J126039-1 Std_Tal_L4 Final Report_Part4.pdf

PDF 20 MB Posted Apr 12, 2023

Attached to: Maintenance Dredging of New York and New Jersey Harbor – Arthur Kill 50’ Reach, Federal Navigation Project
Solicitation number: W912DS23B0004
Issued by: Department of the Army Corps of Engineers Engineering District New York

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Written by GovTribe AI · Dec 27, 2023

This document summarizes a federal contract solicitation for maintenance dredging services. The U.S. Army Corps of Engineers is seeking a contractor to dredge approximately 125,000 cubic yards of sediment from the Arthur Kill 50' Reach in New York and New Jersey Harbor to a depth of -50 feet MLLW plus one foot allowable overdepth. The dredged material consists primarily of silt and clay and must meet all applicable federal, state, and local placement criteria. Bidders must be prepared to furnish permitted upland placement sites, transport dredged material via barge, and maintain a production rate of at least 2,500 cubic yards per day. The contract is estimated to cost between $10-25 million and will be awarded in June/July 2023 for work to be completed between August and October 2023. Liquidated damages of $2,540 per calendar day of delay will be assessed. This is an unrestricted procurement conducted by the U.S. Army Corps of Engineers New York District.

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Report Date: 13-Sep-2021 12:55:52 Chrom Revision: 2.3 13-May-2021 07:57:40 Eurofins TestAmerica, Pittsburgh

Data File: \\chromfs\Pittsburgh\ChromData\CHGC15\20210913-39090.b\Q0913210000015.D Injection Date: 13-Sep-2021 12:34:00 Instrument ID: CHGC15 Operator ID: 402331 Lims ID: MB 180-369080/1-B Worklist Smp#: 15 Client ID:

Injection Vol: 1.0 uL Dil. Factor: 1.0000 ALS Bottle#: 15 Method: IS PEST_CHGC15 Limit Group: GCS 8081B ICAL with IS Column: MR-1 ( 0.53 mm)

0.0 1.0 2.0 3.0 4.0 5.0 6.0 7.0 8.0 9.0 10.0 11.0 12.0 Min

Y (X

GC ECD1A, Q0913210000015.D

B ro m o-

2-ni tro be nz en e(

Te tra ch lo ro

-m -x yl en e(

H ex ac hl or ob en ze ne

I so dr in

'-D D

D ib ut yl ch lo re nd at e

C B

D ec ac hl or ob ip he ny l (

S ur

r) ( 1

Column: MR-2 ( 0.53 mm)

0.0 1.0 2.0 3.0 4.0 5.0 6.0 7.0 8.0 9.0 10.0 11.0 12.0 Min

Y (X

GC ECD2B, Q0913210000015.D

B ro m o-

2-ni tro be nz en e(

Te tra ch lo ro

-m -x yl en e(

H ex ac hl or ob en ze ne

I so dr in

'-D D

D ib ut yl ch lo re nd at e

C B

D ec ac hl or ob ip he ny l (

S ur

r) ( 1

Report Date: 13-Sep-2021 12:55:52 Chrom Revision: 2.3 13-May-2021 07:57:40

Recovery Report

Data File: \\chromfs\Pittsburgh\ChromData\CHGC15\20210913-39090.b\Q0913210000015.D Lims ID: MB 180-369080/1-B Client ID:

Sample Type: MB Inject. Date: 13-Sep-2021 12:34:00 ALS Bottle#: 15 Worklist Smp#: 15 Injection Vol: 1.0 uL Dil. Factor: 1.0000 Sample Info: 180-0039090-015 Operator ID: 402331 Instrument ID: CHGC15

Method: \\chromfs\Pittsburgh\ChromData\CHGC15\20210913-39090.b\IS PEST_CHGC15.m Limit Group: GCS 8081B ICAL with IS Last Update: 13-Sep-2021 12:55:41 Calib Date: 01-Sep-2021 15:22:50 Integrator: Falcon Quant Method: Internal Standard Quant By: Initial Calibration Last ICal File: \\chromfs\Pittsburgh\ChromData\CHGC15\20210901-38917.b\Q0901210000006.D

Column 1 : MR-1 ( 0.53 mm) Det: GC ECD1A Column 2 : MR-2 ( 0.53 mm) Det: GC ECD2B Process Host: CTX1666

First Level Reviewer: eppinged Date: 13-Sep-2021 12:55:41

Surrogate Recovery, Detector: GC ECD1A

Compound Amount Added

Amount Recovered % Rec.

$ 3 Tetrachloro-m-xylene 0.0400 0.0159 39.80

$ 39 DCB Decachlorobiphenyl (Surr) 0.0400 0.0257 64.33

Surrogate Recovery, Detector: GC ECD2B

Compound Amount Added

Amount Recovered % Rec.

$ 3 Tetrachloro-m-xylene 0.0400 0.0175 43.69

$ 39 DCB Decachlorobiphenyl (Surr) 0.0400 0.0234 58.60

Report Date: 13-Sep-2021 12:55:53 Chrom Revision: 2.3 13-May-2021 07:57:40 User Disabled Compound Report

Eurofins TestAmerica, Pittsburgh Data File: \\chromfs\Pittsburgh\ChromData\CHGC15\20210913-39090.b\Q0913210000015.D Injection Date: 13-Sep-2021 12:34:00 Instrument ID: CHGC15 Lims ID: MB 180-369080/1-B Client ID:

Operator ID: 402331 ALS Bottle#: 15 Worklist Smp#: 15 Injection Vol: 1.0 uL Dil. Factor: 1.0000 Method: IS PEST_CHGC15 Limit Group: GCS 8081B ICAL with IS

Column: MR-1 ( 0.53 mm) Detector GC ECD1A 13 Aldrin, CAS: 309-00-2, Signal: 1

RT: 6.25

Response: 2202687 Amount: 0.000436

6.0 6.2 6.4 Min

GC ECD1A, Q0913210000015.D

Column: MR-2 ( 0.53 mm) Detector GC ECD2B 13 Aldrin, CAS: 309-00-2, Signal: 2

RT: 6.54

Response: 1340463 Amount: 0.000275

6.4 6.6 Min

Y (X

GC ECD2B, Q0913210000015.D

Reviewer: eppinged, 13-Sep-2021 12:55:41 Audit Action: Marked Compound Undetected Audit Reason: Invalid Compound ID

Operator ID: 402331 ALS Bottle#: 15 Worklist Smp#: 15 Injection Vol: 1.0 uL Dil. Factor: 1.0000 Method: IS PEST_CHGC15 Limit Group: GCS 8081B ICAL with IS

Column: MR-1 ( 0.53 mm) Detector GC ECD1A 35 Endosulfan sulfate, CAS: 1031-07-8, Signal: 1

RT: 7.93

Response: 2712672 Amount: 0.000934

7.8 8.0 Min

Y (X

GC ECD1A, Q0913210000015.D

Column: MR-2 ( 0.53 mm) Detector GC ECD2B 35 Endosulfan sulfate, CAS: 1031-07-8, Signal: 2

RT: 8.51

Response: 711216 Amount: 0.000329

8.4 8.6 Min

Y (X

GC ECD2B, Q0913210000015.D

Reviewer: eppinged, 13-Sep-2021 12:55:41

FORM I

PESTICIDES ORGANICS ANALYSIS DATA SHEET

Client Sample ID:

Lab Name: Job No.:

SDG No.:

180-126039-1

Lab Sample ID: MB 180-369080/1-B

Eurofins TestAmerica, Pittsburgh

Matrix: Q0913210000015.DLab File ID:

Date Collected:EPA 8081B LLAnalysis Method:

Sediment

Con. Extract Vol.:

Injection Volume:

GPC Cleanup:(Y/N)

Date Extracted:

Date Analyzed:

Dilution Factor: 1

Extraction Method: 3541 08/25/2021 09:32

09/13/2021 12:34

0.5(mL)

1(uL)

Sample wt/vol: 30.0(g)

% Moisture:

GC Column: ID: 0.53(mm)MR-2

Analysis Batch No.: 371152 ug/KgUnits:

%RECCAS NO. LIMITSQSURROGATE

44 20-137877-09-8 Tetrachloro-m-xylene (Surr)

59 46-1302051-24-3 DCB Decachlorobiphenyl (Surr)

FORM I EPA 8081B LL

Target Compound Quantitation Report

Data File: \\chromfs\Pittsburgh\ChromData\CHGC15\20210913-39090.b\Q0913210000015.D Lims ID: MB 180-369080/1-B Client ID:

Sample Type: MB Inject. Date: 13-Sep-2021 12:34:00 ALS Bottle#: 15 Worklist Smp#: 15 Injection Vol: 1.0 uL Dil. Factor: 1.0000 Sample Info: 180-0039090-015 Operator ID: 402331 Instrument ID: CHGC15

Column 1 : MR-1 ( 0.53 mm) Det: GC ECD1A Column 2 : MR-2 ( 0.53 mm) Det: GC ECD2B Process Host: CTX1666

First Level Reviewer: eppinged Date: 13-Sep-2021 12:55:41

Col

(min.)

Exp RT (min.)

