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SECTION 32 12 03 ASPHALT MATERIAL

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SECTOIN 32 12 03

SECTION 32 12 03

ASPHALT MATERIAL

PART 1 GENERAL

1.1SECTION INCLUDES
A.Asphalt materials
1.2REFERENCES
A.AASHTO M 81: Cut-Back Asphalt (Rapid-Curing Type)
B.AASHTO M 82: Cut-Back Asphalt (Medium-Curing Type)
C.AASHTO M 140: Emulsified Asphalt
D.AASHTO M 208: Cationic Emulsified Asphalt
E.AASHTO M 226: Viscosity Graded Asphalt Cement
F.AASHTO M 320: Performance Graded Asphalt Cement
G.AASHTO R 28: Accelerated Aging of Asphalt Binder Using a Pressurized Aging Vessel (PAV)
H.AASHTO T 44: Solubility of Bituminous Materials
I.AASHTO T 48: Flash and Fire Points by Cleveland Open Cup
J.AASHTO T 49: Penetration of Bituminous Materials
K.AASHTO T 50: Float Test for Bituminous Materials
L.AASHTO T 51: Ductility of Bituminous Materials
M.AASHTO T 59: Testing Emulsified Asphalt
N.AASHTO T 201: Kinematic Viscosity of Asphalts
O.AASHTO T 228: Specific Gravity of Semi-Solid Bituminous Materials
P.AASHTO T 240: Effect of Heat and Air on a Moving Film of Asphalt (Rolling Thin-Film Oven Test)
Q.AASHTO T 300: Force Ductility of Bituminous Materials
R.AASHTO T 301: Elastic Recovery Test of Bituminous Materials by Means of a Ductilometer
S.AASHTO T 313: Determining the Flexural Creep Stiffness of Asphalt Binder Using the Bending Beam Rheometer (BBR)
T.AASHTO T 314: Determining the Fracture Properties of Asphalt Binder in Direct Tension
U.AASHTO T 315: Determining the Rheological Properties of Asphalt Binder Using a Dynamic Shear Rheometer (DSR)
V.AASHTO T 316: Viscosity Determination of Asphalt Binder Using Rotational Viscometer
W.ASTM D 92: Flash and Fire Points by Cleveland Open Cup
X.ASTM D 1190: Concrete Joint Sealer, Hot-Applied Elastic Type
Y.ASTM D 2006: Method of Test for Characteristic Groups in Rubber Extender and Processing Oils by the Precipitation Method.
Z.ASTM D 2007: Characteristic Groups in Rubber Extender and Processing Oils and Other Petroleum-Derived Oils by the Clay-Gel Absorption Chromatographic Method
AA.ASTM D 2026: Cutback Asphalt (Slow-Curing Type)
BB.ASTM D 3405: Joint Sealants, Hot-Applied, for Concrete and Asphalt Pavements
CC.ASTM D 4402: Viscosity Determinations of Unfilled Asphalts Using the Brookfield Thermosel Apparatus
DD.ASTM D 5329: Sealants and Fillers, Hot-Applied, For Joints and Cracks in Asphaltic and Portland Cement Concrete Pavements
EE.ASTM D 5801: Toughness and Tenacity of Bituminous Materials
FF.California Test Methods
GG.UDOT Materials Manual of Instruction
HH.UDOT Minimum Sampling and Testing Guide
1.3SUBMITTALS
A.Supply a vendor-prepared bill of lading showing the following information for each material shipment:
1.Type and grade of material
2.Type and amount of additives used, if applicable
3.Destination
4.Consignee’s name
5.Date of Shipment
6.Railroad car or truck identification
7.Project number
8.Loading temperature
9.Net weight in tons or net gallons corrected to 60 degrees F, when requested
10.Specific gravity
11.Bill of lading number
12.Manufacturer of asphalt material
1.4DELIVERY, STORAGE, AND HANDLING
A.Each shipment of asphalt material must:
1.Be uniform in appearance and consistency.
2.Show no foaming when heated to the specified loading temperature.
B.Do not supply shipments contaminated with other asphalt types or grades than those specified.

PART 2 PRODUCTS

2.1PERFORMANCE GRADED ASPHALT BINDER (PGAB)
A.Supply PGABs under the Approved Supplier Certification (ASC) System. Refer to the UDOT Minimum Sampling and Testing Guide, Section 509, Asphalt Binder Management Plan.
B.Refer to AASHTO M 320 for all PGABs having algebraic differences less than 92 degrees between the high and low design temperatures.
C.Refer to Tables 1, 2, 3, 4, 5, 6, 7, and 8 for all PGABs having algebraic differences equal to or greater than 92 degrees between the high and low design temperatures.

