Attachment 2 - Specifications_ATTACHMENTS_Part 5 of 5.pdf

PDF 22 MB Posted Oct 30, 2020

Attached to: Sacramento River East Levee (SREL) Contract 2
Solicitation number: W9123821B0001
Issued by: Department of the Army Corps of Engineers Engineering District Sacramento

About this file

Written by GovTribe AI · Dec 27, 2023

This document provides details on a federal contract opportunity for construction work on the Sacramento River East Levee. The Army Corps of Engineers seeks a firm-fixed price contract for construction of approximately 1.8 miles of seepage cutoff walls along with utility relocations and modifications to relief wells. Work must be completed by December 2021 and includes soil-bentonite, slag cement-bentonite, and jet grout cutoff walls. An invitation for bid will be issued on or about October 30, 2020, with bids due by November 30, 2020. The contract value is estimated between $25-100 million and is set aside for contractors on the Corps' Pre-Qualified Sources List.

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Other files

File	Type	Posted
Bid Abstract.pdf	PDF	Dec 15, 2020
Amendment 0004 - Pricing Schedule.pdf	PDF	Dec 11, 2020
Amendment 0004 - Summary of Changes.pdf	PDF	Dec 11, 2020
Amendment 0004 - Specification Revision.pdf	PDF	Dec 11, 2020
Amendment 0004.pdf	PDF	Dec 11, 2020
Amendment 0004 - Revised Drawing.pdf	PDF	Dec 11, 2020
Amendment 0003 - Specification ATTACHMENTS.pdf	PDF	Dec 8, 2020
Amendment 0003 - Specifications.pdf	PDF	Dec 8, 2020
Amendment 0003.pdf	PDF	Dec 8, 2020
Amendment 0003 - Summary.pdf	PDF	Dec 8, 2020
Amendment 0003 - Drawings.pdf	PDF	Dec 8, 2020
Amendment 0002 - Revised Drawings.pdf	PDF	Nov 25, 2020
Amendment 0002.pdf	PDF	Nov 25, 2020
Amendment 0002 - Specifications ATTACHMENTS.pdf	PDF	Nov 25, 2020
Amendment 0002 - Revised 2342 Specifications.pdf	PDF	Nov 25, 2020
Amendment 0002 - Revised Pricing_Schedule.pdf	PDF	Nov 25, 2020
Amendment 0002 - Summary.pdf	PDF	Nov 25, 2020
Site Visit Sign-In Sheet.pdf	PDF	Nov 18, 2020
ARCF SREL C2 Site Visit 10NOV20.pdf	PDF	Nov 10, 2020
Solicitation W9123821B0001.pdf	PDF	Nov 3, 2020
Amendment 1.pdf	PDF	Nov 3, 2020
Site Visit Map.pdf	PDF	Nov 3, 2020
Attachment 3 - Drawings.10.29.2020.pdf	PDF	Oct 30, 2020
Attachment 2 - Specifications_ATTACHMENTS_Part 1 of 5.pdf	PDF	Oct 30, 2020
Attachment 1 - Specifications_10.23.2020.pdf	PDF	Oct 30, 2020
Attachment 7 - Pre-Award Survey.pdf	PDF	Oct 30, 2020
Attachment 2 - Specifications_ATTACHMENTS_Part 2 of 5.pdf	PDF	Oct 30, 2020
Attachment 6 - Past Performance Questionnaire.pdf	PDF	Oct 30, 2020
Attachment 5 - Pricing Schedule.pdf	PDF	Oct 30, 2020
Attachment 2 - Specifications_ATTACHMENTS_Part 4 of 5.pdf	PDF	Oct 30, 2020
Attachment 4 - Wage Determination.CA20200007.10.9.2020.pdf	PDF	Oct 30, 2020
Solicitation W9123821B0001.pdf	PDF	Oct 30, 2020
Attachment 2 - Specifications_ATTACHMENTS_Part 3 of 5.pdf	PDF	Oct 30, 2020

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QC Sample Results Job ID: 320-61753-1Client: Kleinfelder Inc

Project/Site: SACFA SREL 2

Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)

Client Sample ID: Lab Control SampleLab Sample ID: LCS 320-387615/3 Matrix: Solid Prep Type: Total/NA Analysis Batch: 387615 m-Xylene & p-Xylene 50.0 50.9 ug/Kg 102 77 - 124

Analyte

LCS LCS

DUnitResult Qualifier %Rec

Spike

Added

%Rec.

Limits

Methyl tert-butyl ether 50.0 48.9 ug/Kg 98 73 - 125

Methylene Chloride 50.0 49.6 ug/Kg 99 70 - 128 n-Butylbenzene 50.0 51.8 ug/Kg 104 70 - 128

N-Propylbenzene 50.0 52.6 ug/Kg 105 73 - 125 o-Xylene 50.0 51.9 ug/Kg 104 77 - 123 sec-Butylbenzene 50.0 53.3 ug/Kg 107 73 - 126

Styrene 50.0 52.6 ug/Kg 105 76 - 124 trans-1,4-Dichloro-2-butene 50.0 53.9 ug/Kg 108 62 - 136 tert-Butylbenzene 50.0 57.3 ug/Kg 115 73 - 125

Tetrachloroethene 50.0 49.8 ug/Kg 100 73 - 128

Toluene 50.0 52.4 ug/Kg 105 77 - 121 trans-1,2-Dichloroethene 50.0 48.3 ug/Kg 97 74 - 125 trans-1,3-Dichloropropene 50.0 48.0 ug/Kg 96 71 - 130

Trichloroethene 50.0 50.8 ug/Kg 102 77 - 123

Trichlorofluoromethane 50.0 49.0 ug/Kg 98 62 - 140

Vinyl acetate 50.0 51.5 ug/Kg 103 50 - 151

Vinyl chloride 50.0 55.3 ug/Kg 111 56 - 135

Xylenes, Total 100 103 ug/Kg 103 78 - 124

1,2-Dichloroethane-d4 (Surr) 71 - 136

Surrogate

LCS LCS

Qualifier Limits%Recovery

884-Bromofluorobenzene (Surr) 79 - 119

92Dibromofluoromethane (Surr) 78 - 119

89Toluene-d8 (Surr) 85 - 116

Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 320-387615/4 Matrix: Solid Prep Type: Total/NA Analysis Batch: 387615

1,1,1,2-Tetrachloroethane 50.0 52.0 ug/Kg 104 78 - 125 1 20

Analyte

LCSD LCSD

DUnitResult Qualifier %Rec

Spike

Added

%Rec.

Limits LimitRPD

RPD

1,1,1-Trichloroethane 50.0 49.0 ug/Kg 98 73 - 130 2 20

1,1,2,2-Tetrachloroethane 50.0 53.8 ug/Kg 108 70 - 124 2 20

1,1,2-Trichloroethane 50.0 53.8 ug/Kg 108 78 - 121 2 20

1,1,2-Trichloro-1,2,2-trifluoroetha ne

50.0 47.5 ug/Kg 95 66 - 136 6 20

1,1-Dichloroethane 50.0 51.0 ug/Kg 102 76 - 125 2 20

1,1-Dichloroethene 50.0 49.4 ug/Kg 99 70 - 131 3 20

1,1-Dichloropropene 50.0 49.0 ug/Kg 98 76 - 125 3 20

1,2,3-Trichlorobenzene 50.0 54.4 ug/Kg 109 66 - 130 3 20

1,2,3-Trichloropropane 50.0 51.5 ug/Kg 103 73 - 125 1 20

1,2,4-Trichlorobenzene 50.0 54.1 ug/Kg 108 67 - 129 1 20

1,2,4-Trimethylbenzene 50.0 52.1 ug/Kg 104 75 - 123 2 20

Ethylene Dibromide 50.0 52.3 ug/Kg 105 78 - 122 1 20

1,2-Dichlorobenzene 50.0 53.7 ug/Kg 107 78 - 121 2 20

1,2-Dichloroethane 50.0 51.6 ug/Kg 103 73 - 128 1 20

1,2-Dichloropropane 50.0 51.8 ug/Kg 104 76 - 123 0 20

1,3,5-Trimethylbenzene 50.0 51.7 ug/Kg 103 73 - 124 2 20

Eurofins TestAmerica, Sacramento

Page 40 of 66 7/31/2020 (Rev. 1)

Project/Site: SACFA SREL 2

Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)

Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 320-387615/4 Matrix: Solid Prep Type: Total/NA Analysis Batch: 387615

1,3-Dichlorobenzene 50.0 51.9 ug/Kg 104 77 - 121 1 20

Analyte

LCSD LCSD

DUnitResult Qualifier %Rec

Spike

Added

%Rec.

Limits LimitRPD

RPD

1,3-Dichloropropane 50.0 52.4 ug/Kg 105 77 - 121 3 20

1,4-Dichlorobenzene 50.0 51.0 ug/Kg 102 75 - 120 1 20

2,2-Dichloropropane 50.0 46.7 ug/Kg 93 67 - 133 0 20

2-Butanone (MEK) 50.0 57.3 ug/Kg 115 51 - 148 2 20

2-Chlorotoluene 50.0 52.1 ug/Kg 104 75 - 122 1 20

2-Hexanone 50.0 60.6 ug/Kg 121 53 - 145 9 20

4-Chlorotoluene 50.0 51.8 ug/Kg 104 72 - 124 1 20

4-Isopropyltoluene 50.0 50.6 ug/Kg 101 73 - 127 6 20

4-Methyl-2-pentanone (MIBK) 50.0 55.4 ug/Kg 111 65 - 135 5 20

Acetone 50.0 57.6 ug/Kg 115 36 - 164 3 20

Benzene 50.0 50.2 ug/Kg 100 77 - 121 1 20

Bromobenzene 50.0 52.2 ug/Kg 104 78 - 121 1 20

Chlorobromomethane 50.0 51.2 ug/Kg 102 78 - 125 2 20

Dichlorobromomethane 50.0 50.4 ug/Kg 101 75 - 127 0 20

Bromoform 50.0 49.6 ug/Kg 99 67 - 132 4 20

Bromomethane 50.0 48.7 ug/Kg 97 53 - 143 0 20

Carbon disulfide 50.0 47.6 ug/Kg 95 63 - 132 6 20

Carbon tetrachloride 50.0 48.8 ug/Kg 98 70 - 135 2 20

Chlorobenzene 50.0 51.1 ug/Kg 102 79 - 120 2 20

Chloroethane 50.0 50.1 ug/Kg 100 59 - 139 2 20

Chloroform 50.0 49.6 ug/Kg 99 78 - 123 1 20

Chloromethane 50.0 55.5 ug/Kg 111 50 - 136 3 20 cis-1,2-Dichloroethene 50.0 50.4 ug/Kg 101 77 - 123 3 20 cis-1,3-Dichloropropene 50.0 49.9 ug/Kg 100 74 - 126 1 20