Dlt RT (min.) Response

Cal Amt ng

OnCol Amt ng Flags

* 43 1-Bromo-2-nitrobenzene 1 3.858 3.859 -0.001 583321341H 0.1000 0.1000 2 4.315 4.313 0.002 467545932H 0.1000 0.1000

$ 3 Tetrachloro-m-xylene 1 4.851 4.854 -0.003 108875636H 0.0400 0.0159 2 5.182 5.182 0.000 102090241H 0.0400 0.0175

RPD = 9.32

4 Diallate

1 5.004 ND

1 5.095 2 5.297 2 5.383

5 alpha-BHC

1 5.229 ND

2 5.644

6 Hexachlorobenzene M 1 5.259 5.259 0.000 22333335H 0.003374 2 5.605 5.608 -0.003 10557438H 0.002019 M

RPD = 50.27

7 gamma-BHC (Lindane)

1 5.498 ND

2 5.944

8 beta-BHC

1 5.666 ND

2 6.176

10 delta-BHC

1 5.868 ND

2 6.409

Data File: \\chromfs\Pittsburgh\ChromData\CHGC15\20210913-39090.b\Q0913210000015.D

Col

(min.)

Exp RT (min.)

Dlt RT (min.) Response

Cal Amt ng

OnCol Amt ng Flags

9 Chlordane (technical)

1 5.965 ND

1 6.228 1 6.834 1 6.903 2 6.115 2 6.275 2 7.226 2 7.272

11 Heptachlor

1 5.969 ND

2 6.275

12 DCPA

1 6.181 ND

2 6.530

13 Aldrin U

1 6.253 ND

2 6.544

14 Isodrin M 1 6.534 6.534 0.000 1642792H 0.000335 M 2 6.885 6.895 -0.010 3583449H 0.000510 M

RPD = 41.27

15 oxy-Chlordane

1 6.570 ND

2 6.895

16 Heptachlor epoxide

1 6.618 ND

2 6.987

17 2,4'-DDE

1 6.752 ND

2 7.120

18 trans-Chlordane

1 6.837 ND

2 7.212

19 Chlorobenside

1 6.859 ND

2 7.282

22 trans-Nonachlor

1 6.904 ND

2 7.228

20 cis-Chlordane

1 6.905 ND

2 7.273

21 Endosulfan I 7

1 6.952 ND

2 7.340

23 4,4'-DDE

1 7.055 ND

2 7.398

Col

(min.)

Exp RT (min.)

Dlt RT (min.) Response

Cal Amt ng

OnCol Amt ng Flags

34 Toxaphene

1 7.095 ND

1 7.368 1 7.825 1 7.904 2 7.522 2 7.571 2 8.316 2 8.824

25 2,4'-DDD M

1 7.141 7.147 -0.006 957261H 0.000392 2 7.555 7.555 0.000 1319196H 0.000509 M

RPD = 26.00

24 Dieldrin

1 7.194 ND

2 7.582

27 Endrin

1 7.398 ND

2 7.846

28 2,4'-DDT

1 7.423 ND

2 7.801

30 cis-Nonachlor 7

1 7.483 ND

2 7.883

29 4,4'-DDD

1 7.520 ND

2 7.910

31 Endosulfan II

1 7.599 ND

2 8.108

32 Endrin aldehyde

1 7.716 ND

2 8.283

33 4,4'-DDT

1 7.799 ND

2 8.164

35 Endosulfan sulfate U

1 7.928 ND

2 8.520

36 Methoxychlor

1 8.258 ND

2 8.760

* 44 Dibutylchlorendate ISTD 1 8.324 8.327 -0.003 260708535H 0.1000 0.1000 2 8.576 8.579 -0.003 252013882H 0.1000 0.1000

37 Endrin ketone

1 8.408 ND

2 9.173

Col

(min.)

Exp RT (min.)

Dlt RT (min.) Response

Cal Amt ng

OnCol Amt ng Flags

38 Mirex

1 8.929 ND

2 9.482

$ 39 DCB Decachlorobiphenyl (Surr) 1 10.208 10.209 -0.001 41340801H 0.0400 0.0257 2 10.987 10.993 -0.006 35819559H 0.0400 0.0234

RPD = 9.33

QC Flag Legend Processing Flags 7 - Failed Limit of Detection H - Response Measured by Height Review Flags M - Manually Integrated U - Marked Undetected Reagents:

GCPESTISSPK2_00024 Amount Added: 0.02 Units: mL Run Reagent

Injection Vol: 1.0 uL Dil. Factor: 1.0000 ALS Bottle#: 15 Method: IS PEST_CHGC15 Limit Group: GCS 8081B ICAL with IS Column: MR-1 ( 0.53 mm)

0.0 1.0 2.0 3.0 4.0 5.0 6.0 7.0 8.0 9.0 10.0 11.0 12.0 Min

Y (X

GC ECD1A, Q0913210000015.D

B ro m o-

2-ni tro be nz en e(

Te tra ch lo ro

-m -x yl en e(

H ex ac hl or ob en ze ne

I so dr in

'-D D

D ib ut yl ch lo re nd at e

C B

D ec ac hl or ob ip he ny l (

S ur

r) ( 1

Column: MR-2 ( 0.53 mm)

0.0 1.0 2.0 3.0 4.0 5.0 6.0 7.0 8.0 9.0 10.0 11.0 12.0 Min

Y (X

GC ECD2B, Q0913210000015.D

B ro m o-

2-ni tro be nz en e(

Te tra ch lo ro

-m -x yl en e(

H ex ac hl or ob en ze ne

I so dr in

'-D D

D ib ut yl ch lo re nd at e

C B

D ec ac hl or ob ip he ny l (

S ur

r) ( 1

Recovery Report

Data File: \\chromfs\Pittsburgh\ChromData\CHGC15\20210913-39090.b\Q0913210000015.D Lims ID: MB 180-369080/1-B Client ID:

Sample Type: MB Inject. Date: 13-Sep-2021 12:34:00 ALS Bottle#: 15 Worklist Smp#: 15 Injection Vol: 1.0 uL Dil. Factor: 1.0000 Sample Info: 180-0039090-015 Operator ID: 402331 Instrument ID: CHGC15

Column 1 : MR-1 ( 0.53 mm) Det: GC ECD1A Column 2 : MR-2 ( 0.53 mm) Det: GC ECD2B Process Host: CTX1666

First Level Reviewer: eppinged Date: 13-Sep-2021 12:55:41

Surrogate Recovery, Detector: GC ECD1A

Compound Amount Added

Amount Recovered % Rec.

$ 3 Tetrachloro-m-xylene 0.0400 0.0159 39.80

$ 39 DCB Decachlorobiphenyl (Surr) 0.0400 0.0257 64.33

Surrogate Recovery, Detector: GC ECD2B

Compound Amount Added

Amount Recovered % Rec.

$ 3 Tetrachloro-m-xylene 0.0400 0.0175 43.69

$ 39 DCB Decachlorobiphenyl (Surr) 0.0400 0.0234 58.60

Operator ID: 402331 ALS Bottle#: 15 Worklist Smp#: 15 Injection Vol: 1.0 uL Dil. Factor: 1.0000 Method: IS PEST_CHGC15 Limit Group: GCS 8081B ICAL with IS

Column: MR-1 ( 0.53 mm) Detector GC ECD1A 13 Aldrin, CAS: 309-00-2, Signal: 1

RT: 6.25

Response: 2202687 Amount: 0.000436

6.0 6.2 6.4 Min

GC ECD1A, Q0913210000015.D

Column: MR-2 ( 0.53 mm) Detector GC ECD2B 13 Aldrin, CAS: 309-00-2, Signal: 2

RT: 6.54

Response: 1340463 Amount: 0.000275

6.4 6.6 Min

Y (X

GC ECD2B, Q0913210000015.D

Reviewer: eppinged, 13-Sep-2021 12:55:41

Operator ID: 402331 ALS Bottle#: 15 Worklist Smp#: 15 Injection Vol: 1.0 uL Dil. Factor: 1.0000 Method: IS PEST_CHGC15 Limit Group: GCS 8081B ICAL with IS

Column: MR-1 ( 0.53 mm) Detector GC ECD1A 35 Endosulfan sulfate, CAS: 1031-07-8, Signal: 1

RT: 7.93

Response: 2712672 Amount: 0.000934

7.8 8.0 Min

Y (X

GC ECD1A, Q0913210000015.D

Column: MR-2 ( 0.53 mm) Detector GC ECD2B 35 Endosulfan sulfate, CAS: 1031-07-8, Signal: 2

RT: 8.51

Response: 711216 Amount: 0.000329

8.4 8.6 Min

Y (X

GC ECD2B, Q0913210000015.D

Reviewer: eppinged, 13-Sep-2021 12:55:41

Client Sample ID:

Lab Name: Job No.:

SDG No.:

180-126039-1

Lab Sample ID: MB 180-370070/1-A

Eurofins TestAmerica, Pittsburgh

Matrix: Q0907210000006.DLab File ID:

Date Collected:EPA 8081B LLAnalysis Method:

Sediment

Con. Extract Vol.:

Injection Volume:

GPC Cleanup:(Y/N)

Date Extracted:

Date Analyzed:

Dilution Factor: 1

Extraction Method: 3510C 09/02/2021 06:45

09/07/2021 14:52

1.0(mL)

1(uL)

Sample wt/vol: 1000(mL)

% Moisture:

GC Column: ID: 0.53(mm)MR-1

Analysis Batch No.: 370468 ug/LUnits:

CAS NO. COMPOUND NAME RESULT Q MDLRL

0.0013 0.00036U309-00-2 Aldrin 0.0013

0.0013 0.00024U319-84-6 alpha-BHC 0.0013

0.0013 0.00037U319-85-7 beta-BHC 0.0013

0.0013 0.00064U319-86-8 delta-BHC 0.0013

0.0013 0.00029U58-89-9 gamma-BHC (Lindane) 0.0013

0.0013 0.00037U5103-71-9 cis-Chlordane 0.0013

0.0013 0.00041U5103-74-2 trans-Chlordane 0.0013

0.0013 0.00053U72-54-8 4,4'-DDD 0.0013

0.0013 0.00030U72-55-9 4,4'-DDE 0.0013

0.0013 0.00030U50-29-3 4,4'-DDT 0.0013

0.0013 0.00027U60-57-1 Dieldrin 0.0013

0.0013 0.00069U959-98-8 Endosulfan I 0.0013

0.0013 0.00032U33213-65-9 Endosulfan II 0.0013

0.0013 0.00064U1031-07-8 Endosulfan sulfate 0.0013

0.0013 0.00023U72-20-8 Endrin 0.0013

0.0013 0.00045U76-44-8 Heptachlor 0.0013

0.0013 0.00034U1024-57-3 Heptachlor epoxide 0.0013

0.0013 0.00078U72-43-5 Methoxychlor 0.0013

0.0013 0.00021U2385-85-5 Mirex 0.0013

0.10 0.049U8001-35-2 Toxaphene 0.10

%RECCAS NO. LIMITSQSURROGATE

86 25-122877-09-8 Tetrachloro-m-xylene (Surr)

109 32-1352051-24-3 DCB Decachlorobiphenyl (Surr)

Report Date: 08-Sep-2021 06:59:08 Chrom Revision: 2.3 13-May-2021 07:57:40

Target Compound Quantitation Report

Data File: \\chromfs\Pittsburgh\ChromData\CHGC15\20210907-38994.b\Q0907210000006.D Lims ID: MB 180-370070/1-A Client ID:

Sample Type: MB Inject. Date: 07-Sep-2021 14:52:34 ALS Bottle#: 6 Worklist Smp#: 6 Injection Vol: 1.0 uL Dil. Factor: 1.0000 Sample Info: 180-0038994-006 Operator ID: 402331 Instrument ID: CHGC15

Method: \\chromfs\Pittsburgh\ChromData\CHGC15\20210907-38994.b\IS PEST_CHGC15.m Limit Group: GCS 8081B ICAL with IS Last Update: 08-Sep-2021 06:59:07 Calib Date: 01-Sep-2021 15:22:50 Integrator: Falcon Quant Method: Internal Standard Quant By: Initial Calibration Last ICal File: \\chromfs\Pittsburgh\ChromData\CHGC15\20210901-38917.b\Q0901210000006.D

Column 1 : MR-1 ( 0.53 mm) Det: GC ECD1A Column 2 : MR-2 ( 0.53 mm) Det: GC ECD2B Process Host: CTX1636

First Level Reviewer: eppinged Date: 08-Sep-2021 06:40:31

Col

(min.)

Exp RT (min.)

Dlt RT (min.) Response

Cal Amt ng

OnCol Amt ng Flags

* 43 1-Bromo-2-nitrobenzene 1 3.858 3.859 -0.001 580005555H 0.1000 0.1000 2 4.317 4.314 0.003 475611920H 0.1000 0.1000

$ 3 Tetrachloro-m-xylene 1 4.853 4.853 0.000 117601852H 0.0200 0.0173 2 5.183 5.181 0.002 113851336H 0.0200 0.0192

RPD = 10.23

4 Diallate

1 5.007 ND

1 5.098 2 5.287 2 5.373

5 alpha-BHC

1 5.228 ND

2 5.642

6 Hexachlorobenzene

1 5.260 ND

2 5.604

7 gamma-BHC (Lindane)

1 5.497 ND

2 5.942

8 beta-BHC

1 5.665 ND

2 6.173

10 delta-BHC

1 5.865 ND

2 6.406

Data File: \\chromfs\Pittsburgh\ChromData\CHGC15\20210907-38994.b\Q0907210000006.D

Col

(min.)

Exp RT (min.)

Dlt RT (min.) Response

Cal Amt ng

OnCol Amt ng Flags

9 Chlordane (technical)

1 5.968 ND

1 6.230 1 6.835 1 6.905 2 6.111 2 6.271 2 7.223 2 7.269

11 Heptachlor

1 5.968 ND

2 6.273

12 DCPA

1 6.183 ND

2 6.527

13 Aldrin

1 6.252 ND

2 6.542

14 Isodrin

1 6.537 ND

2 6.892

15 oxy-Chlordane

1 6.572 ND

2 6.892

16 Heptachlor epoxide

1 6.616 ND

2 6.983

17 2,4'-DDE

1 6.755 ND

2 7.110

18 trans-Chlordane

1 6.836 ND

2 7.209

19 Chlorobenside

1 6.863 ND

2 7.281

20 cis-Chlordane

1 6.904 ND

2 7.270

22 trans-Nonachlor

1 6.907 ND

2 7.218

21 Endosulfan I

1 6.950 ND

2 7.338

23 4,4'-DDE

1 7.054 ND

2 7.396

Col

(min.)

Exp RT (min.)

Dlt RT (min.) Response

Cal Amt ng

OnCol Amt ng Flags

34 Toxaphene

1 7.098 ND

1 7.369 1 7.827 1 7.906 2 7.518 2 7.565 2 8.313 2 8.820

25 2,4'-DDD

1 7.149 ND

2 7.545

24 Dieldrin

1 7.192 ND

2 7.579

27 Endrin

1 7.396 ND

2 7.845

28 2,4'-DDT

1 7.426 ND

2 7.795

30 cis-Nonachlor

1 7.483 ND

2 7.872

29 4,4'-DDD

1 7.517 ND

2 7.908

31 Endosulfan II

1 7.598 ND

2 8.106

32 Endrin aldehyde

1 7.715 ND

2 8.281

33 4,4'-DDT

1 7.798 ND

2 8.162

35 Endosulfan sulfate

1 7.926 ND

2 8.518

36 Methoxychlor

1 8.256 ND

2 8.758

* 44 Dibutylchlorendate ISTD 1 8.326 8.326 -0.001 284778489H 0.1000 0.1000 2 8.577 8.577 0.000 283514353H 0.1000 0.1000

37 Endrin ketone

1 8.406 ND

2 9.171

Col

(min.)

Exp RT (min.)

Dlt RT (min.) Response

Cal Amt ng

OnCol Amt ng Flags

38 Mirex

1 8.934 ND

2 9.483

$ 39 DCB Decachlorobiphenyl (Surr) 1 10.212 10.209 0.003 38165983H 0.0200 0.0217 2 10.992 10.991 0.001 33324665H 0.0200 0.0194

RPD = 11.50

QC Flag Legend Processing Flags H - Response Measured by Height Reagents:

Data File: \\chromfs\Pittsburgh\ChromData\CHGC15\20210907-38994.b\Q0907210000006.D Injection Date: 07-Sep-2021 14:52:34 Instrument ID: CHGC15 Operator ID: 402331 Lims ID: MB 180-370070/1-A Worklist Smp#: 6 Client ID:

Injection Vol: 1.0 uL Dil. Factor: 1.0000 ALS Bottle#: 6 Method: IS PEST_CHGC15 Limit Group: GCS 8081B ICAL with IS Column: MR-1 ( 0.53 mm)

0.0 1.0 2.0 3.0 4.0 5.0 6.0 7.0 8.0 9.0 10.0 11.0 12.0 Min

Y (X

GC ECD1A, Q0907210000006.D

B ro m o-

2-ni tro be nz en e(

Te tra ch lo ro

-m -x yl en e(

D ib ut yl ch lo re nd at e

C B

D ec ac hl or ob ip he ny l (

S ur

r) ( 1

Column: MR-2 ( 0.53 mm)

0.0 1.0 2.0 3.0 4.0 5.0 6.0 7.0 8.0 9.0 10.0 11.0 12.0 Min

Y (X

GC ECD2B, Q0907210000006.D

B ro m o-

2-ni tro be nz en e(

Te tra ch lo ro

-m -x yl en e(

D ib ut yl ch lo re nd at e

C B

D ec ac hl or ob ip he ny l (

S ur

r) ( 1

Recovery Report

Data File: \\chromfs\Pittsburgh\ChromData\CHGC15\20210907-38994.b\Q0907210000006.D Lims ID: MB 180-370070/1-A Client ID:

Sample Type: MB Inject. Date: 07-Sep-2021 14:52:34 ALS Bottle#: 6 Worklist Smp#: 6 Injection Vol: 1.0 uL Dil. Factor: 1.0000 Sample Info: 180-0038994-006 Operator ID: 402331 Instrument ID: CHGC15

Column 1 : MR-1 ( 0.53 mm) Det: GC ECD1A Column 2 : MR-2 ( 0.53 mm) Det: GC ECD2B Process Host: CTX1636

First Level Reviewer: eppinged Date: 08-Sep-2021 06:40:31

Surrogate Recovery, Detector: GC ECD1A

Compound Amount Added

Amount Recovered % Rec.

$ 3 Tetrachloro-m-xylene 0.0200 0.0173 86.48

$ 39 DCB Decachlorobiphenyl (Surr) 0.0200 0.0217 108.75

Surrogate Recovery, Detector: GC ECD2B

Compound Amount Added

Amount Recovered % Rec.

