Attachment 2 Appendix A revised 4 10 12.pdf

MINIMUM REQUIREMENTS FOR STORAGE SAMPLING AND TESTING

ATTACHMENT B SP0600-12-R-0518 APPENDIX – A

LOCATION OF

STOCKS

T Y

PE

ST

O

R A

G E

WHEN SAMPLED TYPE SAMPLE

(SEE NOTE 1)

TESTING

REQUIRED

(SEE NOTE 2 &

4)

REMARKS (SEE NOTE 5)

1/ Storage Tanks and Pipelines, for Pipeline Shipments or Vessel Loading of Government Stocks.

For all stock locations and operations, at the discretion of the QAR, and with DESC-QA concurrence, additional sampling and testing may be requested as conditions warrant.

1a Storage tanks Bulk Before Shipment or Loading and or receipts

Upper, Middle and Lower Composite or All-Level Composite from each storage tank.

Appearance, API Gravity, Color, Flash Point, Particulate Content, Filtration Time, FSII, Water Reaction (as applicable)

Government-owned stocks in tanks which have been tested previously within 90 days need only Type C.

Referee sample will be retained.

2/ Dock Pipeline Bulk Before Start of Loading/After Line Pack Operations

Line Sample C Test results should be within reproducibility of shipping tank.

2a Pipelines Bulk Immediately after Start of Shipment or Loading

Line Sample C

2b Pipelines Bulk Hourly After Starting Shipment or Loading

Line Sample Visual

2c Pipelines Bulk During Loading or Shipment

Representative Line Composite IAW API MPMS, Chapters 8.1 or 8.2.

Retained Composite Sample to be retained as Referee.

Testing to be conducted will be based on the situation.

3/ Vessel Loading

3a Tankers and Barges First-In

Bulk After receipt of line displacement or 1 meter in the tank which ever is greater

Spot C-Plus Particulate if Sample fails appearance

First in quanity may vary at the direction of the QAR, as warranted by quality concerns.

3b Tankers and Barges Bulk After Loading All-Level from each compartment a. Appearance & Density [For

CONSOL: C]

b. Conductivity and Fuel System Icing Inhibitor, as appropriate

a. For Government Owned Product Only

b. For Procurement and GOP, when SDA and FSII additives are line injected, and ship’s composite fails SDA and FSII additives values. (test

ATTACHMENT B SP0600-12-R-0518 APPENDIX – A

LOCATION OF

STOCKS

T

R A

G E

WHEN SAMPLED TYPE SAMPLE

(SEE NOTE 1)

TESTING

REQUIRED

(SEE NOTE 2 &

4)

REMARKS (SEE NOTE 5)

each compartment) For intermediate discharges, sample remaining compartments and retain till discharge at destination.

Volumetric Composite of Cargo Tanks B-1 Vessel may sail after “C” Tests;

Remainder of tests to be completed before arrival at next Load or Discharge Port.

3c Yard Oilers Bulk After Loading Volumetric Composite of Cargo Tanks API, Flash, BS&W Normally Yard Oils are in dedicated service and carry ships’ fuels.

4/ Vessel Discharge

4a Tankers and Barges (Multi-Product Cargo)

Bulk Prior to Discharge All Level from each Tank

Appearance and density

If on-spec, discharge authorized.

Volumetric Composite of Each Cargo on board.

B-1 These tests will be performed prior to or during discharge of cargo. In the event the capability for testing does not exist at the discharge point, a composite sample from the vessel will be retained, type B-1 tests performed on an all-level sample taken from the receiving tank. If receiving tank fails spec requirements, perform B-1 tests on the tanker retain composite sample to determine the cause of the off-spec problem.

Tankers and Barges (Single-Product Cargo)

Bulk Before Discharge Composite sample of ship or barge tanks.

Type C Discharge is authorized after conformance with Type C tests. Retain composite sample until the receiving tank analysis is complete. If product fails, perform Type B-1 tests on retained composite to help determine the cause of the off-specification problem.

ATTACHMENT B SP0600-12-R-0518 APPENDIX – A

LOCATION OF

STOCKS

T

R A

G E

WHEN SAMPLED TYPE SAMPLE

(SEE NOTE 1)

TESTING

REQUIRED

(SEE NOTE 2 &

4)

REMARKS (SEE NOTE 5)

4b Dock/Discharge Manifold Header

Bulk During discharge Sample IAW API MPMS, Chapter 8, commencing one half hour after start of discharge and each hour after until completion of the discharge. One- half quart to be taken each time. Sample to be composited after completion of discharge.

Also, one gallon at one hour, midpoint and one hour prior to completion.

