J126039-1 Std_Tal_L4 Final Report_Part7.pdf

PDF 20 MB Posted Apr 12, 2023

Attached to: Maintenance Dredging of New York and New Jersey Harbor – Arthur Kill 50’ Reach, Federal Navigation Project
Solicitation number: W912DS23B0004
Issued by: Department of the Army Corps of Engineers Engineering District New York

About this file

Written by GovTribe AI · Dec 27, 2023

This document summarizes a federal contract solicitation for maintenance dredging services. The U.S. Army Corps of Engineers seeks to dredge approximately 125,000 cubic yards of sediment from the Arthur Kill 50' Reach in New York and New Jersey Harbor to a depth of -50 feet MLLW plus one foot allowable overdepth. The dredged material consists primarily of silt and clay and must meet all applicable federal, state, and local placement criteria. Bidders must be able to transport, dewater, process, and place the dredged material at a contractor-provided, state-permitted upland site. The apparent low bidder must provide all required placement permits within 35 days of notification. Work is estimated to cost between $10-25 million and shall commence within 5 days of notice to proceed at a rate of at least 2,500 cubic yards per day to minimize channel closure impacts. The Corps intends to award the contract in June/July 2023 for work to be completed between August and October 2023, with $2,540 in liquidated damages per day of delay. This is an unrestricted procurement by the New York District Corps of Engineers.

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Report Date: 07-Sep-2021 07:01:19 Chrom Revision: 2.3 13-May-2021 07:57:40 Eurofins TestAmerica, Pittsburgh

Data File: \\chromfs\Pittsburgh\ChromData\CGC1\20210906-38968.b\0906210000044.D Injection Date: 06-Sep-2021 19:43:18 Instrument ID: CGC1 Operator ID:

Lims ID: LB 180-369612/1-E Worklist Smp#: 40 Client ID:

Injection Vol: 1.0 ul Dil. Factor: 20.0000 ALS Bottle#: 40 Method: Herbicides_CGC1 Limit Group: GCS 8151A ICAL Column: RTX-50 ( 0.53 mm)

0.0 1.0 2.0 3.0 4.0 5.0 6.0 7.0 8.0 9.0 10.0 11.0 12.0 13.0 14.0 15.0 16.0 17.0 Min

Y (X

GC ECD1A, 0906210000044.D

2, 4- D ic hl or op he ny la ce tic a ci d(

Column: RTX-1701 ( 0.53 mm)

0.0 1.0 2.0 3.0 4.0 5.0 6.0 7.0 8.0 9.0 10.0 11.0 12.0 13.0 14.0 15.0 16.0 17.0 Min

Y (X

GC ECD2B, 0906210000044.D

2, 4- D ic hl or op he ny la ce tic a ci d(

Report Date: 07-Sep-2021 07:01:19 Chrom Revision: 2.3 13-May-2021 07:57:40

Recovery Report

Data File: \\chromfs\Pittsburgh\ChromData\CGC1\20210906-38968.b\0906210000044.D Lims ID: LB 180-369612/1-E Client ID:

Sample Type: LB Inject. Date: 06-Sep-2021 19:43:18 ALS Bottle#: 40 Worklist Smp#: 40 Injection Vol: 1.0 ul Dil. Factor: 20.0000 Sample Info: 180-0038968-040 Operator ID: Instrument ID: CGC1

Method: \\chromfs\Pittsburgh\ChromData\CGC1\20210906-38968.b\Herbicides_CGC1.m Limit Group: GCS 8151A ICAL Last Update: 07-Sep-2021 07:01:08 Calib Date: 04-Jun-2021 09:39:01 Integrator: Falcon Quant Method: External Standard Quant By: Initial Calibration Last ICal File: \\chromfs\Pittsburgh\ChromData\CGC1\20210604-37539.b\0604210000011.D

Column 1 : RTX-50 ( 0.53 mm) Det: GC ECD1A Column 2 : RTX-1701 ( 0.53 mm) Det: GC ECD2B Process Host: CTX1633

First Level Reviewer: oravecj Date: 07-Sep-2021 06:52:02

Surrogate Recovery, Detector: GC ECD1A

Compound Amount Added

Amount Recovered % Rec.

$ 2 2,4-Dichlorophenylacetic acid 1.00 0.0246 49.11

Surrogate Recovery, Detector: GC ECD2B

Compound Amount Added

Amount Recovered % Rec.

$ 2 2,4-Dichlorophenylacetic acid 1.00 0.0214 42.90

FORM I

HERBICIDES ORGANICS ANALYSIS DATA SHEET

Client Sample ID:

Lab Name: Job No.:

SDG No.:

180-126039-1

Lab Sample ID: LB 180-369295/1-E

Eurofins TestAmerica, Pittsburgh

Matrix: 0906210000045.DLab File ID:

Date Collected:EPA 8151AAnalysis Method:

Sediment (SPLP East)

Con. Extract Vol.:

Injection Volume:

GPC Cleanup:(Y/N)

Date Extracted:

Date Analyzed:

Dilution Factor: 20

Extraction Method: 8151A 09/02/2021 08:45

09/06/2021 20:03

10.0(mL)

1(uL)

Sample wt/vol: 1000(mL)

% Moisture:

GC Column: ID: 0.53(mm)RTX-50

Analysis Batch No.: 370330 ug/LUnits:

CAS NO. COMPOUND NAME RESULT Q MDLRL

1.0 0.64U93-72-1 Silvex (2,4,5-TP) 1.0

%RECCAS NO. LIMITSQSURROGATE

66 54-11619719-28-9 2,4-Dichlorophenylacetic acid

FORM I EPA 8151A

Report Date: 07-Sep-2021 07:01:16 Chrom Revision: 2.3 13-May-2021 07:57:40

Target Compound Quantitation Report

Data File: \\chromfs\Pittsburgh\ChromData\CGC1\20210906-38968.b\0906210000045.D Lims ID: LB 180-369295/1-E Client ID:

Sample Type: LB Inject. Date: 06-Sep-2021 20:03:01 ALS Bottle#: 41 Worklist Smp#: 41 Injection Vol: 1.0 ul Dil. Factor: 20.0000 Sample Info: 180-0038968-041 Operator ID: Instrument ID: CGC1

Column 1 : RTX-50 ( 0.53 mm) Det: GC ECD1A Column 2 : RTX-1701 ( 0.53 mm) Det: GC ECD2B Process Host: CTX1633

First Level Reviewer: oravecj Date: 07-Sep-2021 06:52:08

Col

(min.)

Exp RT (min.)

Dlt RT (min.) Response

Cal Amt ng

OnCol Amt ng Flags

1 Dalapon

1 2.218 ND

2 2.399

$ 2 2,4-Dichlorophenylacetic acid 1 7.995 7.997 -0.002 7533362H 0.0500 0.0332 2 8.030 8.032 -0.002 8034842H 0.0500 0.0298

RPD = 10.79

3 MCPP

1 8.215 ND

2 8.456

4 Dicamba 7

1 8.293 ND

2 8.299

5 MCPA 7

1 8.632 ND

2 8.763

6 Dichlorprop 7

1 8.911 ND

2 9.125

7 2,4-D 7

1 9.401 ND

2 9.519

8 Pentachlorophenol

1 9.927 ND

2 9.736

9 Silvex (2,4,5-TP)

1 10.083 ND

2 10.290

Data File: \\chromfs\Pittsburgh\ChromData\CGC1\20210906-38968.b\0906210000045.D

Col

(min.)

Exp RT (min.)

Dlt RT (min.) Response

Cal Amt ng

OnCol Amt ng Flags

10 2,4,5-T 7

1 10.629 ND

2 10.744

11 Dinoseb 7

1 10.884 ND

2 11.818

12 2,4-DB 7

1 11.012 ND

2 11.171

QC Flag Legend Processing Flags 7 - Failed Limit of Detection H - Response Measured by Height

Data File: \\chromfs\Pittsburgh\ChromData\CGC1\20210906-38968.b\0906210000045.D Injection Date: 06-Sep-2021 20:03:01 Instrument ID: CGC1 Operator ID:

Lims ID: LB 180-369295/1-E Worklist Smp#: 41 Client ID:

Injection Vol: 1.0 ul Dil. Factor: 20.0000 ALS Bottle#: 41 Method: Herbicides_CGC1 Limit Group: GCS 8151A ICAL Column: RTX-50 ( 0.53 mm)

0.0 1.0 2.0 3.0 4.0 5.0 6.0 7.0 8.0 9.0 10.0 11.0 12.0 13.0 14.0 15.0 16.0 17.0 Min

Y (X

GC ECD1A, 0906210000045.D

2, 4- D ic hl or op he ny la ce tic a ci d(

Column: RTX-1701 ( 0.53 mm)

0.0 1.0 2.0 3.0 4.0 5.0 6.0 7.0 8.0 9.0 10.0 11.0 12.0 13.0 14.0 15.0 16.0 17.0 Min

Y (X

GC ECD2B, 0906210000045.D

2, 4- D ic hl or op he ny la ce tic a ci d(

Recovery Report

Data File: \\chromfs\Pittsburgh\ChromData\CGC1\20210906-38968.b\0906210000045.D Lims ID: LB 180-369295/1-E Client ID:

Sample Type: LB Inject. Date: 06-Sep-2021 20:03:01 ALS Bottle#: 41 Worklist Smp#: 41 Injection Vol: 1.0 ul Dil. Factor: 20.0000 Sample Info: 180-0038968-041 Operator ID: Instrument ID: CGC1

Column 1 : RTX-50 ( 0.53 mm) Det: GC ECD1A Column 2 : RTX-1701 ( 0.53 mm) Det: GC ECD2B Process Host: CTX1633

First Level Reviewer: oravecj Date: 07-Sep-2021 06:52:08

Surrogate Recovery, Detector: GC ECD1A

Compound Amount Added

Amount Recovered % Rec.

