J152563-1 Std_Tal_L4 Final Report_Part6.pdf

Sample Report

4/21/2023 11:14 AM

Name Mass ISTD Tune Mode Conc. Conc. RSD CPS LDR QC Flag

Sn 118 115 He 0.189 8.5 328.897 5400

Sb 121 115 He 0.052 8.5 63.333 5400

(Sb) 123 115 He 0.053 58.6 57.780 5400

Ba 137 115 He 1.427 13.9 378.673 11250

(Tl) 203 209 He 0.044 47.9 123.333 9000

Tl 205 209 He 0.026 62.4 248.897 9000

[Pb] 206 209 He 0.412 24.3 467.790 11250

[Pb] 207 209 He 0.413 1.9 412.230 11250

Pb 208 209 He 0.413 7.6 1861.173 11250

Th 232 209 He 0.100 10.6 542.237 4500

U 238 209 He 0.076 4.9 268.893 4500

QC ISTD Table

Name Mass Tune Mode CPS CPS RSD Ref CPS % Rec %QC Low %QC High QC Flag

Li (IS) 6 No Gas 179083.913 0.7 190968.166666667 93.78 30 150

Sc (IS) 45 No Gas 1283682.453 1.0 1216826.10333333 105.49 30 150

Rh (IS) 103 No Gas 2182307.103 1.0 2070097.26 105.42 30 150

Sc (IS) 45 H2 369962.303 0.8 330192.953333333 112.04 30 150

Rh (IS) 103 H2 74286.223 1.8 71284.46 104.21 30 150

115In 115 H2 462849.223 3.1 405267.2 114.21 30 150

Sc (IS) 45 He 105928.563 0.7 94674.3733333333 111.89 30 150

Rh (IS) 103 He 1997565.270 1.8 1876006.17333333 106.48 30 150

115In 115 He 156925.600 2.0 144409.67 108.67 30 150

Tb (IS) 159 He 151640.970 2.3 141797.306666667 106.94 30 150

Ho (IS) 165 He 150294.630 1.8 137651.08 109.19 30 150

Bi (IS) 209 He 1450051.157 2.8 1425412.13 101.73 30 150

4/21/2023 11:15 AM

Sample Name 180-153493-a-2-b @50

File Name 184SMPL.d

Data Path Name C:\Agilent\ICPMH\1\DATA\D30420A.b

4/20/2023 2:29:08 PMAcq Time

Sample Type Sample

Total Dilution 1.0000

Comment ---

ISTD Ref FileName 008CALB.d

PassSample QC Pass/Fial

PassISTD QC Pass/Fail

QC Analyte Table

Name Mass ISTD Tune Mode Conc. Conc. RSD CPS LDR QC Flag

Li 7 45 No Gas 959.080 1.0 1235170.377 3000

Be 9 45 No Gas -0.048 N/A 14.667 3600

Si 28 45 H2 100.951 3.4 2644.693 10000

Fe 56 45 H2 312.436 0.6 406024.430 625000

Se 78 45 H2 0.357 7.8 25.347 2250

(Sn) 118 115 H2 0.109 36.9 753.377 5400

Na 23 45 He 170524.841 4.3 24572833.467 625000

{Mg} 24 45 He 16763.802 2.2 1213609.397 625000

{Mg} 25 45 He 16644.261 0.9 178626.590 625000

Mg 26 45 He 16752.132 2.3 229109.940 625000

Al 27 45 He 1.031 45.6 111.333 225000

P 31 45 He -49.471 N/A 97.780 15000

K 39 45 He 7965.959 1.6 605219.610 625000

{Ca} 43 45 He 13527.096 1.5 2781.387 625000

Ca 44 45 He 12584.606 3.4 45309.567 625000

Ti 47 45 He -0.028 N/A 3.000 6750

V 51 45 He 0.036 52.6 96.667 11250

Cr 52 45 He -0.179 N/A 646.683 11250

(Cr) 53 45 He -0.222 N/A 91.110 11250

Mn 55 45 He 22.615 1.1 13587.480 22050

Co 59 103 He -0.008 N/A 68.890 6750

Ni 60 103 He 1.913 2.6 937.813 11250

(Cu) 63 103 He 1.103 3.8 1816.793 11250

Cu 65 103 He 1.221 8.7 926.703 11250

Zn 66 103 He 8.818 8.1 1954.587 11250

(Zn) 68 103 He 8.799 5.4 1468.970 11250

As 75 103 He 0.131 77.7 38.000 2250

(Se) 78 103 He 0.737 196.0 93.333 2250

(Se) 82 103 He -0.584 N/A 40.000 2250

Sr 88 103 He 150.795 2.4 107543.407 11250

(Mo) 95 103 He 0.250 3.7 210.667 6750

Mo 98 103 He 0.265 19.4 353.340 6750

Ag 107 103 He -0.439 N/A 323.340 600

(Ag) 109 103 He -0.488 N/A 258.893 600

Cd 111 115 He 0.005 44.1 5.667 6750

(Cd) 114 115 He 0.004 31.9 22.667 6750

Name Mass ISTD Tune Mode Conc. Conc. RSD CPS LDR QC Flag

Sn 118 115 He 0.089 101.1 267.783 5400

Sb 121 115 He -0.004 N/A 23.333 5400

(Sb) 123 115 He 0.030 103.2 44.443 5400

Ba 137 115 He 1.420 7.5 374.010 11250

(Tl) 203 209 He -0.021 N/A 51.110 9000

Tl 205 209 He -0.017 N/A 134.447 9000

[Pb] 206 209 He 0.315 7.0 384.453 11250

[Pb] 207 209 He 0.264 3.6 296.673 11250

Pb 208 209 He 0.303 1.7 1473.377 11250

Th 232 209 He 0.055 8.1 394.453 4500

U 238 209 He 0.050 8.0 182.227 4500

QC ISTD Table

Name Mass Tune Mode CPS CPS RSD Ref CPS % Rec %QC Low %QC High QC Flag

Li (IS) 6 No Gas 188419.437 1.4 190968.166666667 98.67 30 150

Sc (IS) 45 No Gas 1288760.293 1.2 1216826.10333333 105.91 30 150

Rh (IS) 103 No Gas 2192465.903 2.0 2070097.26 105.91 30 150

Sc (IS) 45 H2 368112.207 1.5 330192.953333333 111.48 30 150

Rh (IS) 103 H2 76326.257 2.5 71284.46 107.07 30 150

115In 115 H2 461820.393 4.4 405267.2 113.95 30 150

Sc (IS) 45 He 106817.073 1.4 94674.3733333333 112.83 30 150

Rh (IS) 103 He 2017232.210 3.5 1876006.17333333 107.53 30 150

115In 115 He 155739.227 3.0 144409.67 107.85 30 150

Tb (IS) 159 He 150592.570 3.0 141797.306666667 106.2 30 150

Ho (IS) 165 He 148662.260 2.2 137651.08 108 30 150

Bi (IS) 209 He 1456066.263 3.6 1425412.13 102.15 30 150

Sample Name 180-153493-a-3-b @50

File Name 185SMPL.d

Data Path Name C:\Agilent\ICPMH\1\DATA\D30420A.b

4/20/2023 2:32:46 PMAcq Time

Sample Type Sample

Total Dilution 1.0000

Comment ---

ISTD Ref FileName 008CALB.d

PassSample QC Pass/Fial

PassISTD QC Pass/Fail

QC Analyte Table

Name Mass ISTD Tune Mode Conc. Conc. RSD CPS LDR QC Flag

Li 7 45 No Gas 997.463 0.8 1319362.330 3000

Be 9 45 No Gas -0.047 N/A 15.333 3600

Si 28 45 H2 93.201 2.9 2569.123 10000

Fe 56 45 H2 156.585 2.0 215357.037 625000

Se 78 45 H2 0.392 36.2 28.587 2250

(Sn) 118 115 H2 0.115 74.2 776.713 5400

Na 23 45 He 248574.408 0.9 37452144.067 625000

{Mg} 24 45 He 24959.327 0.5 1889225.340 625000

{Mg} 25 45 He 24574.929 0.4 275713.697 625000

Mg 26 45 He 24727.857 0.6 353599.223 625000

Al 27 45 He 0.333 95.4 96.667 225000

P 31 45 He -40.396 N/A 120.003 15000

K 39 45 He 11271.787 0.2 878680.223 625000

{Ca} 43 45 He 21416.227 1.2 4595.187 625000

Ca 44 45 He 19633.720 0.3 73785.190 625000

Ti 47 45 He -0.069 N/A 2.000 6750

V 51 45 He 0.001 2383.9 67.777 11250

Cr 52 45 He -0.154 N/A 705.580 11250

(Cr) 53 45 He -0.195 N/A 98.890 11250

Mn 55 45 He 38.686 2.5 24238.977 22050

Co 59 103 He 0.054 21.7 182.227 6750

Ni 60 103 He 4.467 2.8 2191.287 11250

(Cu) 63 103 He 1.607 3.3 2533.567 11250

Cu 65 103 He 1.701 5.5 1264.503 11250

Zn 66 103 He 10.623 2.7 2407.987 11250

(Zn) 68 103 He 10.937 5.4 1853.460 11250

As 75 103 He 0.080 25.8 32.000 2250

(Se) 78 103 He 2.461 77.3 115.333 2250

(Se) 82 103 He 1.029 6.5 50.000 2250

Sr 88 103 He 231.929 0.7 171069.293 11250

(Mo) 95 103 He 0.286 5.8 239.333 6750

Mo 98 103 He 0.302 16.5 401.343 6750

Ag 107 103 He -0.461 N/A 293.340 600

(Ag) 109 103 He -0.464 N/A 312.227 600

Cd 111 115 He 0.470 5.5 136.333 6750

(Cd) 114 115 He 0.497 2.2 361.343 6750

Name Mass ISTD Tune Mode Conc. Conc. RSD CPS LDR QC Flag

Sn 118 115 He 0.063 154.0 265.560 5400

Sb 121 115 He 0.032 47.1 51.110 5400

(Sb) 123 115 He 0.013 88.9 36.667 5400

Ba 137 115 He 1.965 1.7 538.677 11250

(Tl) 203 209 He -0.033 N/A 38.887 9000

Tl 205 209 He -0.022 N/A 126.670 9000