Chlorodibromomethane 50.0 53.7 ug/Kg 107 74 - 126 3 20

Dibromomethane 50.0 48.6 ug/Kg 97 78 - 125 2 20

Dichlorodifluoromethane 50.0 44.5 ug/Kg 89 29 - 149 2 20

Ethylbenzene 50.0 51.5 ug/Kg 103 76 - 122 1 20

Hexachlorobutadiene 50.0 49.3 ug/Kg 99 61 - 135 5 20

Isopropylbenzene 50.0 49.4 ug/Kg 99 68 - 134 6 20 m-Xylene & p-Xylene 50.0 50.9 ug/Kg 102 77 - 124 0 20

Methyl tert-butyl ether 50.0 47.7 ug/Kg 95 73 - 125 2 20

Methylene Chloride 50.0 49.1 ug/Kg 98 70 - 128 1 20 n-Butylbenzene 50.0 50.5 ug/Kg 101 70 - 128 3 20

N-Propylbenzene 50.0 51.0 ug/Kg 102 73 - 125 3 20 o-Xylene 50.0 50.2 ug/Kg 100 77 - 123 3 20 sec-Butylbenzene 50.0 50.9 ug/Kg 102 73 - 126 5 20

Styrene 50.0 51.0 ug/Kg 102 76 - 124 3 20 trans-1,4-Dichloro-2-butene 50.0 53.6 ug/Kg 107 62 - 136 1 20 tert-Butylbenzene 50.0 55.8 ug/Kg 112 73 - 125 3 20

Tetrachloroethene 50.0 49.4 ug/Kg 99 73 - 128 1 20

Toluene 50.0 50.8 ug/Kg 102 77 - 121 3 20 trans-1,2-Dichloroethene 50.0 47.7 ug/Kg 95 74 - 125 1 20 trans-1,3-Dichloropropene 50.0 50.1 ug/Kg 100 71 - 130 4 20

Trichloroethene 50.0 49.3 ug/Kg 99 77 - 123 3 20

Trichlorofluoromethane 50.0 46.7 ug/Kg 93 62 - 140 5 20

Vinyl acetate 50.0 54.9 ug/Kg 110 50 - 151 6 20

Vinyl chloride 50.0 54.4 ug/Kg 109 56 - 135 2 20

Eurofins TestAmerica, Sacramento

Page 41 of 66 7/31/2020 (Rev. 1)

Project/Site: SACFA SREL 2

Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)

Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 320-387615/4 Matrix: Solid Prep Type: Total/NA Analysis Batch: 387615

Xylenes, Total 100 101 ug/Kg 101 78 - 124 2 20

Analyte

LCSD LCSD

DUnitResult Qualifier %Rec

Spike

Added

%Rec.

Limits LimitRPD

RPD

1,2-Dichloroethane-d4 (Surr) 71 - 136

Surrogate

LCSD LCSD

Qualifier Limits%Recovery

864-Bromofluorobenzene (Surr) 79 - 119

91Dibromofluoromethane (Surr) 78 - 119

91Toluene-d8 (Surr) 85 - 116

Client Sample ID: Method BlankLab Sample ID: MB 320-388939/10 Matrix: Solid Prep Type: Total/NA Analysis Batch: 388939

LOQ DL

1,1,1,2-Tetrachloroethane 1.0 U 5.0 0.41 ug/Kg 06/24/20 13:04 1

MB MB

Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier

1.0 U 0.365.0 ug/Kg 06/24/20 13:04 11,1,1-Trichloroethane

2.0 U 0.685.0 ug/Kg 06/24/20 13:04 11,1,2,2-Tetrachloroethane

1.0 U 0.445.0 ug/Kg 06/24/20 13:04 11,1,2-Trichloroethane

1.0 U 0.8310 ug/Kg 06/24/20 13:04 11,1,2-Trichloro-1,2,2-trifluoroethane

1.0 U 0.295.0 ug/Kg 06/24/20 13:04 11,1-Dichloroethane

1.0 U 0.265.0 ug/Kg 06/24/20 13:04 11,1-Dichloroethene

1.0 U 0.375.0 ug/Kg 06/24/20 13:04 11,1-Dichloropropene

2.0 U 0.755.0 ug/Kg 06/24/20 13:04 11,2,3-Trichlorobenzene

2.0 U 0.765.0 ug/Kg 06/24/20 13:04 11,2,3-Trichloropropane

2.0 U 0.755.0 ug/Kg 06/24/20 13:04 11,2,4-Trichlorobenzene

2.0 U 0.515.0 ug/Kg 06/24/20 13:04 11,2,4-Trimethylbenzene

2.0 U 0.8810 ug/Kg 06/24/20 13:04 11,2-Dibromo-3-Chloropropane

1.0 U 0.2710 ug/Kg 06/24/20 13:04 1Ethylene Dibromide

2.0 U 0.645.0 ug/Kg 06/24/20 13:04 11,2-Dichlorobenzene

2.0 U 0.735.0 ug/Kg 06/24/20 13:04 11,2-Dichloroethane

2.0 U 0.605.0 ug/Kg 06/24/20 13:04 11,2-Dichloropropane

1.0 U 0.355.0 ug/Kg 06/24/20 13:04 11,3,5-Trimethylbenzene

1.0 U 0.305.0 ug/Kg 06/24/20 13:04 11,3-Dichlorobenzene

2.0 U 0.575.0 ug/Kg 06/24/20 13:04 11,3-Dichloropropane

2.0 U 0.785.0 ug/Kg 06/24/20 13:04 11,4-Dichlorobenzene

1.0 U 0.385.0 ug/Kg 06/24/20 13:04 12,2-Dichloropropane

5.0 U 1.410 ug/Kg 06/24/20 13:04 12-Butanone (MEK)

2.0 U 0.625.0 ug/Kg 06/24/20 13:04 12-Chlorotoluene

2.0 U 0.7410 ug/Kg 06/24/20 13:04 12-Hexanone

2.0 U 0.865.0 ug/Kg 06/24/20 13:04 14-Chlorotoluene

2.0 U 0.635.0 ug/Kg 06/24/20 13:04 14-Isopropyltoluene

2.0 U 0.9210 ug/Kg 06/24/20 13:04 14-Methyl-2-pentanone (MIBK)

5.0 U 1.420 ug/Kg 06/24/20 13:04 1Acetone

1.0 U 0.265.0 ug/Kg 06/24/20 13:04 1Benzene

2.0 U 0.525.0 ug/Kg 06/24/20 13:04 1Bromobenzene

2.0 U 0.945.0 ug/Kg 06/24/20 13:04 1Chlorobromomethane

2.0 U 0.535.0 ug/Kg 06/24/20 13:04 1Dichlorobromomethane

1.0 U 0.405.0 ug/Kg 06/24/20 13:04 1Bromoform

2.0 U 0.865.0 ug/Kg 06/24/20 13:04 1Bromomethane

Eurofins TestAmerica, Sacramento

Page 42 of 66 7/31/2020 (Rev. 1)

Project/Site: SACFA SREL 2

Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)

Client Sample ID: Method BlankLab Sample ID: MB 320-388939/10 Matrix: Solid Prep Type: Total/NA Analysis Batch: 388939

LOQ DL

Carbon disulfide 1.0 U 10 0.49 ug/Kg 06/24/20 13:04 1

MB MB

Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier

2.0 U 0.535.0 ug/Kg 06/24/20 13:04 1Carbon tetrachloride

1.0 U 0.295.0 ug/Kg 06/24/20 13:04 1Chlorobenzene

1.0 U 0.455.0 ug/Kg 06/24/20 13:04 1Chloroethane

1.0 U 0.265.0 ug/Kg 06/24/20 13:04 1Chloroform

1.0 U 0.505.0 ug/Kg 06/24/20 13:04 1Chloromethane

2.0 U 0.895.0 ug/Kg 06/24/20 13:04 1cis-1,2-Dichloroethene

2.0 U 0.645.0 ug/Kg 06/24/20 13:04 1cis-1,3-Dichloropropene

1.0 U 0.265.0 ug/Kg 06/24/20 13:04 1Chlorodibromomethane

2.0 U 0.585.0 ug/Kg 06/24/20 13:04 1Dibromomethane

2.0 U 0.895.0 ug/Kg 06/24/20 13:04 1Dichlorodifluoromethane

1.0 U 0.345.0 ug/Kg 06/24/20 13:04 1Ethylbenzene

1.0 U 0.335.0 ug/Kg 06/24/20 13:04 1Hexachlorobutadiene

2.0 U 0.525.0 ug/Kg 06/24/20 13:04 1Isopropylbenzene

2.0 U 0.815.0 ug/Kg 06/24/20 13:04 1m-Xylene & p-Xylene

2.0 U 0.605.0 ug/Kg 06/24/20 13:04 1Methyl tert-butyl ether

2.0 U 0.845.0 ug/Kg 06/24/20 13:04 1Methylene Chloride

2.0 U 0.665.0 ug/Kg 06/24/20 13:04 1n-Butylbenzene

1.0 U 0.295.0 ug/Kg 06/24/20 13:04 1N-Propylbenzene

2.0 U 0.635.0 ug/Kg 06/24/20 13:04 1Naphthalene

1.0 U 0.335.0 ug/Kg 06/24/20 13:04 1o-Xylene

2.0 U 0.755.0 ug/Kg 06/24/20 13:04 1sec-Butylbenzene

1.0 U 0.315.0 ug/Kg 06/24/20 13:04 1Styrene

2.5 U 0.3110 ug/Kg 06/24/20 13:04 1trans-1,4-Dichloro-2-butene

2.0 U 0.545.0 ug/Kg 06/24/20 13:04 1tert-Butylbenzene

2.0 U 0.615.0 ug/Kg 06/24/20 13:04 1Tetrachloroethene

2.0 U 0.615.0 ug/Kg 06/24/20 13:04 1Toluene

1.0 U 0.385.0 ug/Kg 06/24/20 13:04 1trans-1,2-Dichloroethene

2.0 U 0.755.0 ug/Kg 06/24/20 13:04 1trans-1,3-Dichloropropene

2.0 U 0.605.0 ug/Kg 06/24/20 13:04 1Trichloroethene

1.0 U 0.345.0 ug/Kg 06/24/20 13:04 1Trichlorofluoromethane

1.0 U 0.695.0 ug/Kg 06/24/20 13:04 1Vinyl acetate

1.0 U 0.365.0 ug/Kg 06/24/20 13:04 1Vinyl chloride

1.5 U 0.815.0 ug/Kg 06/24/20 13:04 1Xylenes, Total

1,2-Dichloroethane-d4 (Surr) 88 71 - 136 06/24/20 13:04 1

MB MB

Surrogate Dil FacPrepared AnalyzedQualifier Limits%Recovery

90 06/24/20 13:04 14-Bromofluorobenzene (Surr) 79 - 119

90 06/24/20 13:04 1Dibromofluoromethane (Surr) 78 - 119

90 06/24/20 13:04 1Toluene-d8 (Surr) 85 - 116

Client Sample ID: Lab Control SampleLab Sample ID: LCS 320-388939/7 Matrix: Solid Prep Type: Total/NA Analysis Batch: 388939

