FSR_sample.pdf

PDF 724 KB Posted Sep 9, 2019

Attached to: MDA Soil Vapor Monitoring
Solicitation number: RFP-0000476
Issued by: Department of Energy Los Alamos National Laboratory

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Appendix D-7 FSR_Sample

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Event ID: 12199 Appendix A Samples Taken Table

MDA C

Field Matrix

Location ID Sample ID Port

Depth (ft)

Analysis Date

Collected Sample Purpose

Flow Rate

(slpm)

Static Pressure

(KpA)

Start Pressure

End Pressure

(psi)

Vapor Gain (g)

CH4 (%) CO2 (ppm) O2 (%) VOC (ppm)

Notes

Tritium 1/24/2019 -19 VOCs 1/23/2019 0 Tritium 1/24/2019 -19 VOCs 1/23/2019 -10 Tritium 1/24/2019 -20 VOCs 1/23/2019 0 Tritium 1/24/2019 -19 VOCs 1/23/2019 0 Tritium 1/24/2019 -20 VOCs 1/23/2019 0 Tritium 1/24/2019 -19 VOCs 1/23/2019 0 Tritium n/a -19 VOCs 1/23/2019 0 Tritium 1/25/2019 -20 VOCs 1/24/2019 0 Tritium 1/25/2019 -20 VOCs 1/24/2019 -10 Tritium 1/25/2019 -20 VOCs 1/24/2019 0 Tritium 1/25/2019 -19 VOCs 1/24/2019 0 Tritium 1/25/2019 -19 VOCs 1/24/2019 0 Tritium 1/28/2019 -20 VOCs 1/25/2019 0 Tritium 1/28/2019 -20 VOCs 1/25/2019 -10 Tritium 1/28/2019 -20 VOCs 1/25/2019 0 Tritium 1/28/2019 -20 VOCs 1/25/2019 0 Tritium 1/28/2019 -20 VOCs 1/25/2019 0 Tritium 1/28/2019 -20 VOCs 1/25/2019 0

01.4

1.4

7160 20 1.8

MD50-19-166054 337 INV 5 0 4550 20.2 0.51.4

3750 20.3 0

MD50-19-166500 450 FD INV 5.41 0 3750 20.3 0

MD50-19-166055 450 INV 3.49

12,000

0 10,000 20.1

0 7,020 20.2 1.3

MD50-19-166124 122 FB QC 6.68 n/a n/a n/a n/a

MD50-19-166052 122 INV 5.02

Gas 50-603064

MD50-19-166061 113 INV 2.17

MD50-19-166125 113 FB QC 5.47

MD50-19-166062 214

3.45

INV 5.15

6.1

Port 5 (214') was the only port to collect 5 grams in the silica column.

n/a n/a n/a n/a

19.7 11.3

0 7,860 19.9 4.5

0.50 4,060 20.2

0 3,930 20.1 2.5

4.75

5.08

5.2

3.86

5.12

4.49 n/a

0 5,410 20 5

0 3,930 20.1 2.5

0 7,720 19.9 5.1

050-24822

MD50-19-166063 332 INV 1.22

MD50-19-166064 500 INV

Gas 50-603062

Gas

INV

MD50-19-166114 450 FD

INV

6,880

0 10,600 n/a n/a

2.3 n/a Some ports did not collect 5g. We continued to collect silica columns for tritium at 50-24822 and collected summa canisters for VOCs at 50-603064.

The FD for silica columns was cancelled.

MD50-19-166042

MD50-19-166122

MD50-19-166043

MD50-19-166044

MD50-19-166045

MD50-19-166046

25 FB

Two of the ports did not collect 5 grams, but all silica columns collected more than

2.5 grams.