[Pb] 206 209 He 0.367 3.2 446.680 11250

[Pb] 207 209 He 0.371 3.1 394.453 11250

Pb 208 209 He 0.381 1.5 1817.843 11250

Th 232 209 He 0.031 15.1 327.787 4500

U 238 209 He 0.079 3.1 292.230 4500

QC ISTD Table

Name Mass Tune Mode CPS CPS RSD Ref CPS % Rec %QC Low %QC High QC Flag

Li (IS) 6 No Gas 198920.343 1.5 190968.166666667 104.16 30 150

Sc (IS) 45 No Gas 1324031.960 1.5 1216826.10333333 108.81 30 150

Rh (IS) 103 No Gas 2227166.427 1.2 2070097.26 107.59 30 150

Sc (IS) 45 H2 383917.400 1.1 330192.953333333 116.27 30 150

Rh (IS) 103 H2 78866.410 1.8 71284.46 110.64 30 150

115In 115 H2 471143.603 2.2 405267.2 116.26 30 150

Sc (IS) 45 He 111661.830 0.9 94674.3733333333 117.94 30 150

Rh (IS) 103 He 2085450.957 0.7 1876006.17333333 111.16 30 150

115In 115 He 163230.437 0.6 144409.67 113.03 30 150

Tb (IS) 159 He 156644.250 1.3 141797.306666667 110.47 30 150

Ho (IS) 165 He 154068.270 2.2 137651.08 111.93 30 150

Bi (IS) 209 He 1509678.133 1.6 1425412.13 105.91 30 150

Sample Name 180-153493-a-4-b @50

File Name 186SMPL.d

Data Path Name C:\Agilent\ICPMH\1\DATA\D30420A.b

4/20/2023 2:36:24 PMAcq Time

Sample Type Sample

Total Dilution 1.0000

Comment ---

ISTD Ref FileName 008CALB.d

PassSample QC Pass/Fial

PassISTD QC Pass/Fail

QC Analyte Table

Name Mass ISTD Tune Mode Conc. Conc. RSD CPS LDR QC Flag

Li 7 45 No Gas 1022.620 0.5 1382425.627 3000

Be 9 45 No Gas -0.049 N/A 14.667 3600

Si 28 45 H2 115.013 1.8 3145.897 10000

Fe 56 45 H2 299.966 2.9 412424.707 625000

Se 78 45 H2 0.226 25.2 18.760 2250

(Sn) 118 115 H2 0.077 110.5 733.377 5400

Na 23 45 He 196185.271 1.2 29436055.497 625000

{Mg} 24 45 He 19856.018 0.3 1496370.567 625000

{Mg} 25 45 He 19636.758 0.6 219341.870 625000

Mg 26 45 He 19507.656 0.4 277715.293 625000

Al 27 45 He 5.783 33.3 249.340 225000

P 31 45 He -52.204 N/A 96.667 15000

K 39 45 He 8871.267 0.4 697019.400 625000

{Ca} 43 45 He 16317.000 6.4 3491.540 625000

Ca 44 45 He 14963.871 1.8 56031.730 625000

Ti 47 45 He 0.216 80.1 10.000 6750

V 51 45 He 0.037 48.3 101.113 11250

Cr 52 45 He -0.024 N/A 855.587 11250

(Cr) 53 45 He -0.015 N/A 124.443 11250

Mn 55 45 He 25.440 1.5 15897.573 22050

Co 59 103 He 0.003 428.9 91.110 6750

Ni 60 103 He 2.533 4.6 1271.177 11250

(Cu) 63 103 He 1.141 3.6 1934.583 11250

Cu 65 103 He 1.304 5.4 1015.600 11250

Zn 66 103 He 9.165 2.6 2106.830 11250

(Zn) 68 103 He 9.523 5.8 1638.993 11250

As 75 103 He 0.062 44.2 29.667 2250

(Se) 78 103 He 1.112 46.9 101.000 2250

(Se) 82 103 He 3.298 28.7 62.223 2250

Sr 88 103 He 174.704 0.7 129432.383 11250

(Mo) 95 103 He 0.270 3.4 230.667 6750

Mo 98 103 He 0.271 3.4 372.677 6750

Ag 107 103 He -0.467 N/A 283.337 600

(Ag) 109 103 He -0.484 N/A 277.783 600

Cd 111 115 He 0.020 46.6 10.000 6750

(Cd) 114 115 He 0.014 43.1 30.333 6750

Name Mass ISTD Tune Mode Conc. Conc. RSD CPS LDR QC Flag

Sn 118 115 He 0.084 55.9 275.560 5400

Sb 121 115 He 0.008 204.3 33.333 5400

(Sb) 123 115 He -0.005 N/A 25.557 5400

Ba 137 115 He 1.536 2.7 419.343 11250

(Tl) 203 209 He 0.036 351.4 121.150 9000

Tl 205 209 He 0.030 330.6 274.613 9000

[Pb] 206 209 He 0.433 28.3 512.253 11250

[Pb] 207 209 He 0.381 24.3 405.577 11250

Pb 208 209 He 0.408 23.1 1933.487 11250

Th 232 209 He 0.042 32.5 367.790 4500

U 238 209 He 0.082 14.1 305.567 4500

QC ISTD Table

Name Mass Tune Mode CPS CPS RSD Ref CPS % Rec %QC Low %QC High QC Flag

Li (IS) 6 No Gas 209132.110 0.9 190968.166666667 109.51 30 150

Sc (IS) 45 No Gas 1353648.107 0.6 1216826.10333333 111.24 30 150

Rh (IS) 103 No Gas 2270911.527 1.2 2070097.26 109.7 30 150

Sc (IS) 45 H2 389254.667 0.7 330192.953333333 117.89 30 150

Rh (IS) 103 H2 80354.967 0.2 71284.46 112.72 30 150

115In 115 H2 479810.133 3.7 405267.2 118.39 30 150

Sc (IS) 45 He 111172.413 1.8 94674.3733333333 117.43 30 150

Rh (IS) 103 He 2094533.873 0.4 1876006.17333333 111.65 30 150

115In 115 He 161633.160 0.9 144409.67 111.93 30 150

Tb (IS) 159 He 157535.267 1.1 141797.306666667 111.1 30 150

Ho (IS) 165 He 153630.610 1.8 137651.08 111.61 30 150

Bi (IS) 209 He 1520531.363 1.5 1425412.13 106.67 30 150

4/21/2023 11:16 AM

Sample Name 180-153493-a-5-b @50

File Name 187SMPL.d

Data Path Name C:\Agilent\ICPMH\1\DATA\D30420A.b

4/20/2023 2:40:03 PMAcq Time

Sample Type Sample

Total Dilution 1.0000

Comment ---

ISTD Ref FileName 008CALB.d

PassSample QC Pass/Fial

PassISTD QC Pass/Fail

QC Analyte Table

Name Mass ISTD Tune Mode Conc. Conc. RSD CPS LDR QC Flag

Li 7 45 No Gas 796.067 2.1 1085325.127 3000

Be 9 45 No Gas -0.053 N/A 13.333 3600

Si 28 45 H2 102.912 3.2 2903.633 10000

Fe 56 45 H2 263.267 0.5 370183.650 625000

Se 78 45 H2 0.158 52.9 14.920 2250

(Sn) 118 115 H2 0.250 30.5 1023.407 5400

Na 23 45 He 210488.744 1.5 31233603.203 625000

{Mg} 24 45 He 22395.100 1.1 1669415.247 625000

{Mg} 25 45 He 22288.016 1.0 246290.930 625000

Mg 26 45 He 22403.344 0.9 315509.797 625000

Al 27 45 He 1.654 36.2 132.000 225000

P 31 45 He -48.186 N/A 103.333 15000

K 39 45 He 9474.721 1.2 733724.467 625000

{Ca} 43 45 He 18122.496 2.6 3831.623 625000

Ca 44 45 He 16715.983 0.2 61904.017 625000

Ti 47 45 He 0.041 154.1 5.000 6750

V 51 45 He -0.005 N/A 61.110 11250

Cr 52 45 He -0.114 N/A 741.133 11250

(Cr) 53 45 He 0.027 519.8 128.887 11250

Mn 55 45 He 26.200 1.3 16194.557 22050

Co 59 103 He 0.003 292.9 90.000 6750

Ni 60 103 He 2.116 5.2 1055.600 11250

(Cu) 63 103 He 1.458 5.3 2316.863 11250

Cu 65 103 He 1.607 10.1 1192.280 11250

Zn 66 103 He 12.362 3.1 2752.500 11250

(Zn) 68 103 He 12.180 3.4 2030.153 11250

As 75 103 He 0.031 157.9 25.000 2250

(Se) 78 103 He 0.953 57.0 98.000 2250

(Se) 82 103 He -1.624 N/A 35.557 2250

Sr 88 103 He 197.332 2.3 144225.003 11250

(Mo) 95 103 He 0.294 4.3 241.333 6750

Mo 98 103 He 0.307 5.3 402.677 6750

Ag 107 103 He -0.474 N/A 265.560 600

(Ag) 109 103 He -0.487 N/A 268.890 600

Cd 111 115 He 0.084 9.2 27.667 6750

(Cd) 114 115 He 0.056 15.4 58.333 6750

Name Mass ISTD Tune Mode Conc. Conc. RSD CPS LDR QC Flag

Sn 118 115 He 0.202 21.0 345.560 5400

Sb 121 115 He 0.001 2733.6 27.777 5400

(Sb) 123 115 He 0.012 170.1 35.557 5400

Ba 137 115 He 1.574 15.0 427.343 11250

(Tl) 203 209 He -0.034 N/A 36.667 9000

Tl 205 209 He -0.033 N/A 95.553 9000

[Pb] 206 209 He 0.305 25.1 384.453 11250

[Pb] 207 209 He 0.291 15.4 325.560 11250

Pb 208 209 He 0.305 11.7 1518.930 11250

Th 232 209 He 0.020 20.7 286.673 4500

U 238 209 He 0.054 14.2 200.003 4500

QC ISTD Table

Name Mass Tune Mode CPS CPS RSD Ref CPS % Rec %QC Low %QC High QC Flag

Li (IS) 6 No Gas 207074.737 1.2 190968.166666667 108.43 30 150