Table 1

PG58-34

Original Binder
Dynamic Shear Rheometer, AASHTO T 315@58C, G*, kPa
@58C, phase angle, degrees
Rotational Viscometer, AASHTO T 316@135C, Pa.s
Flash Point, AASHTO T 48C

RTFO Residue, AASHTO T 240

Dynamic Shear Rheometer, AASHTO T 315@58C, G*/sinδ, kPa
Elastic Recovery, AASHTO T 301 mod (a)%

PAV Residue, 20 hours, 2.10 MPa, 100 C, AASHTO R 28

Dynamic Shear Rheometer, AASHTO T 315@16C, kPa
Bending Beam Rheometer, AASHTO T 313@-24C, S, MPa@-24C, m-value
Direct Tension Test, AASHTO T 314@-24C, Failure Strain, %
@-24C, Failure Stress (b), MPa

1.30 Min.

74.0 Max.

3 Max.

260 Min.

2.20 Min.

65 Min.

5000 Max.

300 Max.

0.300 Min.

1.5 Min.

4.0 Min.

(a)Modify paragraph 4.5 as follows: Stop the ductilometer after 20 cm has been reached and within 2 seconds. Sever the specimen at its center with a pair of scissors…
(b)No allowances will be given for passing at a colder grade.

Table 2

PG64-28

Original Binder
Dynamic Shear Rheometer, AASHTO T 315@64C, G*, kPa
@64C, phase angle, degrees
Rotational Viscometer, AASHTO T 316@135C, Pa.s
Flash Point, AASHTO T 48C

RTFO Residue, AASHTO T 240

Dynamic Shear Rheometer, AASHTO T 315@64C, G*/sinδ, kPa
Elastic Recovery, AASHTO T 301 mod (a)%

PAV Residue, 20 hours, 2.10 MPa, 100 C, AASHTO R 28

Dynamic Shear Rheometer, AASHTO T 315@22C, kPa
Bending Beam Rheometer, AASHTO T 313@-18C, S, MPa
@-18C, m-value
Direct Tension Test, AASHTO T 314@-18C, Failure Strain, %
@-18C, Failure Stress (b), MPa

1.30 Min.

74.0 Max.

3 Max.

260 Min.

2.20 Min.

65 Min.

5000 Max.

300 Max.

0.300 Min.

1.5 Min.

4.0 Min.

(a)Modify paragraph 4.5 as follows: Stop the ductilometer after 20 cm has been reached and within 2 seconds. Sever the specimen at its center with a pair of scissors…
(b)No allowances will be given for passing at a colder grade.

Table 3

PG64-34

Original Binder
Dynamic Shear Rheometer, AASHTO T 315@64C, G*, kPa
@64C, phase angle, degrees
Rotational Viscometer, AASHTO T 316@135C, Pa.s
Flash Point, AASHTO T 48C

RTFO Residue, AASHTO T-240

Dynamic Shear Rheometer, AASHTO T 315@64C, G*/sinδ, kPa
Elastic Recovery, AASHTO T 301 mod (a)%

PAV Residue, 20 hours, 2.10 MPa, 100 C, AASHTO R 28

Dynamic Shear Rheometer, AASHTO T 315@19C, kPa
Bending Beam Rheometer, AASHTO T 313@-24C, S, MPa
@-24C, m-value
Direct Tension Test, AASHTO T 314@-24C, Failure Strain, %
@-24C, Failure Stress (b), MPa

1.30 Min.

71.0 Max.

3 Max.

260 Min.

2.20 Min.

70 Min.

5000 Max.

300 Max.

0.300 Min.

1.5 Min.

4.0 Min.

(a)Modify paragraph 4.5 as follows: Stop the ductilometer after 20 cm has been reached and within 2 seconds. Sever the specimen at its center with a pair of scissors…
(b)No allowances will be given for passing at a colder grade.

Table 4

PG70-22

Original Binder
Dynamic Shear Rheometer, AASHTO T 315@70C, G*, kPa
@70C, phase angle, degrees
Rotational Viscometer, AASHTO T 316@135C, Pa.s
Flash Point, AASHTO T 48C

RTFO Residue, AASHTO T 240

Dynamic Shear Rheometer, AASHTO T 315@70C, G*/sinδ, kPa
Elastic Recovery, AASHTO T 301 mod (a)%

PAV Residue, 20 hours, 2.10 MPa, 100 C, AASHTO R 28

Dynamic Shear Rheometer, AASHTO T 315@28C, kPa
Bending Beam Rheometer, AASHTO T 313@-12C, S, MPa
@-12C, m-value
Direct Tension Test, AASHTO T 314@-12C, Failure Strain, %
@-12C, Failure Stress (b), MPa

1.30 Min.

74.0 Max.

3 Max.

260 Min.

2.20 Min.

65 Min.

5000 Max.

300 Max.

0.300 Min.

1.5 Min.

4.0 Min.

(a)Modify paragraph 4.5 as follows: Stop the ductilometer after 20 cm has been reached and within 2 seconds. Sever the specimen at its center with a pair of scissors…
(b)No allowances will be given for passing at a colder grade.

