Attachment B Appendix A Revision Dated 8 7 2012.pdf

ATTACHMENT B SP0600-12-R-0518 APPENDIX – A Dated August 7, 2012

MINIMUM REQUIREMENTS FOR STORAGE SAMPLING AND TESTING

SERIES

LOCATION OF

STOCKS

TYPE

STORAGE

WHEN

SAMPLED

TYPE

SAMPLE 1

TESTING

REQUIRED 2,4

REMARKS 9

1 Upon procurement at: refineries, blending installations, etc. and at main installations including national depots & ocean-importing points on establishment of new batches.

Bulk Before acceptance of new material and after establishment of new batch.

Upper, middle, and lower composite, or all-level composite from each storage tank.

A Samples shall be retained IAW solicitation, contract and/or QCP requirements.

2 / Storage tanks and pipelines, for Pipeline Shipments or Vessel Loadings of Government Stocks.

For all stock locations and operations, at the direction of the QAR, and with the concurrence of DLA- ENERGY-QA, additional sampling and testing maybe required as the conditions warrant.

2a Storage tanks Bulk Before shipment or loading

Upper, middle, and lower composite, or all-level composite from each storage tank.

Appearance, API gravity, color, flash point, particulate content, filtration time, FSII, water reaction (as applicable)

Government-owned stocks in tanks that have been tested previously within 90 days need only Type C. Referee sample will be retained.

3 Pipelines Bulk Before start of loading and after line pack operations

Line sample C for Dedicated Line.

B for Common Line

Test results should be within reproducibility of shipping tank

3a Pipelines Bulk Immediately after start of shipment or loading

Line sample, downstream of filter

C

3b Pipelines Bulk Hourly after starting shipment or loading

Line sample, downstream of filter

Visual, plus additive analysis for FSII & SDA, if line injected

3c Pipelines Bulk During Loading or Shipment

Representative line Composite IAW API MPMS, Chapters 8.1 or 8.2.

Retained composite Sample to be retained as Referee. Testing to be conducted will be based on the situation.

ATTACHMENT B SP0600-12-R-0518 APPENDIX – A Dated August 7, 2012

STOCKS

TYPE

STORAGE

WHEN

SAMPLED

TYPE

SAMPLE 1

4 Vessel loading

4a Tankers and barges First-In

Bulk After receipt of line displacement or 1 meter in tank whichever is greater

Spot C-plus Particulate if sample fails appearance, and additive analysis for FSII & SDA, if line injected

4b Tankers and barges Dock Pipeline

Bulk

Before Start of Loading/After Line Pack Operations

Line Sample C Test results should be within reproducibility of shipping tank.

4c Tankers and barges Bulk After loading All-level from each compartment

a. Appearance and density

b. C

c. Conductivity and FSII, as appropriate

a. For Government owned product only

b. Navy underway replenishment / fueling at sea

c. (Only) For procurement and government owned product where SDA and FSII additives are line injected, and ship’s composite fails SDA and FSII additives values.

(Test each compartment). For intermediate discharges, sample remaining compartments and retain till discharge at destination.

Volumetric composite of cargo tanks

B-1 Vessel may sail after “C” Tests;

Remainder of tests to be completed before arrival at next load or discharge port.

ATTACHMENT B SP0600-12-R-0518 APPENDIX – A Dated August 7, 2012

STOCKS

TYPE

STORAGE

WHEN

SAMPLED

TYPE

SAMPLE 1

4d Yard Oilers Bulk After Loading Volumetric composite of cargo tanks API, flash, BS&W

Normally yard oilers are in dedicated service and carry ships’ fuels.

5 Vessel discharge 5a Tankers and barges

(multi-product cargo) Bulk Prior to discharge All level from each tank C If on-spec, discharge authorized.

Volumetric composite of each cargo on board.

B-1 These tests will be performed prior to or during discharge of cargo. In the event the capability for testing does not exist at the discharge point, a composite sample from the vessel will be retained, type B-1 tests performed on an all-level sample taken from the receiving tank. If receiving tank fails spec requirements, perform B-1 tests on the tanker retain composite sample to determine the cause of the off-spec problem.

5b Dock/discharge manifold header

Bulk During discharge a. Sample IAW API MPMS, Chapter 8, commencing one half hour after start of discharge and each hour after until completion of the discharge.

One-half quart to be taken each time.