$ 2 2,4-Dichlorophenylacetic acid 1.00 0.0332 66.45

Surrogate Recovery, Detector: GC ECD2B

Compound Amount Added

Amount Recovered % Rec.

$ 2 2,4-Dichlorophenylacetic acid 1.00 0.0298 59.64

Client Sample ID:

Lab Name: Job No.:

SDG No.:

180-126039-1

Lab Sample ID: LB 180-369295/1-E

Eurofins TestAmerica, Pittsburgh

Matrix: 0906210000045.DLab File ID:

Date Collected:EPA 8151AAnalysis Method:

Sediment (SPLP East)

Con. Extract Vol.:

Injection Volume:

GPC Cleanup:(Y/N)

Date Extracted:

Date Analyzed:

Dilution Factor: 20

Extraction Method: 8151A 09/02/2021 08:45

09/06/2021 20:03

10.0(mL)

1(uL)

Sample wt/vol: 1000(mL)

% Moisture:

GC Column: ID: 0.53(mm)RTX-1701

Analysis Batch No.: 370330 ug/LUnits:

%RECCAS NO. LIMITSQSURROGATE

60 54-11619719-28-9 2,4-Dichlorophenylacetic acid

Report Date: 07-Sep-2021 07:01:17 Chrom Revision: 2.3 13-May-2021 07:57:40

Target Compound Quantitation Report

Data File: \\chromfs\Pittsburgh\ChromData\CGC1\20210906-38968.b\0906210000045.D Lims ID: LB 180-369295/1-E Client ID:

Sample Type: LB Inject. Date: 06-Sep-2021 20:03:01 ALS Bottle#: 41 Worklist Smp#: 41 Injection Vol: 1.0 ul Dil. Factor: 20.0000 Sample Info: 180-0038968-041 Operator ID: Instrument ID: CGC1

Column 1 : RTX-50 ( 0.53 mm) Det: GC ECD1A Column 2 : RTX-1701 ( 0.53 mm) Det: GC ECD2B Process Host: CTX1633

First Level Reviewer: oravecj Date: 07-Sep-2021 06:52:08

Col

(min.)

Exp RT (min.)

Dlt RT (min.) Response

Cal Amt ng

OnCol Amt ng Flags

1 Dalapon

1 2.218 ND

2 2.399

$ 2 2,4-Dichlorophenylacetic acid 1 7.995 7.997 -0.002 7533362H 0.0500 0.0332 2 8.030 8.032 -0.002 8034842H 0.0500 0.0298

RPD = 10.79

3 MCPP

1 8.215 ND

2 8.456

4 Dicamba 7

1 8.293 ND

2 8.299

5 MCPA 7

1 8.632 ND

2 8.763

6 Dichlorprop 7

1 8.911 ND

2 9.125

7 2,4-D 7

1 9.401 ND

2 9.519

8 Pentachlorophenol

1 9.927 ND

2 9.736

9 Silvex (2,4,5-TP)

1 10.083 ND

2 10.290

Data File: \\chromfs\Pittsburgh\ChromData\CGC1\20210906-38968.b\0906210000045.D

Col

(min.)

Exp RT (min.)

Dlt RT (min.) Response

Cal Amt ng

OnCol Amt ng Flags

10 2,4,5-T 7

1 10.629 ND

2 10.744

11 Dinoseb 7

1 10.884 ND

2 11.818

12 2,4-DB 7

1 11.012 ND

2 11.171

QC Flag Legend Processing Flags 7 - Failed Limit of Detection

Data File: \\chromfs\Pittsburgh\ChromData\CGC1\20210906-38968.b\0906210000045.D Injection Date: 06-Sep-2021 20:03:01 Instrument ID: CGC1 Operator ID:

Lims ID: LB 180-369295/1-E Worklist Smp#: 41 Client ID:

Injection Vol: 1.0 ul Dil. Factor: 20.0000 ALS Bottle#: 41 Method: Herbicides_CGC1 Limit Group: GCS 8151A ICAL Column: RTX-50 ( 0.53 mm)

0.0 1.0 2.0 3.0 4.0 5.0 6.0 7.0 8.0 9.0 10.0 11.0 12.0 13.0 14.0 15.0 16.0 17.0 Min

Y (X

GC ECD1A, 0906210000045.D

2, 4- D ic hl or op he ny la ce tic a ci d(

Column: RTX-1701 ( 0.53 mm)

0.0 1.0 2.0 3.0 4.0 5.0 6.0 7.0 8.0 9.0 10.0 11.0 12.0 13.0 14.0 15.0 16.0 17.0 Min

Y (X

GC ECD2B, 0906210000045.D

2, 4- D ic hl or op he ny la ce tic a ci d(

Recovery Report

Data File: \\chromfs\Pittsburgh\ChromData\CGC1\20210906-38968.b\0906210000045.D Lims ID: LB 180-369295/1-E Client ID:

Sample Type: LB Inject. Date: 06-Sep-2021 20:03:01 ALS Bottle#: 41 Worklist Smp#: 41 Injection Vol: 1.0 ul Dil. Factor: 20.0000 Sample Info: 180-0038968-041 Operator ID: Instrument ID: CGC1

Column 1 : RTX-50 ( 0.53 mm) Det: GC ECD1A Column 2 : RTX-1701 ( 0.53 mm) Det: GC ECD2B Process Host: CTX1633

First Level Reviewer: oravecj Date: 07-Sep-2021 06:52:08

Surrogate Recovery, Detector: GC ECD1A

Compound Amount Added

Amount Recovered % Rec.

$ 2 2,4-Dichlorophenylacetic acid 1.00 0.0332 66.45

Surrogate Recovery, Detector: GC ECD2B

Compound Amount Added

Amount Recovered % Rec.

$ 2 2,4-Dichlorophenylacetic acid 1.00 0.0298 59.64

Client Sample ID:

Lab Name: Job No.:

SDG No.:

180-126039-1

Lab Sample ID: LCS 180-368981/2-A

Eurofins TestAmerica, Pittsburgh

Matrix: 0901210000036.DLab File ID:

Date Collected:EPA 8151AAnalysis Method:

Sediment

Con. Extract Vol.:

Injection Volume:

GPC Cleanup:(Y/N)

Date Extracted:

Date Analyzed:

Dilution Factor: 1

Extraction Method: 8151A 08/24/2021 06:45

09/01/2021 16:35

40.0(mL)

1(uL)

Sample wt/vol: 10.0(g)

% Moisture:

GC Column: ID: 0.53(mm)RTX-50

Analysis Batch No.: 369833 ug/KgUnits:

CAS NO. COMPOUND NAME RESULT Q MDLRL

20 1193-72-1 Silvex (2,4,5-TP) 57.9

%RECCAS NO. LIMITSQSURROGATE

66 48-12719719-28-9 2,4-Dichlorophenylacetic acid

Report Date: 02-Sep-2021 08:36:58 Chrom Revision: 2.3 13-May-2021 07:57:40

Target Compound Quantitation Report

Data File: \\chromfs\Pittsburgh\ChromData\CGC1\20210901-38900.b\0901210000036.D Lims ID: LCS 180-368981/2-A Client ID:

Sample Type: LCS Inject. Date: 01-Sep-2021 16:35:36 ALS Bottle#: 32 Worklist Smp#: 32 Injection Vol: 1.0 ul Dil. Factor: 1.0000 Sample Info: 180-0038900-032 Operator ID: Instrument ID: CGC1

Method: \\chromfs\Pittsburgh\ChromData\CGC1\20210901-38900.b\Herbicides_CGC1.m Limit Group: GCS 8151A ICAL Last Update: 02-Sep-2021 08:36:53 Calib Date: 04-Jun-2021 09:39:01 Integrator: Falcon Quant Method: External Standard Quant By: Initial Calibration Last ICal File: \\chromfs\Pittsburgh\ChromData\CGC1\20210604-37539.b\0604210000011.D

Column 1 : RTX-50 ( 0.53 mm) Det: GC ECD1A Column 2 : RTX-1701 ( 0.53 mm) Det: GC ECD2B Process Host: CTX1657

Col

(min.)

Exp RT (min.)

Dlt RT (min.) Response

Cal Amt ng

OnCol Amt ng Flags

1 Dalapon 1 2.217 2.220 -0.003 22233659 0.1000 0.0374 2 2.398 2.402 -0.004 25242080 0.1000 0.0391

RPD = 4.34

$ 2 2,4-Dichlorophenylacetic acid 1 8.001 8.003 -0.002 7474199H 0.0500 0.0330 2 8.038 8.041 -0.003 9364086H 0.0500 0.0348

RPD = 5.29

3 MCPP

1 8.217 8.219 -0.002 4951438H 10.0 6.69 2 8.462 8.464 -0.002 7549714H 10.0 6.39

RPD = 4.51

4 Dicamba 1 8.299 8.300 -0.001 21831134H 0.0500 0.0270 2 8.306 8.308 -0.002 28732996H 0.0500 0.0290

RPD = 7.36

5 MCPA

1 8.637 8.639 -0.002 7631255H 10.0 6.13 2 8.768 8.771 -0.003 10801491H 10.0 6.06

RPD = 1.14

6 Dichlorprop 1 8.916 8.919 -0.003 12896901H 0.1000 0.0579 2 9.130 9.134 -0.004 15587161H 0.1000 0.0555

RPD = 4.15

7 2,4-D 1 9.406 9.409 -0.003 14796884H 0.1000 0.0571 2 9.525 9.529 -0.004 17919824H 0.1000 0.0582

RPD = 1.89

8 Pentachlorophenol 1 9.934 9.936 -0.002 24452474H 0.0250 0.0102 2 9.742 9.745 -0.003 32660234H 0.0250 0.009220

RPD = 9.75Page 5934 of 9555

Data File: \\chromfs\Pittsburgh\ChromData\CGC1\20210901-38900.b\0901210000036.D

Col

(min.)

