AMENDMENT 0005 - Soil Boring Environmental Sample Results.pdf

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Design-Bid-Build (DBB), Building 633 River Water Cooling System, Philadelphia Naval Business Center (PNBC), Philadelphia, PA
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N4008520R0079
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This is a solicitation for a design-build-build contract opportunity from the Department of the Navy Naval Facilities Engineering Command. The solicitation is for the replacement of an aging 77-year old river water cooling system at the Philadelphia Naval Business Center in Philadelphia, Pennsylvania. The project will replace the existing 50,000 gallon per minute system with a new 8,200 gallon per minute cooling tower capable of rejecting up to 75 million British Thermal Units per hour of heat. The new cooling water system must be able to reliably supply up to 8,200 gallons of cooling water per minute on demand to support research, development, testing and evaluation activities performed at Building 633, including testing of the Columbia Class Program Integrated Power System.

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Ref O CTF COVID-19 Screening Questionnaire_REV2_2020.07.06.pdf PDF
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COVID-19 Building Access and Badge Instructions_2020-11-20.docx DOCX document
Ref B TD_CO VISIT APPROVALS _REVISED_5_13_20.xlsx XLSX spreadsheet
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TABLE 1

SUMMARY OF LABORATORY RESULLTS

PHILADELPHIA NAVY YARD

Building 633 Cooling Tower

CT-1 1-5' CT-2 1-5'

10/25/2018 10/25/2018

Petroleum Hydrocarbons

TPH-GRO ug/kg ND (10600) ND (11700)

TPH-DRO mg/kg 90.6 20.0

BTEX

Benzene ug/kg ND (53.1) ND (58.4)

Toluene ug/kg ND (53.1) ND (58.4)

Ethylbenzene ug/kg ND (53.1) ND (58.4)

Total Xylenes ug/kg ND (159) ND (175)

TCLP Volatile Organic Compounds

Benzene ug/L ND (20.0) ND (20.0)

2-Butanone ug/L ND (200) ND (200)

Carbon Tetrachloride ug/L ND (20.0) ND (20.0)

Chlorobenzene ug/L ND (20.0) ND (20.0)

Chloroform ug/L ND (20.0) ND (20.0)

1,2-Dichloroethane ug/L ND (20.0) ND (20.0)

1,1-Dichloroethene ug/L ND (20.0) ND (20.0)

Tetrachloroethene ug/L ND (20.0) ND (20.0)

Trichloroethene ug/L ND (20.0) ND (20.0)

Vinly Chloride ug/L ND (20.0) ND (20.0)

TCLP Metals

Arsenic mg/L ND (0.14) ND (0.14)

Barium mg/L ND (2.8) ND (2.8)

Cadmium mg/L ND (0.011) ND (0.011)

Chromium mg/L ND (0.028) ND (0.028)

Lead mg/L 0.62 2.3

Mercury mg/L ND (0.0020) ND (0.0020)

Selenium mg/L ND (0.11) ND (0.11)

Silver mg/L ND (0.022) ND (0.022)

TCLP Semi-Volatile Organic Compounds mp-Cresol ug/L ND (60.0) ND (60.0) o-Cresol ug/L ND (60.0) ND (60.0)

1,4-Dichlorobenzene ug/L ND (60.0) ND (60.0)

2,4-Dinitrotoluene ug/L ND (60.0) ND (60.0)

Hexachlorobenzene ug/L ND (60.0) ND (60.0)

Hexachlorobutadiene ug/L ND (60.0) ND (60.0)

Hexachloeoethane ug/L ND (60.0) ND (60.0)

Nitrobenzene ug/L ND (60.0) ND (60.0)

Pentachlorophenol ug/L ND (120) ND (120)

Pyridine ug/L ND (60.0) ND (60.0)

2,4,5-Trichlorophenol ug/L ND (60.0) ND (60.0)

2,4,6-Trichlorophenol ug/L ND (60.0) ND (60.0)

TCLP Pesticides gamma-BHC ug/L ND (0.40) ND (0.40)

Chlordane ug/L ND (10.0) ND (10.0)

Endrin ug/L ND (0.40) ND (0.40)

Heptachlor ug/L ND (0.40) ND (0.40)

Heptachlor Epoxide ug/L ND (0.40) ND (0.40)

Methoxychlor ug/L ND (0.40) ND (0.40)

Toxaphene ug/L ND (20.0) ND (20.0)

TCLP Herbicides

2,4-D ug/L ND (4.0) ND (4.0)

2,4,5-TP ug/L ND (6.0) ND (6.0)

NOTES:

mg/kg = milligrams per kilogram ug/L = micrograms per Liter ug/kg = micrograms per kilogram mg/L = milligrams per Liter

ND = Not Detected (the Reporting Limit is in parentheses)

Bold cell = Analyte reported.

Analyte Units

Report ID: 2346880 - 11/7/2018 Page 1 of 12

Mr. David Leety ARC Environmental 1311 Haubert St Baltimore, MD 21230

November 7, 2018

Dear Mr. Leety:

Certificate of Analysis Project Name:

Purchase Order:

Philadelphia Navy Yard Workorder:

Workorder ID:

2346880 PNY-Bldg 633 Cooling

This page is included as part of the Analytical Report and must be retained as a permanent record thereof. Project Coordinator

Mrs. Kelli L Wolfgang

Enclosed are the analytical results for samples received by the laboratory on Monday, October 29, 2018.

