

TOLUENE 6791543 9.13

ETHYLBENZENE 6159228 8.02

M&P-XYLENE 6693279 18.97

O-XYLENE 6430898 13.33

NAPHTHALENE 4179691 9.53

2,5-DIBROMOTOLUENE(PID) 7348947 8.21

UNADJUSTED C9-C10 AROMATICS 11199590000 37.22 0.999

ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:

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SGS North America Inc. - Orlando, FL 457005 L1576330 01/20/23 10:26 22 of 86

Response = 7.44e+009 * Amt + 3.05e+008 Coef of Det (r^2) = 0.999 Curve Fit: Linear

1.00e+009

2.00e+009

3.00e+009

4.00e+009

5.00e+009

6.00e+009

7.00e+009

8.00e+009

0 0.5 1

Unadjusted C9-C10 Aromatics Response

Amount

Method Name: C:\msdchem\1\methods\VP02A14W.M

SGS North America Inc. - Orlando, FL 457005 L1576330 01/20/23 10:26 23 of 86

Response Factor Report VOCGC2

Method Path : C:\msdchem\1\methods\ Method File : VP02A14W.M Title : Volatile Organics by GC/FID/PID Last Update : Sun Jan 15 09:18:27 2023 Response Via : Initial Calibration

Calibration Files = = 2.5 =0114_07.d 5 =0114_08.d 10 =0114_09.d 25 =0114_10.d

Compound 2.5 5 10 25 Avg %RSD

1) H Unadjusted C5... 1.219 1.205 1.057 1.296 1.275 1.207 1.208 E9 5.86

2) H C9 - C12 Alip... 1.855 1.527 1.295 1.435 1.399 1.454 1.516 E9 11.15

3) H TPH C5-C12 1.943 1.482 1.223 1.371 1.325 1.326 1.431 E9 15.36

4) H LRH (C5-C8) 1.219 1.205 1.057 1.296 1.275 1.207 1.208 E9 5.86

5) H C6-C8 Aliphatics 1.062 1.024 0.952 1.205 1.167 1.079 1.074 E9 7.47

6) H C8-C10 Alipha... 1.242 1.376 1.249 1.436 1.455 1.515 1.450 E9 11.33

7) T Pentane 0.000 -1.00

8) T 2-Methylpentane 0.000 -1.00

9) T 2,2,4-trimeth... 0.000 -1.00

10) T Nonane 0.000 -1.00

11) T n-Decane 0.000 -1.00

12) T Butylcyclohexane 0.000 -1.00

13) S 2,5-Dibromoto... 6.964 6.989 6.509 8.269 8.217 8.480 7.749 E5 10.15

Signal #2 Calibration Files = = 2.5 =0114_07.d 5 =0114_08.d 10 =0114_09.d 25 =0114_10.d

Compound 2.5 5 10 25 Avg %RSD

15) S 2,5-Dibromoto... 6.992 7.027 6.655 8.204 8.108 7.755 7.349 E6 8.21

16) H Unadjusted C9... 17.628 13.130 9.200 8.380 11.200 E9 37.22

17) H C8-C10 Aromatics 7.994 8.684 7.464 7.211 6.602 6.436 6.889 E9 17.87

18) T,M Methyl tert-b... 2.770 2.682 2.400 2.672 2.436 2.037 2.321 E6 17.42

19) T,M Benzene 8.183 8.221 7.525 7.985 6.928 6.611 7.257 E6 11.47

20) T,M Toluene 7.359 7.568 6.852 7.534 6.470 6.170 6.792 E6 9.13

21) T,M Ethylbenzene 6.669 6.816 6.209 6.556 5.893 5.784 6.159 E6 8.02

22) T,M m&p-Xylene 8.075 8.125 7.210 6.875 6.704 6.597 6.693 E6 18.97

23) T,M o-Xylene 7.529 7.381 6.722 6.743 6.161 6.052 6.431 E6 13.33

24) T,M 1,2,4-Trimeth... 8.216 7.973 7.168 7.348 6.831 6.456 6.771 E6 18.33

25) T,M Naphthalene 4.324 4.165 3.596 4.797 4.342 4.365 4.180 E6 9.53 (#) = Out of Range ### Number of calibration levels exceeded format ###