Retained Composite, Particulate

Retained for Referee Tests.

For barge receipts directly into A.F.

bases, refer to agreement of minimum standards

Dock/Discharge Manifold Header

During Discharge For split cargo discharges where one product is JP5 or F76 and other product is JP8, JP4, MOGAS or AVGAS, a dock header sample will be taken during discharge of the JP5 or F76 one half hour after start of discharge and hourly thereafter.

Flash Point

4c Receiving Tank:

After receipt of fuel by waterborne transport.

Bulk After receipt of fuel. Upper, Middle and Lower Composite or All-Level Composite.(from each storage tank)

Type B-1 Also, JFTOT after turbine fuel receipt by tanker

5/ Pipeline Receipts.

5a Pipeline receipts Bulk During receipt Representative Line Composite IAW API MPMS, Chapters 8.1 or 8.2 prior to tank entry

Sample to be retained as Referee.

Testing to be conducted will be based on the situation.

5b Receiving Tank:

After receipt of fuel by pipeline systems used for more than one product.

Bulk After Receipt of Fuel Upper, Middle and Lower Composite or All-Level Composite. (from each storage tank)

Type B-1

ATTACHMENT B SP0600-12-R-0518 APPENDIX – A

LOCATION OF

STOCKS

T

R A

G E

WHEN SAMPLED TYPE SAMPLE

(SEE NOTE 1)

TESTING

REQUIRED

(SEE NOTE 2 &

4)

REMARKS (SEE NOTE 5)

5c Receiving Tank:

After receipt of fuel through a dedicated system.

Bulk After receipt of fuel. Upper, Middle and Lower Composite or All-Level Composite. (from each storage tank)

Type C, except on initial filling or change of grade.

Then, B-1 would be required.

6/ Transfers within Installation or Depot

6a Receiving Tank:

Through a dedicated system.

In st al la tio ns an d D ep ot s

After receipt of fuel Upper, Middle and Lower Composite or All-Level Composite.

Type C Samples will be retained for 45 days for referee purposes.

7 Dormant Stocks wherever Located.

Bulk Minimum testing frequency 6 months

Upper, Middle and Lower Composite or All-Level Composite. (see Remarks)

B-2 or A (see Remarks b.)

a. Separate samples; upper, middle and lower, shall be taken and tested to establish homogeneity. If homogenous, these samples shall be mixed for required tests. If not homogeneous, perform a B-2 on each layer of product.

Additional testing may be performed.

b. At the discretion of the owning or custodial authority, having regard to type of product, age of stock, conditions of storage, etc.

8 Filling Points for road and rail tank car containers or other equipment.

Bulk Daily on first container filled and on changeover to fresh feed tank after completion of line displacement from the fresh feed tank.

Line sample, downstream of filter. Type C

ATTACHMENT B SP0600-12-R-0518 APPENDIX – A

LOCATION OF

STOCKS

T

R A

G E

WHEN SAMPLED TYPE SAMPLE

(SEE NOTE 1)

TESTING

REQUIRED

(SEE NOTE 2 &

4)

REMARKS (SEE NOTE 5)

9 In rail tank cars and road tank vehicles and refuelers used in over the road transportation

Bulk Both after loading and before discharge

All level sample from the rail car or vehicle.

Appearance on each compartment Gravity/Density on composite

If product contains additives (FSII and/or SDA) which have been line injected, then each mode of transportation shall be tested for FSII and/or SDA.

10 Refueler trucks, skid mounted refuelers or other dispensing equipment.

Bulk (a) Daily

(b) Monthly

Line sample, downstream of filter.

Note: After recirculation of fuel prior to the first refueling of the day.

(see Remarks and Note 3)

(a) Visual check for appearance and Water & Sediment.

(b) Lab analyses for Water & Sediment

11 Individual Tests as directed by the responsible Quality Office

Bulk As directed by responsible Quality Office

As directed by responsible Quality Office

Up to and including Type A (see Remarks)

Test for Sulfides in Water shall be performed IAW clause E34 (Tests for Sulfides in Water) QAR to periodically witness water draining and if water is present and is of a brownish-greenish tint, then perform sulfides test.

LEGEND

Type “A” Test Complete specification inspection tests.

Type “B-1” Test Partial analysis comprising the checking of principal characteristics most likely to have been affected in the course of moving the product Type “B-2” Test Partial analysis to verify characteristics susceptible to deterioration because of age.

Type “B-3” Test Partial analysis for contamination; in particular, for controlling the re-injection of pipeline interface products Type “C” Test Specific Gravity, Flash Point, Color and Appearance, including visible sediment and water.