Sc (IS) 45 No Gas 1361209.667 0.9 1216826.10333333 111.87 30 150

Rh (IS) 103 No Gas 2276870.017 1.3 2070097.26 109.99 30 150

Sc (IS) 45 H2 397190.420 0.6 330192.953333333 120.29 30 150

Rh (IS) 103 H2 82448.223 2.7 71284.46 115.66 30 150

115In 115 H2 486778.597 2.9 405267.2 120.11 30 150

Sc (IS) 45 He 109975.613 0.9 94674.3733333333 116.16 30 150

Rh (IS) 103 He 2066806.167 2.1 1876006.17333333 110.17 30 150

115In 115 He 160992.570 1.5 144409.67 111.48 30 150

Tb (IS) 159 He 154820.793 1.3 141797.306666667 109.18 30 150

Ho (IS) 165 He 151865.543 1.6 137651.08 110.33 30 150

Bi (IS) 209 He 1497126.883 2.7 1425412.13 105.03 30 150

Sample Name 180-153493-a-6-b @50

File Name 188SMPL.d

Data Path Name C:\Agilent\ICPMH\1\DATA\D30420A.b

4/20/2023 2:43:42 PMAcq Time

Sample Type Sample

Total Dilution 1.0000

Comment ---

ISTD Ref FileName 008CALB.d

PassSample QC Pass/Fial

PassISTD QC Pass/Fail

QC Analyte Table

Name Mass ISTD Tune Mode Conc. Conc. RSD CPS LDR QC Flag

Li 7 45 No Gas 957.703 1.2 1306540.623 3000

Be 9 45 No Gas -0.048 N/A 15.333 3600

Si 28 45 H2 100.620 4.7 2834.733 10000

Fe 56 45 H2 189.184 3.3 266636.847 625000

Se 78 45 H2 0.236 36.3 19.667 2250

(Sn) 118 115 H2 0.108 43.0 780.043 5400

Na 23 45 He 253517.156 1.4 37696681.837 625000

{Mg} 24 45 He 26859.950 0.6 2006610.893 625000

{Mg} 25 45 He 26432.598 1.1 292742.340 625000

Mg 26 45 He 26456.137 0.7 373424.783 625000

Al 27 45 He 10.123 69.4 370.727 225000

P 31 45 He -29.315 N/A 140.000 15000

K 39 45 He 11316.283 0.7 870616.790 625000

{Ca} 43 45 He 22677.390 2.4 4801.917 625000

Ca 44 45 He 21052.018 1.0 78070.217 625000

Ti 47 45 He 0.123 147.0 7.333 6750

V 51 45 He 0.063 156.7 125.577 11250

Cr 52 45 He -0.013 N/A 861.170 11250

(Cr) 53 45 He 0.079 78.4 136.670 11250

Mn 55 45 He 40.592 1.2 25100.457 22050

Co 59 103 He 0.084 67.6 232.240 6750

Ni 60 103 He 4.367 1.1 2113.500 11250

(Cu) 63 103 He 1.370 13.7 2192.467 11250

Cu 65 103 He 1.350 15.3 1025.603 11250

Zn 66 103 He 13.278 1.5 2931.423 11250

(Zn) 68 103 He 12.379 3.7 2051.267 11250

As 75 103 He 0.062 84.8 29.000 2250

(Se) 78 103 He 1.157 37.5 99.667 2250

(Se) 82 103 He -0.141 N/A 43.330 2250

Sr 88 103 He 241.991 1.6 175988.750 11250

(Mo) 95 103 He 0.365 16.0 281.337 6750

Mo 98 103 He 0.312 7.9 405.343 6750

Ag 107 103 He -0.475 N/A 262.223 600

(Ag) 109 103 He -0.491 N/A 260.007 600

Cd 111 115 He 0.170 7.9 51.000 6750

(Cd) 114 115 He 0.138 10.2 112.667 6750

Name Mass ISTD Tune Mode Conc. Conc. RSD CPS LDR QC Flag

Sn 118 115 He 0.143 83.7 306.673 5400

Sb 121 115 He 0.018 112.6 40.000 5400

(Sb) 123 115 He 0.011 131.3 34.443 5400

Ba 137 115 He 2.030 9.9 543.347 11250

(Tl) 203 209 He -0.010 N/A 64.447 9000

Tl 205 209 He -0.016 N/A 140.000 9000

[Pb] 206 209 He 0.480 12.7 545.570 11250

[Pb] 207 209 He 0.427 2.5 434.453 11250

Pb 208 209 He 0.463 5.4 2100.080 11250

Th 232 209 He 0.019 80.5 281.113 4500

U 238 209 He 0.086 9.5 313.340 4500

QC ISTD Table

Name Mass Tune Mode CPS CPS RSD Ref CPS % Rec %QC Low %QC High QC Flag

Li (IS) 6 No Gas 211681.263 1.8 190968.166666667 110.85 30 150

Sc (IS) 45 No Gas 1365182.947 2.0 1216826.10333333 112.19 30 150

Rh (IS) 103 No Gas 2257953.247 1.2 2070097.26 109.07 30 150

Sc (IS) 45 H2 395475.410 1.4 330192.953333333 119.77 30 150

Rh (IS) 103 H2 81718.123 1.4 71284.46 114.64 30 150

115In 115 H2 479609.960 2.7 405267.2 118.34 30 150

Sc (IS) 45 He 110215.500 1.2 94674.3733333333 116.42 30 150

Rh (IS) 103 He 2056410.820 1.0 1876006.17333333 109.62 30 150

115In 115 He 159662.870 1.4 144409.67 110.56 30 150

Tb (IS) 159 He 152852.177 1.3 141797.306666667 107.8 30 150

Ho (IS) 165 He 151130.433 1.7 137651.08 109.79 30 150

Bi (IS) 209 He 1490788.240 1.6 1425412.13 104.59 30 150

Sample Name 180-153493-a-7-b @50

File Name 189SMPL.d

Data Path Name C:\Agilent\ICPMH\1\DATA\D30420A.b

4/20/2023 2:47:20 PMAcq Time

Sample Type Sample

Total Dilution 1.0000

Comment ---

ISTD Ref FileName 008CALB.d

PassSample QC Pass/Fial

PassISTD QC Pass/Fail

QC Analyte Table

Name Mass ISTD Tune Mode Conc. Conc. RSD CPS LDR QC Flag

Li 7 45 No Gas 1058.118 0.5 1388965.583 3000

Be 9 45 No Gas -0.054 N/A 12.667 3600

Si 28 45 H2 79.332 2.4 2234.627 10000

Fe 56 45 H2 98.211 1.0 137653.830 625000

Se 78 45 H2 0.158 48.7 14.507 2250

(Sn) 118 115 H2 0.095 202.7 743.383 5400

Na 23 45 He 240386.674 1.7 35360940.817 625000

{Mg} 24 45 He 24906.314 1.0 1840477.430 625000

{Mg} 25 45 He 24658.515 0.9 270087.610 625000

Mg 26 45 He 24870.772 1.1 347196.690 625000

Al 27 45 He 1.570 13.5 128.667 225000

P 31 45 He -48.863 N/A 101.113 15000

K 39 45 He 10855.525 0.4 827590.973 625000

{Ca} 43 45 He 20354.364 3.9 4265.080 625000

Ca 44 45 He 19491.742 1.5 71518.317 625000

Ti 47 45 He -0.006 N/A 3.667 6750

V 51 45 He 0.001 1518.8 66.667 11250

Cr 52 45 He -0.187 N/A 650.020 11250

(Cr) 53 45 He -0.299 N/A 82.220 11250

Mn 55 45 He 40.100 0.2 24528.383 22050

Co 59 103 He 0.039 10.9 151.113 6750

Ni 60 103 He 4.529 5.1 2155.727 11250

(Cu) 63 103 He 1.044 4.7 1747.890 11250

Cu 65 103 He 1.061 7.7 831.140 11250

Zn 66 103 He 9.735 2.4 2154.613 11250

(Zn) 68 103 He 10.105 3.8 1672.327 11250

As 75 103 He -0.053 N/A 13.000 2250

(Se) 78 103 He 1.236 45.5 99.000 2250

(Se) 82 103 He 0.456 247.1 45.557 2250

Sr 88 103 He 227.394 1.4 162828.783 11250

(Mo) 95 103 He 0.160 25.5 160.000 6750

Mo 98 103 He 0.231 12.9 322.000 6750

Ag 107 103 He -0.490 N/A 231.113 600

(Ag) 109 103 He -0.504 N/A 233.337 600

Cd 111 115 He 0.043 35.6 16.000 6750

(Cd) 114 115 He 0.020 87.0 33.000 6750

Name Mass ISTD Tune Mode Conc. Conc. RSD CPS LDR QC Flag

Sn 118 115 He 0.119 73.4 288.893 5400

Sb 121 115 He 0.017 124.9 38.890 5400

(Sb) 123 115 He 0.009 154.5 33.333 5400

Ba 137 115 He 1.816 4.6 480.677 11250

(Tl) 203 209 He -0.040 N/A 30.000 9000

Tl 205 209 He -0.040 N/A 74.447 9000

[Pb] 206 209 He 0.437 1.4 498.903 11250

[Pb] 207 209 He 0.428 5.7 430.010 11250

Pb 208 209 He 0.424 6.7 1931.180 11250

Th 232 209 He 0.016 59.0 264.447 4500

U 238 209 He 0.086 17.0 308.897 4500

QC ISTD Table

Name Mass Tune Mode CPS CPS RSD Ref CPS % Rec %QC Low %QC High QC Flag

Li (IS) 6 No Gas 204780.287 1.3 190968.166666667 107.23 30 150

Sc (IS) 45 No Gas 1314891.567 0.7 1216826.10333333 108.06 30 150

Rh (IS) 103 No Gas 2189764.810 0.9 2070097.26 105.78 30 150

Sc (IS) 45 H2 384569.253 0.7 330192.953333333 116.47 30 150

Rh (IS) 103 H2 80057.750 1.9 71284.46 112.31 30 150

115In 115 H2 468651.093 2.9 405267.2 115.64 30 150

Sc (IS) 45 He 109009.607 1.0 94674.3733333333 115.14 30 150

Rh (IS) 103 He 2024584.990 1.7 1876006.17333333 107.92 30 150