MD50-19-166053 217 INV 4 0

INV

19.9 8.5

19.8 0.9 n/a n/a

1.9

1.7

1.8

1.5

1.5 n/a

1.6

1.4

1.2

1.6 n/a

1.6

0.135 n/a

0.355

0.397

0.181

0.134

0.135 n/a

0.079

0.025

-0.56

0.106 n/a

0.119

0.097

0.051

Page A-1RFP-0000476

MDA C

Field Matrix

Location ID Sample ID Port

Depth (ft)

Analysis Date

Collected Sample Purpose

Flow Rate

(slpm)

Static Pressure

(KpA)

Start Pressure

End Pressure

(psi)

Vapor Gain (g)

CH4 (%) CO2 (ppm) O2 (%) VOC (ppm)

Notes

Tritium 1/29/2019 -20 VOCs 1/28/2019 0 Tritium 1/29/2019 -20 VOCs 1/28/2019 -10 Tritium 1/29/2019 -20 VOCs 1/28/2019 0 Tritium 1/29/2019 -20 VOCs 1/28/2019 0 Tritium 1/29/2019 -20 VOCs 1/28/2019 0 Tritium 1/29/2019 -20 VOCs 1/28/2019 0 Tritium 1/30/2019 -20 VOCs 1/29/2019 0 Tritium 1/30/2019 -20 VOCs 1/29/2019 0 Tritium 1/30/2019 -20 VOCs 1/29/2019 0 Tritium 1/30/2019 -20 VOCs 1/29/2019 0 Tritium 1/30/2019 -20 VOCs 1/29/2019 0 Tritium 1/30/2019 -20 VOCs 1/29/2019 0 Tritium 1/30/2019 -20 VOCs 1/29/2019 0 Tritium 1/31/2019 -20 VOCs 1/30/2019 0 Tritium 1/31/2019 -20 VOCs 1/30/2019 0

None of the ports collected 5g, but all silica columns collected more than

2.5g.

MD50-19-166102 450 INV 3.94 0 5060 19.8 4.2

MD50-19-166099 146 INV 4.03 0 5,410 20.2 3

2.55 0

1.4

Gas 50-603472

MD50-19-166098 27 INV

8000 19.8 9.8

MD50-19-166101 364 INV 2.52 0 6390 19.8 6.6

MD50-19-166100 292 INV 4.73 0

5270 20.3 0.4

6530 19.9

8,210 19.8 1 n/a

1.7

0 3440 20

20 1 None of the ports collected 5g, but all silica columns collected more than 2.5g.

MD50-19-166104 632.5 INV 3.7 0 2,090 20.3 0

Two of the ports did not collect 5 grams, but all silica columns collected more than

2.5 grams.

MD50-19-166126 155 FB QC 5.9 n/a n/a n/a n/a

MD50-19-166033

1.8

0.2

MD50-19-166116 450 FD INV 2.94

Gas 50-24784

MD50-19-166034 362 INV 4.35 0 4730 19.9 0.7

MD50-19-166535 450

MD50-19-166032 155 INV 3.1 0

244 INV 4.7 0

3440 20 0.2

INV 3.9

Gas 50-613182

MD50-19-166103 550 INV 4.2 0 3400

MD50-19-166093

Gas 50-613183

MD50-19-166094

642.5

None of the ports collected 5g.

1.1

19.8

20.1

3,750

3,080

INV

3.7

4.22

1.3

1.6

1.4

1.3

1.4

1.6

1.5

-0.176

-0.42

-0.095

-0.124

-0.127

-0.252

-0.272

-0.03 n/a

-0.125

-0.249

-0.254

-0.151

Page A-2RFP-0000476

MDA C

Field Matrix

Location ID Sample ID Port

Depth (ft)

Analysis Date

Collected Sample Purpose

Flow Rate

(slpm)

Static Pressure

(KpA)

Start Pressure

End Pressure

(psi)

Vapor Gain (g)

CH4 (%) CO2 (ppm) O2 (%) VOC

Tritium 1/31/2019 -19 VOCs 1/30/2019 0 Tritium 1/31/2019 -20 VOCs 1/30/2019 0 Tritium 1/31/2019 -20 VOCs 1/30/2019 0 Tritium 1/31/2019 -20 VOCs 1/30/2019 0 Tritium 1/31/2019 -19 VOCs 1/30/2019 0 Tritium 1/31/2019 -20 VOCs 1/30/2019 0 Tritium 2/1/2019 -20 VOCs 2/1/2019 0 Tritium 2/1/2019 -20 VOCs 2/1/2019 0 Tritium 2/1/2019 -20 VOCs 2/1/2019 0 Tritium 2/1/2019 -20 VOCs 2/1/2019 0 Tritium 2/1/2019 -20 VOCs 2/1/2019 0 Tritium 2/4/2019 -21 VOCs 2/4/2019 0 Tritium 2/4/2019 -20 VOCs 2/4/2019 0 Tritium 2/4/2019 -20 VOCs 2/4/2019 0 Tritium 2/4/2019 -21 VOCs 2/4/2019 0 Tritium 2/4/2019 -20 VOCs 2/4/2019 0 Tritium 2/4/2019 -20 VOCs 2/4/2019 0 Tritium 2/4/2019 -20 VOCs 2/4/2019 0 Tritium 2/4/2019 -20 VOCs 2/4/2019 -10