1,1,1,2-Tetrachloroethane 50.0 53.0 ug/Kg 106 78 - 125

Analyte

LCS LCS

DUnitResult Qualifier %Rec

Spike

Added

%Rec.

Limits

1,1,1-Trichloroethane 50.0 55.5 ug/Kg 111 73 - 130

Eurofins TestAmerica, Sacramento

Page 43 of 66 7/31/2020 (Rev. 1)

Project/Site: SACFA SREL 2

Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)

Client Sample ID: Lab Control SampleLab Sample ID: LCS 320-388939/7 Matrix: Solid Prep Type: Total/NA Analysis Batch: 388939

1,1,2,2-Tetrachloroethane 50.0 52.9 ug/Kg 106 70 - 124

Analyte

LCS LCS

DUnitResult Qualifier %Rec

Spike

Added

%Rec.

Limits

1,1,2-Trichloroethane 50.0 51.4 ug/Kg 103 78 - 121

1,1,2-Trichloro-1,2,2-trifluoroetha ne

50.0 57.1 ug/Kg 114 66 - 136

1,1-Dichloroethane 50.0 54.9 ug/Kg 110 76 - 125

1,1-Dichloroethene 50.0 55.0 ug/Kg 110 70 - 131

1,1-Dichloropropene 50.0 56.7 ug/Kg 113 76 - 125

1,2,3-Trichlorobenzene 50.0 50.3 ug/Kg 101 66 - 130

1,2,3-Trichloropropane 50.0 54.6 ug/Kg 109 73 - 125

1,2,4-Trichlorobenzene 50.0 49.2 ug/Kg 98 67 - 129

1,2,4-Trimethylbenzene 50.0 55.9 ug/Kg 112 75 - 123

1,2-Dibromo-3-Chloropropane 50.0 51.4 ug/Kg 103 61 - 132

Ethylene Dibromide 50.0 51.4 ug/Kg 103 78 - 122

1,2-Dichlorobenzene 50.0 52.7 ug/Kg 105 78 - 121

1,2-Dichloroethane 50.0 51.5 ug/Kg 103 73 - 128

1,2-Dichloropropane 50.0 52.6 ug/Kg 105 76 - 123

1,3,5-Trimethylbenzene 50.0 57.0 ug/Kg 114 73 - 124

1,3-Dichlorobenzene 50.0 54.0 ug/Kg 108 77 - 121

1,3-Dichloropropane 50.0 51.5 ug/Kg 103 77 - 121

1,4-Dichlorobenzene 50.0 52.0 ug/Kg 104 75 - 120

2,2-Dichloropropane 50.0 52.7 ug/Kg 105 67 - 133

2-Butanone (MEK) 50.0 45.4 ug/Kg 91 51 - 148

2-Chlorotoluene 50.0 55.5 ug/Kg 111 75 - 122

2-Hexanone 50.0 43.5 ug/Kg 87 53 - 145

4-Chlorotoluene 50.0 55.2 ug/Kg 110 72 - 124

4-Isopropyltoluene 50.0 58.7 ug/Kg 117 73 - 127

4-Methyl-2-pentanone (MIBK) 50.0 45.5 ug/Kg 91 65 - 135

Acetone 50.0 44.7 ug/Kg 89 36 - 164

Benzene 50.0 52.9 ug/Kg 106 77 - 121

Bromobenzene 50.0 53.2 ug/Kg 106 78 - 121

Chlorobromomethane 50.0 49.2 ug/Kg 98 78 - 125

Dichlorobromomethane 50.0 50.3 ug/Kg 101 75 - 127

Bromoform 50.0 50.5 ug/Kg 101 67 - 132

Bromomethane 50.0 48.9 ug/Kg 98 53 - 143

Carbon disulfide 50.0 54.5 ug/Kg 109 63 - 132

Carbon tetrachloride 50.0 56.7 ug/Kg 113 70 - 135

Chlorobenzene 50.0 54.4 ug/Kg 109 79 - 120

Chloroethane 50.0 48.9 ug/Kg 98 59 - 139

Chloroform 50.0 51.2 ug/Kg 102 78 - 123

Chloromethane 50.0 55.5 ug/Kg 111 50 - 136 cis-1,2-Dichloroethene 50.0 52.5 ug/Kg 105 77 - 123 cis-1,3-Dichloropropene 50.0 48.2 ug/Kg 96 74 - 126

Chlorodibromomethane 50.0 51.9 ug/Kg 104 74 - 126

Dibromomethane 50.0 46.3 ug/Kg 93 78 - 125

Dichlorodifluoromethane 50.0 54.3 ug/Kg 109 29 - 149

Ethylbenzene 50.0 57.5 ug/Kg 115 76 - 122

Hexachlorobutadiene 50.0 58.9 ug/Kg 118 61 - 135

Isopropylbenzene 50.0 57.6 ug/Kg 115 68 - 134 m-Xylene & p-Xylene 50.0 56.9 ug/Kg 114 77 - 124

Eurofins TestAmerica, Sacramento

Page 44 of 66 7/31/2020 (Rev. 1)

Project/Site: SACFA SREL 2

Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)

Client Sample ID: Lab Control SampleLab Sample ID: LCS 320-388939/7 Matrix: Solid Prep Type: Total/NA Analysis Batch: 388939

Methyl tert-butyl ether 50.0 46.8 ug/Kg 94 73 - 125

Analyte

LCS LCS

DUnitResult Qualifier %Rec

Spike

Added

%Rec.

Limits

Methylene Chloride 50.0 50.3 ug/Kg 101 70 - 128 n-Butylbenzene 50.0 57.3 ug/Kg 115 70 - 128

N-Propylbenzene 50.0 58.4 ug/Kg 117 73 - 125

Naphthalene 50.0 53.0 ug/Kg 106 62 - 129 o-Xylene 50.0 54.1 ug/Kg 108 77 - 123 sec-Butylbenzene 50.0 59.7 ug/Kg 119 73 - 126

Styrene 50.0 54.9 ug/Kg 110 76 - 124 trans-1,4-Dichloro-2-butene 50.0 55.3 ug/Kg 111 62 - 136 tert-Butylbenzene 50.0 63.4 Q ug/Kg 127 73 - 125

Tetrachloroethene 50.0 56.3 ug/Kg 113 73 - 128

Toluene 50.0 55.5 ug/Kg 111 77 - 121 trans-1,2-Dichloroethene 50.0 52.9 ug/Kg 106 74 - 125 trans-1,3-Dichloropropene 50.0 48.6 ug/Kg 97 71 - 130

Trichloroethene 50.0 53.7 ug/Kg 107 77 - 123

Trichlorofluoromethane 50.0 55.6 ug/Kg 111 62 - 140

Vinyl acetate 50.0 51.9 ug/Kg 104 50 - 151

Vinyl chloride 50.0 55.2 ug/Kg 110 56 - 135

Xylenes, Total 100 111 ug/Kg 111 78 - 124

1,2-Dichloroethane-d4 (Surr) 71 - 136

Surrogate

LCS LCS

Qualifier Limits%Recovery

884-Bromofluorobenzene (Surr) 79 - 119

88Dibromofluoromethane (Surr) 78 - 119

90Toluene-d8 (Surr) 85 - 116

Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 320-388939/8 Matrix: Solid Prep Type: Total/NA Analysis Batch: 388939

1,1,1,2-Tetrachloroethane 50.0 51.0 ug/Kg 102 78 - 125 4 20

Analyte

LCSD LCSD

DUnitResult Qualifier %Rec

Spike

Added

%Rec.

Limits LimitRPD

RPD

1,1,1-Trichloroethane 50.0 54.1 ug/Kg 108 73 - 130 3 20

1,1,2,2-Tetrachloroethane 50.0 50.9 ug/Kg 102 70 - 124 4 20

1,1,2-Trichloroethane 50.0 53.1 ug/Kg 106 78 - 121 3 20

1,1,2-Trichloro-1,2,2-trifluoroetha ne

50.0 54.2 ug/Kg 108 66 - 136 5 20

1,1-Dichloroethane 50.0 52.2 ug/Kg 104 76 - 125 5 20

1,1-Dichloroethene 50.0 53.0 ug/Kg 106 70 - 131 4 20

1,1-Dichloropropene 50.0 54.0 ug/Kg 108 76 - 125 5 20

1,2,3-Trichlorobenzene 50.0 49.0 ug/Kg 98 66 - 130 2 20

1,2,3-Trichloropropane 50.0 51.2 ug/Kg 102 73 - 125 7 20

1,2,4-Trichlorobenzene 50.0 46.7 ug/Kg 93 67 - 129 5 20

1,2,4-Trimethylbenzene 50.0 53.3 ug/Kg 107 75 - 123 5 20

1,2-Dibromo-3-Chloropropane 50.0 51.1 ug/Kg 102 61 - 132 1 20

Ethylene Dibromide 50.0 51.6 ug/Kg 103 78 - 122 0 20

1,2-Dichlorobenzene 50.0 50.2 ug/Kg 100 78 - 121 5 20

1,2-Dichloroethane 50.0 48.9 ug/Kg 98 73 - 128 5 20

1,2-Dichloropropane 50.0 51.7 ug/Kg 103 76 - 123 2 20

Eurofins TestAmerica, Sacramento

Page 45 of 66 7/31/2020 (Rev. 1)

Project/Site: SACFA SREL 2

Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)

Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 320-388939/8 Matrix: Solid Prep Type: Total/NA Analysis Batch: 388939

1,3,5-Trimethylbenzene 50.0 54.1 ug/Kg 108 73 - 124 5 20

Analyte

LCSD LCSD

DUnitResult Qualifier %Rec

Spike

Added

%Rec.