$ 3 Tetrachloro-m-xylene 0.0200 0.0192 95.80

$ 39 DCB Decachlorobiphenyl (Surr) 0.0200 0.0194 96.92

Client Sample ID:

Lab Name: Job No.:

SDG No.:

180-126039-1

Lab Sample ID: MB 180-370070/1-A

Eurofins TestAmerica, Pittsburgh

Matrix: Q0907210000006.DLab File ID:

Date Collected:EPA 8081B LLAnalysis Method:

Sediment

Con. Extract Vol.:

Injection Volume:

GPC Cleanup:(Y/N)

Date Extracted:

Date Analyzed:

Dilution Factor: 1

Extraction Method: 3510C 09/02/2021 06:45

09/07/2021 14:52

1.0(mL)

1(uL)

Sample wt/vol: 1000(mL)

% Moisture:

GC Column: ID: 0.53(mm)MR-2

Analysis Batch No.: 370468 ug/LUnits:

%RECCAS NO. LIMITSQSURROGATE

96 25-122877-09-8 Tetrachloro-m-xylene (Surr)

97 32-1352051-24-3 DCB Decachlorobiphenyl (Surr)

Target Compound Quantitation Report

Data File: \\chromfs\Pittsburgh\ChromData\CHGC15\20210907-38994.b\Q0907210000006.D Lims ID: MB 180-370070/1-A Client ID:

Sample Type: MB Inject. Date: 07-Sep-2021 14:52:34 ALS Bottle#: 6 Worklist Smp#: 6 Injection Vol: 1.0 uL Dil. Factor: 1.0000 Sample Info: 180-0038994-006 Operator ID: 402331 Instrument ID: CHGC15

Column 1 : MR-1 ( 0.53 mm) Det: GC ECD1A Column 2 : MR-2 ( 0.53 mm) Det: GC ECD2B Process Host: CTX1636

First Level Reviewer: eppinged Date: 08-Sep-2021 06:40:31

Col

(min.)

Exp RT (min.)

Dlt RT (min.) Response

Cal Amt ng

OnCol Amt ng Flags

* 43 1-Bromo-2-nitrobenzene 1 3.858 3.859 -0.001 580005555H 0.1000 0.1000 2 4.317 4.314 0.003 475611920H 0.1000 0.1000

$ 3 Tetrachloro-m-xylene 1 4.853 4.853 0.000 117601852H 0.0200 0.0173 2 5.183 5.181 0.002 113851336H 0.0200 0.0192

RPD = 10.23

4 Diallate

1 5.007 ND

1 5.098 2 5.287 2 5.373

5 alpha-BHC

1 5.228 ND

2 5.642

6 Hexachlorobenzene

1 5.260 ND

2 5.604

7 gamma-BHC (Lindane)

1 5.497 ND

2 5.942

8 beta-BHC

1 5.665 ND

2 6.173

10 delta-BHC

1 5.865 ND

Col

(min.)

Exp RT (min.)

Dlt RT (min.) Response

Cal Amt ng

OnCol Amt ng Flags

9 Chlordane (technical)

1 5.968 ND

1 6.230 1 6.835 1 6.905 2 6.111 2 6.271 2 7.223 2 7.269

11 Heptachlor

1 5.968 ND

2 6.273

12 DCPA

1 6.183 ND

2 6.527

13 Aldrin

1 6.252 ND

2 6.542

14 Isodrin

1 6.537 ND

2 6.892

15 oxy-Chlordane

1 6.572 ND

2 6.892

16 Heptachlor epoxide

1 6.616 ND

2 6.983

17 2,4'-DDE

1 6.755 ND

2 7.110

18 trans-Chlordane

1 6.836 ND

2 7.209

19 Chlorobenside

1 6.863 ND

2 7.281

20 cis-Chlordane

1 6.904 ND

2 7.270

22 trans-Nonachlor

1 6.907 ND

2 7.218

21 Endosulfan I

1 6.950 ND

2 7.338

23 4,4'-DDE

1 7.054 ND

Col

(min.)

Exp RT (min.)

Dlt RT (min.) Response

Cal Amt ng

OnCol Amt ng Flags

34 Toxaphene

1 7.098 ND

1 7.369 1 7.827 1 7.906 2 7.518 2 7.565 2 8.313 2 8.820

25 2,4'-DDD

1 7.149 ND

2 7.545

24 Dieldrin

1 7.192 ND

2 7.579

27 Endrin

1 7.396 ND

2 7.845

28 2,4'-DDT

1 7.426 ND

2 7.795

30 cis-Nonachlor

1 7.483 ND

2 7.872

29 4,4'-DDD

1 7.517 ND

2 7.908

31 Endosulfan II

1 7.598 ND

2 8.106

32 Endrin aldehyde

1 7.715 ND

2 8.281

33 4,4'-DDT

1 7.798 ND

2 8.162

35 Endosulfan sulfate

1 7.926 ND

2 8.518

36 Methoxychlor

1 8.256 ND

2 8.758

* 44 Dibutylchlorendate ISTD 1 8.326 8.326 -0.001 284778489H 0.1000 0.1000 2 8.577 8.577 0.000 283514353H 0.1000 0.1000

37 Endrin ketone

1 8.406 ND

Col

(min.)

Exp RT (min.)

Dlt RT (min.) Response

Cal Amt ng

OnCol Amt ng Flags

38 Mirex

1 8.934 ND

2 9.483

$ 39 DCB Decachlorobiphenyl (Surr) 1 10.212 10.209 0.003 38165983H 0.0200 0.0217 2 10.992 10.991 0.001 33324665H 0.0200 0.0194

RPD = 11.50

QC Flag Legend Processing Flags H - Response Measured by Height Reagents:

Report Date: 08-Sep-2021 06:59:09 Chrom Revision: 2.3 13-May-2021 07:57:40

Injection Vol: 1.0 uL Dil. Factor: 1.0000 ALS Bottle#: 6 Method: IS PEST_CHGC15 Limit Group: GCS 8081B ICAL with IS Column: MR-1 ( 0.53 mm)

0.0 1.0 2.0 3.0 4.0 5.0 6.0 7.0 8.0 9.0 10.0 11.0 12.0 Min

Y (X

GC ECD1A, Q0907210000006.D

B ro m o-

2-ni tro be nz en e(

Te tra ch lo ro

-m -x yl en e(

D ib ut yl ch lo re nd at e

C B

D ec ac hl or ob ip he ny l (

S ur

r) ( 1

Column: MR-2 ( 0.53 mm)

0.0 1.0 2.0 3.0 4.0 5.0 6.0 7.0 8.0 9.0 10.0 11.0 12.0 Min

Y (X

GC ECD2B, Q0907210000006.D

B ro m o-

2-ni tro be nz en e(

Te tra ch lo ro

-m -x yl en e(

D ib ut yl ch lo re nd at e

C B

D ec ac hl or ob ip he ny l (

S ur

r) ( 1

Recovery Report

Data File: \\chromfs\Pittsburgh\ChromData\CHGC15\20210907-38994.b\Q0907210000006.D Lims ID: MB 180-370070/1-A Client ID:

Sample Type: MB Inject. Date: 07-Sep-2021 14:52:34 ALS Bottle#: 6 Worklist Smp#: 6 Injection Vol: 1.0 uL Dil. Factor: 1.0000 Sample Info: 180-0038994-006 Operator ID: 402331 Instrument ID: CHGC15

Column 1 : MR-1 ( 0.53 mm) Det: GC ECD1A Column 2 : MR-2 ( 0.53 mm) Det: GC ECD2B Process Host: CTX1636

First Level Reviewer: eppinged Date: 08-Sep-2021 06:40:31

Surrogate Recovery, Detector: GC ECD1A

Compound Amount Added

Amount Recovered % Rec.

$ 3 Tetrachloro-m-xylene 0.0200 0.0173 86.48

$ 39 DCB Decachlorobiphenyl (Surr) 0.0200 0.0217 108.75

Surrogate Recovery, Detector: GC ECD2B

Compound Amount Added

Amount Recovered % Rec.