Exp RT (min.)

Dlt RT (min.) Response

Cal Amt ng

OnCol Amt ng Flags

9 Silvex (2,4,5-TP) 1 10.088 10.091 -0.003 15927564H 0.0250 0.0145 2 10.299 10.300 -0.001 20305027H 0.0250 0.0138

RPD = 4.69

10 2,4,5-T 1 10.635 10.637 -0.002 15729558H 0.0250 0.0143 2 10.750 10.753 -0.003 18855140H 0.0250 0.0143

RPD = 0.09

11 Dinoseb 1 10.889 10.891 -0.002 6972543H 0.1000 0.0121 2 11.824 11.827 -0.003 6605986H 0.1000 0.0150

RPD = 21.81

12 2,4-DB

1 11.019 11.020 -0.001 8581115H 0.1000 0.0570 2 11.180 11.180 0.000 9760574H 0.1000 0.0571

RPD = 0.26

Data File: \\chromfs\Pittsburgh\ChromData\CGC1\20210901-38900.b\0901210000036.D Injection Date: 01-Sep-2021 16:35:36 Instrument ID: CGC1 Operator ID:

Lims ID: LCS 180-368981/2-A Worklist Smp#: 32 Client ID:

Injection Vol: 1.0 ul Dil. Factor: 1.0000 ALS Bottle#: 32 Method: Herbicides_CGC1 Limit Group: GCS 8151A ICAL Column: RTX-50 ( 0.53 mm)

0.0 1.0 2.0 3.0 4.0 5.0 6.0 7.0 8.0 9.0 10.0 11.0 12.0 13.0 14.0 15.0 16.0 17.0 Min

Y (X

GC ECD1A, 0901210000036.D

D al ap on

2, 4- D ic hl or op he ny la ce tic a ci d(

M C

P P

D ic am ba

M C

P A

D ic hl or pr op

-D

P en ta ch lo ro ph en ol

4) S ilv ex

(2 ,4

,5 -T

( 1 0.

D in os eb

( 1 0.

-D B

( 1 1.

Column: RTX-1701 ( 0.53 mm)

0.0 1.0 2.0 3.0 4.0 5.0 6.0 7.0 8.0 9.0 10.0 11.0 12.0 13.0 14.0 15.0 16.0 17.0 Min

Y (X

GC ECD2B, 0901210000036.D

D al ap on

2, 4- D ic hl or op he ny la ce tic a ci d(

D ic am ba

M C

P P

M C

P A

D ic hl or pr op

-D

5) P en ta ch lo ro ph en ol

S ilv ex (2

,4 ,5

-T P

,5 -T

( 1 0.

-D B

( 1 1.

D in os eb

( 1 1.

Recovery Report

Data File: \\chromfs\Pittsburgh\ChromData\CGC1\20210901-38900.b\0901210000036.D Lims ID: LCS 180-368981/2-A Client ID:

Sample Type: LCS Inject. Date: 01-Sep-2021 16:35:36 ALS Bottle#: 32 Worklist Smp#: 32 Injection Vol: 1.0 ul Dil. Factor: 1.0000 Sample Info: 180-0038900-032 Operator ID: Instrument ID: CGC1

Column 1 : RTX-50 ( 0.53 mm) Det: GC ECD1A Column 2 : RTX-1701 ( 0.53 mm) Det: GC ECD2B Process Host: CTX1657

Surrogate Recovery, Detector: GC ECD1A

Compound Amount Added

Amount Recovered % Rec.

$ 2 2,4-Dichlorophenylacetic acid 0.0500 0.0330 65.92

Surrogate Recovery, Detector: GC ECD2B

Compound Amount Added

Amount Recovered % Rec.

$ 2 2,4-Dichlorophenylacetic acid 0.0500 0.0348 69.51

Client Sample ID:

Lab Name: Job No.:

SDG No.:

180-126039-1

Lab Sample ID: LCS 180-368981/2-A

Eurofins TestAmerica, Pittsburgh

Matrix: 0901210000036.DLab File ID:

Date Collected:EPA 8151AAnalysis Method:

Sediment

Con. Extract Vol.:

Injection Volume:

GPC Cleanup:(Y/N)

Date Extracted:

Date Analyzed:

Dilution Factor: 1

Extraction Method: 8151A 08/24/2021 06:45

09/01/2021 16:35

40.0(mL)

1(uL)

Sample wt/vol: 10.0(g)

% Moisture:

GC Column: ID: 0.53(mm)RTX-1701

Analysis Batch No.: 369833 ug/KgUnits:

%RECCAS NO. LIMITSQSURROGATE

70 48-12719719-28-9 2,4-Dichlorophenylacetic acid

Report Date: 02-Sep-2021 08:36:59 Chrom Revision: 2.3 13-May-2021 07:57:40

Target Compound Quantitation Report

Data File: \\chromfs\Pittsburgh\ChromData\CGC1\20210901-38900.b\0901210000036.D Lims ID: LCS 180-368981/2-A Client ID:

Sample Type: LCS Inject. Date: 01-Sep-2021 16:35:36 ALS Bottle#: 32 Worklist Smp#: 32 Injection Vol: 1.0 ul Dil. Factor: 1.0000 Sample Info: 180-0038900-032 Operator ID: Instrument ID: CGC1

Column 1 : RTX-50 ( 0.53 mm) Det: GC ECD1A Column 2 : RTX-1701 ( 0.53 mm) Det: GC ECD2B Process Host: CTX1657

Col

(min.)

Exp RT (min.)

Dlt RT (min.) Response

Cal Amt ng

OnCol Amt ng Flags

1 Dalapon 1 2.217 2.220 -0.003 22233659 0.1000 0.0374 2 2.398 2.402 -0.004 25242080 0.1000 0.0391

RPD = 4.34

$ 2 2,4-Dichlorophenylacetic acid 1 8.001 8.003 -0.002 7474199H 0.0500 0.0330 2 8.038 8.041 -0.003 9364086H 0.0500 0.0348

RPD = 5.29

3 MCPP

1 8.217 8.219 -0.002 4951438H 10.0 6.69 2 8.462 8.464 -0.002 7549714H 10.0 6.39

RPD = 4.51

4 Dicamba 1 8.299 8.300 -0.001 21831134H 0.0500 0.0270 2 8.306 8.308 -0.002 28732996H 0.0500 0.0290

RPD = 7.36

5 MCPA

1 8.637 8.639 -0.002 7631255H 10.0 6.13 2 8.768 8.771 -0.003 10801491H 10.0 6.06

RPD = 1.14

6 Dichlorprop 1 8.916 8.919 -0.003 12896901H 0.1000 0.0579 2 9.130 9.134 -0.004 15587161H 0.1000 0.0555

RPD = 4.15

7 2,4-D 1 9.406 9.409 -0.003 14796884H 0.1000 0.0571 2 9.525 9.529 -0.004 17919824H 0.1000 0.0582

RPD = 1.89

8 Pentachlorophenol 1 9.934 9.936 -0.002 24452474H 0.0250 0.0102 2 9.742 9.745 -0.003 32660234H 0.0250 0.009220

RPD = 9.75Page 5939 of 9555

Data File: \\chromfs\Pittsburgh\ChromData\CGC1\20210901-38900.b\0901210000036.D

Col

(min.)

Exp RT (min.)

Dlt RT (min.) Response

Cal Amt ng

OnCol Amt ng Flags

9 Silvex (2,4,5-TP) 1 10.088 10.091 -0.003 15927564H 0.0250 0.0145 2 10.299 10.300 -0.001 20305027H 0.0250 0.0138

RPD = 4.69

10 2,4,5-T 1 10.635 10.637 -0.002 15729558H 0.0250 0.0143 2 10.750 10.753 -0.003 18855140H 0.0250 0.0143

RPD = 0.09

11 Dinoseb 1 10.889 10.891 -0.002 6972543H 0.1000 0.0121 2 11.824 11.827 -0.003 6605986H 0.1000 0.0150

RPD = 21.81

12 2,4-DB

1 11.019 11.020 -0.001 8581115H 0.1000 0.0570 2 11.180 11.180 0.000 9760574H 0.1000 0.0571

RPD = 0.26

Data File: \\chromfs\Pittsburgh\ChromData\CGC1\20210901-38900.b\0901210000036.D Injection Date: 01-Sep-2021 16:35:36 Instrument ID: CGC1 Operator ID:

Lims ID: LCS 180-368981/2-A Worklist Smp#: 32 Client ID:

Injection Vol: 1.0 ul Dil. Factor: 1.0000 ALS Bottle#: 32 Method: Herbicides_CGC1 Limit Group: GCS 8151A ICAL Column: RTX-50 ( 0.53 mm)

0.0 1.0 2.0 3.0 4.0 5.0 6.0 7.0 8.0 9.0 10.0 11.0 12.0 13.0 14.0 15.0 16.0 17.0 Min

Y (X

GC ECD1A, 0901210000036.D

D al ap on

2, 4- D ic hl or op he ny la ce tic a ci d(

M C

P P

D ic am ba

M C

P A

D ic hl or pr op

-D

P en ta ch lo ro ph en ol

4) S ilv ex

(2 ,4

,5 -T

( 1 0.