Sample to be composited after completion of discharge.

b. Also, USG at one hour, midpoint, and one hour prior to completion.

a. Particulate and Retained composite

b. Particulate 3

a. Retained for referee tests.

b. For barge receipts directly into A.F.

bases, refer to agreement of minimum standards.

5c After receipt of fuel by waterborne transport.

Bulk After receipt of fuel.

Upper, middle, and lower composite, or all-level Composite. (from each storage tank)

Type B-1 Also, Thermal Oxidation Stability testing after turbine fuel receipt by tanker.

5d Shipboard JP-5 De-fuels for return to Defense Working Capital Fund inventory

Bulk Before Discharge Upper, middle, and lower composite or all-level composite (from each storage tank).

Type B-1 plus thermal oxidation stability testing

ATTACHMENT B SP0600-12-R-0518 APPENDIX – A Dated August 7, 2012

STOCKS

TYPE

STORAGE

WHEN

SAMPLED

TYPE

SAMPLE 1

5e Shipboard F-76 De-fuels for return to Defense Working Capital Fund inventory

Bulk Before Discharge Upper, middle, and lower composite or all-level composite (from each storage tank).

Type B-1

Pipeline/TC/TT receipts.

During pipeline receipt

Bulk During receipt at custody transfer point

Representative Line sample, IAW API MPMS, Chapter 8 (5 gallon minimum)

Retain sample for 45 days.

Retained sample to be used as referee sample if testing of receipt tank fails.

After receipt of fuel via multi product pipeline

Bulk After receipt of fuel Upper, middle, and lower composite, or all-level composite. (from each storage tank)

Type B-1

TC/TT receipt Bulk Prior to discharge Representative sample from each compartment

Visual

TC/TT receipt Bulk During receipt at custody transfer point

Line sample, after line displacement

Type C 11 First TC/TT of the day will sampled from each supplier or new batch.

After receipt of fuel via a dedicated mode.

Bulk After receipt of fuel. Upper, middle, and Lower composite, or all-level composite. (from each storage tank)

Type C, except on initial filling or change of grade then, B-1 is required.

Transfers within installation or depot

Receiving Tank: Through a dedicated system.

Installations and Depots

After receipt of fuel Upper, middle, and lower composite, or all-level composite.

Type C Samples will be retained for 45 days for referee purposes.

Through a common system. Installations and Depots

After receipt of fuel. Upper, middle, and lower composite, or all-level composite.

Type B-1 Samples will be retained for 45 days for referee purposes.

ATTACHMENT B SP0600-12-R-0518 APPENDIX – A Dated August 7, 2012

STOCKS

TYPE

STORAGE

WHEN

SAMPLED

TYPE

SAMPLE 1

7c Receiving Tank/Initial fill or Product Conversion

Installations and Depots

Initial fill or product conversion/

Upper, middle, and lower composite, or all- level composite

Type B-1

8 Long term storage wherever located.

Bulk Periodically, as required by Table VIII.

Upper, middle, and lower composite or all-level composite (see remarks).

B-2 or A (see remarks)

a. Separate samples; upper, middle, and lower shall be taken and tested to establish homogeneity. If homogenous these samples shall be mixed for required tests. If not, perform B-2 tests on each level of product.

b. Additional tests may be performed at the discretion of the owning or custodial authority, with regard to type of product, age of stock, conditions of storage, etc..

9 Filling Points for road and rail tank car containers, or other equipment.

Bulk Daily on first container filled, and on changeover to fresh feed tank after comple-tion of line displacement from the fresh feed tank.

Line sample, downstream of filter

Type C

9 Filling Points for road and rail tank car containers, or other equipment.

Bulk Daily on first container filled, and on changeover to fresh feed tank after comple-tion of line displacement from the fresh feed tank.

Line sample, downstream of filter

Type C

10 In rail tank cars, Inter-Modal Containers (ISO-Containers), and road tank vehicles and refuelers used in over the road transportation

Bulk Both after loading and before discharge

All level sample from the rail car or vehicle.

Appearance on each compartment Type C on composite

Note 5 – Road vehicles with multi-compartments shall have sample obtained (proportional) from each compartment sufficient to permit a quart sample. If product contains additives (FSII and /or SDA), which have been line injected, then each mode of transportation shall be tested for FSII.

ATTACHMENT B SP0600-12-R-0518 APPENDIX – A Dated August 7, 2012

STOCKS

TYPE

STORAGE

WHEN

SAMPLED

TYPE

SAMPLE 1

REMARKS9

11 Tanks containing interface mixtures from pipeline for re-injection.

Bulk Before re-injection Upper, middle, and lower composite, or all-level composite.