Table 5

PG70-28

Original Binder
Dynamic Shear Rheometer, AASHTO T 315@70C, G*, kPa
@70C, phase angle, degrees
Rotational Viscometer, AASHTO T 316@135C, Pa.s
Flash Point, AASHTO T 48C

RTFO Residue, AASHTO T 240

Dynamic Shear Rheometer, AASHTO T 315@70C, G*/sinδ, kPa
Elastic Recovery, AASHTO T 301 mod (a)%

PAV Residue, 20 hours, 2.10 MPa, 100 C, AASHTO R 28

Dynamic Shear Rheometer, AASHTO T 315@25C, kPa
Bending Beam Rheometer, AASHTO T 313@-18C, S, MPa
@-18C, m-value
Direct Tension Test, AASHTO T 314@-18C, Failure Strain, %
@-18C, Failure Stress (b), MPa

1.30 Min.

71.0 Max.

3 Max.

260 Min.

2.20 Min.

70 Min.

5000 Max.

300 Max.

0.300 Min.

1.5 Min.

4.0 Min.

(a)Modify paragraph 4.5 as follows: Stop the ductilometer after 20 cm has been reached and within 2 seconds. Sever the specimen at its center with a pair of scissors…
(b)No allowances will be given for passing at a colder grade.

Table 6

PG70-34

Original Binder
Dynamic Shear Rheometer, AASHTO T 315@70C, G*, kPa
@70C, phase angle, degrees
Rotational Viscometer, AASHTO T 316@135 C, Pa.s
Flash Point, AASHTO T 48C

RTFO Residue, AASHTO T 240

Dynamic Shear Rheometer, AASHTO T 315@70C, G*/sinδ, kPa
Elastic Recovery, AASHTO T 301 mod (a)%

PAV Residue, 20 hours, 2.10 MPa, 100 C, AASHTO R 28

Dynamic Shear Rheometer, AASHTO T 315@22C, kPa
Bending Beam Rheometer, AASHTO T 313@-24C, S, MPa
@-24C, m-value
Direct Tension Test, AASHTO T 314@-24C, Failure Strain, %
@-24C, Failure Stress (b), MPa

1.30 Min.

71.0 Max.

3 Max.

260 Min.

2.20 Min.

75 Min.

5000 Max.

300 Max.

0.300 Min.

1.5 Min.

4.0 Min.

(a)Modify paragraph 4.5 as follows: Stop the ductilometer after 20 cm has been reached and within 2 seconds. Sever the specimen at its center with a pair of scissors.
(b)No allowances will be given for passing at a colder grade.

Table 7

PG76-22

Original Binder
Dynamic Shear Rheometer, AASHTO T 315@76C, G*, kPa
@76C, phase angle, degrees
Rotational Viscometer, AASHTO T 316@135C, Pa.s
Flash Point, AASHTO T 48C

RTFO Residue, AASHTO T 240

Dynamic Shear Rheometer, AASHTO T 315@76C, G*/sinδ, kPa
Elastic Recovery, AASHTO T 301 mod (a)%

PAV Residue, 20 hours, 2.10 MPa, 100 C, AASHTO R 28

Dynamic Shear Rheometer, AASHTO T 315@ 31C, kPa
Bending Beam Rheometer, AASHTO T 313@-12C, S, MPa
@-12C, m-value
Direct Tension Test, AASHTO T 314@-12C, Failure Strain, %
@-12C, Failure Stress (b), MPa

1.30 Min.

71.0 Max.

3 Max.

260 Min.

2.20 Min.

70 Min.

5000 Max.

300 Max.

0.300 Min.

1.5 Min.

4.0 Min.

(a)Modify paragraph 4.5 as follows: Stop the ductilometer after 20 cm has been reached and within 2 seconds. Sever the specimen at its center with a pair of scissors…
(b)No allowances will be given for passing at a colder grade.

Table 8

PG76-28

Original Binder
Dynamic Shear Rheometer, AASHTO T 315@76C, G*, kPa
@76C, phase angle, degrees
Rotational Viscometer, AASHTO T 316@135C, Pa.s
Flash Point, AASHTO T 48C

RTFO Residue, AASHTO T 240

Dynamic Shear Rheometer, AASHTO T 315@76C, G*/sinδ, kPa
Elastic Recovery, AASHTO T 301 mod (a)%

PAV Residue, 20 hours, 2.10 MPa, 100 C, AASHTO R 28

Dynamic Shear Rheometer, AASHTO T 315@28C, kPa
Bending Beam Rheometer, AASHTO T 313@-18C, S, MPa
@-18C, m-value
Direct Tension Test, AASHTO T 314@-18C, Failure Strain, %
@-18C, Failure Stress (b), MPa

1.30 Min.

71. 0 Max.