Limits LimitRPD

RPD

1,3-Dichlorobenzene 50.0 51.0 ug/Kg 102 77 - 121 6 20

1,3-Dichloropropane 50.0 51.2 ug/Kg 102 77 - 121 1 20

1,4-Dichlorobenzene 50.0 50.3 ug/Kg 101 75 - 120 3 20

2,2-Dichloropropane 50.0 49.2 ug/Kg 98 67 - 133 7 20

2-Butanone (MEK) 50.0 46.4 ug/Kg 93 51 - 148 2 20

2-Chlorotoluene 50.0 53.0 ug/Kg 106 75 - 122 5 20

2-Hexanone 50.0 46.2 ug/Kg 92 53 - 145 6 20

4-Chlorotoluene 50.0 52.6 ug/Kg 105 72 - 124 5 20

4-Isopropyltoluene 50.0 55.5 ug/Kg 111 73 - 127 6 20

4-Methyl-2-pentanone (MIBK) 50.0 45.9 ug/Kg 92 65 - 135 1 20

Acetone 50.0 49.5 ug/Kg 99 36 - 164 10 20

Benzene 50.0 51.1 ug/Kg 102 77 - 121 4 20

Bromobenzene 50.0 50.4 ug/Kg 101 78 - 121 6 20

Chlorobromomethane 50.0 49.3 ug/Kg 99 78 - 125 0 20

Dichlorobromomethane 50.0 47.7 ug/Kg 95 75 - 127 5 20

Bromoform 50.0 49.5 ug/Kg 99 67 - 132 2 20

Bromomethane 50.0 47.6 ug/Kg 95 53 - 143 3 20

Carbon disulfide 50.0 53.0 ug/Kg 106 63 - 132 3 20

Carbon tetrachloride 50.0 54.5 ug/Kg 109 70 - 135 4 20

Chlorobenzene 50.0 53.0 ug/Kg 106 79 - 120 3 20

Chloroethane 50.0 48.7 ug/Kg 97 59 - 139 0 20

Chloroform 50.0 49.8 ug/Kg 100 78 - 123 3 20

Chloromethane 50.0 52.3 ug/Kg 105 50 - 136 6 20 cis-1,2-Dichloroethene 50.0 48.9 ug/Kg 98 77 - 123 7 20 cis-1,3-Dichloropropene 50.0 46.8 ug/Kg 94 74 - 126 3 20

Chlorodibromomethane 50.0 50.7 ug/Kg 101 74 - 126 2 20

Dibromomethane 50.0 45.3 ug/Kg 91 78 - 125 2 20

Dichlorodifluoromethane 50.0 52.6 ug/Kg 105 29 - 149 3 20

Ethylbenzene 50.0 56.1 ug/Kg 112 76 - 122 2 20

Hexachlorobutadiene 50.0 55.0 ug/Kg 110 61 - 135 7 20

Isopropylbenzene 50.0 55.2 ug/Kg 110 68 - 134 4 20 m-Xylene & p-Xylene 50.0 55.2 ug/Kg 110 77 - 124 3 20

Methyl tert-butyl ether 50.0 44.9 ug/Kg 90 73 - 125 4 20

Methylene Chloride 50.0 48.5 ug/Kg 97 70 - 128 4 20 n-Butylbenzene 50.0 55.1 ug/Kg 110 70 - 128 4 20

N-Propylbenzene 50.0 55.7 ug/Kg 111 73 - 125 5 20

Naphthalene 50.0 50.9 ug/Kg 102 62 - 129 4 20 o-Xylene 50.0 53.0 ug/Kg 106 77 - 123 2 20 sec-Butylbenzene 50.0 56.2 ug/Kg 112 73 - 126 6 20

Styrene 50.0 53.5 ug/Kg 107 76 - 124 3 20 trans-1,4-Dichloro-2-butene 50.0 52.6 ug/Kg 105 62 - 136 5 20 tert-Butylbenzene 50.0 60.3 ug/Kg 121 73 - 125 5 20

Tetrachloroethene 50.0 55.4 ug/Kg 111 73 - 128 2 20

Toluene 50.0 54.8 ug/Kg 110 77 - 121 1 20 trans-1,2-Dichloroethene 50.0 51.1 ug/Kg 102 74 - 125 4 20 trans-1,3-Dichloropropene 50.0 45.3 ug/Kg 91 71 - 130 7 20

Trichloroethene 50.0 53.1 ug/Kg 106 77 - 123 1 20

Trichlorofluoromethane 50.0 54.0 ug/Kg 108 62 - 140 3 20

Eurofins TestAmerica, Sacramento

Page 46 of 66 7/31/2020 (Rev. 1)

Project/Site: SACFA SREL 2

Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)

Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 320-388939/8 Matrix: Solid Prep Type: Total/NA Analysis Batch: 388939

Vinyl acetate 50.0 49.5 ug/Kg 99 50 - 151 5 20

Analyte

LCSD LCSD

DUnitResult Qualifier %Rec

Spike

Added

%Rec.

Limits LimitRPD

RPD

Vinyl chloride 50.0 52.2 ug/Kg 104 56 - 135 6 20

Xylenes, Total 100 108 ug/Kg 108 78 - 124 3 20

1,2-Dichloroethane-d4 (Surr) 71 - 136

Surrogate

LCSD LCSD

Qualifier Limits%Recovery

874-Bromofluorobenzene (Surr) 79 - 119

87Dibromofluoromethane (Surr) 78 - 119

90Toluene-d8 (Surr) 85 - 116

Method: 8270C - Semivolatile Organic Compounds (GC/MS)

Client Sample ID: Method BlankLab Sample ID: MB 320-387837/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 389231 Prep Batch: 387837

LOQ DL

Acenaphthene 170 U M 330 83 ug/Kg 06/19/20 15:40 06/24/20 23:31 1

MB MB

Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier

170 U 85330 ug/Kg 06/19/20 15:40 06/24/20 23:31 1Acenaphthylene

170 U 86330 ug/Kg 06/19/20 15:40 06/24/20 23:31 1Anthracene

170 U 92330 ug/Kg 06/19/20 15:40 06/24/20 23:31 1Azobenzene

170 U M 92330 ug/Kg 06/19/20 15:40 06/24/20 23:31 1Benzo[a]anthracene

170 U 95330 ug/Kg 06/19/20 15:40 06/24/20 23:31 1Benzo[b]fluoranthene

170 U 110330 ug/Kg 06/19/20 15:40 06/24/20 23:31 1Benzo[k]fluoranthene

660 U 2901600 ug/Kg 06/19/20 15:40 06/24/20 23:31 1Benzoic acid

170 U 110330 ug/Kg 06/19/20 15:40 06/24/20 23:31 1Benzo[g,h,i]perylene

170 U 94330 ug/Kg 06/19/20 15:40 06/24/20 23:31 1Benzo[a]pyrene

370 U 170510 ug/Kg 06/19/20 15:40 06/24/20 23:31 1Benzyl alcohol

170 U 88330 ug/Kg 06/19/20 15:40 06/24/20 23:31 1Bis(2-chloroethoxy)methane

170 U 81330 ug/Kg 06/19/20 15:40 06/24/20 23:31 1Bis(2-chloroethyl)ether

170 U 79330 ug/Kg 06/19/20 15:40 06/24/20 23:31 12,2'-oxybis[1-chloropropane]

170 U M 98330 ug/Kg 06/19/20 15:40 06/24/20 23:31 1Bis(2-ethylhexyl) phthalate

170 U 85330 ug/Kg 06/19/20 15:40 06/24/20 23:31 14-Bromophenyl phenyl ether

170 U 95330 ug/Kg 06/19/20 15:40 06/24/20 23:31 1Butyl benzyl phthalate

170 U 95330 ug/Kg 06/19/20 15:40 06/24/20 23:31 1Carbazole

170 U 58330 ug/Kg 06/19/20 15:40 06/24/20 23:31 14-Chloroaniline

170 U 92330 ug/Kg 06/19/20 15:40 06/24/20 23:31 14-Chloro-3-methylphenol

170 U 88330 ug/Kg 06/19/20 15:40 06/24/20 23:31 12-Chlorophenol

170 U 81330 ug/Kg 06/19/20 15:40 06/24/20 23:31 12-Chloronaphthalene

170 U 93330 ug/Kg 06/19/20 15:40 06/24/20 23:31 14-Chlorophenyl phenyl ether

170 U M 84330 ug/Kg 06/19/20 15:40 06/24/20 23:31 1Chrysene

170 U 100330 ug/Kg 06/19/20 15:40 06/24/20 23:31 1Dibenz(a,h)anthracene

170 U 86330 ug/Kg 06/19/20 15:40 06/24/20 23:31 1Dibenzofuran

170 U 97330 ug/Kg 06/19/20 15:40 06/24/20 23:31 1Di-n-butyl phthalate

170 U 75330 ug/Kg 06/19/20 15:40 06/24/20 23:31 11,2-Dichlorobenzene

170 U 78330 ug/Kg 06/19/20 15:40 06/24/20 23:31 11,3-Dichlorobenzene

170 U 77330 ug/Kg 06/19/20 15:40 06/24/20 23:31 11,4-Dichlorobenzene

170 U 941600 ug/Kg 06/19/20 15:40 06/24/20 23:31 13,3'-Dichlorobenzidine

170 U 89330 ug/Kg 06/19/20 15:40 06/24/20 23:31 12,4-Dichlorophenol

Eurofins TestAmerica, Sacramento

Page 47 of 66 7/31/2020 (Rev. 1)