D in os eb

( 1 0.

-D B

( 1 1.

Column: RTX-1701 ( 0.53 mm)

0.0 1.0 2.0 3.0 4.0 5.0 6.0 7.0 8.0 9.0 10.0 11.0 12.0 13.0 14.0 15.0 16.0 17.0 Min

Y (X

GC ECD2B, 0901210000036.D

D al ap on

2, 4- D ic hl or op he ny la ce tic a ci d(

D ic am ba

M C

P P

M C

P A

D ic hl or pr op

-D

5) P en ta ch lo ro ph en ol

S ilv ex (2

,4 ,5

-T P

,5 -T

( 1 0.

-D B

( 1 1.

D in os eb

( 1 1.

Recovery Report

Data File: \\chromfs\Pittsburgh\ChromData\CGC1\20210901-38900.b\0901210000036.D Lims ID: LCS 180-368981/2-A Client ID:

Sample Type: LCS Inject. Date: 01-Sep-2021 16:35:36 ALS Bottle#: 32 Worklist Smp#: 32 Injection Vol: 1.0 ul Dil. Factor: 1.0000 Sample Info: 180-0038900-032 Operator ID: Instrument ID: CGC1

Column 1 : RTX-50 ( 0.53 mm) Det: GC ECD1A Column 2 : RTX-1701 ( 0.53 mm) Det: GC ECD2B Process Host: CTX1657

Surrogate Recovery, Detector: GC ECD1A

Compound Amount Added

Amount Recovered % Rec.

$ 2 2,4-Dichlorophenylacetic acid 0.0500 0.0330 65.92

Surrogate Recovery, Detector: GC ECD2B

Compound Amount Added

Amount Recovered % Rec.

$ 2 2,4-Dichlorophenylacetic acid 0.0500 0.0348 69.51

Client Sample ID:

Lab Name: Job No.:

SDG No.:

180-126039-1

Lab Sample ID: LCS 180-370087/2-A

Eurofins TestAmerica, Pittsburgh

Matrix: 0906210000037.DLab File ID:

Date Collected:EPA 8151AAnalysis Method:

Sediment

Con. Extract Vol.:

Injection Volume:

GPC Cleanup:(Y/N)

Date Extracted:

Date Analyzed:

Dilution Factor: 20

Extraction Method: 8151A 09/02/2021 08:45

09/06/2021 17:26

10.0(mL)

1(uL)

Sample wt/vol: 1000(mL)

% Moisture:

GC Column: ID: 0.53(mm)RTX-50

Analysis Batch No.: 370330 ug/LUnits:

%RECCAS NO. LIMITSQSURROGATE

67 54-11619719-28-9 2,4-Dichlorophenylacetic acid

Report Date: 07-Sep-2021 07:01:32 Chrom Revision: 2.3 13-May-2021 07:57:40

Target Compound Quantitation Report

Data File: \\chromfs\Pittsburgh\ChromData\CGC1\20210906-38968.b\0906210000037.D Lims ID: LCS 180-370087/2-A Client ID:

Sample Type: LCS Inject. Date: 06-Sep-2021 17:26:22 ALS Bottle#: 33 Worklist Smp#: 33 Injection Vol: 1.0 ul Dil. Factor: 20.0000 Sample Info: 180-0038968-033 Operator ID: Instrument ID: CGC1

Method: \\chromfs\Pittsburgh\ChromData\CGC1\20210906-38968.b\Herbicides_CGC1.m Limit Group: GCS 8151A ICAL Last Update: 07-Sep-2021 07:01:30 Calib Date: 04-Jun-2021 09:39:01 Integrator: Falcon Quant Method: External Standard Quant By: Initial Calibration Last ICal File: \\chromfs\Pittsburgh\ChromData\CGC1\20210604-37539.b\0604210000011.D

Column 1 : RTX-50 ( 0.53 mm) Det: GC ECD1A Column 2 : RTX-1701 ( 0.53 mm) Det: GC ECD2B Process Host: CTX1633

First Level Reviewer: oravecj Date: 07-Sep-2021 06:51:05

Col

(min.)

Exp RT (min.)

Dlt RT (min.) Response

Cal Amt ng

OnCol Amt ng Flags

1 Dalapon 1 2.211 2.218 -0.007 29699160 0.1000 0.0520 2 2.392 2.399 -0.007 35419350 0.1000 0.0549

RPD = 5.36

$ 2 2,4-Dichlorophenylacetic acid 1 7.995 7.997 -0.002 7545701H 0.0500 0.0333 2 8.030 8.032 -0.002 7642455H 0.0500 0.0284

RPD = 15.94

3 MCPP

1 8.212 8.215 -0.003 5706047H 10.0 7.70 2 8.454 8.456 -0.002 8316965H 10.0 7.04

RPD = 9.01

4 Dicamba 1 8.290 8.293 -0.003 27323600H 0.0500 0.0338 2 8.295 8.299 -0.004 34444966H 0.0500 0.0348

RPD = 3.05

5 MCPA

1 8.630 8.632 -0.002 6529989H 10.0 5.25 2 8.759 8.763 -0.004 10019476H 10.0 5.63

RPD = 6.93

6 Dichlorprop 1 8.907 8.911 -0.004 12383411H 0.1000 0.0556 2 9.121 9.125 -0.004 14800894H 0.1000 0.0527

RPD = 5.26

7 2,4-D 1 9.397 9.401 -0.004 10908069H 0.1000 0.0421 2 9.516 9.519 -0.003 12665378H 0.1000 0.0412

RPD = 2.32

Data File: \\chromfs\Pittsburgh\ChromData\CGC1\20210906-38968.b\0906210000037.D

Col

(min.)

Exp RT (min.)

Dlt RT (min.) Response

Cal Amt ng

OnCol Amt ng Flags

8 Pentachlorophenol 1 9.925 9.927 -0.002 45449563H 0.0250 0.0189 2 9.734 9.736 -0.002 64327665H 0.0250 0.0182

RPD = 3.97

9 Silvex (2,4,5-TP) 1 10.080 10.083 -0.003 17589720H 0.0250 0.0160 2 10.286 10.290 -0.004 23961890H 0.0250 0.0163

RPD = 1.94

10 2,4,5-T 1 10.627 10.629 -0.002 13876352H 0.0250 0.0126 2 10.740 10.744 -0.004 16281449H 0.0250 0.0124

RPD = 2.05

11 Dinoseb 1 10.881 10.884 -0.003 42534732H 0.1000 0.0736 2 11.815 11.818 -0.003 46639112H 0.1000 0.1061

RPD = 36.11

12 2,4-DB

1 11.009 11.012 -0.003 5854662H 0.1000 0.0389 2 11.169 11.171 -0.002 6016547H 0.1000 0.0352

RPD = 9.88

QC Flag Legend Processing Flags

Data File: \\chromfs\Pittsburgh\ChromData\CGC1\20210906-38968.b\0906210000037.D Injection Date: 06-Sep-2021 17:26:22 Instrument ID: CGC1 Operator ID:

Lims ID: LCS 180-370087/2-A Worklist Smp#: 33 Client ID:

Injection Vol: 1.0 ul Dil. Factor: 20.0000 ALS Bottle#: 33 Method: Herbicides_CGC1 Limit Group: GCS 8151A ICAL Column: RTX-50 ( 0.53 mm)

0.0 1.0 2.0 3.0 4.0 5.0 6.0 7.0 8.0 9.0 10.0 11.0 12.0 13.0 14.0 15.0 16.0 17.0 Min

Y (X

GC ECD1A, 0906210000037.D

D al ap on

2, 4- D ic hl or op he ny la ce tic a ci d(

M C

P P

D ic am ba

M C

P A

D ic hl or pr op

-D

P en ta ch lo ro ph en ol

5) S ilv ex

(2 ,4

,5 -T

( 1 0.

7) D in os eb ( 1

,4 -D

B ( 1

Column: RTX-1701 ( 0.53 mm)

0.0 1.0 2.0 3.0 4.0 5.0 6.0 7.0 8.0 9.0 10.0 11.0 12.0 13.0 14.0 15.0 16.0 17.0 Min

Y (X

GC ECD2B, 0906210000037.D

D al ap on

2, 4- D ic hl or op he ny la ce tic a ci d(

D ic am ba

M C

P P

M C

P A

D ic hl or pr op

-D

6) P en ta ch lo ro ph en ol

S ilv ex (2

,4 ,5

-T P

,5 -T

( 1 0.

-D B

( 1 1.

D in os eb

( 1 1.

Recovery Report

Data File: \\chromfs\Pittsburgh\ChromData\CGC1\20210906-38968.b\0906210000037.D Lims ID: LCS 180-370087/2-A Client ID:

Sample Type: LCS Inject. Date: 06-Sep-2021 17:26:22 ALS Bottle#: 33 Worklist Smp#: 33 Injection Vol: 1.0 ul Dil. Factor: 20.0000 Sample Info: 180-0038968-033 Operator ID: Instrument ID: CGC1

Column 1 : RTX-50 ( 0.53 mm) Det: GC ECD1A Column 2 : RTX-1701 ( 0.53 mm) Det: GC ECD2B Process Host: CTX1633

First Level Reviewer: oravecj Date: 07-Sep-2021 06:51:05

Surrogate Recovery, Detector: GC ECD1A

Compound Amount Added

Amount Recovered % Rec.