3 Max.

260 Min.

2.20 Min.

75 Min.

5000 Max.

300 Max.

0.300 Min.

1.5 Min.

4.0 Min.

(a)Modify paragraph 4.5 as follows: Stop the ductilometer after 20 cm has been reached and within 2 seconds. Sever the specimen at its center with a pair of scissors…
(b)No allowances will be given for passing at a colder grade.
2.2ASPHALTIC CEMENT, LIQUID ASPHALTS, AND REJUVENATING AGENTS
A.Refer to AASHTO M 226, Table 2 with the following modifications:
1.Delete and replace ductility at 77 degrees F (25 degrees C) with ductility at 39.2 degrees F (4 degrees C) with values as detailed below.
AC - 2.5AC - 5AC - 10AC - 20
50+25+15+5+
B.As specified for cationic and anionic emulsified asphalt.
1.All standard Slow Setting (SS, CSS), Medium Setting (MS, CMS), and Rapid Setting (RS, CRS) grades; inclusive of all High-Float designations (HF).
2.Supply under the Approved Supplier Certification System (ASC).
3.Meet AASHTO M 208 and M 140.
C.Conform to the requirements of one of these tables:
1.Table 9: Cationic Rapid Setting Emulsified Polymerized Asphalt (CRS2P)
2.Table 10: Latex Modified Cationic Rapid Setting Emulsified Asphalt (LMCRS-2)
3.Table 11: Cationic Medium Setting Emulsified Asphalt (CMS-2S)
4.Table 12: High Float Medium Setting Emulsified Asphalt (HFMS-2)
5.Table 13: High Float Medium Setting Emulsified Polymerized Asphalt (HFMS-2P)
6.Table 14: High Float Medium Setting Emulsified Polymerized Asphalt (HFMS-2SP)
7.Table 15: High Float Rapid Setting Emulsified Polymerized Asphalt (HFRS-2P).
8.Table 16: Setting Cationic Rapid Emulsified Asphalt (CRS-2A, B)
D.Curing cut-back asphalt:
1.Refer to ASTM D 2026 as specified for slow curing (SC).
2.Refer to AASHTO M 82 as specified for medium curing (MC).
3.Refer to AASHTO M 81 as specified for rapid curing (RC).
E.Conform to requirements for Emulsified Asphalt Pavement Rejuvenating Agent:
1.Table 17: Type A
2.Table 18: Type B
3.Table 19: Type B Modified
4.Table 20: Type C
5.Table 21: Type D

Table 9 Cationic Rapid Setting Emulsified Polymerized Asphalt (CRS-2P)

Tests
AASHTO Test Method
Min.
Max.

Emulsion

Viscosity , SF, 140ºF (60ºC), s (Project-site Acceptance/Rejection Limits)

T59
100
400
Settlement (a) 5 days, percent
T 59
Storage Stability Test (b) 1 d, 24 h, percent
T 59
Demulsibility (c) 35 ml, 0.8% sodium dioctyl Sulfosucinate, percent
T 59
40
Particle Charge Test
T 59
Positive
Sieve Test, percent
T 59

0.10

Distillation

Oil distillate, by volume of emulsion, percent

Residue (d), percent

Residue from Distillation Test

Penetration, 77ºF (25ºC), 100 g, 5 s, dmm
T 49
80
150

Ductility, 39.2ºF (4ºC), 5 cm/min, cm Toughness, lb-in Tenacity, lb-in T 51

ASTM D 5801

ASTM D 5801

Solubility in trichloroethylene, percent
T 44
97.5
(a)The test requirement for settlement may be waived when the emulsified asphalt is used in less than five-days or the purchaser may require that the settlement test be run from the time the sample is received until it is used, if the elapsed time is less than 5 days.
(b)The 24-hour (1-day) storage stability test may be used instead of the five-daysettlement test.
(c)The demulsibility test is made within 30 days from date of shipment.
(d)Distillation is determined by AASHTO T 59, with modifications to include a 350 ±5ºF(177±3ºC) maximum temperature to be held for 15 minutes.

Modify the asphalt cement prior to emulsification.

Table 10 Latex Modified Cationic Rapid Setting Emulsified Asphalt (LMCRS-2)

Tests
AASHTO Test Method
Min.
Max.