VP02A14W.M Sun Jan 15 09:31:51 2023 Page: 1

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Quantitation Report (QT Reviewed)

Data Path : C:\msdchem\1\data\011423\ Data File : 0114_07.d Signal(s) : Signal #1: FID1A.CH Signal #2: ELC2B.CH Acq On : 14 Jan 2023 11:28 am Operator : 859 Sample : STD VPH 2.5 ppm 23A14079 (Sig #1); STD VPH .25 ppm 23A14079 (Sig #2) Misc : water surr 22L01712 ALS Vial : 7 (Sig #1); 0 (Sig #2) Sample Multiplier: 1

Integration File signal 1: EVENTS.E Integration File signal 2: EVENTS2.E Quant Time: Jan 15 09:08:28 2023 Quant Method : C:\msdchem\1\methods\VP02A14W.M Quant Title : Volatile Organics by GC/FID/PID QLast Update : Sun Jan 15 09:06:44 2023 Response via : Initial Calibration Integrator: ChemStation 6890 Scale Mode: Large solvent peaks clipped

Volume Inj. :

Signal #1 Phase : Signal #2 Phase:

Signal #1 Info : Signal #2 Info :

Compound R.T. Response Conc Units

System Monitoring Compounds

13) S 2,5-Dibromotoluene(FID) 25.34 69636114 88.0113454 ppb Spiked Amount 100.0000 Range 70 - 130 Recovery = 88.01%

15) S 2,5-Dibromotoluene(PID) 25.34 699157814 93.2151712 ppb Spiked Amount 100.0000 Range 70 - 130 Recovery = 93.22%

Target Compounds

1) H Unadjusted C5-C8 Alip... 11.00 36568966 0.0321662 ppm

2) H C9 - C12 Aliphatics 20.00 74215382 0.0540245 ppm

3) H TPH C5-C12 15.00 136038084 0.1067763 ppm

4) H LRH (C5-C8) 11.00 36568966 0.0321662 ppm

5) H C6-C8 Aliphatics 10.00 21244797 0.0209077 ppm

6) H C8-C10 Aliphatics 17.00 49662714 0.0358739 ppm

7) T Pentane 5.57 2772131 2.9577614 ppb m

8) T 2-Methylpentane 6.81 2605730 2.5263629 ppb m

9) T 2,2,4-trimethylpentane 9.61 1550687 2.3700153 ppb m

10) T Nonane 17.38 327042 0.6860147 ppb m

11) T n-Decane 19.69 294897 0.8159910 ppb m

12) T Butylcyclohexane 20.63 466382 0.8098895 ppb m

16) H Unadjusted C9-C10 Aro... 22.00 242667852 0.0201039 ppm

17) H C8-C10 Aromatics 17.00 239812613 0.0040327 ppm

18) T,M Methyl tert-butyl ether 7.23 13847589 6.4663317 ppb

19) T,M Benzene 10.24 40916361 6.0771868 ppb

20) T,M Toluene 13.73 36793933 5.8011233 ppb

21) T,M Ethylbenzene 17.86 33344407 5.8138525 ppb

22) T,M m&p-Xylene 18.01 80752751 13.2088213 ppb

23) T,M o-Xylene 18.78 37646483 6.3687070 ppb

24) T,M 1,2,4-Trimethylbenzene 20.52 41078177 6.6215136 ppb

25) T,M Naphthalene 23.69 21617743 5.4880884 ppb

(f)=RT Delta > 1/2 Window (m)=manual int.