$ 3 Tetrachloro-m-xylene 0.0200 0.0192 95.80

$ 39 DCB Decachlorobiphenyl (Surr) 0.0200 0.0194 96.92

Client Sample ID:

Lab Name: Job No.:

SDG No.:

180-126039-1

Lab Sample ID: LB 180-369612/1-D

Eurofins TestAmerica, Pittsburgh

Matrix: Q0907210000008.DLab File ID:

Date Collected:EPA 8081B LLAnalysis Method:

Sediment (SPLP East)

Con. Extract Vol.:

Injection Volume:

GPC Cleanup:(Y/N)

Date Extracted:

Date Analyzed:

Dilution Factor: 1

Extraction Method: 3510C 09/02/2021 06:45

09/07/2021 15:23

1.0(mL)

1(uL)

Sample wt/vol: 1040(mL)

% Moisture:

GC Column: ID: 0.53(mm)MR-1

Analysis Batch No.: 370468 ug/LUnits:

CAS NO. COMPOUND NAME RESULT Q MDLRL

0.0013 0.00034U309-00-2 Aldrin 0.0013

0.0013 0.00023U319-84-6 alpha-BHC 0.0013

0.0013 0.00035U319-85-7 beta-BHC 0.0013

0.0013 0.00062U319-86-8 delta-BHC 0.0013

0.0013 0.00028U58-89-9 gamma-BHC (Lindane) 0.0013

0.0013 0.00035U5103-71-9 cis-Chlordane 0.0013

0.0013 0.00039U5103-74-2 trans-Chlordane 0.0013

0.0013 0.00051U72-54-8 4,4'-DDD 0.0013

0.0013 0.00028U72-55-9 4,4'-DDE 0.0013

0.0013 0.00029U50-29-3 4,4'-DDT 0.0013

0.0013 0.00026U60-57-1 Dieldrin 0.0013

0.0013 0.00066U959-98-8 Endosulfan I 0.0013

0.0013 0.00030U33213-65-9 Endosulfan II 0.0013

0.0013 0.00061U1031-07-8 Endosulfan sulfate 0.0013

0.0013 0.00022U72-20-8 Endrin 0.0013

0.0013 0.00043U76-44-8 Heptachlor 0.0013

0.0013 0.00033U1024-57-3 Heptachlor epoxide 0.0013

0.0013 0.00075U72-43-5 Methoxychlor 0.0013

0.0013 0.00020U2385-85-5 Mirex 0.0013

0.096 0.047U8001-35-2 Toxaphene 0.096

%RECCAS NO. LIMITSQSURROGATE

81 25-122877-09-8 Tetrachloro-m-xylene (Surr)

101 32-1352051-24-3 DCB Decachlorobiphenyl (Surr)

Report Date: 08-Sep-2021 06:59:10 Chrom Revision: 2.3 13-May-2021 07:57:40

Target Compound Quantitation Report

Data File: \\chromfs\Pittsburgh\ChromData\CHGC15\20210907-38994.b\Q0907210000008.D Lims ID: LB 180-369612/1-D Client ID:

Sample Type: LB Inject. Date: 07-Sep-2021 15:23:58 ALS Bottle#: 8 Worklist Smp#: 8 Injection Vol: 1.0 uL Dil. Factor: 1.0000 Sample Info: 180-0038994-008 Operator ID: 402331 Instrument ID: CHGC15

Column 1 : MR-1 ( 0.53 mm) Det: GC ECD1A Column 2 : MR-2 ( 0.53 mm) Det: GC ECD2B Process Host: CTX1636

First Level Reviewer: eppinged Date: 08-Sep-2021 06:40:51

Col

(min.)

Exp RT (min.)

Dlt RT (min.) Response

Cal Amt ng

OnCol Amt ng Flags

* 43 1-Bromo-2-nitrobenzene 1 3.858 3.859 -0.001 637018338H 0.1000 0.1000 2 4.318 4.314 0.004 528801495H 0.1000 0.1000

$ 3 Tetrachloro-m-xylene 1 4.851 4.853 -0.002 121671420H 0.0200 0.0163 2 5.185 5.181 0.004 116373038H 0.0200 0.0176

RPD = 7.80

4 Diallate

1 5.007 ND

1 5.098 2 5.287 2 5.373

5 alpha-BHC

1 5.228 ND

2 5.642

6 Hexachlorobenzene

1 5.260 ND

2 5.604

7 gamma-BHC (Lindane)

1 5.497 ND

2 5.942

8 beta-BHC

1 5.665 ND

2 6.173

10 delta-BHC U

1 5.865 ND

Data File: \\chromfs\Pittsburgh\ChromData\CHGC15\20210907-38994.b\Q0907210000008.D

Col

(min.)

Exp RT (min.)

Dlt RT (min.) Response

Cal Amt ng

OnCol Amt ng Flags

9 Chlordane (technical)

1 5.968 ND

1 6.230 1 6.835 1 6.905 2 6.111 2 6.271 2 7.223 2 7.269

11 Heptachlor

1 5.968 ND

2 6.273

12 DCPA

1 6.183 ND

2 6.527

13 Aldrin

1 6.252 ND

2 6.542

14 Isodrin

1 6.537 ND

2 6.892

15 oxy-Chlordane

1 6.572 ND

2 6.892

16 Heptachlor epoxide

1 6.616 ND

2 6.983

17 2,4'-DDE

1 6.755 ND

2 7.110

18 trans-Chlordane

1 6.836 ND

2 7.209

19 Chlorobenside

1 6.863 ND

2 7.281

20 cis-Chlordane

1 6.904 ND

2 7.270

22 trans-Nonachlor

1 6.907 ND

2 7.218

21 Endosulfan I

1 6.950 ND

2 7.338

23 4,4'-DDE

1 7.054 ND

Col

(min.)

Exp RT (min.)

Dlt RT (min.) Response

Cal Amt ng

OnCol Amt ng Flags

34 Toxaphene

1 7.098 ND

1 7.369 1 7.827 1 7.906 2 7.518 2 7.565 2 8.313 2 8.820

25 2,4'-DDD

1 7.149 ND

2 7.545

24 Dieldrin

1 7.192 ND

2 7.579

27 Endrin

1 7.396 ND

2 7.845

28 2,4'-DDT

1 7.426 ND

2 7.795

30 cis-Nonachlor

1 7.483 ND

2 7.872

29 4,4'-DDD

1 7.517 ND

2 7.908

31 Endosulfan II

1 7.598 ND

2 8.106

32 Endrin aldehyde

1 7.715 ND

2 8.281

33 4,4'-DDT

1 7.798 ND

2 8.162

35 Endosulfan sulfate

1 7.926 ND

2 8.518

36 Methoxychlor

1 8.256 ND

2 8.758

* 44 Dibutylchlorendate ISTD 1 8.324 8.326 -0.002 315025232H 0.1000 0.1000 2 8.580 8.577 0.003 310490431H 0.1000 0.1000

37 Endrin ketone

1 8.406 ND

Col

(min.)

Exp RT (min.)

Dlt RT (min.) Response

Cal Amt ng

OnCol Amt ng Flags

38 Mirex

1 8.934 ND

2 9.483

$ 39 DCB Decachlorobiphenyl (Surr) 1 10.209 10.209 0.000 39062370H 0.0200 0.0201 2 10.997 10.991 0.006 34069826H 0.0200 0.0181

RPD = 10.61

QC Flag Legend Processing Flags H - Response Measured by Height Review Flags U - Marked Undetected Reagents:

Data File: \\chromfs\Pittsburgh\ChromData\CHGC15\20210907-38994.b\Q0907210000008.D Injection Date: 07-Sep-2021 15:23:58 Instrument ID: CHGC15 Operator ID: 402331 Lims ID: LB 180-369612/1-D Worklist Smp#: 8 Client ID:

Injection Vol: 1.0 uL Dil. Factor: 1.0000 ALS Bottle#: 8 Method: IS PEST_CHGC15 Limit Group: GCS 8081B ICAL with IS Column: MR-1 ( 0.53 mm)

0.0 1.0 2.0 3.0 4.0 5.0 6.0 7.0 8.0 9.0 10.0 11.0 12.0 Min

Y (X

GC ECD1A, Q0907210000008.D

B ro m o-

2-ni tro be nz en e(

Te tra ch lo ro

-m -x yl en e(

D ib ut yl ch lo re nd at e

C B

D ec ac hl or ob ip he ny l (

S ur

r) ( 1

Column: MR-2 ( 0.53 mm)

0.0 1.0 2.0 3.0 4.0 5.0 6.0 7.0 8.0 9.0 10.0 11.0 12.0 Min

Y (X

GC ECD2B, Q0907210000008.D

B ro m o-

2-ni tro be nz en e(

Te tra ch lo ro

-m -x yl en e(

D ib ut yl ch lo re nd at e

C B

D ec ac hl or ob ip he ny l (

S ur

r) ( 1

Recovery Report

Data File: \\chromfs\Pittsburgh\ChromData\CHGC15\20210907-38994.b\Q0907210000008.D Lims ID: LB 180-369612/1-D Client ID:

Sample Type: LB Inject. Date: 07-Sep-2021 15:23:58 ALS Bottle#: 8 Worklist Smp#: 8 Injection Vol: 1.0 uL Dil. Factor: 1.0000 Sample Info: 180-0038994-008 Operator ID: 402331 Instrument ID: CHGC15

Column 1 : MR-1 ( 0.53 mm) Det: GC ECD1A Column 2 : MR-2 ( 0.53 mm) Det: GC ECD2B Process Host: CTX1636

First Level Reviewer: eppinged Date: 08-Sep-2021 06:40:51

Surrogate Recovery, Detector: GC ECD1A

Compound Amount Added

Amount Recovered % Rec.

$ 3 Tetrachloro-m-xylene 0.0200 0.0163 81.46

$ 39 DCB Decachlorobiphenyl (Surr) 0.0200 0.0201 100.61

Surrogate Recovery, Detector: GC ECD2B

Compound Amount Added

Amount Recovered % Rec.