Emulsion

Viscosity, SF, 122ºF (50ºC), s (Project Site Acceptance/Rejection Limits)

T59
140
400
Settlement (a) 5 days, percent
T 59
Storage Stability Test (b) 1 d, 24 h, percent
T 59
Demulsibility (c) 35 ml, 0.8% sodium dioctyl Sulfosucinate, percent
T 59
40
Particle Charge Test
T 59
Positive
Sieve Test, percent
T 59

0.3

Distillation

Oil distillate, by volume of emulsion, percent

Residue (d), percent

Residue from Distillation Test

Penetration, 77ºF (25ºC), 100 g, 5 s, dmm
T 49
40
200

Torsional Recovery (e)

(a)The test requirement for settlement may be waived when the emulsified asphalt is usedin less than a five-day time; or the purchaser may require that the settlement test be runfrom the time the sample is received until it is used, if the elapsed time is less than 5days.
(b)May use the 24-hour (1-day) storage stability test instead of the five-day settlement test.
(c)Make the demulsibility test within 30 days from date of shipment.
(d)Determine distillation by AASHTO T 59, with modifications to include a 350 ± 5ºF(177±3ºC) maximum temperature to be held for 15 minutes.
(e)CA 332 (California Test Method)

Co-mill latex and asphalt during emulsification

Table 11 Cationic Medium Setting Emulsified Asphalt (CMS-2S)

Tests
AASHTO Test Method
Specification

Emulsion

Viscosity, SF, 122ºF (50ºC), s
T 59
50 - 450
Percent residue
T 59
60 min
Storage Stability Test, 1d, 24h, percent
T 59
1 max
Sieve, percent
T 59
0.10 max
Particle charge
T 59
Positive
Oil Distillate, percent by volume of emulsion
T 59
5-15

Residue

Penetration, 77ºF (25ºC), 100g, 5 sec, dmm
T 59
100-250
Solubility, percent
T 59
97.5 min.

Table 12 High Float Medium Setting Emulsified Asphalt ( HFMS-2)

Tests
AASHTO

Test Method

Min.
Max.

Emulsion

Viscosity, SF, 122F (50C), s (Project Site Acceptance/Rejection Limits

T59
70
300
Storage Stability Test, 1d, 24 h, percent
T59

1.0

Sieve Test , percent
T59

0.1

Distillation
T59
Oil Distillate, by volume of emulsion, percent
T59
NA
NA
Residue, percent
T59
65

Residue from Distillation Test

Penetration, 77F (25C), 100g, 5 s, dmm
T49
50
200
Float Test, 140F (60C), s
T50
1200
Solubility in Trichloroethylene, percent
T44
97.5
Ductility, 77F (25C) 5cm/min, cm
T51
40

Table 13 High Float Medium Setting Emulsified Polymerized Asphalt (HFMS-2P) (a)

Tests
AASHTO Test method
Min.
Max.

Emulsion

Viscosity, SF, 122ºF (50ºC), s (Project Site Acceptance/Rejection Limits)

T 59
100
450
Storage Stability Test, 1 d, 24 h, percent
T 59

1.0

Sieve Test, percent
T 59

0.1

Distillation

Oil distillate, by volume of emulsion, percent
T 59
Residue (b), percent
T 59
65

Residue from Distillation Test

Penetration, 77ºF (25ºC), 100 g, 5 s, dmm
T 49
70
300
Float Test, 140ºF (60ºC), s
T 50
1200
Solubility in trichloroethylene, percent
T 44
97.5
Elastic Recovery, 77ºF (25ºC), percent
T 301
50
(a)Supply an HFMS-2P (anionic, polymerized, high-float) as an emulsified blend ofpolymerized asphalt cement, water, and emulsifiers. Polymerize the asphalt cementwith a minimum of 3.0% polymer by weight of the asphalt cement prior to emulsification.The emulsion must be smooth and homogeneous throughout with no white, milkyseparation, pumpable, and suitable for application through a distributor after standingundisturbed for a minimum of 24 hours.
(b)Determine the distillation by AASHTO T 59, with modifications to include a 350± 5ºF(177±3ºC) maximum temperature to be held for 15 minutes.

Table 14 High Float Medium Setting Emulsified Polymerized Asphalt (HFMS-2SP) (a)

Tests
AASHTO Test method
Min.
Max.

Emulsion

Viscosity, SF, 122ºF (50ºC), s (Project Site Acceptance/Rejection Limits)

T 59
50
450
Storage Stability Test, 1 d, 24 h, percent
T 59
Sieve Test, percent
T 59

0.1

Distillation

Oil distillate, by volume of emulsion, percent
T 59
Residue (b), percent
T 59
65

Residue from Distillation Test

Penetration, 77ºF (25ºC), 100 g, 5 s, dmm
T 49
150
300(c)
Float Test, 140ºF (60ºC), s
T 50
1200
Solubility in trichloroethylene, percent
T 44
97.5
Elastic Recovery(d), 77ºF (25ºC), percent
T 301
50
(a)Supply an HFMS-2SP (anionic, polymerized, high-float) as an emulsified blend ofpolymerized asphalt cement, water, and emulsifiers. Polymerize the asphalt cementwith a minimum of 3.0% polymer by weight of the asphalt cement prior to emulsification.The emulsion must be smooth and homogeneous throughout with no white, milkyseparation, pumpable, and suitable for application through a distributor after standingundisturbed for a minimum of 24 hours.
(b)Determine the distillation by AASHTO T 59, with modifications to include a 350± 5ºF(177±3ºC) maximum temperature to be held for 15 minutes.
(c) Emulsified Asphalt (HFMS-2SP) with a residual penetration greater than 300 dmm maybe used with Cold Bituminous Pavement (Recycle) to address problems with coolweather or extremely aged existing pavement when approved by the Engineer.