Type B-3 Re-injection of interface product is to be under the technical control of the pipeline authority, or IAW with O.A.

12 Packaged fuel stocks wherever stored

Packaged (a) Periodically as required by Table VIII.

(see remark)

(b) When contamination or deterioration of product is suspected.

(c) When identity is uncertain.

Representative sample IAW API MPMS, Chapter 8

Type B-2 6 Where an agreed inspection period has not been stipulated the product is to be inspected at least annually.

13 Refueler trucks, skid mounted refuelers, or other dispensing equipment.

Note: If the product is Capitalized these instructions are to be followed. If the product is non Capitalized then individual service technical guidance is to be followed.

Bulk (a) Daily

(b) Monthly 7

(a) Drain sample taken from sump.

(b) Line sample, downstream of filter. After re-circulation of fuel.

See remarks (a) Check for (visual) color and appearance.,

(b) Laboratory analyses for water & Sediment10

14 Collapsible fabric tanks (bags) and drums on the establishment of tactical refueling systems.

followed. If the product is non Capitalized then individual service technical guidance is to be followed.

Bulk (a) Initial fill and before issue

(b) Daily - before issue

(c) Monthly 7

(a) After the filter-separator

(b) After filter-separator.

Note: After re-circulation of fuel prior to the first refueling of the day.

(c) After filter separator

See Remarks (a) API, visual check for appearance, water, sediment and fiber (Aqua-Glo or AEL and filter membrane color rating for turbine fuels)

(b) Visual check for color, appearance, free water (Aqua- Glo or AEL for Turbine Fuels)and particulates (AEL or equivalent)

(c) Laboratory analysis for water and sediment. 10

ATTACHMENT B SP0600-12-R-0518 APPENDIX – A Dated August 7, 2012

11. For aviation delivery, FSII and SDA will be tested where capability exists.

STOCKS

TYPE

STORAGE

WHEN

SAMPLED

TYPE

SAMPLE 1

REQUIRED 2

REMARKS

Collapsible fabric tanks (bags) and drums used for wholesale and retail other than series 13 above (Aviation and Ground fuel) followed. If the product is non Capitalized then individual service technical guidance is to be followed.

Bulk (a) Initial fill-before issue-Note: after recirculation of fuel

(b)Daily-before use, Note: after recirculation of fuel prior to the first refueling of the day.

(c)Monthly7

(a)After the filter-separator

(b)After the filter-separator

(c)After the filter-separator

(b) C and

(c) See

(b) Aviation Turbine Fuels containing additives be checked for FSII and conductivity.

(c) Laboratory analysis for sediment and water. 10

NOTES:

1. Use the API MPMS for sampling methods (see 4.7).

2. See Tables X through XXII for the types of test required on the various products. The legend for the types of testing required is as follows:

a. Type “A” Test - Complete specification, Water separation index, modified, testing is not performed if the fuel contains conductivity additive (DO NOT PERFORM DOWNSTREAM

OF SDA INJECTION.

b. Type “B-1” Test - Partial analysis comprising the checking of principal characteristics most likely to have been affected in the course of moving the product.

c. Type “B-2” Test - Partial analysis to check characteristics susceptible to deterioration because of age.

d. Type “B-3” Test - Partial analysis for contamination; in particular, for controlling the return (or reintroduction) of pipeline interface products.

e. Type “C” Test – Quick, simple, partial analysis for verification of product quality, to ensure that no change has taken place.

3. The average particulate content of the 3 fuel samples should not exceed 2 mg/L; however, the first and last samples are obtained under severe discharge conditions they may show high particulate content. Solid contamination while extremely objectionable is a physical contaminant which can be removed under proper conditions with proper equipment, and since the product at this point is Government owned, discharge operations will not be discontinued for this reason. However, the contracting officer, DLA Energy, and the Quality Assurance Representative at the loading point will be advised of any high particulate results obtained. This information will be used for future planning purposes and for determining possible cleaning actions necessary on the vessel involved. This note is not applicable to internal Navy transfers.

4. Flash Point at the receiving point is not required for product that is to be use by the U.S. Army. This fuel is tested in accordance with Army quality surveillance program AR 710-2.

5. If unable to take an all-level sample from the compartment prior to discharge, then take an in-line sample at or near the off-loading header during the discharge, immediately upon product displacement of the receipt manifold/hose.

6. No receiving tests are necessary on packaged products, provided the containers are intact and markings adequately identify the product.