-0.057

19.6

19.8 Gas 50-603471

9.3

MD50-19-166089 209 INV 3.96 0 20 17.2

MD50-19-166090 288 INV 3.95 0 8,280 19.9 18.8

-0.068

-0.14

MD50-19-166091 360 INV 1.7 0 7,580

MD50-19-166088 90 INV 4.38 0 10,400

6,950

5.2 0 2,060

Gas 50-613185

MD50-19-166109 145 INV 1.83 0 8,140 20

20.9

1.8

None of the ports collected 5g, and 2 ports collected below 2.5g. Port

"PINK" is an unknown depth and referred to by the pink colored tag marking the port.

MD50-19-166130 PINK INV 2.14 0 7,860 19.8 4.6

15.9

MD50-19-166092 450 INV 4.07 0 4,820 19.9

0.2

MD50-19-166113 600 INV 5.92 0 1,780 20.7 0

1.7

1.5

0.4

Port 2 was the only port to collect below

5g.

MD50-19-166110 235 INV 5.56 0 4,820 20.3 1.2

MD50-19-166111 350 INV 5.68 0 2,400 20.5 0.6

MD50-19-166112 450 INV

Gas 50-603470 0 5,870

MD50-19-166082 83 INV 3.45 0 9,210 19.7

19.6

7,580 19.7

1.7

1.5

19.7 3

MD50-19-166083 203 INV 3.67 0 8,000 19.8 11.6

MD50-19-166084 278 INV 3.51

1.7

MD50-19-166086 450 INV 3 0 6,040 19.7

All tritium columns collected below 5g and above 2.5g except for Port 7

(351').

MD50-19-166127 650 FB QC 5.81 n/a n/a n/a n/a

5.5

MD50-19-166087 650 INV 2.73 0 2,560 20 0

14.3

MD50-19-166085 351 INV 1.59 0 11

MD50-19-166117 83 FD INV 3.43 0 9,210

1.6

1.5

1.4

1.3

1.8

1.4

1.4 n/a

0.037

0.044

0.078

0.019

-0.018

-0.074

0.11

0.029

0.08

-0.017

-0.06

-0.017

-0.135 n/a

Page A-3RFP-0000476

MDA C

Field Matrix

Location ID Sample ID Port

Depth (ft)

Analysis Date

Collected Sample Purpose

Flow Rate

(slpm)

Static Pressure

(KpA)

Start Pressure

End Pressure

(psi)

Vapor Gain (g)

CH4 (%) CO2 (ppm) O2 (%) VOC

Tritium 2/5/2019 -20 VOCs 2/5/2019 0 Tritium 2/5/2019 -20 VOCs 2/5/2019 0 Tritium 2/5/2019 -20 VOCs 2/5/2019 0 Tritium 2/5/2019 -20 VOCs 2/5/2019 0 Tritium 2/5/2019 -20 VOCs 2/5/2019 0 Tritium 2/5/2019 -20 VOCs 2/5/2019 0 Tritium 2/5/2019 -20 VOCs 2/5/2019 0 Tritium 2/5/2019 -20 VOCs 2/5/2019 0 Tritium 2/6/2019 -20 VOCs 2/6/2019 0 Tritium 2/6/2019 -20 VOCs 2/6/2019 0 Tritium 2/6/2019 -20 VOCs 2/6/2019 0 Tritium 2/6/2019 -20 VOCs 2/6/2019 0 Tritium 2/6/2019 -20 VOCs 2/6/2019 0 Tritium 2/6/2019 -20 VOCs 2/6/2019 0 Tritium 2/6/2019 -20 VOCs 2/6/2019 -10

0.5

0.2

MD50-19-166129 450 FB QC 6.75 n/a n/a n/a n/a

0.5

All of the ports collected above 2.5g. Two ports collected 5g.