(d) Report only when penetration is greater than 300 dmm.

Table 15 High Float Rapid Setting Emulsified Polymerized Asphalt (HFRS-2P) (a)

Tests
AASHTO Test method
Min.
Max.

Emulsion

Viscosity, SF @ 122ºF (50ºC), s (Project Site Acceptance/Rejection Limits)

T 59
50
450
Storage Stability Test (b) 1 d, 24 h, percent
T 59
Demulsibility 0.02 N Ca Cl2, percent
T 59
40
Sieve Test, percent
T 59

0.1

Distillation

Oil distillate, by volume of emulsion, percent
T 59
Residue (b), percent
T 59
65

Residue from Distillation Test

Penetration, 77ºF (25ºC), 100 g, 5 s, dmm
T 49
70
150
Float Test, 140ºF (60ºC), s
T 50
1200
Solubility in trichloroethylene, percent
T 44
97.5
Elastic Recovery, 77ºF (25ºC), percent
T 301
58
(a)Supply an HFMS-2SP (anionic, polymerized, high-float) as an emulsified blend ofpolymerizedasphalt cement, water, and emulsifiers. Polymerize the asphalt cementwith a minimum of 3.0% polymer by weight of the asphalt cement prior to emulsification.The emulsion must be smooth and homogeneous throughout with no white, milkyseparation, pumpable, and suitable for application through a distributor after standingundisturbed for a minimum of 24 hours.
(b)Determine the distillation by AASHTO T 59, with modifications to include a 350 ± 5ºF(177±3ºC) maximum temperature to be held for 15 minutes.

Table 16 Cationic Rapid Setting Emulsified Asphalt (CRS-2A,B)

Tests
AASHTO Test Method
Min
Max

Emulsion

Viscosity, SF, 122ºF (50ºC), s (Project Site Rejection/Acceptance Limits)

T 59
140
400
Storage stability test, 24 h, percent
T 59
Demulsibility, 35 mL 0.8 percent Sodium Dioctyl Sulfosucinate, percent
T 59
Particle charge test
T 59
Positive
Sieve test, percent
T 59

0.10

Distillation

Oil distillate, by volume of emulsion, percent
T 59
Residue, percent
T 59
65

Use PG58-22 and PG64-22 as base asphalt cement for CRS-2A, B, respectively. Specification for high temperature performance: original and RTFO G*/sinδ within 3ºC of grade.

Table 17 Emulsified Type A Asphalt Pavement Rejuvenating Agent Concentrate

Property
Test Method
Limits
Viscosity, SF, 77ºF (25ºC), s
AASHTO T 59
15 Min 40 Max
Residue , percent W (a)
AASHTO T 59
60 Min. 65 Max.
Miscibility Test (b)
AASHTO T 59
No Coagulation
Sieve Test, percent W ( c)
AASHTO T 59
0.20 Max.
5-day Settlement, percent W
AASHTO T 59
5.0 Max.
Particle Charge
AASHTO T 59
Positive
Light Transmittance , %
UDOT MOI 8-973
30 Max.
Cement Mixing
AASHTO T 59
2 Max.

Residue from Distillation (a)

Viscosity, 140ºF (60ºC), mm2/s
ASTM D 4402
150 - 300
Flash Point, COC, ºF (ºC)
AASHTO T 48
385 Min.
Asphaltenes, percent W
ASTM D 2006-70
0.4 Min. 0.75 Max.

Maltene Distribution Ratio (PC + A1)/(S + A2) (d)

ASTM D 2006-70
0.3 Min. 0.6 Max
Saturated Hydrocarbons, S (d)
ASTM D 2006-70
21 Min. 28 Max.
PC/S Ratio (d)
ASTM D 2006-70
1.5 Min.
(a)AASHTO T 59, Evaporation Test, modified as follows: Heat a 50 gram sample to 300ºFuntil foaming ceases, then cool immediately and calculate results.
(b)AASHTO T 59, modified as follows: use a 0.02 Normal Calcium Chloride solution inplace of distilled water.
(c)AASHTO T 59, modified as follows: use distilled water in place of a two percent sodiumoleate solution.
(d)Chemical composition by ASTM Method D-2006-70:
PC= Polar Compounds, A1 = First Acidaffins