$ 3 Tetrachloro-m-xylene 0.0200 0.0176 88.07

$ 39 DCB Decachlorobiphenyl (Surr) 0.0200 0.0181 90.48

Report Date: 08-Sep-2021 06:59:11 Chrom Revision: 2.3 13-May-2021 07:57:40

Eurofins TestAmerica, Pittsburgh Data File: \\chromfs\Pittsburgh\ChromData\CHGC15\20210907-38994.b\Q0907210000008.D Injection Date: 07-Sep-2021 15:23:58 Instrument ID: CHGC15 Lims ID: LB 180-369612/1-D Client ID:

Operator ID: 402331 ALS Bottle#: 8 Worklist Smp#: 8 Injection Vol: 1.0 uL Dil. Factor: 1.0000 Method: IS PEST_CHGC15 Limit Group: GCS 8081B ICAL with IS

Column: MR-1 ( 0.53 mm) Detector GC ECD1A 10 delta-BHC, CAS: 319-86-8, Signal: 1

RT: 5.87

Response: 669088 Amount: 0.000108

5.5 5.7 5.9 6.1 Min

Y (X

GC ECD1A, Q0907210000008.D

Column: MR-2 ( 0.53 mm) Detector GC ECD2B 10 delta-BHC, CAS: 319-86-8, Signal: 2

RT: 6.42

Response: 488240 Amount: 0.000080

6.3 6.5 Min

Y (X

GC ECD2B, Q0907210000008.D

Reviewer: eppinged, 08-Sep-2021 06:40:51

Client Sample ID:

Lab Name: Job No.:

SDG No.:

180-126039-1

Lab Sample ID: LB 180-369612/1-D

Eurofins TestAmerica, Pittsburgh

Matrix: Q0907210000008.DLab File ID:

Date Collected:EPA 8081B LLAnalysis Method:

Sediment (SPLP East)

Con. Extract Vol.:

Injection Volume:

GPC Cleanup:(Y/N)

Date Extracted:

Date Analyzed:

Dilution Factor: 1

Extraction Method: 3510C 09/02/2021 06:45

09/07/2021 15:23

1.0(mL)

1(uL)

Sample wt/vol: 1040(mL)

% Moisture:

GC Column: ID: 0.53(mm)MR-2

Analysis Batch No.: 370468 ug/LUnits:

%RECCAS NO. LIMITSQSURROGATE

88 25-122877-09-8 Tetrachloro-m-xylene (Surr)

90 32-1352051-24-3 DCB Decachlorobiphenyl (Surr)

Target Compound Quantitation Report

Data File: \\chromfs\Pittsburgh\ChromData\CHGC15\20210907-38994.b\Q0907210000008.D Lims ID: LB 180-369612/1-D Client ID:

Sample Type: LB Inject. Date: 07-Sep-2021 15:23:58 ALS Bottle#: 8 Worklist Smp#: 8 Injection Vol: 1.0 uL Dil. Factor: 1.0000 Sample Info: 180-0038994-008 Operator ID: 402331 Instrument ID: CHGC15

Column 1 : MR-1 ( 0.53 mm) Det: GC ECD1A Column 2 : MR-2 ( 0.53 mm) Det: GC ECD2B Process Host: CTX1636

First Level Reviewer: eppinged Date: 08-Sep-2021 06:40:51

Col

(min.)

Exp RT (min.)

Dlt RT (min.) Response

Cal Amt ng

OnCol Amt ng Flags

* 43 1-Bromo-2-nitrobenzene 1 3.858 3.859 -0.001 637018338H 0.1000 0.1000 2 4.318 4.314 0.004 528801495H 0.1000 0.1000

$ 3 Tetrachloro-m-xylene 1 4.851 4.853 -0.002 121671420H 0.0200 0.0163 2 5.185 5.181 0.004 116373038H 0.0200 0.0176

RPD = 7.80

4 Diallate

1 5.007 ND

1 5.098 2 5.287 2 5.373

5 alpha-BHC

1 5.228 ND

2 5.642

6 Hexachlorobenzene

1 5.260 ND

2 5.604

7 gamma-BHC (Lindane)

1 5.497 ND

2 5.942

8 beta-BHC

1 5.665 ND

2 6.173

10 delta-BHC U

1 5.865 ND

Col

(min.)

Exp RT (min.)

Dlt RT (min.) Response

Cal Amt ng

OnCol Amt ng Flags

9 Chlordane (technical)

1 5.968 ND

1 6.230 1 6.835 1 6.905 2 6.111 2 6.271 2 7.223 2 7.269

11 Heptachlor

1 5.968 ND

2 6.273

12 DCPA

1 6.183 ND

2 6.527

13 Aldrin

1 6.252 ND

2 6.542

14 Isodrin

1 6.537 ND

2 6.892

15 oxy-Chlordane

1 6.572 ND

2 6.892

16 Heptachlor epoxide

1 6.616 ND

2 6.983

17 2,4'-DDE

1 6.755 ND

2 7.110

18 trans-Chlordane

1 6.836 ND

2 7.209

19 Chlorobenside

1 6.863 ND

2 7.281

20 cis-Chlordane

1 6.904 ND

2 7.270

22 trans-Nonachlor

1 6.907 ND

2 7.218

21 Endosulfan I

1 6.950 ND

2 7.338

23 4,4'-DDE

1 7.054 ND

Col

(min.)

Exp RT (min.)

Dlt RT (min.) Response

Cal Amt ng

OnCol Amt ng Flags

34 Toxaphene

1 7.098 ND

1 7.369 1 7.827 1 7.906 2 7.518 2 7.565 2 8.313 2 8.820

25 2,4'-DDD

1 7.149 ND

2 7.545

24 Dieldrin

1 7.192 ND

2 7.579

27 Endrin

1 7.396 ND

2 7.845

28 2,4'-DDT

1 7.426 ND

2 7.795

30 cis-Nonachlor

1 7.483 ND

2 7.872

29 4,4'-DDD

1 7.517 ND

2 7.908

31 Endosulfan II

1 7.598 ND

2 8.106

32 Endrin aldehyde

1 7.715 ND

2 8.281

33 4,4'-DDT

1 7.798 ND

2 8.162

35 Endosulfan sulfate

1 7.926 ND

2 8.518

36 Methoxychlor

1 8.256 ND

2 8.758

* 44 Dibutylchlorendate ISTD 1 8.324 8.326 -0.002 315025232H 0.1000 0.1000 2 8.580 8.577 0.003 310490431H 0.1000 0.1000

37 Endrin ketone

1 8.406 ND

Col

(min.)

Exp RT (min.)

Dlt RT (min.) Response

Cal Amt ng

OnCol Amt ng Flags

38 Mirex

1 8.934 ND

2 9.483

$ 39 DCB Decachlorobiphenyl (Surr) 1 10.209 10.209 0.000 39062370H 0.0200 0.0201 2 10.997 10.991 0.006 34069826H 0.0200 0.0181

RPD = 10.61

QC Flag Legend Processing Flags H - Response Measured by Height Review Flags U - Marked Undetected Reagents:

Injection Vol: 1.0 uL Dil. Factor: 1.0000 ALS Bottle#: 8 Method: IS PEST_CHGC15 Limit Group: GCS 8081B ICAL with IS Column: MR-1 ( 0.53 mm)

0.0 1.0 2.0 3.0 4.0 5.0 6.0 7.0 8.0 9.0 10.0 11.0 12.0 Min

Y (X

GC ECD1A, Q0907210000008.D

B ro m o-

2-ni tro be nz en e(

Te tra ch lo ro

-m -x yl en e(

D ib ut yl ch lo re nd at e

C B

D ec ac hl or ob ip he ny l (

S ur

r) ( 1

Column: MR-2 ( 0.53 mm)

0.0 1.0 2.0 3.0 4.0 5.0 6.0 7.0 8.0 9.0 10.0 11.0 12.0 Min

Y (X

GC ECD2B, Q0907210000008.D

B ro m o-

2-ni tro be nz en e(

Te tra ch lo ro

-m -x yl en e(

D ib ut yl ch lo re nd at e

C B

D ec ac hl or ob ip he ny l (

S ur

r) ( 1

Recovery Report

Data File: \\chromfs\Pittsburgh\ChromData\CHGC15\20210907-38994.b\Q0907210000008.D Lims ID: LB 180-369612/1-D Client ID:

Sample Type: LB Inject. Date: 07-Sep-2021 15:23:58 ALS Bottle#: 8 Worklist Smp#: 8 Injection Vol: 1.0 uL Dil. Factor: 1.0000 Sample Info: 180-0038994-008 Operator ID: 402331 Instrument ID: CHGC15

Column 1 : MR-1 ( 0.53 mm) Det: GC ECD1A Column 2 : MR-2 ( 0.53 mm) Det: GC ECD2B Process Host: CTX1636

First Level Reviewer: eppinged Date: 08-Sep-2021 06:40:51

Surrogate Recovery, Detector: GC ECD1A

Compound Amount Added

Amount Recovered % Rec.

$ 3 Tetrachloro-m-xylene 0.0200 0.0163 81.46

$ 39 DCB Decachlorobiphenyl (Surr) 0.0200 0.0201 100.61

Surrogate Recovery, Detector: GC ECD2B

Compound Amount Added

Amount Recovered % Rec.