VP02A14W.M Sun Jan 15 09:30:52 2023 Page: 1

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Quantitation Report (QT Reviewed)

Data Path : C:\msdchem\1\data\011423\ Data File : 0114_07.d Signal(s) : Signal #1: FID1A.CH Signal #2: ELC2B.CH Acq On : 14 Jan 2023 11:28 am Operator : 859 Sample : STD VPH 2.5 ppm 23A14079 (Sig #1); STD VPH .25 ppm 23A14079 (Sig #2) Misc : water surr 22L01712 ALS Vial : 7 (Sig #1); 0 (Sig #2) Sample Multiplier: 1

Integration File signal 1: EVENTS.E Integration File signal 2: EVENTS2.E Quant Time: Jan 15 09:08:28 2023 Quant Method : C:\msdchem\1\methods\VP02A14W.M Quant Title : Volatile Organics by GC/FID/PID QLast Update : Sun Jan 15 09:06:44 2023 Response via : Initial Calibration Integrator: ChemStation 6890 Scale Mode: Large solvent peaks clipped

Volume Inj. :

Signal #1 Phase : Signal #2 Phase:

Signal #1 Info : Signal #2 Info :

2.00 4.00 6.00 8.00 10.00 12.00 14.00 16.00 18.00 20.00 22.00 24.00 26.00

5000000

1e+07

1.5e+07

2e+07

2.5e+07

3e+07

3.5e+07

Time

Response_ Signal: 0114_07.d\FID1A.CH

,5

-D ib ro m

B u ty lc y c lo

C

C A n -D e c a n e

N o n a n e

C -C

A li

T P

H C

-C

L R

H

C -C

C -C

A lip ,2

,4 -t ri m

-M e th y lp e

P e n ta n e

U n a d ju s te d

2.00 4.00 6.00 8.00 10.00 12.00 14.00 16.00 18.00 20.00 22.00 24.00 26.00

2000000

4000000

6000000

8000000

1e+07

1.2e+07

1.4e+07

1.6e+07

1.8e+07

2e+07

Time

Response_ Signal: 0114_07.d\ELC2B.CH

,5

-D ib ro m

N a p h th a le n

,2

,4 -T ri m o -X y le n e m p -X y le n e

E th y lb e n z e

C -C

A ro

T o lu e n e

B e n z e n e

M e th y l te r

U n a d ju s te d

VP02A14W.M Sun Jan 15 09:30:53 2023 Page: 2

SGS North America Inc. - Orlando, FL 457005 L1576330 01/20/23 10:26 26 of 86

Quantitation Report (Qedit)

Data Path : C:\msdchem\1\data\011423\ Data File : 0114_07.d Signal(s) : Signal #1: FID1A.CH Signal #2: ELC2B.CH Acq On : 14 Jan 2023 11:28 am Operator : 859 Sample : STD VPH 2.5 ppm 23A14079 (Sig #1); STD VPH .25 ppm 23A14079 (Sig #2) Misc : water ALS Vial : 7 (Sig #1); 0 (Sig #2) Sample Multiplier: 1

Integration File signal 1: EVENTS.E Integration File signal 2: EVENTS2.E Quant Time: Jan 15 09:07:03 2023 Quant Method : C:\msdchem\1\methods\VP02A14W.M Quant Title : Volatile Organics by GC/FID/PID QLast Update : Sun Jan 15 09:06:44 2023 Response via : Initial Calibration Integrator: ChemStation 6890 Scale Mode: Large solvent peaks clipped

Volume Inj. :

Signal #1 Phase : Signal #2 Phase:

Signal #1 Info : Signal #2 Info :

4.60 4.70 4.80 4.90 5.00 5.10 5.20 5.30 5.40 5.50 5.60 5.70 5.80 5.90 6.00 6.10 6.20 6.30 6.40 6.50 6.60

50000

100000

150000

200000

250000

300000

350000

400000

Time

Response_ Signal: 0114_07.d\FID1A.CH

QEdit response 0

5.585min 0.0000000 ppb

(7) Pentane (T)

(+) = Expected Retention Time VP02A14W.M Sun Jan 15 09:07:18 2023 Page: 1

SGS North America Inc. - Orlando, FL 457005 L1576330 01/20/23 10:26 27 of 86

Quantitation Report (Qedit)