115In 115 He 157426.753 1.8 144409.67 109.01 30 150

Tb (IS) 159 He 151121.807 1.8 141797.306666667 106.58 30 150

Ho (IS) 165 He 148881.390 1.5 137651.08 108.16 30 150

Bi (IS) 209 He 1470836.640 3.7 1425412.13 103.19 30 150

4/21/2023 11:17 AM

Sample Name CCV 5343245

File Name 191_CCV.d

Data Path Name C:\Agilent\ICPMH\1\DATA\D30420A.b

4/20/2023 2:54:39 PMAcq Time

Sample Type CCV

Total Dilution 1.0000

Comment ---

ISTD Ref FileName 008CALB.d

FailSample QC Pass/Fial

PassISTD QC Pass/Fail

QC Analyte Table

Name Mass ISTD Tune Mode Conc. Conc. RSD CPS LDR QC Flag

Li 7 45 No Gas 194.138 2.9 267900.230 200

Be 9 45 No Gas 197.275 2.8 69951.230 200

(B) 10 45 No Gas 544.773 1.9 21191.660 500

B 11 45 No Gas 556.761 3.3 104237.637 500 >+\-10%

Si 28 45 H2 2008.449 0.9 49086.263 2000

Fe 56 45 H2 50107.987 1.3 66526539.577 50000

Se 78 45 H2 206.152 1.9 12341.950 200

(Sn) 118 115 H2 198.982 0.9 311763.010 200

Na 23 45 He 50398.913 0.2 7509885.260 50000

{Mg} 24 45 He 50306.570 0.6 3758418.043 50000

{Mg} 25 45 He 49426.413 0.7 547357.477 50000

Mg 26 45 He 49615.974 0.7 700322.177 50000

Al 27 45 He 49264.295 0.4 1377423.373 50000

P 31 45 He 2410.350 1.7 4851.923 2500

K 39 45 He 51439.268 0.5 3816936.097 50000

{Ca} 43 45 He 52556.374 1.2 11110.887 50000

Ca 44 45 He 51035.275 0.2 188950.893 50000

Ti 47 45 He 198.061 1.5 5505.373 200

V 51 45 He 195.316 0.8 182689.763 200

Cr 52 45 He 194.273 1.1 227553.760 200

(Cr) 53 45 He 196.976 1.7 28016.843 200

Mn 55 45 He 196.028 0.2 120930.407 200

Co 59 103 He 199.002 2.4 359733.960 200

Ni 60 103 He 198.785 1.4 95886.937 200

(Cu) 63 103 He 195.264 1.5 256571.490 200

Cu 65 103 He 195.945 1.0 125900.403 200

Zn 66 103 He 101.885 1.7 21974.457 100

(Zn) 68 103 He 115.287 2.6 18388.377 100 >+\-10%

As 75 103 He 198.841 1.5 27974.317 200

(Se) 78 103 He 199.860 3.7 2300.853 200

(Se) 82 103 He 200.336 6.6 1107.827 200

Sr 88 103 He 203.710 1.8 151321.827 200

(Mo) 95 103 He 202.189 0.4 119550.660 200

Mo 98 103 He 203.136 0.8 200196.413 200

Ag 107 103 He 97.405 0.6 184647.893 100

(Ag) 109 103 He 97.919 0.9 177485.400 100

Name Mass ISTD Tune Mode Conc. Conc. RSD CPS LDR QC Flag

Cd 111 115 He 198.457 0.1 54904.593 200

(Cd) 114 115 He 200.033 0.7 135085.937 200

Sn 118 115 He 200.603 0.4 120776.147 200

Sb 121 115 He 193.590 0.5 139449.687 200

(Sb) 123 115 He 193.446 0.3 110551.703 200

Ba 137 115 He 198.684 0.4 52565.193 200

(Tl) 203 209 He 201.508 0.3 241013.357 200

Tl 205 209 He 200.618 1.1 573143.693 200

[Pb] 206 209 He 201.136 0.6 190649.087 200

[Pb] 207 209 He 199.699 1.3 165081.353 200

Pb 208 209 He 200.095 1.1 756622.627 200

Th 232 209 He 100.171 1.0 353539.797 100

U 238 209 He 101.377 0.8 363327.237 100

QC ISTD Table

Name Mass Tune Mode CPS CPS RSD Ref CPS % Rec %QC Low %QC High QC Flag

Li (IS) 6 No Gas 198880.753 0.7 190968.166666667 104.14 30 150

Sc (IS) 45 No Gas 1322647.400 2.4 1216826.10333333 108.7 30 150

Rh (IS) 103 No Gas 2173189.967 1.2 2070097.26 104.98 30 150

Sc (IS) 45 H2 381698.100 0.6 330192.953333333 115.6 30 150

Rh (IS) 103 H2 80400.627 1.2 71284.46 112.79 30 150

115In 115 H2 464462.577 3.2 405267.2 114.61 30 150

Sc (IS) 45 He 110222.990 0.7 94674.3733333333 116.42 30 150

Rh (IS) 103 He 2100762.067 2.6 1876006.17333333 111.98 30 150

115In 115 He 160878.787 1.9 144409.67 111.4 30 150

Tb (IS) 159 He 155848.400 3.5 141797.306666667 109.91 30 150

Ho (IS) 165 He 155168.133 2.4 137651.08 112.73 30 150

Bi (IS) 209 He 1528974.243 3.6 1425412.13 107.27 30 150

Sample Name CCB

File Name 192_CCB.d

Data Path Name C:\Agilent\ICPMH\1\DATA\D30420A.b

4/20/2023 2:58:17 PMAcq Time

Sample Type CCB

Total Dilution 1.0000

Comment ---

ISTD Ref FileName 008CALB.d

FailSample QC Pass/Fial

PassISTD QC Pass/Fail

QC Analyte Table

Name Mass ISTD Tune Mode Conc. Conc. RSD CPS LDR QC Flag

Li 7 45 No Gas 0.661 28.3 14822.617 5

Be 9 45 No Gas -0.040 N/A 17.333 1

(B) 10 45 No Gas 153.928 5.3 6799.350 80 >DL

B 11 45 No Gas 157.539 3.5 33391.563 80 >DL

Si 28 45 H2 -0.958 N/A 256.670 500

Fe 56 45 H2 0.608 60.6 6776.060 50

Se 78 45 H2 0.183 35.4 15.253 5

(Sn) 118 115 H2 0.055 93.9 666.700 5

Na 23 45 He 87.199 4.0 29468.990 500

{Mg} 24 45 He 1.284 48.3 215.560 500

{Mg} 25 45 He 1.150 3.4 26.670 500

Mg 26 45 He 0.985 90.8 38.887 500

Al 27 45 He 0.380 67.3 91.333 30

P 31 45 He -48.285 N/A 97.780 500

K 39 45 He 3.563 168.9 37660.040 500

{Ca} 43 45 He 32.927 50.7 20.000 500

Ca 44 45 He 1.262 703.0 223.337 500

Ti 47 45 He -0.101 N/A 1.000 5

V 51 45 He -0.017 N/A 47.777 1

Cr 52 45 He -0.224 N/A 580.013 2

(Cr) 53 45 He -0.327 N/A 74.447 2

Mn 55 45 He -0.033 N/A 56.667 5

Co 59 103 He -0.010 N/A 64.447 0.5

Ni 60 103 He -0.038 N/A 33.333 1

(Cu) 63 103 He -0.158 N/A 225.557 2

Cu 65 103 He -0.119 N/A 101.110 2

Zn 66 103 He -0.307 N/A 80.000 15

(Zn) 68 103 He -0.334 N/A 78.890 15

As 75 103 He -0.087 N/A 8.333 1

(Se) 78 103 He 0.598 14.8 91.333 5

(Se) 82 103 He -0.593 N/A 40.000 5

Sr 88 103 He -0.004 N/A 38.887 5

(Mo) 95 103 He -0.008 N/A 64.000 5

Mo 98 103 He 0.018 57.7 119.333 5

Ag 107 103 He -0.235 N/A 687.803 1

(Ag) 109 103 He -0.257 N/A 654.467 1

Name Mass ISTD Tune Mode Conc. Conc. RSD CPS LDR QC Flag

Cd 111 115 He 0.003 281.8 5.000 1

(Cd) 114 115 He -0.003 N/A 17.667 1

Sn 118 115 He 0.073 135.8 256.673 5

Sb 121 115 He 0.109 34.8 101.113 2

(Sb) 123 115 He 0.115 32.4 90.000 2

Ba 137 115 He 0.008 110.2 12.667 10

(Tl) 203 209 He -0.011 N/A 62.220 1

Tl 205 209 He 0.000 16827.8 182.227 1

[Pb] 206 209 He -0.057 N/A 48.890 1

[Pb] 207 209 He -0.035 N/A 61.113 1

Pb 208 209 He -0.039 N/A 242.230 1

QC ISTD Table

Name Mass Tune Mode CPS CPS RSD Ref CPS % Rec %QC Low %QC High QC Flag

Li (IS) 6 No Gas 193941.670 0.3 190968.166666667 101.56 30 150

Sc (IS) 45 No Gas 1293920.503 0.9 1216826.10333333 106.34 30 150

Rh (IS) 103 No Gas 2205590.747 0.2 2070097.26 106.55 30 150

Sc (IS) 45 H2 366814.997 0.6 330192.953333333 111.09 30 150

Rh (IS) 103 H2 79849.777 2.1 71284.46 112.02 30 150

115In 115 H2 461982.207 4.1 405267.2 113.99 30 150

Sc (IS) 45 He 104061.833 1.6 94674.3733333333 109.92 30 150

Rh (IS) 103 He 2006885.340 1.3 1876006.17333333 106.98 30 150

115In 115 He 154004.200 0.9 144409.67 106.64 30 150

Tb (IS) 159 He 147762.407 0.3 141797.306666667 104.21 30 150

Ho (IS) 165 He 145501.773 1.4 137651.08 105.7 30 150

Bi (IS) 209 He 1461518.620 1.0 1425412.13 102.53 30 150

Sample Name 180-153493-a-8-b @50

File Name 193SMPL.d

Data Path Name C:\Agilent\ICPMH\1\DATA\D30420A.b

4/20/2023 3:01:57 PMAcq Time

Sample Type Sample