Note (1) The methods of sampling to be used are those prescribed by API (MPMS Chapter 8.1, Standard Practice for Manual Sampling of Petroleum and

Petroleum Products) Note (2) Where flash point tests are required, a vessel composite(s) shall be run in lieu of each individual tank.

Note (3)

The average particulate content of the 3 fuel samples should not exceed 8 mg/gal (2 mg/L); however, the first and last samples are obtained under severe discharge conditions and may show high particulate content. Solid contamination while extremely objectionable is a physical contaminant which can be removed under proper conditions with proper equipment and since the product at this point is Government owned, discharge operations will not be discontinued for this reason. The Contracting Officer, Defense Energy Support Center and the Quality Assurance Representative at the loading point will be advised, however, of any high particulate results obtained, for future planning purposes and possible cleaning action necessary to the vessel involved. This note is not applicable to internal Navy transfers.

Note (4) Testing maybe to complete specification testing or individual test based on request of the government representative.

Note (5) For retaining of samples (storage) see E28 Contractor Inspection Responsibilities.

ATTACHMENT B

SP0600-12-R-0518 APPENDIX – A

Testing Required, Aviation Turbine Fuel (JP-5, JP-8, Jet A, Jet A-1, TS-1)

PROPERTIES

B-1

TEST

B-2

TEST

B-3

TEST

C

TEST

Water and Solids (Visual) 1 X X X X Color (Visual) X X X X Specific or API Gravity X X X X Solids (Millipore) X X X Distillation X X X Copper Strip Corrosion X X X Freezing Point X X X Existent Gum X X X Flash Point X X X X Water Reaction (JP8 and JET A/A1 only) X X X Lead Content (If contamination with leaded fuels suspected) X X X Fuel System Icing Inhibitor X X X Filtration Time (JP8) X X X Water Separation Index (JP8) 2, 3 X X X Conductivity (JP8) 4 X X X Thermal Stability X Color (Saybolt) X Acid Number X

NOTES

1. Clean and bright and free of non-dissolved water. Obtain sample in a clear round one quart glass bottle, swirl the bottle vigorously so a vortex is formed. Visually check for sediment at the point of the vortex. If sediment is visible, a spot larger than 3 mm in diameter indicates corrective action should be taken to prevent the delivery of contaminated fuel.

2. If the capability does not exist to perform this test at the terminal, a sample will be sent to the nearest service laboratory that does have the capability. In the event operational necessity dictates issue of product before results are obtained from the service laboratory, shipments may be made;

however, when laboratory results indicate failure on a recurring basis, notify COR.

3. Water separation index, modified, testing is not performed if the fuel contains conductivity additive (SDA).

4. If fuel contains conductivity additive (SDA), conductivity readings should be taken within two minutes of sampling.

Tests required F-76, diesel fuels and kerosene.

PROPERTIES B-1 TEST B-2 TEST B-3 TEST C TEST

Appearance 1 X X X X Color X X X X Density and/or API gravity X X X X Distillation X X Flash point X X X X Carbon residue 2 (A-A-52557 and F-76 only)

X

Cloud point X Pour point X Copper strip corrosion X Cetane index X3 Viscosity X Water & sediment by centrifuge X

(A-A-52557 and F-76 only)

Storage stability (F-76 only) X Sulfur 4,5,6 X

NOTES:

1 For NATO F-76, if the sample has no visible particulates, but is otherwise not clear and bright per ASTM D 4176, procedure 1, then the product must meet the requirements of ASTM D 2709, 0.05 percent volume of water and sediment, maximum. The fuel is acceptable for appearance if the water and sediment content is 0.05 percent volume or less. If the sample fails ASTM D 4176, procedure 1, because it contains visible sediment or particulate matter, but meets the requirement of 10 milligrams per liter, maximum, in accordance with ASTM D 5452 or ASTM D 6217, then the fuel shall be considered acceptable provided all other requirements are met.

2 Only required if change in color and/or relative density occurs after procurement.

3 Cetane Index can only be run if no ignition improvers are present. Otherwise, Cetane number shall be given.

4 Kerosene. Grade No.-1K only, if intended for non-flue connected burner.

5 Test to be performed if equipment is available.

6 Sulfur testing is required for ULSD or LSD believed contaminated with a higher sulfur content fuel.

Type B-2 tests for Fuels System Icing Inhibitor (FSII)

CHARACTERISTICS SPECIFICATION

MIL-DTL-85470

Relative density X Color X Appearance / workmanship X Acidity X pH X Water content X Minimum retest frequency (months) 12 NATO numbers S-1745

Tests required F-76, diesel fuels and kerosene.