MD50-19-166120 26 FD INV 5.07 0 15,400 19.1 0.5

MD50-19-166066 139 INV 4.45 0 13,000 19.5 1.3

MD50-19-166067 244 INV 4.86 0 9,210 1.5

MD50-19-166068 359 INV 4.11 0 4,370 20.1

5.81 0 15,400 19.1

19.8

MD50-19-166069 450 INV 3.5 0 3,130 20.2

2.3

1.8

1.7

1.5

1.4

-0.095

-0.098

-0.653

-0.805

-0.728

Gas 50-603383

MD50-19-166065 26 INV

Gas 50-24813

MD50-19-1660036 25 INV 8.18 0 17,100 19

19.6

MD50-19-166040 450 INV 5.81 0 5,270 19.9

MD50-19-166128 600 FB QC 5.67 n/a n/a n/a

13.7

-0.339

-0.569

1.6

All ports collected at least 5g of tritium.

MD50-19-166118 25 FD INV 6.09 0 17,100 19 1.6

MD50-19-166037 150 INV 7.09 0 13,800 19.3 8.9

MD50-19-166038 241 INV 5.68 0 9,570

n/a

6.8

MD50-19-166041 600 INV 5.45 0 3,310 20.1 0.71.4

n/a

-0.595

-0.665 n/a

17.3

MD50-19-166039 358 INV 6.65 0 7,380 19.8

1.9

1.7

1.6

1.4 n/a

-0.083

-0.196

-0.083

Page A-4RFP-0000476

MDA C

Field Matrix

Location ID Sample ID Port

Depth (ft)

Analysis Date

Collected Sample Purpose

Flow Rate

(slpm)

Static Pressure

(KpA)

Start Pressure

End Pressure

(psi)

Vapor Gain (g)

CH4 (%) CO2 (ppm) O2 (%) VOC

Tritium 2/7/2019 -19 VOCs 2/7/2019 0 Tritium 2/7/2019 -19 VOCs 2/7/2019 0 Tritium 2/7/2019 -19 VOCs 2/7/2019 0 Tritium 2/7/2019 -19 VOCs 2/7/2019 0 Tritium 2/7/2019 -19 VOCs 2/7/2019 0 Tritium 2/7/2019 -19 VOCs 2/7/2019 0 Tritium 2/8/2019 -20 VOCs 2/8/2019 0 Tritium 2/8/2019 -20 VOCs 2/8/2019 0 Tritium 2/8/2019 -19 VOCs 2/8/2019 0 Tritium 2/8/2019 -20 VOCs 2/8/2019 0 Tritium 2/8/2019 -21 VOCs 2/8/2019 0 Tritium 2/8/2019 -20 VOCs 2/8/2019 0 Tritium 2/8/2019 -20 VOCs 2/8/2019 0 Tritium 2/11/2019 -19 VOCs 2/11/2019 0 Tritium 2/11/2019 -20 VOCs 2/11/2019 0 Tritium 2/11/2019 -18 VOCs 2/11/2019 0 Tritium 2/11/2019 -20 VOCs 2/11/2019 0 Tritium 2/11/2019 -20 VOCs 2/11/2019 0 Tritium 2/11/2019 -19 VOCs 2/11/2019 0 Tritium 2/11/2019 -20 VOCs 2/11/2019 -10

MD50-19-167340 450 FB QC 5.21 n/a n/a n/a n/a

5.13 0 9,140 19.9 0.9

MD50-19-166050 347 INV 4.22 0 5,480 20.1 0.2

MD50-19-166051 450 INV 3.66 0 3,880 20.3 0

5.3

No ports collected 5g. All ports collected above 2.5g except for Port 3 and Port 5.

Gas 50-603061

MD50-19-166047 25 INV 4.71 0 38,600 16.5 0

All ports collected above 2.5g. Port 5 was the only port to collect 5g.