Total Dilution 1.0000

Comment ---

ISTD Ref FileName 008CALB.d

PassSample QC Pass/Fial

PassISTD QC Pass/Fail

QC Analyte Table

Name Mass ISTD Tune Mode Conc. Conc. RSD CPS LDR QC Flag

Li 7 45 No Gas 1044.579 1.6 1340599.623 3000

Be 9 45 No Gas -0.047 N/A 14.667 3600

Si 28 45 H2 83.189 4.0 2249.070 10000

Fe 56 45 H2 42.631 1.0 61151.727 625000

Se 78 45 H2 0.141 54.7 13.000 2250

(Sn) 118 115 H2 0.092 58.1 713.367 5400

Na 23 45 He 252369.169 1.7 36620940.767 625000

{Mg} 24 45 He 26405.009 1.4 1924947.147 625000

{Mg} 25 45 He 26010.553 0.4 281051.880 625000

Mg 26 45 He 26019.167 0.9 358348.293 625000

Al 27 45 He 1.419 28.8 122.667 225000

P 31 45 He -58.144 N/A 82.220 15000

K 39 45 He 11289.180 0.3 847496.737 625000

{Ca} 43 45 He 21191.246 4.0 4380.677 625000

Ca 44 45 He 19834.097 0.8 71790.850 625000

Ti 47 45 He -0.016 N/A 3.333 6750

V 51 45 He -0.006 N/A 58.887 11250

Cr 52 45 He -0.175 N/A 654.463 11250

(Cr) 53 45 He -0.146 N/A 102.223 11250

Mn 55 45 He 40.732 1.8 24577.360 22050

Co 59 103 He 0.049 26.6 168.893 6750

Ni 60 103 He 4.588 4.7 2192.400 11250

(Cu) 63 103 He 1.001 7.9 1697.887 11250

Cu 65 103 He 1.025 4.3 813.360 11250

Zn 66 103 He 12.267 1.7 2689.157 11250

(Zn) 68 103 He 12.822 5.0 2095.720 11250

As 75 103 He -0.076 N/A 10.000 2250

(Se) 78 103 He 1.789 20.3 105.333 2250

(Se) 82 103 He -0.040 N/A 43.337 2250

Sr 88 103 He 233.622 1.5 167961.403 11250

(Mo) 95 103 He 0.228 26.1 199.333 6750

Mo 98 103 He 0.235 10.2 327.337 6750

Ag 107 103 He -0.383 N/A 426.673 600

(Ag) 109 103 He -0.432 N/A 358.893 600

Cd 111 115 He 0.048 1.2 17.333 6750

(Cd) 114 115 He 0.039 43.3 46.000 6750

Name Mass ISTD Tune Mode Conc. Conc. RSD CPS LDR QC Flag

Sn 118 115 He 0.093 58.3 274.450 5400

Sb 121 115 He 0.062 37.0 71.110 5400

(Sb) 123 115 He 0.053 75.2 57.777 5400

Ba 137 115 He 1.825 5.8 484.677 11250

(Tl) 203 209 He -0.031 N/A 40.000 9000

Tl 205 209 He -0.028 N/A 104.443 9000

[Pb] 206 209 He 0.250 13.8 327.783 11250

[Pb] 207 209 He 0.264 21.5 298.893 11250

Pb 208 209 He 0.247 9.7 1283.363 11250

Th 232 209 He 0.239 4.9 1021.157 4500

U 238 209 He 0.081 8.9 290.003 4500

QC ISTD Table

Name Mass Tune Mode CPS CPS RSD Ref CPS % Rec %QC Low %QC High QC Flag

Li (IS) 6 No Gas 203080.567 1.6 190968.166666667 106.34 30 150

Sc (IS) 45 No Gas 1285633.547 2.2 1216826.10333333 105.65 30 150

Rh (IS) 103 No Gas 2139161.323 2.7 2070097.26 103.34 30 150

Sc (IS) 45 H2 371443.813 0.8 330192.953333333 112.49 30 150

Rh (IS) 103 H2 78273.410 0.9 71284.46 109.8 30 150

115In 115 H2 453989.743 2.8 405267.2 112.02 30 150

Sc (IS) 45 He 107543.360 1.5 94674.3733333333 113.59 30 150

Rh (IS) 103 He 2033382.767 3.6 1876006.17333333 108.39 30 150

115In 115 He 157786.290 2.9 144409.67 109.26 30 150

Tb (IS) 159 He 151785.510 2.8 141797.306666667 107.04 30 150

Ho (IS) 165 He 150724.587 2.9 137651.08 109.5 30 150

Bi (IS) 209 He 1465546.540 3.4 1425412.13 102.82 30 150

4/21/2023 11:18 AM

Sample Name 180-153493-a-9-b @50

File Name 194SMPL.d

Data Path Name C:\Agilent\ICPMH\1\DATA\D30420A.b

4/20/2023 3:05:35 PMAcq Time

Sample Type Sample

Total Dilution 1.0000

Comment ---

ISTD Ref FileName 008CALB.d

PassSample QC Pass/Fial

PassISTD QC Pass/Fail

QC Analyte Table

Name Mass ISTD Tune Mode Conc. Conc. RSD CPS LDR QC Flag

Li 7 45 No Gas 1059.367 0.2 1422720.580 3000

Be 9 45 No Gas -0.040 N/A 18.000 3600

Si 28 45 H2 75.987 5.7 2161.280 10000

Fe 56 45 H2 67.765 19.7 97347.240 625000

Se 78 45 H2 0.263 108.5 20.920 2250

(Sn) 118 115 H2 0.197 101.1 910.143 5400

Na 23 45 He 259589.793 1.3 39373968.433 625000

{Mg} 24 45 He 26111.790 0.8 1989858.047 625000

{Mg} 25 45 He 25765.546 0.9 291041.013 625000

Mg 26 45 He 25820.347 0.9 371723.820 625000

Al 27 45 He 0.705 23.8 108.000 225000

P 31 45 He -55.587 N/A 91.113 15000

K 39 45 He 11405.482 1.4 894643.783 625000

{Ca} 43 45 He 20187.986 4.1 4361.783 625000

Ca 44 45 He 18968.570 1.2 71775.213 625000

Ti 47 45 He -0.081 N/A 1.667 6750

V 51 45 He -0.019 N/A 48.890 11250

Cr 52 45 He -0.183 N/A 675.573 11250

(Cr) 53 45 He -0.162 N/A 104.443 11250

Mn 55 45 He 37.757 1.4 23822.730 22050

Co 59 103 He 0.055 37.5 183.337 6750

Ni 60 103 He 4.705 2.7 2313.530 11250

(Cu) 63 103 He 1.125 7.9 1911.250 11250

Cu 65 103 He 1.163 5.6 925.590 11250

Zn 66 103 He 12.173 2.1 2748.053 11250

(Zn) 68 103 He 12.145 4.8 2050.157 11250

As 75 103 He -0.035 N/A 16.000 2250

(Se) 78 103 He 0.680 140.5 96.000 2250

(Se) 82 103 He -1.765 N/A 35.557 2250

Sr 88 103 He 225.968 1.1 167308.773 11250

(Mo) 95 103 He 0.258 20.3 224.000 6750

Mo 98 103 He 0.268 3.9 369.343 6750

Ag 107 103 He -0.454 N/A 306.673 600

(Ag) 109 103 He -0.482 N/A 280.003 600

Cd 111 115 He 0.479 9.0 138.000 6750

(Cd) 114 115 He 0.453 2.6 329.333 6750

Name Mass ISTD Tune Mode Conc. Conc. RSD CPS LDR QC Flag

Sn 118 115 He 0.203 12.3 348.900 5400

Sb 121 115 He 0.008 107.5 33.337 5400

(Sb) 123 115 He 0.013 180.2 36.667 5400

Ba 137 115 He 1.850 9.6 506.010 11250

(Tl) 203 209 He -0.025 N/A 47.777 9000

Tl 205 209 He -0.027 N/A 113.333 9000

[Pb] 206 209 He 0.258 6.5 346.673 11250

[Pb] 207 209 He 0.253 17.6 298.897 11250

Pb 208 209 He 0.269 8.4 1408.933 11250

Th 232 209 He 0.141 9.1 713.357 4500

U 238 209 He 0.077 1.5 284.450 4500

QC ISTD Table

Name Mass Tune Mode CPS CPS RSD Ref CPS % Rec %QC Low %QC High QC Flag

Li (IS) 6 No Gas 208233.733 0.4 190968.166666667 109.04 30 150

Sc (IS) 45 No Gas 1345235.967 0.6 1216826.10333333 110.55 30 150

Rh (IS) 103 No Gas 2234401.323 1.1 2070097.26 107.94 30 150

Sc (IS) 45 H2 386065.710 0.9 330192.953333333 116.92 30 150

Rh (IS) 103 H2 81068.633 1.1 71284.46 113.73 30 150

115In 115 H2 473312.840 1.7 405267.2 116.79 30 150

Sc (IS) 45 He 112429.327 1.2 94674.3733333333 118.75 30 150

Rh (IS) 103 He 2093719.570 2.9 1876006.17333333 111.61 30 150

115In 115 He 162386.030 2.8 144409.67 112.45 30 150

Tb (IS) 159 He 157092.853 3.3 141797.306666667 110.79 30 150

Ho (IS) 165 He 155055.290 4.0 137651.08 112.64 30 150

Bi (IS) 209 He 1518606.397 2.9 1425412.13 106.54 30 150

Sample Name 180-153493-a-10-b @50

File Name 195SMPL.d

Data Path Name C:\Agilent\ICPMH\1\DATA\D30420A.b

4/20/2023 3:09:14 PMAcq Time

Sample Type Sample

Total Dilution 1.0000

Comment ---

ISTD Ref FileName 008CALB.d

PassSample QC Pass/Fial

PassISTD QC Pass/Fail

QC Analyte Table

Name Mass ISTD Tune Mode Conc. Conc. RSD CPS LDR QC Flag

Li 7 45 No Gas 939.688 0.4 1317744.170 3000

Be 9 45 No Gas -0.058 N/A 12.000 3600

Si 28 45 H2 75.216 7.0 2289.080 10000

Fe 56 45 H2 55.952 1.3 87041.040 625000