A2 = Second Acidaffins, S = Saturated Hydrocarbons

Table 18 Emulsified Type B Asphalt Pavement Rejuvenating Agent Concentrate

Tests
Test Method
Limits
Viscosity, SF, 77ºF (25ºC), s
AASHTO T 59
25-150
Residue, percent W
AASHTO T 59 (mod) (a)
62 Min.
Sieve Test, percent W
AASHTO T 59
0.10 Max.
5-day Settlement
AASHTO T 59
5.0 Max.
Particle Charge
AASHTO T 59
Positive
Pumping Stability (b)
Pass

Residue from Distillation (a)

Viscosity @ 140ºF (60ºC), mm2/s
AASHTO T 201
2500-7500
Solubility in 1,1,1 Trichloroethylene, percent
AASHTO T 44
98 Min.
Flash Point, COC
ASTM D 92
204ºC, Min.
Asphaltenes, percent W
ASTM D 2007
15 Max.
Saturates, percent W
ASTM D 2007
30 Max.
Aromatics, percent W
ASTM D 2007
25 Min.
Polar Compounds, percent W
ASTM D 2007
25 Min.
(a) Determine the distillation by AASHTO T 59 with modifications to include a
300 ±5ºF (149±3ºC) maximum temperature to be held for 15 minutes.
(b)Test pumping stability by pumping 475 ml of Type B diluted 1 part concentrate to 1part water, at 77ºF (25ºC) through a ¼ inch gear pump operating at 1750 rpm for 10minutes with no significant separation or coagulation in pumped material.

Type B: an emulsified blend of lube oil or lube oil extract and petroleum asphalt.

Table 19 Emulsified Type B Modified Asphalt Pavement Rejuvenating Agent Concentrate

Property
Test Method
Limits
Viscosity, SF, 77ºF (25ºC), s
AASHTO T 59
50-200
Residue(a), percent W
AASHTO T 59
62 Min.
Sieve Test, percent W
AASHTO T 59
0.20 Max.
5-day Settlement, percent W
AASHTO T 59
5.0 Max.
Particle Charge
AASHTO T 59
Positive
Pumping Stability (b)
Pass

Residue from Distillation (a)

Viscosity (c) 275ºF (135ºC), cP
ASTM D 4402
150 – 300
Penetration, 77ºF (25ºC), dmm
AASHTO T 49
180 Min.
Solubility in 1,1,1 Trichloroethylene, percent
AASHTO T 44
98 Min.
Flash Point, COC, ºF (ºC)
AASHTO T 48
400(204) Min.
Asphaltenes, percent W
ASTM D 2007
20-40
Saturates, percent % W
ASTM D 2007
20 Max.
Polar Compounds, percent W
ASTM D 2007
25 Min.
Aromatics, percent W
ASTM D 2007
20 Min.
PC/S Ratio
ASTM D 2007
1.5 Min.
(a)Determine the distillation by AASHTO T 59 with modifications to include a 300±5ºF(149±3ºC) maximum temperature to be held for 15 minutes.
(b)Pumping stability is tested by pumping 475 ml of Type B diluted 1 part concentrate to 1part water, at 77ºF (25ºC) through a ¼ inch gear pump operating at 1750 rpm for 10minutes with no significant separation or coagulation in pumped material.
(c)Brookfield Thermocel Apparatus-LV model. 50 rpm with a #21 spindle, 7.1 g residue,at 10 torque

As required by the Asphalt Emulsion Quality Management Plan, UDOT Minimum Sampling and Testing Guide, Section 508) the supplier certifies that the base stock contains a minimum of 15% by weight of Gilsonite Ore. Use the HCL precipitation method as a qualitative test to detect the presence of Gilsonite.

Table 20 Emulsified Type C Asphalt Pavement Rejuvenating Agent Concentrate

Property
Test Method
Limits
Viscosity, SF, 77ºF (25ºC), s
AASHTO T 59
10-100
Residue (a), percent W (Type C supplied ready to use 1:1 or 2:1.
AASHTO T 59
30 Min. 1:1

40 Min. 2:1

Sieve Test, percent W (b)

0.10 Max.

5-day Settlement, percent W
AASHTO T 59
5.0 Max.
Particle Charge
AASHTO T 59
Positive
pH (May be used if particle charge test is inconclusive)
2.0 - 7.0
Pumping Stability (c)
Pass

Tests of Residue from Distillation (a)