MD50-19-166119 25 FD INV 4.53 0 38,600 16.5 0

MD50-19-166048 128 INV 4.67 0 24,500 18.6 0.7

MD50-19-166049 228 INV

6.6

MD50-19-166075 142 INV 2.16 0 2,460 20.5 4.5

MD50-19-166076 233 INV 1.39 0 4,950 20.2 5.2

Gas 50-603468

MD50-19-166078 403 INV 3.71 0 3,750 20.4

1.9

1.7

1.6

1.5

0.592

0.608

MD50-19-166077 354 INV 3.52 0 4,340 20.2

0.13

0.458

2,390 20.3 1.3

INV 2.52 0 5,760 19.8

MD50-19-166080 600 INV 3.16 0 1,060 20.2 0.1

No ports collected 5g. All ports collected above 2.5g.

INV 3.88 0 1,900 20.2 0MD50-19-166081

0.424

0.333

0.264

0 5,200

Gas 50-613184

664.5

3.9

MD50-19-166060 450 INV 3.54 0 5,760 19.8 2.9

Gas 50-603063

MD50-19-166056 25 INV 3.53 0 8,070 20

MD50-19-166121 450 FD 2.9

MD50-19-166081 500 INV 3.29 0

0 Manhole cover frozen.

Crew spent 1 hour removing manhole.

Crew observed standing water in well with no oily sheen and a pH of 7. P. Baucom and R. Desotel confrimed crew could dump water out. No ports collected 5 g. All Ports collected above

2.5 g.

MD50-19-166057 128 INV 3.05 0 10,500 19.7 1.7

MD50-19-166058 228 INV 3.22 0 10,400 19.7 5.8

MD50-19-166059 347 INV 3.45

2.1

1.8

1.7

1.5

2.6

0.165

-0.053

-0.111

2.6

1.9

1.8

1.6 n/a

0.18

0.388

-0.283

-0.474

-0.712

-0.962

-0.922

Page A-5RFP-0000476

MDA C

Field Matrix

Location ID Sample ID Port

Depth (ft)

Analysis Date

Collected Sample Purpose

Flow Rate

(slpm)

Static Pressure

(KpA)

Start Pressure

End Pressure

(psi)

Vapor Gain (g)

CH4 (%) CO2 (ppm) O2 (%) VOC

Tritium 2/15/2019 -20 VOCs 2/15/2019 0 Tritium 2/15/2019 -20 VOCs 2/15/2019 0 Tritium 2/15/2019 -20 VOCs 2/15/2019 0 Tritium 2/15/2019 -19 VOCs 2/15/2019 -1 Tritium 2/15/2019 -20 VOCs 2/15/2019 -2 Tritium 2/15/2019 -20 VOCs 2/15/2019 0 Tritium 2/22/2019 -20 VOCs 2/22/2019 0 Tritium 2/22/2019 -20 VOCs 2/22/2019 0 Tritium 2/22/2019 -20 VOCs 2/22/2019 0 Tritium 2/22/2019 -20 VOCs 2/22/2019 0

Shaded cell indicates vapor gain less than 5 grams.

Gas 50-603503

MD50-19-166105 133 INV 4.46 0 3,880

0.5

02.2

1.9

1.8

1.7

No ports were able to collect 5g.

MD50-19-166106 237 INV 3.56 0 4,020 20.4 1.2

MD50-19-166107 347 INV 3.63 0 2,840 20.4 1

MD50-19-166108 450 INV 2.54 0

20.9

20.42,150

Port 10 collected below 2.5g (1.91g).

No ports were able to collect 5g.

MD50-19-166071 244 INV 4.5 0 5,900 20.3 4.3

MD50-19-166072 360 INV 2.97 0 3,350 20.5 0.8

MD50-19-166073 500 INV 4.25 0 2,840 20.3

2,120

INV 3.68 0

Gas 50-603467

MD50-19-166070 143 INV 4.57 0 8,000 20 4

1.6

MD50-19-166074 600 INV 1.91 0

1.5

1.6

1.3

1.4

1.4 2,120 20.5 0.6

20.5 0.6

MD50-19-167342 600 FD

1.8

0.014

-0.07

-0.435

-0.567

0.051

Page A-6RFP-0000476

Sheet1

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