Project/Site: SACFA SREL 2

Method: 8270C - Semivolatile Organic Compounds (GC/MS) (Continued)

Client Sample ID: Method BlankLab Sample ID: MB 320-387837/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 389231 Prep Batch: 387837

LOQ DL

Diethyl phthalate 170 U 330 90 ug/Kg 06/19/20 15:40 06/24/20 23:31 1

MB MB

Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier

330 U 170500 ug/Kg 06/19/20 15:40 06/24/20 23:31 12,4-Dimethylphenol

170 U 87330 ug/Kg 06/19/20 15:40 06/24/20 23:31 1Dimethyl phthalate

330 U 812000 ug/Kg 06/19/20 15:40 06/24/20 23:31 14,6-Dinitro-2-methylphenol

330 U 2102000 ug/Kg 06/19/20 15:40 06/24/20 23:31 12,4-Dinitrophenol

170 U 89330 ug/Kg 06/19/20 15:40 06/24/20 23:31 12,4-Dinitrotoluene

170 U 99330 ug/Kg 06/19/20 15:40 06/24/20 23:31 12,6-Dinitrotoluene

170 U 97330 ug/Kg 06/19/20 15:40 06/24/20 23:31 1Di-n-octyl phthalate

170 U 95330 ug/Kg 06/19/20 15:40 06/24/20 23:31 1Fluoranthene

170 U 92330 ug/Kg 06/19/20 15:40 06/24/20 23:31 1Fluorene

170 U 89330 ug/Kg 06/19/20 15:40 06/24/20 23:31 1Hexachlorobenzene

170 U 82330 ug/Kg 06/19/20 15:40 06/24/20 23:31 1Hexachlorobutadiene

170 U 81330 ug/Kg 06/19/20 15:40 06/24/20 23:31 1Hexachloroethane

170 U 96330 ug/Kg 06/19/20 15:40 06/24/20 23:31 1Indeno[1,2,3-cd]pyrene

170 U 93330 ug/Kg 06/19/20 15:40 06/24/20 23:31 1Isophorone

170 U 85330 ug/Kg 06/19/20 15:40 06/24/20 23:31 12-Methylnaphthalene

170 U 58330 ug/Kg 06/19/20 15:40 06/24/20 23:31 12-Methylphenol

660 U 3301000 ug/Kg 06/19/20 15:40 06/24/20 23:31 13 & 4 Methylphenol

170 U 82330 ug/Kg 06/19/20 15:40 06/24/20 23:31 1Naphthalene

330 U 841600 ug/Kg 06/19/20 15:40 06/24/20 23:31 12-Nitroaniline

330 U 1701600 ug/Kg 06/19/20 15:40 06/24/20 23:31 13-Nitroaniline

170 U 881600 ug/Kg 06/19/20 15:40 06/24/20 23:31 14-Nitroaniline

170 U 76330 ug/Kg 06/19/20 15:40 06/24/20 23:31 1Nitrobenzene

170 U 82330 ug/Kg 06/19/20 15:40 06/24/20 23:31 12-Nitrophenol

330 U 2802000 ug/Kg 06/19/20 15:40 06/24/20 23:31 14-Nitrophenol

170 U 96330 ug/Kg 06/19/20 15:40 06/24/20 23:31 1N-Nitrosodimethylamine

170 U 86330 ug/Kg 06/19/20 15:40 06/24/20 23:31 1N-Nitrosodiphenylamine

170 U 84330 ug/Kg 06/19/20 15:40 06/24/20 23:31 1N-Nitrosodi-n-propylamine

170 U 511600 ug/Kg 06/19/20 15:40 06/24/20 23:31 1Pentachlorophenol

170 U 94330 ug/Kg 06/19/20 15:40 06/24/20 23:31 1Phenanthrene

170 U 83330 ug/Kg 06/19/20 15:40 06/24/20 23:31 1Phenol

170 U 94330 ug/Kg 06/19/20 15:40 06/24/20 23:31 1Pyrene

170 U 83330 ug/Kg 06/19/20 15:40 06/24/20 23:31 11,2,4-Trichlorobenzene

170 U 83330 ug/Kg 06/19/20 15:40 06/24/20 23:31 12,4,5-Trichlorophenol

170 U 84330 ug/Kg 06/19/20 15:40 06/24/20 23:31 12,4,6-Trichlorophenol

2,4,6-Tribromophenol (Surr) 79 39 - 132 06/24/20 23:31 1

MB MB

Surrogate

06/19/20 15:40

Dil FacPrepared AnalyzedQualifier Limits%Recovery

92 06/19/20 15:40 06/24/20 23:31 12-Fluorobiphenyl (Surr) 44 - 115

89 06/19/20 15:40 06/24/20 23:31 12-Fluorophenol (Surr) 35 - 115

84 06/19/20 15:40 06/24/20 23:31 1Nitrobenzene-d5 (Surr) 37 - 122

91 06/19/20 15:40 06/24/20 23:31 1Phenol-d5 (Surr) 33 - 122

103 06/19/20 15:40 06/24/20 23:31 1Terphenyl-d14 (Surr) 54 - 127

Eurofins TestAmerica, Sacramento

Page 48 of 66 7/31/2020 (Rev. 1)

Project/Site: SACFA SREL 2

Method: 8270C - Semivolatile Organic Compounds (GC/MS) (Continued)

Client Sample ID: Lab Control SampleLab Sample ID: LCS 320-387837/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 389231 Prep Batch: 387837

Acenaphthene 3330 2840 ug/Kg 85 40 - 123

Analyte

LCS LCS

DUnitResult Qualifier %Rec

Spike

Added

%Rec.

Limits

Acenaphthylene 3330 2910 ug/Kg 87 32 - 132

Anthracene 3330 3030 ug/Kg 91 47 - 123

Azobenzene 3330 3000 ug/Kg 90 39 - 125

Benzo[a]anthracene 3330 3100 ug/Kg 93 49 - 126

Benzo[b]fluoranthene 3330 3190 ug/Kg 96 45 - 132

Benzo[k]fluoranthene 3330 3140 ug/Kg 94 47 - 132

Benzoic acid 6670 4650 ug/Kg 70 10 - 97

Benzo[g,h,i]perylene 3330 3160 ug/Kg 95 43 - 134

Benzo[a]pyrene 3330 3220 ug/Kg 97 45 - 129

Benzyl alcohol 3330 2690 ug/Kg 81 29 - 122

Bis(2-chloroethoxy)methane 3330 2610 ug/Kg 78 36 - 121

Bis(2-chloroethyl)ether 3330 2540 ug/Kg 76 31 - 120

2,2'-oxybis[1-chloropropane] 3330 2250 ug/Kg 68 33 - 131

Bis(2-ethylhexyl) phthalate 3330 3050 ug/Kg 92 51 - 133

4-Bromophenyl phenyl ether 3330 3100 ug/Kg 93 46 - 124

Butyl benzyl phthalate 3330 3090 ug/Kg 93 48 - 132

Carbazole 3330 3080 ug/Kg 93 50 - 123

4-Chloroaniline 3330 1740 ug/Kg 52 17 - 106

4-Chloro-3-methylphenol 3330 3030 ug/Kg 91 45 - 122

2-Chlorophenol 3330 2620 ug/Kg 79 34 - 121

2-Chloronaphthalene 3330 2760 ug/Kg 83 41 - 114

4-Chlorophenyl phenyl ether 3330 2880 ug/Kg 86 45 - 121

Chrysene 3330 3070 ug/Kg 92 50 - 124

Dibenz(a,h)anthracene 3330 3250 ug/Kg 97 45 - 134

Dibenzofuran 3330 2840 ug/Kg 85 44 - 120

Di-n-butyl phthalate 3330 3160 ug/Kg 95 51 - 128

1,2-Dichlorobenzene 3330 2480 ug/Kg 74 33 - 117

1,3-Dichlorobenzene 3330 2470 ug/Kg 74 30 - 115

1,4-Dichlorobenzene 3330 2500 ug/Kg 75 31 - 115

3,3'-Dichlorobenzidine 3330 2380 ug/Kg 72 22 - 121

2,4-Dichlorophenol 3330 2850 ug/Kg 85 40 - 122

Diethyl phthalate 3330 3070 ug/Kg 92 50 - 124

Dimethyl phthalate 3330 2970 ug/Kg 89 48 - 124

4,6-Dinitro-2-methylphenol 6670 5170 ug/Kg 78 29 - 132

2,4-Dinitrophenol 6670 3430 ug/Kg 51 10 - 60

2,4-Dinitrotoluene 3330 3140 ug/Kg 94 48 - 126

2,6-Dinitrotoluene 3330 3070 ug/Kg 92 46 - 124

Di-n-octyl phthalate 3330 3020 ug/Kg 91 45 - 140

Fluoranthene 3330 3120 ug/Kg 94 50 - 127

Fluorene 3330 2890 ug/Kg 87 43 - 125

Hexachlorobenzene 3330 3100 ug/Kg 93 45 - 122

Hexachlorobutadiene 3330 2700 ug/Kg 81 32 - 123

Hexachloroethane 3330 2560 ug/Kg 77 28 - 117

Indeno[1,2,3-cd]pyrene 3330 3290 ug/Kg 99 45 - 133

Isophorone 3330 2720 ug/Kg 82 30 - 122

2-Methylnaphthalene 3330 2700 ug/Kg 81 38 - 122

2-Methylphenol 3330 2610 ug/Kg 78 32 - 122

Eurofins TestAmerica, Sacramento

Page 49 of 66 7/31/2020 (Rev. 1)

Project/Site: SACFA SREL 2

Method: 8270C - Semivolatile Organic Compounds (GC/MS) (Continued)

Client Sample ID: Lab Control SampleLab Sample ID: LCS 320-387837/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 389231 Prep Batch: 387837

3 & 4 Methylphenol 3330 2640 ug/Kg 79 34 - 119

Analyte

LCS LCS

DUnitResult Qualifier %Rec

Spike

Added

%Rec.