$ 2 2,4-Dichlorophenylacetic acid 1.00 0.0333 66.55

Surrogate Recovery, Detector: GC ECD2B

Compound Amount Added

Amount Recovered % Rec.

$ 2 2,4-Dichlorophenylacetic acid 1.00 0.0284 56.73

Client Sample ID:

Lab Name: Job No.:

SDG No.:

180-126039-1

Lab Sample ID: LCS 180-370087/2-A

Eurofins TestAmerica, Pittsburgh

Matrix: 0906210000037.DLab File ID:

Date Collected:EPA 8151AAnalysis Method:

Sediment

Con. Extract Vol.:

Injection Volume:

GPC Cleanup:(Y/N)

Date Extracted:

Date Analyzed:

Dilution Factor: 20

Extraction Method: 8151A 09/02/2021 08:45

09/06/2021 17:26

10.0(mL)

1(uL)

Sample wt/vol: 1000(mL)

% Moisture:

GC Column: ID: 0.53(mm)RTX-1701

Analysis Batch No.: 370330 ug/LUnits:

CAS NO. COMPOUND NAME RESULT Q MDLRL

1.0 0.6493-72-1 Silvex (2,4,5-TP) 3.26

%RECCAS NO. LIMITSQSURROGATE

57 54-11619719-28-9 2,4-Dichlorophenylacetic acid

Report Date: 07-Sep-2021 07:01:33 Chrom Revision: 2.3 13-May-2021 07:57:40

Target Compound Quantitation Report

Data File: \\chromfs\Pittsburgh\ChromData\CGC1\20210906-38968.b\0906210000037.D Lims ID: LCS 180-370087/2-A Client ID:

Sample Type: LCS Inject. Date: 06-Sep-2021 17:26:22 ALS Bottle#: 33 Worklist Smp#: 33 Injection Vol: 1.0 ul Dil. Factor: 20.0000 Sample Info: 180-0038968-033 Operator ID: Instrument ID: CGC1

Column 1 : RTX-50 ( 0.53 mm) Det: GC ECD1A Column 2 : RTX-1701 ( 0.53 mm) Det: GC ECD2B Process Host: CTX1633

First Level Reviewer: oravecj Date: 07-Sep-2021 06:51:05

Col

(min.)

Exp RT (min.)

Dlt RT (min.) Response

Cal Amt ng

OnCol Amt ng Flags

1 Dalapon 1 2.211 2.218 -0.007 29699160 0.1000 0.0520 2 2.392 2.399 -0.007 35419350 0.1000 0.0549

RPD = 5.36

$ 2 2,4-Dichlorophenylacetic acid 1 7.995 7.997 -0.002 7545701H 0.0500 0.0333 2 8.030 8.032 -0.002 7642455H 0.0500 0.0284

RPD = 15.94

3 MCPP

1 8.212 8.215 -0.003 5706047H 10.0 7.70 2 8.454 8.456 -0.002 8316965H 10.0 7.04

RPD = 9.01

4 Dicamba 1 8.290 8.293 -0.003 27323600H 0.0500 0.0338 2 8.295 8.299 -0.004 34444966H 0.0500 0.0348

RPD = 3.05

5 MCPA

1 8.630 8.632 -0.002 6529989H 10.0 5.25 2 8.759 8.763 -0.004 10019476H 10.0 5.63

RPD = 6.93

6 Dichlorprop 1 8.907 8.911 -0.004 12383411H 0.1000 0.0556 2 9.121 9.125 -0.004 14800894H 0.1000 0.0527

RPD = 5.26

7 2,4-D 1 9.397 9.401 -0.004 10908069H 0.1000 0.0421 2 9.516 9.519 -0.003 12665378H 0.1000 0.0412

RPD = 2.32

Data File: \\chromfs\Pittsburgh\ChromData\CGC1\20210906-38968.b\0906210000037.D

Col

(min.)

Exp RT (min.)

Dlt RT (min.) Response

Cal Amt ng

OnCol Amt ng Flags

8 Pentachlorophenol 1 9.925 9.927 -0.002 45449563H 0.0250 0.0189 2 9.734 9.736 -0.002 64327665H 0.0250 0.0182

RPD = 3.97

9 Silvex (2,4,5-TP) 1 10.080 10.083 -0.003 17589720H 0.0250 0.0160 2 10.286 10.290 -0.004 23961890H 0.0250 0.0163

RPD = 1.94

10 2,4,5-T 1 10.627 10.629 -0.002 13876352H 0.0250 0.0126 2 10.740 10.744 -0.004 16281449H 0.0250 0.0124

RPD = 2.05

11 Dinoseb 1 10.881 10.884 -0.003 42534732H 0.1000 0.0736 2 11.815 11.818 -0.003 46639112H 0.1000 0.1061

RPD = 36.11

12 2,4-DB

1 11.009 11.012 -0.003 5854662H 0.1000 0.0389 2 11.169 11.171 -0.002 6016547H 0.1000 0.0352

RPD = 9.88

QC Flag Legend Processing Flags

Data File: \\chromfs\Pittsburgh\ChromData\CGC1\20210906-38968.b\0906210000037.D Injection Date: 06-Sep-2021 17:26:22 Instrument ID: CGC1 Operator ID:

Lims ID: LCS 180-370087/2-A Worklist Smp#: 33 Client ID:

Injection Vol: 1.0 ul Dil. Factor: 20.0000 ALS Bottle#: 33 Method: Herbicides_CGC1 Limit Group: GCS 8151A ICAL Column: RTX-50 ( 0.53 mm)

0.0 1.0 2.0 3.0 4.0 5.0 6.0 7.0 8.0 9.0 10.0 11.0 12.0 13.0 14.0 15.0 16.0 17.0 Min

Y (X

GC ECD1A, 0906210000037.D

D al ap on

2, 4- D ic hl or op he ny la ce tic a ci d(

M C

P P

D ic am ba

M C

P A

D ic hl or pr op

-D

P en ta ch lo ro ph en ol

5) S ilv ex

(2 ,4

,5 -T

( 1 0.

7) D in os eb ( 1

,4 -D

B ( 1

Column: RTX-1701 ( 0.53 mm)

0.0 1.0 2.0 3.0 4.0 5.0 6.0 7.0 8.0 9.0 10.0 11.0 12.0 13.0 14.0 15.0 16.0 17.0 Min

Y (X

GC ECD2B, 0906210000037.D

D al ap on

2, 4- D ic hl or op he ny la ce tic a ci d(

D ic am ba

M C

P P

M C

P A

D ic hl or pr op

-D

6) P en ta ch lo ro ph en ol

S ilv ex (2

,4 ,5

-T P

,5 -T

( 1 0.

-D B

( 1 1.

D in os eb

( 1 1.

Recovery Report

Data File: \\chromfs\Pittsburgh\ChromData\CGC1\20210906-38968.b\0906210000037.D Lims ID: LCS 180-370087/2-A Client ID:

Sample Type: LCS Inject. Date: 06-Sep-2021 17:26:22 ALS Bottle#: 33 Worklist Smp#: 33 Injection Vol: 1.0 ul Dil. Factor: 20.0000 Sample Info: 180-0038968-033 Operator ID: Instrument ID: CGC1

Column 1 : RTX-50 ( 0.53 mm) Det: GC ECD1A Column 2 : RTX-1701 ( 0.53 mm) Det: GC ECD2B Process Host: CTX1633

First Level Reviewer: oravecj Date: 07-Sep-2021 06:51:05

Surrogate Recovery, Detector: GC ECD1A

Compound Amount Added

Amount Recovered % Rec.

$ 2 2,4-Dichlorophenylacetic acid 1.00 0.0333 66.55

Surrogate Recovery, Detector: GC ECD2B

Compound Amount Added

Amount Recovered % Rec.

$ 2 2,4-Dichlorophenylacetic acid 1.00 0.0284 56.73

Client Sample ID:

Lab Name: Job No.:

SDG No.:

180-126039-1

Lab Sample ID: LCSD 180-368981/3-A

Eurofins TestAmerica, Pittsburgh

Matrix: 0901210000037.DLab File ID:

Date Collected:EPA 8151AAnalysis Method:

Sediment

Con. Extract Vol.:

Injection Volume:

GPC Cleanup:(Y/N)

Date Extracted:

Date Analyzed:

Dilution Factor: 1

Extraction Method: 8151A 08/24/2021 06:45

09/01/2021 16:55

40.0(mL)

1(uL)

Sample wt/vol: 10.0(g)

% Moisture:

GC Column: ID: 0.53(mm)RTX-50

Analysis Batch No.: 369833 ug/KgUnits:

CAS NO. COMPOUND NAME RESULT Q MDLRL

20 1193-72-1 Silvex (2,4,5-TP) 63.9

%RECCAS NO. LIMITSQSURROGATE

69 48-12719719-28-9 2,4-Dichlorophenylacetic acid

Report Date: 02-Sep-2021 08:36:56 Chrom Revision: 2.3 13-May-2021 07:57:40

Target Compound Quantitation Report

Data File: \\chromfs\Pittsburgh\ChromData\CGC1\20210901-38900.b\0901210000037.D Lims ID: LCSD 180-368981/3-A Client ID:

Sample Type: LCSD Inject. Date: 01-Sep-2021 16:55:05 ALS Bottle#: 33 Worklist Smp#: 33 Injection Vol: 1.0 ul Dil. Factor: 1.0000 Sample Info: 180-0038900-033 Operator ID: Instrument ID: CGC1

Column 1 : RTX-50 ( 0.53 mm) Det: GC ECD1A Column 2 : RTX-1701 ( 0.53 mm) Det: GC ECD2B Process Host: CTX1657

Col

(min.)