Se 78 45 H2 0.104 39.7 12.000 2250

(Sn) 118 115 H2 0.113 76.1 833.383 5400

Na 23 45 He 171869.972 1.7 28929165.517 625000

{Mg} 24 45 He 17154.572 2.3 1450184.390 625000

{Mg} 25 45 He 16997.661 2.0 212988.997 625000

Mg 26 45 He 17068.287 1.8 272609.703 625000

Al 27 45 He -0.071 N/A 95.333 225000

P 31 45 He -69.792 N/A 70.000 15000

K 39 45 He 7854.782 2.0 697487.300 625000

{Ca} 43 45 He 13691.465 0.5 3287.053 625000

Ca 44 45 He 12674.433 2.7 53290.630 625000

Ti 47 45 He -0.045 N/A 3.000 6750

V 51 45 He -0.018 N/A 55.557 11250

Cr 52 45 He -0.243 N/A 670.020 11250

(Cr) 53 45 He -0.339 N/A 87.780 11250

Mn 55 45 He 22.744 2.1 15956.540 22050

Co 59 103 He -0.013 N/A 68.890 6750

Ni 60 103 He 1.478 6.1 852.253 11250

(Cu) 63 103 He 0.942 2.5 1870.133 11250

Cu 65 103 He 1.046 7.6 948.923 11250

Zn 66 103 He 7.792 5.6 2024.600 11250

(Zn) 68 103 He 8.306 1.2 1615.653 11250

As 75 103 He -0.060 N/A 14.000 2250

(Se) 78 103 He 0.365 308.5 103.333 2250

(Se) 82 103 He -0.543 N/A 46.663 2250

Sr 88 103 He 151.628 2.4 125457.533 11250

(Mo) 95 103 He 0.224 2.9 227.333 6750

Mo 98 103 He 0.239 8.3 381.343 6750

Ag 107 103 He -0.482 N/A 283.340 600

(Ag) 109 103 He -0.493 N/A 291.117 600

Cd 111 115 He 0.103 25.8 37.000 6750

(Cd) 114 115 He 0.078 21.0 81.667 6750

Name Mass ISTD Tune Mode Conc. Conc. RSD CPS LDR QC Flag

Sn 118 115 He 0.095 116.8 313.340 5400

Sb 121 115 He 0.008 103.6 36.667 5400

(Sb) 123 115 He -0.008 N/A 26.667 5400

Ba 137 115 He 1.175 2.7 360.010 11250

(Tl) 203 209 He -0.036 N/A 38.887 9000

Tl 205 209 He -0.039 N/A 86.667 9000

[Pb] 206 209 He 0.203 5.8 327.783 11250

[Pb] 207 209 He 0.208 32.9 291.117 11250

Pb 208 209 He 0.224 6.1 1375.593 11250

Th 232 209 He 0.078 17.1 546.683 4500

U 238 209 He 0.050 12.7 208.893 4500

QC ISTD Table

Name Mass Tune Mode CPS CPS RSD Ref CPS % Rec %QC Low %QC High QC Flag

Li (IS) 6 No Gas 218768.180 1.5 190968.166666667 114.56 30 150

Sc (IS) 45 No Gas 1402827.480 0.9 1216826.10333333 115.29 30 150

Rh (IS) 103 No Gas 2350087.933 0.8 2070097.26 113.53 30 150

Sc (IS) 45 H2 412602.727 0.2 330192.953333333 124.96 30 150

Rh (IS) 103 H2 86441.523 0.5 71284.46 121.26 30 150

115In 115 H2 506496.623 3.0 405267.2 124.98 30 150

Sc (IS) 45 He 124712.290 1.2 94674.3733333333 131.73 30 150

Rh (IS) 103 He 2339643.030 3.6 1876006.17333333 124.71 30 150

115In 115 He 179969.073 1.9 144409.67 124.62 30 150

Tb (IS) 159 He 175098.300 2.0 141797.306666667 123.48 30 150

Ho (IS) 165 He 167976.767 3.0 137651.08 122.03 30 150

Bi (IS) 209 He 1683435.243 2.8 1425412.13 118.1 30 150

Sample Name 180-153493-a-11-b @50

File Name 196SMPL.d

Data Path Name C:\Agilent\ICPMH\1\DATA\D30420A.b

4/20/2023 3:12:51 PMAcq Time

Sample Type Sample

Total Dilution 1.0000

Comment ---

ISTD Ref FileName 008CALB.d

PassSample QC Pass/Fial

PassISTD QC Pass/Fail

QC Analyte Table

Name Mass ISTD Tune Mode Conc. Conc. RSD CPS LDR QC Flag

Li 7 45 No Gas 1066.680 1.5 1548481.790 3000

Be 9 45 No Gas -0.056 N/A 13.333 3600

Si 28 45 H2 68.587 2.6 2150.167 10000

Fe 56 45 H2 10.327 2.2 21935.423 625000

Se 78 45 H2 0.085 14.7 11.000 2250

(Sn) 118 115 H2 0.121 21.5 853.380 5400

Na 23 45 He 185805.683 1.1 29425407.717 625000

{Mg} 24 45 He 18783.096 1.2 1494239.387 625000

{Mg} 25 45 He 18653.103 0.4 219968.363 625000

Mg 26 45 He 18802.714 1.0 282578.453 625000

Al 27 45 He 0.479 108.4 106.000 225000

P 31 45 He -55.286 N/A 95.557 15000

K 39 45 He 8435.777 0.3 701759.573 625000

{Ca} 43 45 He 15537.133 2.4 3507.103 625000

Ca 44 45 He 13989.857 1.1 55323.517 625000

Ti 47 45 He -0.105 N/A 1.000 6750

V 51 45 He -0.025 N/A 45.557 11250

Cr 52 45 He -0.182 N/A 706.687 11250

(Cr) 53 45 He -0.305 N/A 87.777 11250

Mn 55 45 He 27.291 1.9 17998.890 22050

Co 59 103 He -0.010 N/A 70.000 6750

Ni 60 103 He 1.614 3.0 861.140 11250

(Cu) 63 103 He 1.049 3.6 1883.467 11250

Cu 65 103 He 1.161 3.7 960.040 11250

Zn 66 103 He 11.058 3.2 2608.027 11250

(Zn) 68 103 He 11.471 2.9 2021.263 11250

As 75 103 He -0.081 N/A 10.000 2250

(Se) 78 103 He -0.094 N/A 91.000 2250

(Se) 82 103 He 0.431 705.5 48.890 2250

Sr 88 103 He 166.235 0.5 127899.270 11250

(Mo) 95 103 He 0.251 1.1 228.000 6750

Mo 98 103 He 0.251 6.5 366.677 6750

Ag 107 103 He -0.516 N/A 197.783 600

(Ag) 109 103 He -0.514 N/A 232.227 600

Cd 111 115 He 0.022 26.9 11.000 6750

(Cd) 114 115 He 0.011 75.3 28.667 6750

Name Mass ISTD Tune Mode Conc. Conc. RSD CPS LDR QC Flag

Sn 118 115 He 0.200 17.0 358.897 5400

Sb 121 115 He 0.018 98.4 42.223 5400

(Sb) 123 115 He -0.013 N/A 22.220 5400

Ba 137 115 He 1.318 4.1 375.343 11250

(Tl) 203 209 He -0.048 N/A 21.113 9000

Tl 205 209 He -0.042 N/A 72.223 9000

[Pb] 206 209 He 0.228 8.3 331.120 11250

[Pb] 207 209 He 0.202 12.7 267.783 11250

Pb 208 209 He 0.236 6.9 1335.597 11250

Th 232 209 He 0.057 18.0 434.453 4500

U 238 209 He 0.057 10.8 222.227 4500

QC ISTD Table

Name Mass Tune Mode CPS CPS RSD Ref CPS % Rec %QC Low %QC High QC Flag

Li (IS) 6 No Gas 228555.563 1.0 190968.166666667 119.68 30 150

Sc (IS) 45 No Gas 1454466.540 1.7 1216826.10333333 119.53 30 150

Rh (IS) 103 No Gas 2435962.623 2.4 2070097.26 117.67 30 150

Sc (IS) 45 H2 419580.173 2.4 330192.953333333 127.07 30 150

Rh (IS) 103 H2 89006.477 1.7 71284.46 124.86 30 150

115In 115 H2 512254.463 3.4 405267.2 126.4 30 150

Sc (IS) 45 He 117360.997 2.1 94674.3733333333 123.96 30 150

Rh (IS) 103 He 2175086.717 0.3 1876006.17333333 115.94 30 150

115In 115 He 167803.490 0.7 144409.67 116.2 30 150

Tb (IS) 159 He 163053.823 1.1 141797.306666667 114.99 30 150

Ho (IS) 165 He 158836.550 1.7 137651.08 115.39 30 150

Bi (IS) 209 He 1577920.630 0.6 1425412.13 110.7 30 150

4/21/2023 11:19 AM

Sample Name 180-153493-a-12-b @50

File Name 197SMPL.d

Data Path Name C:\Agilent\ICPMH\1\DATA\D30420A.b

4/20/2023 3:16:30 PMAcq Time

Sample Type Sample

Total Dilution 1.0000

Comment ---

ISTD Ref FileName 008CALB.d

PassSample QC Pass/Fial

PassISTD QC Pass/Fail

QC Analyte Table

Name Mass ISTD Tune Mode Conc. Conc. RSD CPS LDR QC Flag

Li 7 45 No Gas 1004.334 2.3 1458419.373 3000

Be 9 45 No Gas -0.045 N/A 17.333 3600

Si 28 45 H2 68.676 2.5 2185.727 10000

Fe 56 45 H2 11.512 2.8 24018.663 625000

Se 78 45 H2 0.123 17.3 13.667 2250

(Sn) 118 115 H2 0.103 51.6 833.390 5400

Na 23 45 He 168438.678 1.4 27988706.110 625000

{Mg} 24 45 He 16679.163 0.9 1392072.513 625000

{Mg} 25 45 He 16494.711 0.9 204062.430 625000

Mg 26 45 He 16517.626 1.4 260446.380 625000

Al 27 45 He 0.847 101.0 122.667 225000

P 31 45 He -56.975 N/A 96.667 15000

K 39 45 He 7599.299 1.1 667629.507 625000