7. Filter-separator performance is to be checked every 30 days.

8. For retaining of samples (storage) see E28 Contractor Inspection Responsibilities.

9. Testing maybe complete specification testing or an individual test based on the request of the Government Representative.

10. When laboratory tests of material from dispensing and handling equipment show evidence of free water or a sediment level exceeding 0.5 mg/L for aviation fuels (2.0 mg/L for U.S. Army and U.S. Navy), or 10.0 mg/L for diesel fuel, that equipment shall be re-sampled and dead lined pending laboratory confirmation of the initial results. If the second laboratory analysis confirms the presence of free water or sediment exceeding the above limits, improvement in fuel quality must be made.

ATTACHMENT B SP0600-12-R-0518 APPENDIX – A

Testing Required, Aviation Turbine Fuel (JP-5, JP-8, Jet A, Jet A-1, TS-1)

PROPERTIES B-1 TEST B-2 TEST B-3 TEST C TEST

Appearance 1 X X X X Color (visual) X X X X Density or API gravity X X X X Particulate matter X X X Distillation X X X Copper strip corrosion X X X Freezing point X X X Existent gum X X X Vapor pressure (JP-4 only) X X X Flash point (except JP-4) X X X X Water reaction 6 X X X Lead content (If contaminated with leaded fuels suspected) X X X Fuel system icing inhibitor 2 X X X Filtration time X X X Water separation index 3, 4 X X X Conductivity (JP-4 and JP-8) 5 X X X Thermal stability (B-1 requirement applies only to JPTS and marine mode receipt tank sample) X X

Color (Saybolt) X Acid number X

NOTES:

1 Obtain sample in a clear round one quart glass bottle, swirl the bottle vigorously so a vortex is formed. Visually check for sediment at the point of the vortex. If sediment is visible, an investigation is necessary in order to determine the source of the contaminant (a spot larger than 3 mm diameter indicates corrective action may be required to prevent the delivery of contaminated fuel).

2 If product contains FSII, product should be check on delivery into a bulk storage tank and every month thereafter if stock remains dormant, and no deliveries have been made into the tank.

3 If the capability does not exist to perform this test at the terminal, a sample will be sent to the nearest Service laboratory that does have the capability. In the event operational necessity dictates issue of product before results are obtained from the Service laboratory, shipments may be made, however, when laboratory results indicate failure, notify DLA-ENERGY-QA.

4 Water separation index, modified, testing is not performed if the fuel contains conductivity additive.

5 If fuel contains conductivity additive, CU readings should be taken within two minutes of sampling.

6 Not performed on JP-5.

ATTACHMENT B SP0600-12-R-0518 APPENDIX – A

Tests required F-76, diesel fuels and kerosene.

PROPERTIES B-1 TEST B-2 TEST B-3 TEST C TEST

Appearance 1 X X X X Color X X X X Density and API gravity X X X X Distillation X X Flash point X X X X Carbon residue 2

(F-76 only)

X

Cloud point X Pour point X Copper strip corrosion X Cetane index X3 Viscosity X Water & sediment by centrifuge X Particulate (F-76 only)

Storage stability (F-76 only) X Sulfur 4,5,6 X

NOTES:

1 For NATO F-76, if the sample has no visible particulates, but is otherwise not clear and bright per ASTM D 4176, procedure 1, then the product must meet the requirements of ASTM D 2709, 0.05 percent volume of water and sediment, maximum. The fuel is acceptable for appearance if the water and sediment content is 0.05 percent volume or less. If the sample fails ASTM D 4176, procedure 1, because it contains visible sediment or particulate matter, but meets the requirement of 10 mg /L, maximum, in accordance with ASTM D 5452 or ASTM D 6217, then the fuel shall be considered acceptable provided all other requirements are met.

2 Only required if change in color and/or density occurs after procurement.

3 Cetane Index can only be run if no ignition improvers are present. Otherwise, Cetane number shall be given.

4 Kerosene. Grade No.-1K only, if intended for non-flue connected burner.

5 Test to be performed if equipment is available.

6 Sulfur testing is required for ULSD or LSD believed contaminated with a higher sulfur content fuel.

Type B-2 tests for Fuels System Icing Inhibitor (FSII)

CHARACTERISTICS SPECIFICATION

MIL-DTL-85470

Relative density X Color X Appearance / workmanship X Acidity X pH X Water content X Minimum retest frequency (months) 18 Visual check frequency (months)

1 1

NATO numbers S-1745 Note:

1 One month after receipt