Exp RT (min.)

Dlt RT (min.) Response

Cal Amt ng

OnCol Amt ng Flags

1 Dalapon 1 2.214 2.220 -0.006 22937699 0.1000 0.0388 2 2.396 2.402 -0.006 20397518 0.1000 0.0316

RPD = 20.50

$ 2 2,4-Dichlorophenylacetic acid 1 7.998 8.003 -0.005 7816058H 0.0500 0.0345 2 8.036 8.041 -0.005 9587405H 0.0500 0.0356

RPD = 3.18

3 MCPP

1 8.213 8.219 -0.006 5494555H 10.0 7.42 2 8.459 8.464 -0.005 7996034H 10.0 6.77

RPD = 9.17

4 Dicamba 1 8.294 8.300 -0.006 24043383H 0.0500 0.0297 2 8.301 8.308 -0.007 30575003H 0.0500 0.0309

RPD = 3.92

5 MCPA

1 8.633 8.639 -0.006 8232975H 10.0 6.62 2 8.765 8.771 -0.006 11512306H 10.0 6.46

RPD = 2.35

6 Dichlorprop 1 8.911 8.919 -0.008 13921792H 0.1000 0.0625 2 9.128 9.134 -0.006 17005059H 0.1000 0.0606

RPD = 3.09

7 2,4-D 1 9.403 9.409 -0.006 16425274H 0.1000 0.0634 2 9.523 9.529 -0.006 19552258H 0.1000 0.0635

RPD = 0.17

8 Pentachlorophenol 1 9.929 9.936 -0.007 26368370H 0.0250 0.0110 2 9.739 9.745 -0.006 35431491H 0.0250 0.0100

RPD = 9.16Page 5954 of 9555

Data File: \\chromfs\Pittsburgh\ChromData\CGC1\20210901-38900.b\0901210000037.D

Col

(min.)

Exp RT (min.)

Dlt RT (min.) Response

Cal Amt ng

OnCol Amt ng Flags

9 Silvex (2,4,5-TP) 1 10.084 10.091 -0.007 17586592H 0.0250 0.0160 2 10.293 10.300 -0.007 22537281H 0.0250 0.0153

RPD = 4.17

10 2,4,5-T 1 10.631 10.637 -0.006 16995872H 0.0250 0.0155 2 10.746 10.753 -0.007 20717509H 0.0250 0.0157

RPD = 1.77

11 Dinoseb 1 10.886 10.891 -0.005 7622132H 0.1000 0.0132 2 11.821 11.827 -0.006 7166875H 0.1000 0.0163

RPD = 21.06

12 2,4-DB

1 11.015 11.020 -0.005 9464186H 0.1000 0.0628 2 11.175 11.180 -0.005 10819256H 0.1000 0.0633

RPD = 0.76

Data File: \\chromfs\Pittsburgh\ChromData\CGC1\20210901-38900.b\0901210000037.D Injection Date: 01-Sep-2021 16:55:05 Instrument ID: CGC1 Operator ID:

Lims ID: LCSD 180-368981/3-A Worklist Smp#: 33 Client ID:

Injection Vol: 1.0 ul Dil. Factor: 1.0000 ALS Bottle#: 33 Method: Herbicides_CGC1 Limit Group: GCS 8151A ICAL Column: RTX-50 ( 0.53 mm)

0.0 1.0 2.0 3.0 4.0 5.0 6.0 7.0 8.0 9.0 10.0 11.0 12.0 13.0 14.0 15.0 16.0 17.0 Min

Y (X

GC ECD1A, 0901210000037.D

D al ap on

2, 4- D ic hl or op he ny la ce tic a ci d(

M C

P P

D ic am ba

M C

P A

D ic hl or pr op

-D

P en ta ch lo ro ph en ol

9) S ilv ex

(2 ,4

,5 -T

( 1 0.

D in os eb

( 1 0.

-D B

( 1 1.

Column: RTX-1701 ( 0.53 mm)

0.0 1.0 2.0 3.0 4.0 5.0 6.0 7.0 8.0 9.0 10.0 11.0 12.0 13.0 14.0 15.0 16.0 17.0 Min

Y (X

GC ECD2B, 0901210000037.D

D al ap on

2, 4- D ic hl or op he ny la ce tic a ci d(

D ic am ba

M C

P P

M C

P A

D ic hl or pr op

-D

3) P en ta ch lo ro ph en ol

S ilv ex (2

,4 ,5

-T P

,5 -T

( 1 0.

-D B

( 1 1.

D in os eb

( 1 1.

Recovery Report

Data File: \\chromfs\Pittsburgh\ChromData\CGC1\20210901-38900.b\0901210000037.D Lims ID: LCSD 180-368981/3-A Client ID:

Sample Type: LCSD Inject. Date: 01-Sep-2021 16:55:05 ALS Bottle#: 33 Worklist Smp#: 33 Injection Vol: 1.0 ul Dil. Factor: 1.0000 Sample Info: 180-0038900-033 Operator ID: Instrument ID: CGC1

Column 1 : RTX-50 ( 0.53 mm) Det: GC ECD1A Column 2 : RTX-1701 ( 0.53 mm) Det: GC ECD2B Process Host: CTX1657

Surrogate Recovery, Detector: GC ECD1A

Compound Amount Added

Amount Recovered % Rec.

$ 2 2,4-Dichlorophenylacetic acid 0.0500 0.0345 68.94

Surrogate Recovery, Detector: GC ECD2B

Compound Amount Added

Amount Recovered % Rec.

$ 2 2,4-Dichlorophenylacetic acid 0.0500 0.0356 71.17

Client Sample ID:

Lab Name: Job No.:

SDG No.:

180-126039-1

Lab Sample ID: LCSD 180-368981/3-A

Eurofins TestAmerica, Pittsburgh

Matrix: 0901210000037.DLab File ID:

Date Collected:EPA 8151AAnalysis Method:

Sediment

Con. Extract Vol.:

Injection Volume:

GPC Cleanup:(Y/N)

Date Extracted:

Date Analyzed:

Dilution Factor: 1

Extraction Method: 8151A 08/24/2021 06:45

09/01/2021 16:55

40.0(mL)

1(uL)

Sample wt/vol: 10.0(g)

% Moisture:

GC Column: ID: 0.53(mm)RTX-1701

Analysis Batch No.: 369833 ug/KgUnits:

%RECCAS NO. LIMITSQSURROGATE

71 48-12719719-28-9 2,4-Dichlorophenylacetic acid

Report Date: 02-Sep-2021 08:36:57 Chrom Revision: 2.3 13-May-2021 07:57:40

Target Compound Quantitation Report

Data File: \\chromfs\Pittsburgh\ChromData\CGC1\20210901-38900.b\0901210000037.D Lims ID: LCSD 180-368981/3-A Client ID:

Sample Type: LCSD Inject. Date: 01-Sep-2021 16:55:05 ALS Bottle#: 33 Worklist Smp#: 33 Injection Vol: 1.0 ul Dil. Factor: 1.0000 Sample Info: 180-0038900-033 Operator ID: Instrument ID: CGC1

Column 1 : RTX-50 ( 0.53 mm) Det: GC ECD1A Column 2 : RTX-1701 ( 0.53 mm) Det: GC ECD2B Process Host: CTX1657

Col

(min.)

Exp RT (min.)

Dlt RT (min.) Response

Cal Amt ng

OnCol Amt ng Flags

1 Dalapon 1 2.214 2.220 -0.006 22937699 0.1000 0.0388 2 2.396 2.402 -0.006 20397518 0.1000 0.0316

RPD = 20.50

$ 2 2,4-Dichlorophenylacetic acid 1 7.998 8.003 -0.005 7816058H 0.0500 0.0345 2 8.036 8.041 -0.005 9587405H 0.0500 0.0356

RPD = 3.18

3 MCPP

1 8.213 8.219 -0.006 5494555H 10.0 7.42 2 8.459 8.464 -0.005 7996034H 10.0 6.77

RPD = 9.17

4 Dicamba 1 8.294 8.300 -0.006 24043383H 0.0500 0.0297 2 8.301 8.308 -0.007 30575003H 0.0500 0.0309

RPD = 3.92

5 MCPA

1 8.633 8.639 -0.006 8232975H 10.0 6.62 2 8.765 8.771 -0.006 11512306H 10.0 6.46

RPD = 2.35

6 Dichlorprop 1 8.911 8.919 -0.008 13921792H 0.1000 0.0625 2 9.128 9.134 -0.006 17005059H 0.1000 0.0606

RPD = 3.09

7 2,4-D 1 9.403 9.409 -0.006 16425274H 0.1000 0.0634 2 9.523 9.529 -0.006 19552258H 0.1000 0.0635

RPD = 0.17

8 Pentachlorophenol 1 9.929 9.936 -0.007 26368370H 0.0250 0.0110 2 9.739 9.745 -0.006 35431491H 0.0250 0.0100

RPD = 9.16Page 5959 of 9555

Data File: \\chromfs\Pittsburgh\ChromData\CGC1\20210901-38900.b\0901210000037.D

Col

(min.)

Exp RT (min.)