Limits

Naphthalene 3330 2620 ug/Kg 79 35 - 123

2-Nitroaniline 3330 3130 ug/Kg 94 44 - 127

3-Nitroaniline 3330 2150 ug/Kg 65 33 - 119

4-Nitroaniline 3330 2950 ug/Kg 88 63 - 109

Nitrobenzene 3330 2650 ug/Kg 80 34 - 122

2-Nitrophenol 3330 2810 ug/Kg 84 36 - 123

4-Nitrophenol 6670 6610 ug/Kg 99 30 - 132

N-Nitrosodimethylamine 3330 2350 ug/Kg 71 23 - 120

N-Nitrosodiphenylamine 3330 3040 ug/Kg 91 38 - 127

N-Nitrosodi-n-propylamine 3330 2720 ug/Kg 82 36 - 120

Pentachlorophenol 6670 6800 ug/Kg 102 25 - 133

Phenanthrene 3330 3030 ug/Kg 91 50 - 121

Phenol 3330 2610 ug/Kg 78 34 - 121

Pyrene 3330 3180 ug/Kg 95 47 - 127

1,2,4-Trichlorobenzene 3330 2610 ug/Kg 78 34 - 118

2,4,5-Trichlorophenol 3330 3020 ug/Kg 91 41 - 124

2,4,6-Trichlorophenol 3330 3020 ug/Kg 91 39 - 126

2,4,6-Tribromophenol (Surr) 39 - 132

Surrogate

LCS LCS

Qualifier Limits%Recovery

902-Fluorobiphenyl (Surr) 44 - 115

812-Fluorophenol (Surr) 35 - 115

88Nitrobenzene-d5 (Surr) 37 - 122

85Phenol-d5 (Surr) 33 - 122

101Terphenyl-d14 (Surr) 54 - 127

Method: 8015B DRO - Diesel Range Organics (DRO) (GC)

Client Sample ID: Method BlankLab Sample ID: MB 320-388341/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 388555 Prep Batch: 388341

LOQ DL

Diesel Range Organics [C10-C28] 1.0 U 2.0 0.50 mg/Kg 06/22/20 12:26 06/23/20 10:15 1

MB MB

Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier

10 U 3.820 mg/Kg 06/22/20 12:26 06/23/20 10:15 1Motor Oil Range Organics [C28-C40] o-Terphenyl (Surr) 88 M 45 - 130 06/23/20 10:15 1

MB MB

Surrogate

06/22/20 12:26

Dil FacPrepared AnalyzedQualifier Limits%Recovery

Client Sample ID: Lab Control SampleLab Sample ID: LCS 320-388341/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 388555 Prep Batch: 388341

Diesel Range Organics

[C10-C28]

10.0 10.5 mg/Kg 105 38 - 132

Analyte

LCS LCS

DUnitResult Qualifier %Rec

Spike

Added

%Rec.

Limits

Motor Oil Range Organics

[C28-C40]

30.0 30.7 mg/Kg 102 39 - 106

Eurofins TestAmerica, Sacramento

Page 50 of 66 7/31/2020 (Rev. 1)

Project/Site: SACFA SREL 2

Method: 8015B DRO - Diesel Range Organics (DRO) (GC) (Continued) o-Terphenyl (Surr) 45 - 130

Surrogate

LCS LCS

Qualifier Limits%Recovery

Client Sample ID: KS-SR20-997S-compositeLab Sample ID: 320-61753-17 MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 389449 Prep Batch: 388341

Diesel Range Organics

[C10-C28]

19 Q 11.1 23.1 mg/Kg 41 38 - 132☼

Analyte

MS MS

DUnitResult Qualifier %Rec

Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Motor Oil Range Organics

[C28-C40]

120 Q J1 33.3 87.1 J1 mg/Kg -102 39 - 106☼ o-Terphenyl (Surr) 45 - 130

Surrogate

MS MS

Qualifier Limits%Recovery

Client Sample ID: KS-SR20-997S-compositeLab Sample ID: 320-61753-17 MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 389449 Prep Batch: 388341

Diesel Range Organics

[C10-C28]

19 Q 11.3 27.1 mg/Kg 76 38 - 132 16 30☼

Analyte

MSD MSD

DUnitResult Qualifier %Rec

Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD

Motor Oil Range Organics

[C28-C40]

120 Q J1 33.8 116 J1 mg/Kg -14 39 - 106 29 30☼ o-Terphenyl (Surr) 45 - 130

Surrogate

MSD MSD

Qualifier Limits%Recovery

Method: 6010B - Metals (ICP)

Client Sample ID: Method BlankLab Sample ID: MB 320-386746/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 387635 Prep Batch: 386746

LOQ DL

Antimony 2.0 U 3.0 0.94 mg/Kg 06/16/20 12:53 06/18/20 14:05 1

MB MB

Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier

3.0 U 1.34.0 mg/Kg 06/16/20 12:53 06/18/20 14:05 1Arsenic

0.50 U 0.202.0 mg/Kg 06/16/20 12:53 06/18/20 14:05 1Barium

0.10 U 0.0300.30 mg/Kg 06/16/20 12:53 06/18/20 14:05 1Beryllium

0.10 U 0.0300.30 mg/Kg 06/16/20 12:53 06/18/20 14:05 1Cadmium

0.50 U 0.141.0 mg/Kg 06/16/20 12:53 06/18/20 14:05 1Chromium

0.75 U 0.251.0 mg/Kg 06/16/20 12:53 06/18/20 14:05 1Cobalt

0.50 U 0.221.5 mg/Kg 06/16/20 12:53 06/18/20 14:05 1Copper

0.279 J 0.261.0 mg/Kg 06/16/20 12:53 06/18/20 14:05 1Lead

1.5 U 0.752.0 mg/Kg 06/16/20 12:53 06/18/20 14:05 1Molybdenum

0.50 U 0.241.0 mg/Kg 06/16/20 12:53 06/18/20 14:05 1Nickel

3.0 U 1.44.0 mg/Kg 06/16/20 12:53 06/18/20 14:05 1Selenium

0.20 U 0.0900.50 mg/Kg 06/16/20 12:53 06/18/20 14:05 1Silver

1.0 U 0.843.0 mg/Kg 06/16/20 12:53 06/18/20 14:05 1Thallium

0.50 U 0.192.0 mg/Kg 06/16/20 12:53 06/18/20 14:05 1Vanadium

1.0 U 0.402.0 mg/Kg 06/16/20 12:53 06/18/20 14:05 1Zinc

Eurofins TestAmerica, Sacramento

Page 51 of 66 7/31/2020 (Rev. 1)

Project/Site: SACFA SREL 2

Method: 6010B - Metals (ICP) (Continued)

Client Sample ID: Lab Control SampleLab Sample ID: LCS 320-386746/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 387635 Prep Batch: 386746

Antimony 49.8 44.6 mg/Kg 90 79 - 114

Analyte

LCS LCS

DUnitResult Qualifier %Rec

Spike

Added

%Rec.

Limits

Arsenic 50.0 44.2 mg/Kg 88 82 - 111

Barium 50.0 47.7 mg/Kg 95 83 - 113

Beryllium 25.0 24.0 mg/Kg 96 83 - 113

Cadmium 25.0 23.5 mg/Kg 94 82 - 113

Chromium 25.0 24.1 mg/Kg 96 85 - 113

Cobalt 25.0 23.9 mg/Kg 96 85 - 112

Copper 25.0 23.5 mg/Kg 94 81 - 117

Lead 25.0 23.9 mg/Kg 96 81 - 112

Molybdenum 25.0 23.6 mg/Kg 94 82 - 116

Nickel 25.0 23.4 mg/Kg 94 83 - 113

Selenium 50.0 43.2 mg/Kg 86 78 - 111

Silver 4.98 4.68 mg/Kg 94 82 - 112

Thallium 50.0 47.4 mg/Kg 95 83 - 111

Vanadium 25.0 23.9 mg/Kg 96 82 - 114

Zinc 50.3 47.5 mg/Kg 95 82 - 113

Method: 7471A - Mercury (CVAA)

Client Sample ID: Method BlankLab Sample ID: MB 320-386697/11-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 387110 Prep Batch: 386697

LOQ DL

Mercury 0.025 U 0.040 0.0086 mg/Kg 06/16/20 12:00 06/17/20 09:18 1

MB MB

Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier

Client Sample ID: Lab Control SampleLab Sample ID: LCS 320-386697/12-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 387110 Prep Batch: 386697

Mercury 0.167 0.163 mg/Kg 97 80 - 124

Analyte

LCS LCS

DUnitResult Qualifier %Rec

Spike

Added

%Rec.

Limits

Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 320-386697/13-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 387110 Prep Batch: 386697

Mercury 0.167 0.170 mg/Kg 102 80 - 124 5 20

Analyte

LCSD LCSD

DUnitResult Qualifier %Rec

Spike

Added

%Rec.

Limits LimitRPD

RPD

Method: D 2216 - Percent Moisture

Client Sample ID: KS-SR20-997S-compositeLab Sample ID: 320-61753-17 DU Matrix: Solid Prep Type: Total/NA Analysis Batch: 386594

Percent Moisture 11.5 12.2 % 6 20

Analyte

DU DU

DUnitResult Qualifier

Sample

Result

Sample

Qualifier LimitRPD

RPD

Percent Solids 88.5 87.8 % 0.8 20

Eurofins TestAmerica, Sacramento

Page 52 of 66 7/31/2020 (Rev. 1)

QC Association Summary

Project/Site: SACFA SREL 2

GC/MS VOA

Prep Batch: 386412

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Solid 5035320-61753-11 KS-SR20-002S-22' Total/NA

Solid 5035MB 320-386412/1-A Method Blank Total/NA

Solid 5035LCS 320-386412/2-A Lab Control Sample Total/NA

Solid 5035LCSD 320-386412/3-A Lab Control Sample Dup Total/NA

Prep Batch: 386417

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Solid 5035320-61753-6 - RA KS-SR20-997S-99 Total/NA

Solid 5035320-61753-6 KS-SR20-997S-99 Total/NA

Solid 5035320-61753-11 KS-SR20-002S-22' Total/NA

Solid 5035320-61753-16 KS-SR20-003S-21' Total/NA

Analysis Batch: 386681

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Water 8260/CALUFT

DOD

320-61753-1 Trip Blank Total/NA

Water 8260/CALUFT

DOD

MB 320-386681/9 Method Blank Total/NA

Water 8260/CALUFT

DOD

LCS 320-386681/7 Lab Control Sample Total/NA

Water 8260/CALUFT

DOD

LCSD 320-386681/8 Lab Control Sample Dup Total/NA

Analysis Batch: 386683

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Water 8260B320-61753-1 Trip Blank Total/NA