{Ca} 43 45 He 12888.994 2.2 3055.893 625000

Ca 44 45 He 12463.133 0.7 51738.357 625000

Ti 47 45 He 0.043 114.7 5.667 6750

V 51 45 He -0.017 N/A 55.557 11250

Cr 52 45 He -0.252 N/A 650.017 11250

(Cr) 53 45 He -0.324 N/A 88.890 11250

Mn 55 45 He 19.590 3.3 13580.787 22050

Co 59 103 He -0.009 N/A 76.667 6750

Ni 60 103 He 1.574 4.3 892.253 11250

(Cu) 63 103 He 1.009 6.4 1940.143 11250

Cu 65 103 He 1.044 5.1 935.593 11250

Zn 66 103 He 8.702 4.9 2210.180 11250

(Zn) 68 103 He 8.804 6.2 1678.993 11250

As 75 103 He -0.052 N/A 15.000 2250

(Se) 78 103 He 0.356 261.2 102.000 2250

(Se) 82 103 He -0.822 N/A 44.447 2250

Sr 88 103 He 148.288 1.1 120962.027 11250

(Mo) 95 103 He 0.244 14.4 237.333 6750

Mo 98 103 He 0.219 11.7 354.673 6750

Ag 107 103 He -0.503 N/A 236.673 600

(Ag) 109 103 He -0.514 N/A 245.557 600

Cd 111 115 He 0.080 14.7 29.333 6750

(Cd) 114 115 He 0.079 4.9 82.000 6750

Name Mass ISTD Tune Mode Conc. Conc. RSD CPS LDR QC Flag

Sn 118 115 He 0.067 32.1 292.223 5400

Sb 121 115 He -0.002 N/A 28.890 5400

(Sb) 123 115 He -0.015 N/A 22.223 5400

Ba 137 115 He 1.188 13.9 360.673 11250

(Tl) 203 209 He -0.037 N/A 36.667 9000

Tl 205 209 He -0.035 N/A 96.667 9000

[Pb] 206 209 He 0.215 27.0 334.450 11250

[Pb] 207 209 He 0.238 8.7 314.450 11250

Pb 208 209 He 0.248 9.2 1451.153 11250

Th 232 209 He 0.035 15.4 374.450 4500

U 238 209 He 0.048 12.7 197.783 4500

QC ISTD Table

Name Mass Tune Mode CPS CPS RSD Ref CPS % Rec %QC Low %QC High QC Flag

Li (IS) 6 No Gas 229344.027 0.5 190968.166666667 120.1 30 150

Sc (IS) 45 No Gas 1454097.790 1.7 1216826.10333333 119.5 30 150

Rh (IS) 103 No Gas 2414730.380 1.2 2070097.26 116.65 30 150

Sc (IS) 45 H2 425950.227 0.9 330192.953333333 129 30 150

Rh (IS) 103 H2 89761.087 1.2 71284.46 125.92 30 150

115In 115 H2 517473.097 2.9 405267.2 127.69 30 150

Sc (IS) 45 He 123122.163 0.2 94674.3733333333 130.05 30 150

Rh (IS) 103 He 2306209.213 1.4 1876006.17333333 122.93 30 150

115In 115 He 178207.240 1.2 144409.67 123.4 30 150

Tb (IS) 159 He 170559.600 1.7 141797.306666667 120.28 30 150

Ho (IS) 165 He 168245.590 1.3 137651.08 122.23 30 150

Bi (IS) 209 He 1658213.750 1.2 1425412.13 116.33 30 150

Sample Name 180-153493-a-13-b @50

File Name 198SMPL.d

Data Path Name C:\Agilent\ICPMH\1\DATA\D30420A.b

4/20/2023 3:20:08 PMAcq Time

Sample Type Sample

Total Dilution 1.0000

Comment ---

ISTD Ref FileName 008CALB.d

PassSample QC Pass/Fial

PassISTD QC Pass/Fail

QC Analyte Table

Name Mass ISTD Tune Mode Conc. Conc. RSD CPS LDR QC Flag

Li 7 45 No Gas 909.680 2.1 1370216.170 3000

Be 9 45 No Gas -0.050 N/A 16.000 3600

Si 28 45 H2 87.666 5.5 2756.940 10000

Fe 56 45 H2 38.049 0.7 64672.563 625000

Se 78 45 H2 0.063 25.0 9.920 2250

(Sn) 118 115 H2 0.106 99.8 850.053 5400

Na 23 45 He 191138.421 1.5 31148017.653 625000

{Mg} 24 45 He 20458.976 1.3 1674791.043 625000

{Mg} 25 45 He 20273.528 0.8 245999.573 625000

Mg 26 45 He 20532.801 0.4 317534.790 625000

Al 27 45 He 2.446 12.5 169.333 225000

P 31 45 He -52.962 N/A 103.330 15000

K 39 45 He 8508.346 0.9 727963.687 625000

{Ca} 43 45 He 15895.922 2.4 3692.703 625000

Ca 44 45 He 15131.782 1.5 61559.210 625000

Ti 47 45 He 0.069 56.3 6.333 6750

V 51 45 He -0.015 N/A 56.667 11250

Cr 52 45 He -0.145 N/A 774.470 11250

(Cr) 53 45 He -0.249 N/A 98.890 11250

Mn 55 45 He 22.488 1.1 15276.920 22050

Co 59 103 He -0.005 N/A 82.220 6750

Ni 60 103 He 2.754 3.6 1500.087 11250

(Cu) 63 103 He 1.122 1.0 2079.047 11250

Cu 65 103 He 1.182 6.5 1021.153 11250

Zn 66 103 He 9.933 3.8 2472.447 11250

(Zn) 68 103 He 9.349 4.6 1754.560 11250

As 75 103 He -0.031 N/A 18.000 2250

(Se) 78 103 He -0.129 N/A 95.000 2250

(Se) 82 103 He 4.646 63.4 75.557 2250

Sr 88 103 He 174.646 1.5 140888.543 11250

(Mo) 95 103 He 0.216 9.5 216.667 6750

Mo 98 103 He 0.231 3.9 363.343 6750

Ag 107 103 He -0.509 N/A 221.113 600

(Ag) 109 103 He -0.536 N/A 200.003 600

Cd 111 115 He 0.853 5.3 261.333 6750

(Cd) 114 115 He 0.842 2.3 639.683 6750

Name Mass ISTD Tune Mode Conc. Conc. RSD CPS LDR QC Flag

Sn 118 115 He 0.198 14.5 372.230 5400

Sb 121 115 He 0.006 343.0 34.443 5400

(Sb) 123 115 He 0.002 638.7 32.223 5400

Ba 137 115 He 1.304 4.2 386.677 11250

(Tl) 203 209 He -0.038 N/A 34.443 9000

Tl 205 209 He -0.039 N/A 84.443 9000

[Pb] 206 209 He 0.289 1.3 404.453 11250

[Pb] 207 209 He 0.272 7.3 338.897 11250

Pb 208 209 He 0.265 2.3 1501.153 11250

Th 232 209 He 0.023 43.6 324.450 4500

U 238 209 He 0.065 5.0 260.007 4500

QC ISTD Table

Name Mass Tune Mode CPS CPS RSD Ref CPS % Rec %QC Low %QC High QC Flag

Li (IS) 6 No Gas 235968.327 1.9 190968.166666667 123.56 30 150

Sc (IS) 45 No Gas 1506411.230 0.7 1216826.10333333 123.8 30 150

Rh (IS) 103 No Gas 2493332.410 0.9 2070097.26 120.45 30 150

Sc (IS) 45 H2 434973.073 1.2 330192.953333333 131.73 30 150

Rh (IS) 103 H2 90996.647 2.5 71284.46 127.65 30 150

115In 115 H2 524731.153 3.6 405267.2 129.48 30 150

Sc (IS) 45 He 120760.580 0.4 94674.3733333333 127.55 30 150

Rh (IS) 103 He 2280944.843 1.3 1876006.17333333 121.59 30 150

115In 115 He 174762.413 0.8 144409.67 121.02 30 150

Tb (IS) 159 He 169287.587 1.3 141797.306666667 119.39 30 150

Ho (IS) 165 He 166858.810 2.2 137651.08 121.22 30 150

Bi (IS) 209 He 1632764.620 1.1 1425412.13 114.55 30 150

Sample Name 180-153493-a-14-b @50

File Name 199SMPL.d

Data Path Name C:\Agilent\ICPMH\1\DATA\D30420A.b

4/20/2023 3:23:47 PMAcq Time

Sample Type Sample

Total Dilution 1.0000

Comment ---

ISTD Ref FileName 008CALB.d

PassSample QC Pass/Fial

PassISTD QC Pass/Fail

QC Analyte Table

Name Mass ISTD Tune Mode Conc. Conc. RSD CPS LDR QC Flag

Li 7 45 No Gas 1004.208 0.9 1506794.040 3000

Be 9 45 No Gas -0.063 N/A 10.667 3600

Si 28 45 H2 68.895 3.7 2213.510 10000

Fe 56 45 H2 3.611 4.9 12437.557 625000

Se 78 45 H2 0.068 77.1 10.093 2250

(Sn) 118 115 H2 0.080 19.1 800.043 5400

Na 23 45 He 222019.957 1.6 37700000.723 625000

{Mg} 24 45 He 22253.583 0.2 1898966.730 625000

{Mg} 25 45 He 21903.827 1.2 277121.030 625000

Mg 26 45 He 22057.075 0.4 355550.193 625000

Al 27 45 He 0.602 94.5 117.333 225000

P 31 45 He -55.934 N/A 101.113 15000

K 39 45 He 9757.020 1.2 863373.750 625000

{Ca} 43 45 He 18361.616 1.4 4442.913 625000

Ca 44 45 He 16918.379 0.9 71722.710 625000

Ti 47 45 He -0.065 N/A 2.333 6750

V 51 45 He -0.020 N/A 53.330 11250

Cr 52 45 He -0.234 N/A 686.687 11250

(Cr) 53 45 He -0.383 N/A 81.113 11250

Mn 55 45 He 34.474 1.5 24361.430 22050

Co 59 103 He 0.033 23.1 163.333 6750

Ni 60 103 He 3.466 3.8 1927.913 11250

(Cu) 63 103 He 1.038 6.1 2022.380 11250

Cu 65 103 He 1.175 6.0 1045.600 11250