Dlt RT (min.) Response

Cal Amt ng

OnCol Amt ng Flags

9 Silvex (2,4,5-TP) 1 10.084 10.091 -0.007 17586592H 0.0250 0.0160 2 10.293 10.300 -0.007 22537281H 0.0250 0.0153

RPD = 4.17

10 2,4,5-T 1 10.631 10.637 -0.006 16995872H 0.0250 0.0155 2 10.746 10.753 -0.007 20717509H 0.0250 0.0157

RPD = 1.77

11 Dinoseb 1 10.886 10.891 -0.005 7622132H 0.1000 0.0132 2 11.821 11.827 -0.006 7166875H 0.1000 0.0163

RPD = 21.06

12 2,4-DB

1 11.015 11.020 -0.005 9464186H 0.1000 0.0628 2 11.175 11.180 -0.005 10819256H 0.1000 0.0633

RPD = 0.76

Data File: \\chromfs\Pittsburgh\ChromData\CGC1\20210901-38900.b\0901210000037.D Injection Date: 01-Sep-2021 16:55:05 Instrument ID: CGC1 Operator ID:

Lims ID: LCSD 180-368981/3-A Worklist Smp#: 33 Client ID:

Injection Vol: 1.0 ul Dil. Factor: 1.0000 ALS Bottle#: 33 Method: Herbicides_CGC1 Limit Group: GCS 8151A ICAL Column: RTX-50 ( 0.53 mm)

0.0 1.0 2.0 3.0 4.0 5.0 6.0 7.0 8.0 9.0 10.0 11.0 12.0 13.0 14.0 15.0 16.0 17.0 Min

Y (X

GC ECD1A, 0901210000037.D

D al ap on

2, 4- D ic hl or op he ny la ce tic a ci d(

M C

P P

D ic am ba

M C

P A

D ic hl or pr op

-D

P en ta ch lo ro ph en ol

9) S ilv ex

(2 ,4

,5 -T

( 1 0.

D in os eb

( 1 0.

-D B

( 1 1.

Column: RTX-1701 ( 0.53 mm)

0.0 1.0 2.0 3.0 4.0 5.0 6.0 7.0 8.0 9.0 10.0 11.0 12.0 13.0 14.0 15.0 16.0 17.0 Min

Y (X

GC ECD2B, 0901210000037.D

D al ap on

2, 4- D ic hl or op he ny la ce tic a ci d(

D ic am ba

M C

P P

M C

P A

D ic hl or pr op

-D

3) P en ta ch lo ro ph en ol

S ilv ex (2

,4 ,5

-T P

,5 -T

( 1 0.

-D B

( 1 1.

D in os eb

( 1 1.

Recovery Report

Data File: \\chromfs\Pittsburgh\ChromData\CGC1\20210901-38900.b\0901210000037.D Lims ID: LCSD 180-368981/3-A Client ID:

Sample Type: LCSD Inject. Date: 01-Sep-2021 16:55:05 ALS Bottle#: 33 Worklist Smp#: 33 Injection Vol: 1.0 ul Dil. Factor: 1.0000 Sample Info: 180-0038900-033 Operator ID: Instrument ID: CGC1

Column 1 : RTX-50 ( 0.53 mm) Det: GC ECD1A Column 2 : RTX-1701 ( 0.53 mm) Det: GC ECD2B Process Host: CTX1657

Surrogate Recovery, Detector: GC ECD1A

Compound Amount Added

Amount Recovered % Rec.

$ 2 2,4-Dichlorophenylacetic acid 0.0500 0.0345 68.94

Surrogate Recovery, Detector: GC ECD2B

Compound Amount Added

Amount Recovered % Rec.

$ 2 2,4-Dichlorophenylacetic acid 0.0500 0.0356 71.17

Lab Name: Job No.:

SDG No.:

Instrument ID:

Analysis Batch Number:

HERBICIDES ANALYSIS RUN LOG

DILUTION

FACTOR

COLUMN IDDATE ANALYZEDLAB SAMPLE ID CLIENT SAMPLE ID LAB FILE ID

Eurofins TestAmerica, Pittsburgh 180-126039-1

CGC1

359437

Start Date:

End Date: 06/04/2021 17:28

06/04/2021 07:41

IC 180-359437/1 RTX-50 0.53(mm)106/04/2021 07:41 0604210000005.D

IC 180-359437/1 RTX-1701 0.53(mm)106/04/2021 07:41 0604210000005.D

IC 180-359437/2 RTX-50 0.53(mm)106/04/2021 08:01 0604210000006.D

IC 180-359437/2 RTX-1701 0.53(mm)106/04/2021 08:01 0604210000006.D

IC 180-359437/3 RTX-50 0.53(mm)106/04/2021 08:20 0604210000007.D

IC 180-359437/3 RTX-1701 0.53(mm)106/04/2021 08:20 0604210000007.D

ICRT 180-359437/4 RTX-50 0.53(mm)106/04/2021 08:40 0604210000008.D

ICRT 180-359437/4 RTX-1701 0.53(mm)106/04/2021 08:40 0604210000008.D

IC 180-359437/5 RTX-50 0.53(mm)106/04/2021 09:00 0604210000009.D

IC 180-359437/5 RTX-1701 0.53(mm)106/04/2021 09:00 0604210000009.D

IC 180-359437/6 RTX-50 0.53(mm)106/04/2021 09:19 0604210000010.D

IC 180-359437/6 RTX-1701 0.53(mm)106/04/2021 09:19 0604210000010.D

IC 180-359437/7 RTX-50 0.53(mm)106/04/2021 09:39 0604210000011.D

IC 180-359437/7 RTX-1701 0.53(mm)106/04/2021 09:39 0604210000011.D

ICV 180-359437/8 RTX-50 0.53(mm)106/04/2021 09:58 0604210000012.D

ICV 180-359437/8 RTX-1701 0.53(mm)106/04/2021 09:58 0604210000012.D

ZZZZZ RTX-50 0.53(mm)106/04/2021 10:18

ZZZZZ RTX-1701 0.53(mm)106/04/2021 10:18

ZZZZZ RTX-50 0.53(mm)106/04/2021 10:37

ZZZZZ RTX-1701 0.53(mm)106/04/2021 10:37

ZZZZZ RTX-50 0.53(mm)106/04/2021 10:57

ZZZZZ RTX-1701 0.53(mm)106/04/2021 10:57

ZZZZZ RTX-50 0.53(mm)106/04/2021 11:16

ZZZZZ RTX-1701 0.53(mm)106/04/2021 11:16

ZZZZZ RTX-50 0.53(mm)106/04/2021 11:36

ZZZZZ RTX-1701 0.53(mm)106/04/2021 11:36

ZZZZZ RTX-50 0.53(mm)106/04/2021 11:55

ZZZZZ RTX-1701 0.53(mm)106/04/2021 11:55

ZZZZZ RTX-50 0.53(mm)106/04/2021 12:15

ZZZZZ RTX-1701 0.53(mm)106/04/2021 12:15

ZZZZZ RTX-50 0.53(mm)106/04/2021 12:35

ZZZZZ RTX-1701 0.53(mm)106/04/2021 12:35

ZZZZZ RTX-50 0.53(mm)106/04/2021 12:54

ZZZZZ RTX-1701 0.53(mm)106/04/2021 12:54

ZZZZZ RTX-50 0.53(mm)106/04/2021 13:14

ZZZZZ RTX-1701 0.53(mm)106/04/2021 13:14

CCV 180-359437/19 RTX-50 0.53(mm)106/04/2021 13:33

CCV 180-359437/19 RTX-1701 0.53(mm)106/04/2021 13:33

ZZZZZ RTX-50 0.53(mm)106/04/2021 13:53

ZZZZZ RTX-1701 0.53(mm)106/04/2021 13:53

ZZZZZ RTX-50 0.53(mm)106/04/2021 14:12

ZZZZZ RTX-1701 0.53(mm)106/04/2021 14:12

ZZZZZ RTX-50 0.53(mm)106/04/2021 14:32

ZZZZZ RTX-1701 0.53(mm)106/04/2021 14:32

ZZZZZ RTX-50 0.53(mm)106/04/2021 14:51

EPA 8151A

Instrument ID:

Analysis Batch Number:

HERBICIDES ANALYSIS RUN LOG

DILUTION

FACTOR

COLUMN IDDATE ANALYZEDLAB SAMPLE ID CLIENT SAMPLE ID LAB FILE ID

Eurofins TestAmerica, Pittsburgh 180-126039-1

CGC1

359437

Start Date:

End Date: 06/04/2021 17:28

06/04/2021 07:41

ZZZZZ RTX-1701 0.53(mm)106/04/2021 14:51

ZZZZZ RTX-50 0.53(mm)106/04/2021 15:11

ZZZZZ RTX-1701 0.53(mm)106/04/2021 15:11

ZZZZZ RTX-50 0.53(mm)106/04/2021 15:31

ZZZZZ RTX-1701 0.53(mm)106/04/2021 15:31

ZZZZZ RTX-50 0.53(mm)106/04/2021 15:50

ZZZZZ RTX-1701 0.53(mm)106/04/2021 15:50

ZZZZZ RTX-50 0.53(mm)106/04/2021 16:10

ZZZZZ RTX-1701 0.53(mm)106/04/2021 16:10

ZZZZZ RTX-50 0.53(mm)106/04/2021 16:29

ZZZZZ RTX-1701 0.53(mm)106/04/2021 16:29

ZZZZZ RTX-50 0.53(mm)106/04/2021 16:49

ZZZZZ RTX-1701 0.53(mm)106/04/2021 16:49

CCV 180-359437/30 RTX-50 0.53(mm)106/04/2021 17:08

CCV 180-359437/30 RTX-1701 0.53(mm)106/04/2021 17:08

CCVL 180-359437/31 RTX-50 0.53(mm)106/04/2021 17:28

CCVL 180-359437/31 RTX-1701 0.53(mm)106/04/2021 17:28

Instrument ID:

Analysis Batch Number:

HERBICIDES ANALYSIS RUN LOG

DILUTION

FACTOR

COLUMN IDDATE ANALYZEDLAB SAMPLE ID CLIENT SAMPLE ID LAB FILE ID

Eurofins TestAmerica, Pittsburgh 180-126039-1

CGC1

369833

Start Date:

End Date: 09/01/2021 21:28

09/01/2021 06:18

CCVRT 180-369833/1 RTX-50 0.53(mm)109/01/2021 06:18 0901210000005.D

CCVRT 180-369833/1 RTX-1701 0.53(mm)109/01/2021 06:18 0901210000005.D

ZZZZZ RTX-50 0.53(mm)2009/01/2021 06:49

ZZZZZ RTX-1701 0.53(mm)2009/01/2021 06:49

ZZZZZ RTX-50 0.53(mm)2009/01/2021 07:09

ZZZZZ RTX-1701 0.53(mm)2009/01/2021 07:09

ZZZZZ RTX-50 0.53(mm)2009/01/2021 07:28

ZZZZZ RTX-1701 0.53(mm)2009/01/2021 07:28

ZZZZZ RTX-50 0.53(mm)2009/01/2021 07:48

ZZZZZ RTX-1701 0.53(mm)2009/01/2021 07:48

ZZZZZ RTX-50 0.53(mm)2009/01/2021 08:07

ZZZZZ RTX-1701 0.53(mm)2009/01/2021 08:07

ZZZZZ RTX-50 0.53(mm)2009/01/2021 08:27

ZZZZZ RTX-1701 0.53(mm)2009/01/2021 08:27

ZZZZZ RTX-50 0.53(mm)2009/01/2021 08:46

ZZZZZ RTX-1701 0.53(mm)2009/01/2021 08:46

ZZZZZ RTX-50 0.53(mm)2009/01/2021 09:06

ZZZZZ RTX-1701 0.53(mm)2009/01/2021 09:06

ZZZZZ RTX-50 0.53(mm)2009/01/2021 09:26

ZZZZZ RTX-1701 0.53(mm)2009/01/2021 09:26

ZZZZZ RTX-50 0.53(mm)2009/01/2021 09:45

ZZZZZ RTX-1701 0.53(mm)2009/01/2021 09:45

CCV 180-369833/12 RTX-50 0.53(mm)109/01/2021 10:05

CCV 180-369833/12 RTX-1701 0.53(mm)109/01/2021 10:05

ZZZZZ RTX-50 0.53(mm)2009/01/2021 10:24

ZZZZZ RTX-1701 0.53(mm)2009/01/2021 10:24

ZZZZZ RTX-50 0.53(mm)2009/01/2021 10:44

ZZZZZ RTX-1701 0.53(mm)2009/01/2021 10:44

ZZZZZ RTX-50 0.53(mm)2009/01/2021 11:03

ZZZZZ RTX-1701 0.53(mm)2009/01/2021 11:03

ZZZZZ RTX-50 0.53(mm)2009/01/2021 11:23

ZZZZZ RTX-1701 0.53(mm)2009/01/2021 11:23

ZZZZZ RTX-50 0.53(mm)2009/01/2021 11:42

ZZZZZ RTX-1701 0.53(mm)2009/01/2021 11:42

ZZZZZ RTX-50 0.53(mm)2009/01/2021 12:02

ZZZZZ RTX-1701 0.53(mm)2009/01/2021 12:02

ZZZZZ RTX-50 0.53(mm)2009/01/2021 12:21

ZZZZZ RTX-1701 0.53(mm)2009/01/2021 12:21

ZZZZZ RTX-50 0.53(mm)2009/01/2021 12:41

ZZZZZ RTX-1701 0.53(mm)2009/01/2021 12:41

ZZZZZ RTX-50 0.53(mm)2009/01/2021 13:00

ZZZZZ RTX-1701 0.53(mm)2009/01/2021 13:00

ZZZZZ RTX-50 0.53(mm)2009/01/2021 13:20

ZZZZZ RTX-1701 0.53(mm)2009/01/2021 13:20

CCV 180-369833/23 RTX-50 0.53(mm)109/01/2021 13:40 0901210000027.D

Instrument ID:

Analysis Batch Number:

HERBICIDES ANALYSIS RUN LOG

DILUTION

FACTOR

COLUMN IDDATE ANALYZEDLAB SAMPLE ID CLIENT SAMPLE ID LAB FILE ID

Eurofins TestAmerica, Pittsburgh 180-126039-1

CGC1

369833

Start Date:

End Date: 09/01/2021 21:28

09/01/2021 06:18

CCV 180-369833/23 RTX-1701 0.53(mm)109/01/2021 13:40 0901210000027.D

ZZZZZ RTX-50 0.53(mm)2009/01/2021 13:59

ZZZZZ RTX-1701 0.53(mm)2009/01/2021 13:59

ZZZZZ RTX-50 0.53(mm)2009/01/2021 14:18

ZZZZZ RTX-1701 0.53(mm)2009/01/2021 14:18

MB 180-368981/1-A RTX-50 0.53(mm)109/01/2021 14:38 0901210000030.D

MB 180-368981/1-A RTX-1701 0.53(mm)109/01/2021 14:38 0901210000030.D

180-126039-1 #20210909 COMPOSITE

S/DISCRETE S-1

RTX-50 0.53(mm)109/01/2021 14:57 0901210000031.D

180-126039-1 #20210909 COMPOSITE

S/DISCRETE S-1

RTX-1701 0.53(mm)109/01/2021 14:57 0901210000031.D

180-126039-2 #20210941 COMPOSITE T RTX-50 0.53(mm)109/01/2021 15:17 0901210000032.D

180-126039-2 #20210941 COMPOSITE T RTX-1701 0.53(mm)109/01/2021 15:17 0901210000032.D

180-126039-3 #20210942 COMPOSITE U RTX-50 0.53(mm)109/01/2021 15:36 0901210000033.D

180-126039-3 #20210942 COMPOSITE U RTX-1701 0.53(mm)109/01/2021 15:36 0901210000033.D

180-126039-4 #20210943 COMPOSITE V RTX-50 0.53(mm)109/01/2021 15:56 0901210000034.D

180-126039-4 #20210943 COMPOSITE V RTX-1701 0.53(mm)109/01/2021 15:56 0901210000034.D

180-126039-5 #20210944 COMPOSITE W RTX-50 0.53(mm)109/01/2021 16:16 0901210000035.D

180-126039-5 #20210944 COMPOSITE W RTX-1701 0.53(mm)109/01/2021 16:16 0901210000035.D

LCS 180-368981/2-A RTX-50 0.53(mm)109/01/2021 16:35 0901210000036.D

LCS 180-368981/2-A RTX-1701 0.53(mm)109/01/2021 16:35 0901210000036.D

LCSD 180-368981/3-A RTX-50 0.53(mm)109/01/2021 16:55 0901210000037.D

LCSD 180-368981/3-A RTX-1701 0.53(mm)109/01/2021 16:55 0901210000037.D

CCV 180-369833/34 RTX-50 0.53(mm)109/01/2021 17:14 0901210000038.D

CCV 180-369833/34 RTX-1701 0.53(mm)109/01/2021 17:14 0901210000038.D

180-126039-9 #20210951 AMENDED

COMPOSITE S/DISCRETE

S-1

RTX-50 0.53(mm)109/01/2021 17:34 0901210000039.D

180-126039-9 #20210951 AMENDED

COMPOSITE S/DISCRETE

S-1

RTX-1701 0.53(mm)109/01/2021 17:34 0901210000039.D

180-126039-10 #20210952 AMENDED

COMPOSITE T

RTX-50 0.53(mm)109/01/2021 17:53 0901210000040.D

180-126039-10 #20210952 AMENDED

COMPOSITE T

RTX-1701 0.53(mm)109/01/2021 17:53 0901210000040.D

180-126039-11 #20210953 AMENDED

COMPOSITE U

RTX-50 0.53(mm)109/01/2021 18:13 0901210000041.D

180-126039-11 #20210953 AMENDED

COMPOSITE U

RTX-1701 0.53(mm)109/01/2021 18:13 0901210000041.D

180-126039-12 #20210954 AMENDED

COMPOSITE V

RTX-50 0.53(mm)109/01/2021 18:32 0901210000042.D

180-126039-12 #20210954 AMENDED

COMPOSITE V

RTX-1701 0.53(mm)109/01/2021 18:32 0901210000042.D

180-126039-13 #20210955 AMENDED

COMPOSITE W

RTX-50 0.53(mm)109/01/2021 18:52 0901210000043.D

180-126039-13 #20210955 AMENDED

COMPOSITE W

RTX-1701 0.53(mm)109/01/2021 18:52 0901210000043.D

180-126039-6 #20210945 COMPOSITE X RTX-50 0.53(mm)109/01/2021 19:11 0901210000044.D

180-126039-6 #20210945 COMPOSITE X RTX-1701 0.53(mm)109/01/2021 19:11 0901210000044.D

180-126039-7 #20210946 COMPOSITE Y RTX-50 0.53(mm)109/01/2021 19:31 0901210000045.D

180-126039-7 #20210946 COMPOSITE Y RTX-1701 0.53(mm)109/01/2021 19:31 0901210000045.D

180-126039-8 #20210947 COMPOSITE Z RTX-50 0.53(mm)109/01/2021 19:50 0901210000046.D

180-126039-8 #20210947 COMPOSITE Z RTX-1701 0.53(mm)109/01/2021 19:50 0901210000046.D

Instrument ID:

Analy…

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