Data Path : C:\msdchem\1\data\011423\ Data File : 0114_07.d Signal(s) : Signal #1: FID1A.CH Signal #2: ELC2B.CH Acq On : 14 Jan 2023 11:28 am Operator : 859 Sample : STD VPH 2.5 ppm 23A14079 (Sig #1); STD VPH .25 ppm 23A14079 (Sig #2) Misc : water ALS Vial : 7 (Sig #1); 0 (Sig #2) Sample Multiplier: 1

Integration File signal 1: EVENTS.E Integration File signal 2: EVENTS2.E Quant Time: Jan 15 09:07:03 2023 Quant Method : C:\msdchem\1\methods\VP02A14W.M Quant Title : Volatile Organics by GC/FID/PID QLast Update : Sun Jan 15 09:06:44 2023 Response via : Initial Calibration Integrator: ChemStation 6890 Scale Mode: Large solvent peaks clipped

Volume Inj. :

Signal #1 Phase : Signal #2 Phase:

Signal #1 Info : Signal #2 Info :

18.80 18.90 19.00 19.10 19.20 19.30 19.40 19.50 19.60 19.70 19.80 19.90 20.00 20.10 20.20 20.30 20.40 20.50

50000

100000

150000

200000

250000

300000

350000

400000

450000

500000

550000

Time

Response_ Signal: 0114_07.d\FID1A.CH

19.685 ni156

QEdit response 294897

19.685min 0.8159910 ppb m

(11) n-Decane (T)

(+) = Expected Retention Time VP02A14W.M Sun Jan 15 09:08:20 2023 Page: 1

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Quantitation Report (Qedit)

Data Path : C:\msdchem\1\data\011423\ Data File : 0114_07.d Signal(s) : Signal #1: FID1A.CH Signal #2: ELC2B.CH Acq On : 14 Jan 2023 11:28 am Operator : 859 Sample : STD VPH 2.5 ppm 23A14079 (Sig #1); STD VPH .25 ppm 23A14079 (Sig #2) Misc : water ALS Vial : 7 (Sig #1); 0 (Sig #2) Sample Multiplier: 1

Integration File signal 1: EVENTS.E Integration File signal 2: EVENTS2.E Quant Time: Jan 15 09:07:03 2023 Quant Method : C:\msdchem\1\methods\VP02A14W.M Quant Title : Volatile Organics by GC/FID/PID QLast Update : Sun Jan 15 09:06:44 2023 Response via : Initial Calibration Integrator: ChemStation 6890 Scale Mode: Large solvent peaks clipped

Volume Inj. :

Signal #1 Phase : Signal #2 Phase:

Signal #1 Info : Signal #2 Info :

19.90 20.00 20.10 20.20 20.30 20.40 20.50 20.60 20.70 20.80 20.90 21.00 21.10 21.20 21.30 21.40

50000

100000

150000

200000

250000

300000

350000

400000

450000

500000

550000

Time

Response_ Signal: 0114_07.d\FID1A.CH

QEdit response 0

20.634min 0.0000000 ppb

(12) Butylcyclohexane (T)

(+) = Expected Retention Time VP02A14W.M Sun Jan 15 09:08:24 2023 Page: 1

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Quantitation Report (Qedit)

Data Path : C:\msdchem\1\data\011423\ Data File : 0114_07.d Signal(s) : Signal #1: FID1A.CH Signal #2: ELC2B.CH Acq On : 14 Jan 2023 11:28 am Operator : 859 Sample : STD VPH 2.5 ppm 23A14079 (Sig #1); STD VPH .25 ppm 23A14079 (Sig #2) Misc : water ALS Vial : 7 (Sig #1); 0 (Sig #2) Sample Multiplier: 1

Integration File signal 1: EVENTS.E Integration File signal 2: EVENTS2.E Quant Time: Jan 15 09:07:03 2023 Quant Method : C:\msdchem\1\methods\VP02A14W.M Quant Title : Volatile Organics by GC/FID/PID QLast Update : Sun Jan 15…