$ 3 Tetrachloro-m-xylene 0.0200 0.0176 88.07

$ 39 DCB Decachlorobiphenyl (Surr) 0.0200 0.0181 90.48

Operator ID: 402331 ALS Bottle#: 8 Worklist Smp#: 8 Injection Vol: 1.0 uL Dil. Factor: 1.0000 Method: IS PEST_CHGC15 Limit Group: GCS 8081B ICAL with IS

Column: MR-1 ( 0.53 mm) Detector GC ECD1A 10 delta-BHC, CAS: 319-86-8, Signal: 1

RT: 5.87

Response: 669088 Amount: 0.000108

5.5 5.7 5.9 6.1 Min

Y (X

GC ECD1A, Q0907210000008.D

Column: MR-2 ( 0.53 mm) Detector GC ECD2B 10 delta-BHC, CAS: 319-86-8, Signal: 2

RT: 6.42

Response: 488240 Amount: 0.000080

6.3 6.5 Min

Y (X

GC ECD2B, Q0907210000008.D

Reviewer: eppinged, 08-Sep-2021 06:40:51

Client Sample ID:

Lab Name: Job No.:

SDG No.:

180-126039-1

Lab Sample ID: LB 180-369295/1-D

Eurofins TestAmerica, Pittsburgh

Matrix: Q0907210000009.DLab File ID:

Date Collected:EPA 8081B LLAnalysis Method:

Sediment (SPLP East)

Con. Extract Vol.:

Injection Volume:

GPC Cleanup:(Y/N)

Date Extracted:

Date Analyzed:

Dilution Factor: 1

Extraction Method: 3510C 09/02/2021 06:45

09/07/2021 15:39

1.0(mL)

1(uL)

Sample wt/vol: 1040(mL)

% Moisture:

GC Column: ID: 0.53(mm)MR-1

Analysis Batch No.: 370468 ug/LUnits:

CAS NO. COMPOUND NAME RESULT Q MDLRL

0.0013 0.00034U309-00-2 Aldrin 0.0013

0.0013 0.00023U319-84-6 alpha-BHC 0.0013

0.0013 0.00035U319-85-7 beta-BHC 0.0013

0.0013 0.00062U319-86-8 delta-BHC 0.0013

0.0013 0.00028U58-89-9 gamma-BHC (Lindane) 0.0013

0.0013 0.00035U5103-71-9 cis-Chlordane 0.0013

0.0013 0.00039U5103-74-2 trans-Chlordane 0.0013

0.0013 0.00051U72-54-8 4,4'-DDD 0.0013

0.0013 0.00028U72-55-9 4,4'-DDE 0.0013

0.0013 0.00029U50-29-3 4,4'-DDT 0.0013

0.0013 0.00026U60-57-1 Dieldrin 0.0013

0.0013 0.00066U959-98-8 Endosulfan I 0.0013

0.0013 0.00030U33213-65-9 Endosulfan II 0.0013

0.0013 0.00061U1031-07-8 Endosulfan sulfate 0.0013

0.0013 0.00022U72-20-8 Endrin 0.0013

0.0013 0.00043U76-44-8 Heptachlor 0.0013

0.0013 0.00033U1024-57-3 Heptachlor epoxide 0.0013

0.0013 0.00075U72-43-5 Methoxychlor 0.0013

0.0013 0.00020U2385-85-5 Mirex 0.0013

0.096 0.047U8001-35-2 Toxaphene 0.096

%RECCAS NO. LIMITSQSURROGATE

74 25-122877-09-8 Tetrachloro-m-xylene (Surr)

91 32-1352051-24-3 DCB Decachlorobiphenyl (Surr)

Target Compound Quantitation Report

Data File: \\chromfs\Pittsburgh\ChromData\CHGC15\20210907-38994.b\Q0907210000009.D Lims ID: LB 180-369295/1-D Client ID:

Sample Type: LB Inject. Date: 07-Sep-2021 15:39:34 ALS Bottle#: 9 Worklist Smp#: 9 Injection Vol: 1.0 uL Dil. Factor: 1.0000 Sample Info: 180-0038994-009 Operator ID: 402331 Instrument ID: CHGC15

Column 1 : MR-1 ( 0.53 mm) Det: GC ECD1A Column 2 : MR-2 ( 0.53 mm) Det: GC ECD2B Process Host: CTX1636

First Level Reviewer: eppinged Date: 08-Sep-2021 06:40:59

Col

(min.)

Exp RT (min.)

Dlt RT (min.) Response

Cal Amt ng

OnCol Amt ng Flags

* 43 1-Bromo-2-nitrobenzene 1 3.858 3.859 -0.001 713021699H 0.1000 0.1000 2 4.317 4.314 0.003 586924847H 0.1000 0.1000

$ 3 Tetrachloro-m-xylene 1 4.851 4.853 -0.002 122951631H 0.0200 0.0147 2 5.185 5.181 0.004 116675667H 0.0200 0.0159

RPD = 7.85

4 Diallate

1 5.007 ND

1 5.098 2 5.287 2 5.373

5 alpha-BHC

1 5.228 ND

2 5.642

6 Hexachlorobenzene

1 5.260 ND

2 5.604

7 gamma-BHC (Lindane)

1 5.497 ND

2 5.942

8 beta-BHC

1 5.665 ND

2 6.173

10 delta-BHC

1 5.865 ND

Data File: \\chromfs\Pittsburgh\ChromData\CHGC15\20210907-38994.b\Q0907210000009.D

Col

(min.)

Exp RT (min.)

Dlt RT (min.) Response

Cal Amt ng

OnCol Amt ng Flags

9 Chlordane (technical)

1 5.968 ND

1 6.230 1 6.835 1 6.905 2 6.111 2 6.271 2 7.223 2 7.269

11 Heptachlor

1 5.968 ND

2 6.273

12 DCPA

1 6.183 ND

2 6.527

13 Aldrin

1 6.252 ND

2 6.542

14 Isodrin

1 6.537 ND

2 6.892

15 oxy-Chlordane

1 6.572 ND

2 6.892

16 Heptachlor epoxide

1 6.616 ND

2 6.983

17 2,4'-DDE

1 6.755 ND

2 7.110

18 trans-Chlordane

1 6.836 ND

2 7.209

19 Chlorobenside

1 6.863 ND

2 7.281

20 cis-Chlordane

1 6.904 ND

2 7.270

22 trans-Nonachlor

1 6.907 ND

2 7.218

21 Endosulfan I

1 6.950 ND

2 7.338

23 4,4'-DDE

1 7.054 ND

Col

(min.)

Exp RT (min.)

Dlt RT (min.) Response

Cal Amt ng

OnCol Amt ng Flags

34 Toxaphene

1 7.098 ND

1 7.369 1 7.827 1 7.906 2 7.518 2 7.565 2 8.313 2 8.820

25 2,4'-DDD

1 7.149 ND

2 7.545

24 Dieldrin

1 7.192 ND

2 7.579

27 Endrin

1 7.396 ND

2 7.845

28 2,4'-DDT

1 7.426 ND

2 7.795

30 cis-Nonachlor

1 7.483 ND

2 7.872

29 4,4'-DDD

1 7.517 ND

2 7.908

31 Endosulfan II

1 7.598 ND

2 8.106

32 Endrin aldehyde

1 7.715 ND

2 8.281

33 4,4'-DDT

1 7.798 ND

2 8.162

35 Endosulfan sulfate

1 7.926 ND

2 8.518

36 Methoxychlor

1 8.256 ND

2 8.758

* 44 Dibutylchlorendate ISTD 1 8.326 8.326 -0.001 348083992H 0.1000 0.1000 2 8.578 8.577 0.001 345422915H 0.1000 0.1000

37 Endrin ketone

1 8.406 ND

Col

(min.)

Exp RT (min.)

Dlt RT (min.) Response

Cal Amt ng

OnCol Amt ng Flags

38 Mirex

1 8.934 ND

2 9.483

$ 39 DCB Decachlorobiphenyl (Surr) 1 10.208 10.209 -0.001 38870911H 0.0200 0.0181 2 10.993 10.991 0.002 34604087H 0.0200 0.0165

RPD = 9.25

QC Flag Legend Processing Flags H - Response Measured by Height Reagents:

Data File: \\chromfs\Pittsburgh\ChromData\CHGC15\20210907-38994.b\Q0907210000009.D Injection Date: 07-Sep-2021 15:39:34 Instrument ID: CHGC15 Operator ID: 402331 Lims ID: LB 180-369295/1-D Worklist Smp#: 9 Client ID:

Injection Vol: 1.0 uL Dil. Factor: 1.0000 ALS Bottle#: 9 Method: IS PEST_CHGC15 Limit Group: GCS 8081B ICAL with IS Column: MR-1 ( 0.53 mm)

0.0 1.0 2.0 3.0 4.0 5.0 6.0 7.0 8.0 9.0 10.0 11.0 12.0 Min

Y (X

GC ECD1A, Q0907210000009.D

B ro m o-

2-ni tro be nz en e(

Te tra ch lo ro

-m -x yl en e(

D ib ut yl ch lo re nd at e

C B

D ec ac hl or ob ip he ny l (

S ur

r) ( 1

Column: MR-2 ( 0.53 mm)

0.0 1.0 2.0 3.0 4.0 5.0 6.0 7.0 8.0 9.0 10.0 11.0 12.0 Min

Y (X

GC ECD2B, Q0907210000009.D

B ro m o-

2-ni tro be nz en e(

Te tra ch lo ro

-m -x yl en e(

D ib ut yl ch lo re nd at e

C B

D ec ac hl or ob ip he ny l (

S ur

r) ( 1

Recovery Report

Data File: \\chromfs\Pittsburgh\ChromData\CHGC15\20210907-38994.b\Q0907210000009.D Lims ID: LB 180-369295/1-D Client ID:

Sample Type: LB Inject. Date: 07-Sep-2021 15:39:34 ALS Bottle#: 9 Worklist Smp#: 9 Injection Vol: 1.0 uL Dil. Factor: 1.0000 Sample Info: 180-0038994-009 Operator ID: 402331 Instrument ID: CHGC15

Column 1 : MR-1 ( 0.53 mm) Det: GC ECD1A Column 2 : MR-2 ( 0.53 mm) Det: GC ECD2B Process Host: CTX1636

First Level Reviewer: eppinged Date: 08-Sep-2021 06:40:59

Surrogate Recovery, Detector: GC ECD1A

Compound Amount Added

Amount Recovered % Rec.