Water 8260BMB 320-386683/9 Method Blank Total/NA

Water 8260BLCS 320-386683/5 Lab Control Sample Total/NA

Water 8260BLCSD 320-386683/6 Lab Control Sample Dup Total/NA

Analysis Batch: 387614

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Solid 8260/CALUFT

DOD

386417320-61753-6 KS-SR20-997S-99 Total/NA

Solid 8260/CALUFT

DOD

386417320-61753-11 KS-SR20-002S-22' Total/NA

Solid 8260/CALUFT

DOD

386417320-61753-16 KS-SR20-003S-21' Total/NA

Solid 8260/CALUFT

DOD

MB 320-387614/10 Method Blank Total/NA

Solid 8260/CALUFT

DOD

LCS 320-387614/8 Lab Control Sample Total/NA

Solid 8260/CALUFT

DOD

LCSD 320-387614/9 Lab Control Sample Dup Total/NA

Analysis Batch: 387615

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Solid 8260B 386417320-61753-6 KS-SR20-997S-99 Total/NA

Solid 8260B 386417320-61753-16 KS-SR20-003S-21' Total/NA

Solid 8260BMB 320-387615/10 Method Blank Total/NA

Solid 8260BLCS 320-387615/3 Lab Control Sample Total/NA

Solid 8260BLCSD 320-387615/4 Lab Control Sample Dup Total/NA

Eurofins TestAmerica, Sacramento

Page 53 of 66 7/31/2020 (Rev. 1)

Project/Site: SACFA SREL 2

GC/MS VOA

Analysis Batch: 388939

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Solid 8260B 386417320-61753-6 - RA KS-SR20-997S-99 Total/NA

Solid 8260BMB 320-388939/10 Method Blank Total/NA

Solid 8260BLCS 320-388939/7 Lab Control Sample Total/NA

Solid 8260BLCSD 320-388939/8 Lab Control Sample Dup Total/NA

Analysis Batch: 389328

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Solid 8260B 386412320-61753-11 KS-SR20-002S-22' Total/NA

Analysis Batch: 391198

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Solid 8260B 386412MB 320-386412/1-A Method Blank Total/NA

Solid 8260B 386412LCS 320-386412/2-A Lab Control Sample Total/NA

Solid 8260B 386412LCSD 320-386412/3-A Lab Control Sample Dup Total/NA

GC/MS Semi VOA

Prep Batch: 387837

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Solid 3550B320-61753-17 KS-SR20-997S-composite Total/NA

Solid 3550B320-61753-18 KS-SR20-002S-composite Total/NA

Solid 3550B320-61753-19 KS-SR20-003S-composite Total/NA

Solid 3550BMB 320-387837/1-A Method Blank Total/NA

Solid 3550BLCS 320-387837/2-A Lab Control Sample Total/NA

Analysis Batch: 389231

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Solid 8270C 387837320-61753-17 KS-SR20-997S-composite Total/NA

Solid 8270C 387837MB 320-387837/1-A Method Blank Total/NA

Solid 8270C 387837LCS 320-387837/2-A Lab Control Sample Total/NA

Analysis Batch: 389401

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Solid 8270C 387837320-61753-18 KS-SR20-002S-composite Total/NA

Solid 8270C 387837320-61753-19 KS-SR20-003S-composite Total/NA

GC Semi VOA

Prep Batch: 388341

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Solid 3550B320-61753-17 KS-SR20-997S-composite Total/NA

Solid 3550B320-61753-18 KS-SR20-002S-composite Total/NA

Solid 3550B320-61753-19 KS-SR20-003S-composite Total/NA

Solid 3550BMB 320-388341/1-A Method Blank Total/NA

Solid 3550BLCS 320-388341/2-A Lab Control Sample Total/NA

Solid 3550B320-61753-17 MS KS-SR20-997S-composite Total/NA

Solid 3550B320-61753-17 MSD KS-SR20-997S-composite Total/NA

Analysis Batch: 388555

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Solid 8015B DRO 388341MB 320-388341/1-A Method Blank Total/NA

Solid 8015B DRO 388341LCS 320-388341/2-A Lab Control Sample Total/NA

Eurofins TestAmerica, Sacramento

Page 54 of 66 7/31/2020 (Rev. 1)

Project/Site: SACFA SREL 2

GC Semi VOA

Analysis Batch: 389449

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Solid 8015B DRO 388341320-61753-17 KS-SR20-997S-composite Total/NA

Solid 8015B DRO 388341320-61753-18 KS-SR20-002S-composite Total/NA

Solid 8015B DRO 388341320-61753-19 KS-SR20-003S-composite Total/NA

Solid 8015B DRO 388341320-61753-17 MS KS-SR20-997S-composite Total/NA

Solid 8015B DRO 388341320-61753-17 MSD KS-SR20-997S-composite Total/NA

Metals

Prep Batch: 386697

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Solid 7471A320-61753-17 KS-SR20-997S-composite Total/NA

Solid 7471A320-61753-18 KS-SR20-002S-composite Total/NA

Solid 7471A320-61753-19 KS-SR20-003S-composite Total/NA

Solid 7471AMB 320-386697/11-A Method Blank Total/NA

Solid 7471ALCS 320-386697/12-A Lab Control Sample Total/NA

Solid 7471ALCSD 320-386697/13-A Lab Control Sample Dup Total/NA

Prep Batch: 386746

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Solid 3050B320-61753-17 KS-SR20-997S-composite Total/NA

Solid 3050B320-61753-18 KS-SR20-002S-composite Total/NA

Solid 3050B320-61753-19 KS-SR20-003S-composite Total/NA

Solid 3050BMB 320-386746/1-A Method Blank Total/NA

Solid 3050BLCS 320-386746/2-A Lab Control Sample Total/NA

Analysis Batch: 387110

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Solid 7471A 386697320-61753-17 KS-SR20-997S-composite Total/NA

Solid 7471A 386697320-61753-18 KS-SR20-002S-composite Total/NA

Solid 7471A 386697320-61753-19 KS-SR20-003S-composite Total/NA

Solid 7471A 386697MB 320-386697/11-A Method Blank Total/NA

Solid 7471A 386697LCS 320-386697/12-A Lab Control Sample Total/NA

Solid 7471A 386697LCSD 320-386697/13-A Lab Control Sample Dup Total/NA

Analysis Batch: 387635

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Solid 6010B 386746320-61753-17 KS-SR20-997S-composite Total/NA

Solid 6010B 386746320-61753-18 KS-SR20-002S-composite Total/NA

Solid 6010B 386746320-61753-19 KS-SR20-003S-composite Total/NA

Solid 6010B 386746MB 320-386746/1-A Method Blank Total/NA

Solid 6010B 386746LCS 320-386746/2-A Lab Control Sample Total/NA

General Chemistry

Analysis Batch: 386594

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Solid D 2216320-61753-17 KS-SR20-997S-composite Total/NA

Solid D 2216320-61753-18 KS-SR20-002S-composite Total/NA

Solid D 2216320-61753-19 KS-SR20-003S-composite Total/NA

Solid D 2216320-61753-17 DU KS-SR20-997S-composite Total/NA

Eurofins TestAmerica, Sacramento

Page 55 of 66 7/31/2020 (Rev. 1)

Project/Site: SACFA SREL 2

General Chemistry

Analysis Batch: 387123

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Solid D 2216320-61753-6 KS-SR20-997S-99 Total/NA

Solid D 2216320-61753-11 KS-SR20-002S-22' Total/NA

Solid D 2216320-61753-16 KS-SR20-003S-21' Total/NA

Eurofins TestAmerica, Sacramento

Page 56 of 66 7/31/2020 (Rev. 1)

Lab Chronicle Client: Kleinfelder Inc Job ID: 320-61753-1 Project/Site: SACFA SREL 2

Client Sample ID: Trip Blank Lab Sample ID: 320-61753-1 Matrix: WaterDate Collected: 06/12/20 00:00

Date Received: 06/12/20 14:55

Analysis 8260/CALUFT

DOD

SS06/16/20 19:151 TAL SAC386681

Type

Batch

Method

Batch

Prep Type LabAnalystRun

Prepared or Analyzed

Initial

Amount Amount

Final Batch

NumberFactor

Dil

Total/NA 50 mL 50 mL

Analysis 8260B 1 386683 06/16/20 19:15 EMJ TAL SACTotal/NA 50 mL 50 mL

Client Sample ID: KS-SR20-997S-99 Lab Sample ID: 320-61753-6 Matrix: SolidDate Collected: 06/12/20 00:00

Date Received: 06/12/20 14:55

Analysis D 2216 TCS06/17/20 13:091 TAL SAC387123

Type

Batch

Method

Batch

Prep Type LabAnalystRun

Prepared or Analyzed

Initial

Amount Amount

Final Batch

NumberFactor

Dil

Total/NA

Client Sample ID: KS-SR20-997S-99 Lab Sample ID: 320-61753-6 Matrix: SolidDate Collected: 06/12/20 00:00

Percent Solids: 85.3Date Received: 06/12/20 14:55

Prep 5035 EMJ06/12/20 14:55 TAL SAC386417

Type

Batch

Method

Batch

Prep Type LabAnalystRun

Prepared or Analyzed

Initial

Amount Amount

Final Batch

NumberFactor

Dil

Total/NA 6.223 g 5 mL

Analysis 8260/CALUFT

DOD

1 387614 06/19/20 12:00 SS TAL SACTotal/NA 5 mL 5 mL

Prep 5035 386417 06/12/20 14:55 EMJ TAL SACTotal/NA 6.223 g 5 mL

Analysis 8260B 1 387615 06/19/20 12:00 SS TAL SACTotal/NA 5 mL 5 mL

Prep 5035 RA 386417 06/12/20 14:55 EMJ TAL SACTotal/NA 6.121 g 5 mL

Analysis 8260B RA 1 388939 06/24/20 15:23 AZ1 TAL SACTotal/NA 5 mL 5 mL

Client Sample ID: KS-SR20-002S-22' Lab Sample ID: 320-61753-11 Matrix: SolidDate Collected: 06/12/20 09:56