Zn 66 103 He 10.147 1.5 2599.133 11250

(Zn) 68 103 He 10.572 7.9 2024.597 11250

As 75 103 He -0.081 N/A 10.667 2250

(Se) 78 103 He -0.383 N/A 94.667 2250

(Se) 82 103 He -0.037 N/A 50.000 2250

Sr 88 103 He 195.389 1.8 162389.007 11250

(Mo) 95 103 He 0.202 8.5 214.000 6750

Mo 98 103 He 0.224 3.5 366.677 6750

Ag 107 103 He -0.509 N/A 230.007 600

(Ag) 109 103 He -0.526 N/A 226.667 600

Cd 111 115 He 1.988 2.6 626.347 6750

(Cd) 114 115 He 2.016 3.9 1562.757 6750

Name Mass ISTD Tune Mode Conc. Conc. RSD CPS LDR QC Flag

Sn 118 115 He 0.132 21.4 343.343 5400

Sb 121 115 He 0.004 311.2 34.443 5400

(Sb) 123 115 He 0.008 131.0 37.780 5400

Ba 137 115 He 1.679 2.1 514.677 11250

(Tl) 203 209 He -0.020 N/A 61.113 9000

Tl 205 209 He -0.036 N/A 98.890 9000

[Pb] 206 209 He 0.273 12.3 402.230 11250

[Pb] 207 209 He 0.238 22.0 320.007 11250

Pb 208 209 He 0.263 5.6 1542.267 11250

Th 232 209 He 0.027 11.7 350.007 4500

U 238 209 He 0.063 10.1 265.560 4500

QC ISTD Table

Name Mass Tune Mode CPS CPS RSD Ref CPS % Rec %QC Low %QC High QC Flag

Li (IS) 6 No Gas 237547.680 1.6 190968.166666667 124.39 30 150

Sc (IS) 45 No Gas 1502283.833 1.8 1216826.10333333 123.46 30 150

Rh (IS) 103 No Gas 2482384.703 1.3 2070097.26 119.92 30 150

Sc (IS) 45 H2 430131.337 0.6 330192.953333333 130.27 30 150

Rh (IS) 103 H2 89475.960 1.2 71284.46 125.52 30 150

115In 115 H2 522587.527 3.6 405267.2 128.95 30 150

Sc (IS) 45 He 125886.713 3.5 94674.3733333333 132.97 30 150

Rh (IS) 103 He 2350693.517 4.7 1876006.17333333 125.3 30 150

115In 115 He 181777.330 3.6 144409.67 125.88 30 150

Tb (IS) 159 He 175355.127 5.6 141797.306666667 123.67 30 150

Ho (IS) 165 He 171555.853 5.4 137651.08 124.63 30 150

Bi (IS) 209 He 1691719.450 5.3 1425412.13 118.68 30 150

4/21/2023 11:20 AM

Sample Name 180-153493-a-15-b @50

File Name 200SMPL.d

Data Path Name C:\Agilent\ICPMH\1\DATA\D30420A.b

4/20/2023 3:27:26 PMAcq Time

Sample Type Sample

Total Dilution 1.0000

Comment ---

ISTD Ref FileName 008CALB.d

PassSample QC Pass/Fial

PassISTD QC Pass/Fail

QC Analyte Table

Name Mass ISTD Tune Mode Conc. Conc. RSD CPS LDR QC Flag

Li 7 45 No Gas 986.927 2.5 1588099.290 3000

Be 9 45 No Gas -0.059 N/A 13.333 3600

Si 28 45 H2 60.087 3.0 2104.603 10000

Fe 56 45 H2 0.455 19.6 8232.387 625000

Se 78 45 H2 0.055 68.4 9.840 2250

(Sn) 118 115 H2 0.122 84.9 930.057 5400

Na 23 45 He 249685.466 1.9 44962671.547 625000

{Mg} 24 45 He 26958.270 0.8 2439257.750 625000

{Mg} 25 45 He 26559.171 1.6 356192.333 625000

Mg 26 45 He 26716.699 0.8 456657.880 625000

Al 27 45 He 0.327 123.3 115.333 225000

P 31 45 He -50.406 N/A 120.000 15000

K 39 45 He 11685.915 0.9 1087168.880 625000

{Ca} 43 45 He 22036.486 0.9 5652.227 625000

Ca 44 45 He 21158.220 0.8 95024.657 625000

Ti 47 45 He -0.080 N/A 2.000 6750

V 51 45 He -0.009 N/A 70.000 11250

Cr 52 45 He -0.257 N/A 696.687 11250

(Cr) 53 45 He -0.276 N/A 104.443 11250

Mn 55 45 He 44.050 0.7 32984.960 22050

Co 59 103 He 0.198 17.2 518.903 6750

Ni 60 103 He 10.868 2.0 6205.797 11250

(Cu) 63 103 He 12.573 0.2 19850.267 11250

Cu 65 103 He 12.519 2.2 9623.220 11250

Zn 66 103 He 16.897 4.7 4414.030 11250

(Zn) 68 103 He 17.190 2.8 3348.180 11250

As 75 103 He -0.050 N/A 16.333 2250

(Se) 78 103 He -1.028 N/A 91.000 2250

(Se) 82 103 He -1.871 N/A 41.110 2250

Sr 88 103 He 241.535 1.0 210260.020 11250

(Mo) 95 103 He 0.246 9.8 254.000 6750

Mo 98 103 He 0.278 13.8 446.010 6750

Ag 107 103 He -0.513 N/A 231.117 600

(Ag) 109 103 He -0.536 N/A 216.670 600

Cd 111 115 He 130.485 1.4 42936.360 6750

(Cd) 114 115 He 128.940 1.1 103581.190 6750

Name Mass ISTD Tune Mode Conc. Conc. RSD CPS LDR QC Flag

Sn 118 115 He 0.043 46.9 296.673 5400

Sb 121 115 He 0.053 9.8 77.777 5400

(Sb) 123 115 He 0.031 107.5 54.443 5400

Ba 137 115 He 2.012 7.2 645.353 11250

(Tl) 203 209 He -0.037 N/A 38.887 9000

Tl 205 209 He -0.040 N/A 87.777 9000

[Pb] 206 209 He 0.304 6.9 455.567 11250

[Pb] 207 209 He 0.275 11.8 372.230 11250

Pb 208 209 He 0.290 6.3 1742.280 11250

Th 232 209 He 0.019 36.8 332.227 4500

U 238 209 He 0.043 14.8 193.337 4500

QC ISTD Table

Name Mass Tune Mode CPS CPS RSD Ref CPS % Rec %QC Low %QC High QC Flag

Li (IS) 6 No Gas 254502.270 0.5 190968.166666667 133.27 30 150

Sc (IS) 45 No Gas 1610861.070 0.9 1216826.10333333 132.38 30 150

Rh (IS) 103 No Gas 2662262.357 1.6 2070097.26 128.61 30 150

Sc (IS) 45 H2 458957.953 1.1 330192.953333333 139 30 150

Rh (IS) 103 H2 95333.747 2.3 71284.46 133.74 30 150

115In 115 H2 554975.080 2.9 405267.2 136.94 30 150

Sc (IS) 45 He 133480.497 1.1 94674.3733333333 140.99 30 150

Rh (IS) 103 He 2461698.653 2.9 1876006.17333333 131.22 30 150

115In 115 He 191369.260 3.0 144409.67 132.52 30 150

Tb (IS) 159 He 185741.447 2.9 141797.306666667 130.99 30 150

Ho (IS) 165 He 181927.443 3.3 137651.08 132.17 30 150

Bi (IS) 209 He 1774219.860 3.5 1425412.13 124.47 30 150

Sample Name CCV 5343245

File Name 202_CCV.d

Data Path Name C:\Agilent\ICPMH\1\DATA\D30420A.b

4/20/2023 3:34:45 PMAcq Time

Sample Type CCV

Total Dilution 1.0000

Comment ---

ISTD Ref FileName 008CALB.d

FailSample QC Pass/Fial

PassISTD QC Pass/Fail

QC Analyte Table

Name Mass ISTD Tune Mode Conc. Conc. RSD CPS LDR QC Flag

Li 7 45 No Gas 204.102 1.1 350877.167 200

Be 9 45 No Gas 208.911 1.1 92527.173 200

(B) 10 45 No Gas 553.213 2.7 26853.973 500 >+\-10%

B 11 45 No Gas 552.661 0.3 129297.783 500 >+\-10%

Si 28 45 H2 2102.491 1.7 64755.843 2000

Fe 56 45 H2 51529.955 1.7 86244209.907 50000

Se 78 45 H2 207.264 1.9 15643.143 200

(Sn) 118 115 H2 201.944 0.8 402649.550 200

Na 23 45 He 51545.258 0.4 9827656.833 50000

{Mg} 24 45 He 50333.792 0.9 4811936.753 50000

{Mg} 25 45 He 49960.638 2.1 708009.780 50000

Mg 26 45 He 50327.705 2.6 908983.717 50000

Al 27 45 He 50257.541 2.4 1798121.163 50000

P 31 45 He 2552.784 3.3 6561.487 2500

K 39 45 He 51809.766 1.1 4919091.053 50000

{Ca} 43 45 He 52924.922 2.1 14316.987 50000

Ca 44 45 He 51631.281 1.9 244601.327 50000

Ti 47 45 He 200.273 2.5 7124.063 200

V 51 45 He 198.103 2.0 237107.267 200

Cr 52 45 He 196.240 3.3 294143.453 200

(Cr) 53 45 He 194.375 3.3 35377.077 200

Mn 55 45 He 198.447 2.1 156652.903 200

Co 59 103 He 203.125 1.8 464698.453 200

Ni 60 103 He 202.057 0.8 123308.880 200

(Cu) 63 103 He 198.889 2.5 330707.183 200

Cu 65 103 He 198.483 1.9 161350.013 200

Zn 66 103 He 101.324 2.3 27655.267 100

(Zn) 68 103 He 117.828 2.1 23779.600 100 >+\-10%

As 75 103 He 202.895 1.8 36117.650 200

(Se) 78 103 He 207.217 2.5 3015.653 200

(Se) 82 103 He 202.626 4.3 1416.743 200

Sr 88 103…