$ 3 Tetrachloro-m-xylene 0.0200 0.0147 73.55

$ 39 DCB Decachlorobiphenyl (Surr) 0.0200 0.0181 90.61

Surrogate Recovery, Detector: GC ECD2B

Compound Amount Added

Amount Recovered % Rec.

$ 3 Tetrachloro-m-xylene 0.0200 0.0159 79.56

$ 39 DCB Decachlorobiphenyl (Surr) 0.0200 0.0165 82.60

Client Sample ID:

Lab Name: Job No.:

SDG No.:

180-126039-1

Lab Sample ID: LB 180-369295/1-D

Eurofins TestAmerica, Pittsburgh

Matrix: Q0907210000009.DLab File ID:

Date Collected:EPA 8081B LLAnalysis Method:

Sediment (SPLP East)

Con. Extract Vol.:

Injection Volume:

GPC Cleanup:(Y/N)

Date Extracted:

Date Analyzed:

Dilution Factor: 1

Extraction Method: 3510C 09/02/2021 06:45

09/07/2021 15:39

1.0(mL)

1(uL)

Sample wt/vol: 1040(mL)

% Moisture:

GC Column: ID: 0.53(mm)MR-2

Analysis Batch No.: 370468 ug/LUnits:

%RECCAS NO. LIMITSQSURROGATE

80 25-122877-09-8 Tetrachloro-m-xylene (Surr)

83 32-1352051-24-3 DCB Decachlorobiphenyl (Surr)

Report Date: 08-Sep-2021 06:59:12 Chrom Revision: 2.3 13-May-2021 07:57:40

Target Compound Quantitation Report

Data File: \\chromfs\Pittsburgh\ChromData\CHGC15\20210907-38994.b\Q0907210000009.D Lims ID: LB 180-369295/1-D Client ID:

Sample Type: LB Inject. Date: 07-Sep-2021 15:39:34 ALS Bottle#: 9 Worklist Smp#: 9 Injection Vol: 1.0 uL Dil. Factor: 1.0000 Sample Info: 180-0038994-009 Operator ID: 402331 Instrument ID: CHGC15

Column 1 : MR-1 ( 0.53 mm) Det: GC ECD1A Column 2 : MR-2 ( 0.53 mm) Det: GC ECD2B Process Host: CTX1636

First Level Reviewer: eppinged Date: 08-Sep-2021 06:40:59

Col

(min.)

Exp RT (min.)

Dlt RT (min.) Response

Cal Amt ng

OnCol Amt ng Flags

* 43 1-Bromo-2-nitrobenzene 1 3.858 3.859 -0.001 713021699H 0.1000 0.1000 2 4.317 4.314 0.003 586924847H 0.1000 0.1000

$ 3 Tetrachloro-m-xylene 1 4.851 4.853 -0.002 122951631H 0.0200 0.0147 2 5.185 5.181 0.004 116675667H 0.0200 0.0159

RPD = 7.85

4 Diallate

1 5.007 ND

1 5.098 2 5.287 2 5.373

5 alpha-BHC

1 5.228 ND

2 5.642

6 Hexachlorobenzene

1 5.260 ND

2 5.604

7 gamma-BHC (Lindane)

1 5.497 ND

2 5.942

8 beta-BHC

1 5.665 ND

2 6.173

10 delta-BHC

1 5.865 ND

Col

(min.)

Exp RT (min.)

Dlt RT (min.) Response

Cal Amt ng

OnCol Amt ng Flags

9 Chlordane (technical)

1 5.968 ND

1 6.230 1 6.835 1 6.905 2 6.111 2 6.271 2 7.223 2 7.269

11 Heptachlor

1 5.968 ND

2 6.273

12 DCPA

1 6.183 ND

2 6.527

13 Aldrin

1 6.252 ND

2 6.542

14 Isodrin

1 6.537 ND

2 6.892

15 oxy-Chlordane

1 6.572 ND

2 6.892

16 Heptachlor epoxide

1 6.616 ND

2 6.983

17 2,4'-DDE

1 6.755 ND

2 7.110

18 trans-Chlordane

1 6.836 ND

2 7.209

19 Chlorobenside

1 6.863 ND

2 7.281

20 cis-Chlordane

1 6.904 ND

2 7.270

22 trans-Nonachlor

1 6.907 ND

2 7.218

21 Endosulfan I

1 6.950 ND

2 7.338

23 4,4'-DDE

1 7.054 ND

Col

(min.)

Exp RT (min.)

Dlt RT (min.) Response

Cal Amt ng

OnCol Amt ng Flags

34 Toxaphene

1 7.098 ND

1 7.369 1 7.827 1 7.906 2 7.518 2 7.565 2 8.313 2 8.820

25 2,4'-DDD

1 7.149 ND

2 7.545

24 Dieldrin

1 7.192 ND

2 7.579

27 Endrin

1 7.396 ND

2 7.845

28 2,4'-DDT

1 7.426 ND

2 7.795

30 cis-Nonachlor

1 7.483 ND

2 7.872

29 4,4'-DDD

1 7.517 ND

2 7.908

31 Endosulfan II

1 7.598 ND

2 8.106

32 Endrin aldehyde

1 7.715 ND

2 8.281

33 4,4'-DDT

1 7.798 ND

2 8.162

35 Endosulfan sulfate

1 7.926 ND

2 8.518

36 Methoxychlor

1 8.256 ND

2 8.758

* 44 Dibutylchlorendate ISTD 1 8.326 8.326 -0.001 348083992H 0.1000 0.1000 2 8.578 8.577 0.001 345422915H 0.1000 0.1000

37 Endrin ketone

1 8.406 ND

Col

(min.)

Exp RT (min.)

Dlt RT (min.) Response

Cal Amt ng

OnCol Amt ng Flags

38 Mirex

1 8.934 ND

2 9.483

$ 39 DCB Decachlorobiphenyl (Surr) 1 10.208 10.209 -0.001 38870911H 0.0200 0.0181 2 10.993 10.991 0.002 34604087H 0.0200 0.0165

RPD = 9.25

QC Flag Legend Processing Flags H - Response Measured by Height Reagents:

Injection Vol: 1.0 uL Dil. Factor: 1.0000 ALS Bottle#: 9 Method: IS PEST_CHGC15 Limit Group: GCS 8081B ICAL with IS Column: MR-1 ( 0.53 mm)

0.0 1.0 2.0 3.0 4.0 5.0 6.0 7.0 8.0 9.0 10.0 11.0 12.0 Min

Y (X

GC ECD1A, Q0907210000009.D

B ro m o-

2-ni tro be nz en e(

Te tra ch lo ro

-m -x yl en e(

D ib ut yl ch lo re nd at e

C B

D ec ac hl or ob ip he ny l (

S ur

r) ( 1

Column: MR-2 ( 0.53 mm)

0.0 1.0 2.0 3.0 4.0 5.0 6.0 7.0 8.0 9.0 10.0 11.0 12.0 Min

Y (X

GC ECD2B, Q0907210000009.D

B ro m o-

2-ni tro be nz en e(

Te tra ch lo ro

-m -x yl en e(

D ib ut yl ch lo re nd at e

C B

D ec ac hl or ob ip he ny l (

S ur

r) ( 1

Recovery Report

Data File: \\chromfs\Pittsburgh\ChromData\CHGC15\20210907-38994.b\Q0907210000009.D Lims ID: LB 180-369295/1-D Client ID:

Sample Type: LB Inject. Date: 07-Sep-2021 15:39:34 ALS Bottle#: 9 Worklist Smp#: 9 Injection Vol: 1.0 uL Dil. Factor: 1.0000 Sample Info: 180-0038994-009 Operator ID: 402331 Instrument ID: CHGC15

Column 1 : MR-1 ( 0.53 mm) Det: GC ECD1A Column 2 : MR-2 ( 0.53 mm) Det: GC ECD2B Process Host: CTX1636

First Level Reviewer: eppinged Date: 08-Sep-2021 06:40:59

Surrogate Recovery, Detector: GC ECD1A

Compound Amount Added

Amount Recovered % Rec.

$ 3 Tetrachloro-m-xylene 0.0200 0.0147 73.55

$ 39 DCB Decachlorobiphenyl (Surr) 0.0200 0.0181 90.61

Surrogate Recovery, Detector: GC ECD2B

Compound Amount Added

Amount Recovered % Rec.

$ 3 Tetrachloro-m-xylene 0.0200 0.0159 79.56

$ 39 DCB Decachlorobiphenyl (Surr) 0.0200 0.0165 82.60

Client Sample ID:

Lab Name: Job No.:

SDG No.:

180-126039-1

Lab Sample ID: LCS 180-369080/2-B

Eurofins TestAmerica, Pittsburgh

Matrix: Q0913210000026.DLab File ID:

Date Collected:EPA 8081B LLAnalysis Method:

Sediment

Con. Extract Vol.:

Injection Volume:

GPC Cleanup:(Y/N)

Date Extracted:

Date Analyzed:

Dilution Factor: 1

Extraction Method: 3541 08/25/2021 09:32

09/13/2021 15:25

0.5(mL)

1(uL)

Sample…

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File details come from the government source that posted it. Updated Apr 12, 2023.