Date Received: 06/12/20 14:55

Analysis D 2216 TCS06/17/20 13:091 TAL SAC387123

Type

Batch

Method

Batch

Prep Type LabAnalystRun

Prepared or Analyzed

Initial

Amount Amount

Final Batch

NumberFactor

Dil

Total/NA

Client Sample ID: KS-SR20-002S-22' Lab Sample ID: 320-61753-11 Matrix: SolidDate Collected: 06/12/20 09:56

Percent Solids: 84.9Date Received: 06/12/20 14:55

Prep 5035 EMJ06/12/20 14:55 TAL SAC386417

Type

Batch

Method

Batch

Prep Type LabAnalystRun

Prepared or Analyzed

Initial

Amount Amount

Final Batch

NumberFactor

Dil

Total/NA 5.846 g 5 mL

Analysis 8260/CALUFT

DOD

1 387614 06/19/20 12:23 SS TAL SACTotal/NA 5 mL 5 mL

Prep 5035 386412 06/15/20 10:01 EMJ TAL SACTotal/NA 5.602 g 10 mL

Analysis 8260B 4 389328 06/25/20 20:55 BAJ TAL SACTotal/NA 1 mL 50 mL

Eurofins TestAmerica, Sacramento

Page 57 of 66 7/31/2020 (Rev. 1)

Project/Site: SACFA SREL 2

Client Sample ID: KS-SR20-003S-21' Lab Sample ID: 320-61753-16 Matrix: SolidDate Collected: 06/12/20 13:00

Date Received: 06/12/20 14:55

Analysis D 2216 TCS06/17/20 13:091 TAL SAC387123

Type

Batch

Method

Batch

Prep Type LabAnalystRun

Prepared or Analyzed

Initial

Amount Amount

Final Batch

NumberFactor

Dil

Total/NA

Client Sample ID: KS-SR20-003S-21' Lab Sample ID: 320-61753-16 Matrix: SolidDate Collected: 06/12/20 13:00

Percent Solids: 82.8Date Received: 06/12/20 14:55

Prep 5035 EMJ06/12/20 14:55 TAL SAC386417

Type

Batch

Method

Batch

Prep Type LabAnalystRun

Prepared or Analyzed

Initial

Amount Amount

Final Batch

NumberFactor

Dil

Total/NA 6.102 g 5 mL

Analysis 8260/CALUFT

DOD

1 387614 06/19/20 12:46 SS TAL SACTotal/NA 5 mL 5 mL

Prep 5035 386417 06/12/20 14:55 EMJ TAL SACTotal/NA 5.986 g 5 mL

Analysis 8260B 1 387615 06/19/20 16:07 SS TAL SACTotal/NA 5 mL 5 mL

Client Sample ID: KS-SR20-997S-composite Lab Sample ID: 320-61753-17 Matrix: SolidDate Collected: 06/12/20 00:00

Date Received: 06/12/20 14:55

Analysis D 2216 HB06/15/20 16:481 TAL SAC386594

Type

Batch

Method

Batch

Prep Type LabAnalystRun

Prepared or Analyzed

Initial

Amount Amount

Final Batch

NumberFactor

Dil

Total/NA

Client Sample ID: KS-SR20-997S-composite Lab Sample ID: 320-61753-17 Matrix: SolidDate Collected: 06/12/20 00:00

Percent Solids: 88.5Date Received: 06/12/20 14:55

Prep 3550B EDC06/19/20 15:40 TAL SAC387837

Type

Batch

Method

Batch

Prep Type LabAnalystRun

Prepared or Analyzed

Initial

Amount Amount

Final Batch

NumberFactor

Dil

Total/NA 30.25 g 1 mL

Analysis 8270C 20 389231 06/25/20 04:07 Y1S TAL SACTotal/NA

Prep 3550B 388341 06/22/20 12:26 EDC TAL SACTotal/NA 30.67 g 3 mL

Analysis 8015B DRO 1 389449 06/25/20 14:08 K1D TAL SACTotal/NA

Prep 3050B 386746 06/16/20 12:53 JP TAL SACTotal/NA 1.04 g 100 mL

Analysis 6010B 1 387635 06/18/20 16:53 SP TAL SACTotal/NA

Prep 7471A 386697 06/16/20 12:00 IM TAL SACTotal/NA 0.58 g 50 mL

Analysis 7471A 1 387110 06/17/20 10:40 IM TAL SACTotal/NA

Client Sample ID: KS-SR20-002S-composite Lab Sample ID: 320-61753-18 Matrix: SolidDate Collected: 06/12/20 09:51

Date Received: 06/12/20 14:55

Analysis D 2216 HB06/15/20 16:481 TAL SAC386594

Type

Batch

Method

Batch

Prep Type LabAnalystRun

Prepared or Analyzed

Initial

Amount Amount

Final Batch

NumberFactor

Dil

Total/NA

Eurofins TestAmerica, Sacramento

Page 58 of 66 7/31/2020 (Rev. 1)

Project/Site: SACFA SREL 2

Client Sample ID: KS-SR20-002S-composite Lab Sample ID: 320-61753-18 Matrix: SolidDate Collected: 06/12/20 09:51

Percent Solids: 85.6Date Received: 06/12/20 14:55

Prep 3550B EDC06/19/20 15:40 TAL SAC387837

Type

Batch

Method

Batch

Prep Type LabAnalystRun

Prepared or Analyzed

Initial

Amount Amount

Final Batch

NumberFactor

Dil

Total/NA 30.73 g 1 mL

Analysis 8270C 50 389401 06/25/20 12:53 Y1S TAL SACTotal/NA

Prep 3550B 388341 06/22/20 12:26 EDC TAL SACTotal/NA 30.04 g 3 mL

Analysis 8015B DRO 1 389449 06/25/20 15:40 K1D TAL SACTotal/NA

Prep 3050B 386746 06/16/20 12:53 JP TAL SACTotal/NA 1.01 g 100 mL

Analysis 6010B 1 387635 06/18/20 16:57 SP TAL SACTotal/NA

Prep 7471A 386697 06/16/20 12:00 IM TAL SACTotal/NA 0.65 g 50 mL

Analysis 7471A 1 387110 06/17/20 10:42 IM TAL SACTotal/NA

Client Sample ID: KS-SR20-003S-composite Lab Sample ID: 320-61753-19 Matrix: SolidDate Collected: 06/12/20 12:53

Date Received: 06/12/20 14:55

Analysis D 2216 HB06/15/20 16:481 TAL SAC386594

Type

Batch

Method

Batch

Prep Type LabAnalystRun

Prepared or Analyzed

Initial

Amount Amount

Final Batch

NumberFactor

Dil

Total/NA

Client Sample ID: KS-SR20-003S-composite Lab Sample ID: 320-61753-19 Matrix: SolidDate Collected: 06/12/20 12:53

Percent Solids: 87.7Date Received: 06/12/20 14:55

Prep 3550B EDC06/19/20 15:40 TAL SAC387837

Type

Batch

Method

Batch

Prep Type LabAnalystRun

Prepared or Analyzed

Initial

Amount Amount

Final Batch

NumberFactor

Dil

Total/NA 30.91 g 1 mL

Analysis 8270C 20 389401 06/25/20 13:21 Y1S TAL SACTotal/NA

Prep 3550B 388341 06/22/20 12:26 EDC TAL SACTotal/NA 30.35 g 3 mL

Analysis 8015B DRO 1 389449 06/25/20 16:11 K1D TAL SACTotal/NA

Prep 3050B 386746 06/16/20 12:53 JP TAL SACTotal/NA 0.97 g 100 mL

Analysis 6010B 1 387635 06/18/20 17:01 SP TAL SACTotal/NA

Prep 7471A 386697 06/16/20 12:00 IM TAL SACTotal/NA 0.56 g 50 mL

Analysis 7471A 1 387110 06/17/20 10:45 IM TAL SACTotal/NA

Laboratory References:

TAL SAC = Eurofins TestAmerica, Sacramento, 880 Riverside Parkway, West Sacramento, CA 95605, TEL (916)373-5600

Eurofins TestAmerica, Sacramento

Page 59 of 66 7/31/2020 (Rev. 1)

Accreditation/Certification Summary

Project/Site: SACFA SREL 2

Laboratory: Eurofins TestAmerica, Sacramento Unless otherwise noted, all analytes for this laboratory were covered under each accreditation/certification below.

Authority Program Identification Number Expiration Date

ANAB L2468Dept. of Defense ELAP 01-20-21

The following analytes are included in this report, but the laboratory is not certified by the governing authority. This list may include analytes for which the agency does not offer certification.

Analysis Method Prep Method Matrix Analyte

D 2216 Solid Percent Moisture

D 2216 Solid Percent Solids

California State 2897 01-31-22

The following analytes are included in this report, but the laboratory is not certified by the governing authority. This list may include analytes for which the agency does not offer certification.

Analysis Method Prep Method Matrix Analyte

8015B DRO 3550B Solid Motor Oil Range Organics [C28-C40]

D 2216 Solid Percent Moisture

D 2216 Solid Percent Solids

Oregon NELAP 4040 01-29-21

The following analytes are included in this report, but the laboratory is not certified by the governing authority. This list may include analytes for which the agency does not offer certification.

Analysis Method Prep Method Matrix Analyte

D 2216 Solid Percent Moisture

D 2216 Solid Percent Solids

Eurofins TestAmerica, Sacramento

Page 60 of 66 7/31/2020 (Rev. 1)

Method Summary

Project/Site: SACFA SREL 2

Method Method Description LaboratoryProtocol

SW8468260/CALUFT

DOD

Volatile Organic Compounds by GC/MS TAL SAC

SW8468260B Volatile Organic Compounds (GC/MS) TAL SAC

SW8468270C Semivolatile Organic Compounds (GC/MS) TAL SAC

SW8468015B DRO Diesel Range Organics (DRO) (GC) TAL SAC

SW8466010B Metals (ICP) TAL SAC

SW8467471A Mercury (CVAA) TAL SAC

ASTMD 2216 Percent Moisture TAL SAC

SW8463050B Preparation, Metals TAL SAC

SW8463550B Ultrasonic Extraction TAL SAC

SW8465030B Purge and Trap…

This is the start of the file's text. The full file is on GovTribe.

File details come from the government source that posted it. Updated Oct 30, 2020.