Viscosity, 275ºF (135ºC), mm2/s
AASHTO T 201
475-1500
Solubility in 1,1,1 Trichloroethylene, percent
AASHTO T 44
97.5 Min.
RTFO mass loss, percent W
AASHTO T 240
2.5 Max.
Specific Gravity
AASHTO T 228
0.98 Min.
Flash Point, COC
AASHTO T 48
232ºC, Min.
Asphaltenes, percent W
ASTM D 2007
25 Min., 45 Max.
Saturates, percent W
ASTM D 2007
10 Max.
Polar Compounds, percent W
ASTM D 2007
30 Min.
Aromatics, percent W
ASTM D 2007
15 Min.
(a)Determine the distillation by AASHTO T 59 with modifications to include a 300± 5ºF (149± 3ºC) maximum temperature to be held for 15 minutes.
(b)Test method identical to AASHTO T 59 except that distilled water is used in place of 2 %sodium oleate solution.
(c)Test pumping stability by pumping 475 ml of Type diluted 1 part concentrate to 1 partwater, at 77ºF (25ºC) through a ¼ inch gear pump operating at 1750 rpm for 10minutes with no significant separation or coagulation in pumped material.

As required by the Asphalt Emulsion Quality Management Plan, UDOT Minimum Sampling and Testing Guide, Section 508), the supplier certifies that the base stock contains a minimum of 10% by weight of Gilsonite ore. Use the HCL precipitation method as a qualitative test to detect the presence of Gilsonite.

Table 21 Emulsified Type D Asphalt Pavement Rejuvenating Agent Concentrate

Property
Test Method
Limits
Viscosity, SF, 77ºF (25ºC), s
AASHTO T 59
30-90
Residue, (b) percent W
AASHTO T 59
65
Sieve Test, percent W
AASHTO T 59
0.10 Max.
pH
2.0 - 5.0

Residue from Distillation (b)

Viscosity, 140ºF (60ºC), cm2/s
AASHTO T 201
300-1200
Viscosity, 275ºF (135ºC), mm2/s
AASHTO T 201
300 Min.
Modified Torsional Recovery (a) percent
CA 332 (Mod)
40 Min.
Toughness, 77ºF (25ºC), in-lb
ASTM D 5801
8 Min.
Tenacity, 77ºF (25ºC), in-lb
ASTM D 5801
5.3 Min.
Asphaltenes, percent W
ASTM D 2007
16 Max.
Saturates, percent W
ASTM D 2007
20 Max.
(a)Torsional recovery measurement to include first 30 seconds.
(b)Determine the distillation by AASHTO T 59 with modifications to include a 300±5ºF
(149±3ºC) maximum temperature to be held for 15 minutes.
2.3HOT-POUR CRACK SEALANT FOR BITUMINOUS CONCRETE
A.Combine a homogenous blend of materials to produce a sealant meeting properties and tests in Table 22.
B.Packaging and Marking: Supply sealant pre-blended, pre-reacted, and pre-packaged in lined boxes weighing no more than 30 lb.
1.Use a dissolvable lining that will completely melt and become part of the sealant upon subsequent re-melting.
2.Deliver the sealant in the manufacturer’s original sealed container. Clearly mark each container with the manufacturer’s name, trade name of sealant, batch or lot number, and recommended safe heating and application temperatures.

Table 22 Hot-Pour Bituminous Concrete Crack Sealant

Application Properties

Workability:
Pour readily and penetrate 0.25 inch and wider cracks for the entire application temperature range recommended by the manufacturer.
Curing:
No tracking caused by normal traffic after 45 minutes from application.
Asphalt Compatibility: ASTM D 5329, Section 14.
No failure in adhesion. No formation of an oily ooze at the interface between the sealant and the bituminous concrete or softening or other harmful effects on the bituminous concrete.
Material Handling:
Follow the manufacturer’s safe heating and application temperatures.
Test Method
Property
Minimum
Maximum
AASHTO T 51
Ductility, modified, 1cm/min, 39.2ºF (4ºC), cm
30
UDOT method 967
Cold Temperature Flexibility
no cracks
AASHTO T 300 (a)
Force-Ductility, lb force
ASTM D 5329
Flow 140ºF (60ºC), 5 hrs 75º angle, mm
ASTM D 3405 (b)
Tensile-Adhesion, modified
300%
AASHTO T 228
Specific Gravity, 60ºF (15.6ºC)

1.140

ASTM D 5329
Cone Penetration, 77ºF (25ºC), 150 g,

5 sec., dmm

ASTM D 5329
Resilience, 77ºF (25ºC), 20 sec., percent
30

ASTM D 4402

Viscosity, 380ºF (193.3ºC), SC4-27 spindle, 20 rpm, Cp

ASTM D 5329
Bond as per ASTM D 1190, Section 6.4

Pass

(a)Maximum of 4 lb force during the specified elongation of 30 cm @ 1 cm/min, 39.2ºF (4ºC).
(b)Use ASTM D 3405, Section 6.4.1. Delete bond and substitute tensile-adhesion test in accordance to D 5329.

PART 3 EXECUTION Not Used

END OF SECTION

ASPHALT MATERIAL Page 1

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