The ALS Environmental laboratory in Middletown, Pennsylvania is a National Environmental Laboratory Accreditation Program (NELAP) accredited laboratory and as such, certifies that all applicable test results meet the requirements of NELAP.

If you have any questions regarding this certificate of analysis, please contact Mrs. Kelli L Wolfgang (Project Coordinator) at (717) 944-5541.

Analyses were performed according to our laboratory’s NELAP-approved quality assurance program and any applicable state requirements. The test results meet requirements of the current NELAP standards or state requirements, where applicable. For a specific list of accredited analytes, refer to the certifications section of the ALS website at www.alsglobal.com/en/Our-Services/Life-Sciences/Environmental/Downloads.

This laboratory report may not be reproduced, except in full, without the written approval of ALS Environmental.

ALS Spring City: 10 Riverside Drive, Spring City, PA 19475 610-948-4903

NELAP Certifications: NJ PA010 , NY 11759 , PA 22-293 DoD ELAP: A2LA 0818.01 State Certifications: DE ID 11 , MA PA0102 , MD 128 , VA 460157 , WV 343

DL ID - 69377, QC - 0

Report ID: 2346880 - 11/7/2018 Page 2 of 12

Workorder: 2346880 PNY-Bldg 633 Cooling

SAMPLE SUMMARY

Lab ID Sample ID Matrix Date Collected Date Received Collected By

2346880001 CT-1 1-5' Solid 10/25/2018 10:05 10/29/2018 21:45 Collected by Client

2346880002 CT-2 1-5' Solid 10/25/2018 15:15 10/29/2018 21:45 Collected by Client

Report ID: 2346880 - 11/7/2018 Page 3 of 12

SAMPLE SUMMARY

Standard Acronyms/Flags

Notes

-- All Waste Water analyses comply with methodology requirements of 40 CFR Part 136.

-- All Drinking Water analyses comply with methodology requirements of 40 CFR Part 141.

-- Unless otherwise noted, all quantitative results for soils are reported on a dry weight basis.

-- The Chain of Custody document is included as part of this report.

Indicates an estimated value between the Method Detection Limit (MDL) and the Practical Quantitation Limit (PQL) for the analyte Indicates that the analyte was Not Detected (ND)

Method Detection Limit Practical Quantitation Limit

J U

MDL

PQL

Reporting Detection Limit Not Detected - indicates that the analyte was Not Detected at the RDL Analysis was performed using this container Regulatory Limit

RDL

ND

Cntr

RegLmt Laboratory Control Sample Matrix Spike

LCS

MS

Matrix Spike Duplicate Sample Duplicate Percent Recovery

MSD

DUP

%Rec Relative Percent DifferenceRPD

-- Samples collected by ALS personnel are done so in accordance with the procedures set forth in the ALS Field Sampling Plan (20 - Field Services Sampling Plan).

N Indicates presumptive evidence of the presence of a compound

-- All Library Search analytes should be regarded as tentative identifications based on the presumptive evidence of the mass spectra.

Concentrations reported are estimated values.

-- Parameters identified as "analyze immediately" require analysis within 15 minutes of collection. Any "analyze immediately" parameters not listed under the header "Field Parameters" are preformed in the laboratory and are therefore analyzed out of hold time.

LOD DoD Limit of Detection LOQ DoD Limit of Quantitation DL DoD Detection Limit

-- Method references listed on this report beginning with the prefix “S” followed by a method number (such as S2310B-97) refer to methods from “Standard Methods for the Examination of Water and Wastewater”.

I Indicates reported value is greater than or equal to the Method Detection Limit (MDL) but less than the Report Detection Limit (RDL)

(S) Surrogate Compound NC Not Calculated

* Result outside of QC limits

-- For microbiological analyses, the "Prepared" value is the date/time into the incurbator and the "Analyzed" value is the date/time out the incubator.

Report ID: 2346880 - 11/7/2018 Page 4 of 12

ANALYTICAL RESULTS

10/29/2018 21:45CT-1 1-5'

Matrix: Solid

Parameters

Lab ID:

Sample ID:

2346880001

Results Units RDL Prepared By ByAnalyzedFlag

Date Collected:

Date Received:

10/25/2018 10:05

CntrMethod

TCLP VOLATILE ORGANICS

Benzene ND ug/L 20.0 11/5/18 12:55 TMP ESW846 8260C 2-Butanone ND ug/L 200 11/5/18 12:55 TMP ESW846 8260C Carbon Tetrachloride ND ug/L 20.0 11/5/18 12:55 TMP ESW846 8260C Chlorobenzene ND ug/L 20.0 11/5/18 12:55 TMP ESW846 8260C Chloroform ND ug/L 20.0 11/5/18 12:55 TMP ESW846 8260C 1,2-Dichloroethane ND ug/L 20.0 11/5/18 12:55 TMP ESW846 8260C 1,1-Dichloroethene ND ug/L 20.0 11/5/18 12:55 TMP ESW846 8260C Tetrachloroethene ND ug/L 20.0 11/5/18 12:55 TMP ESW846 8260C Trichloroethene ND ug/L 20.0 11/5/18 12:55 TMP ESW846 8260C Vinyl Chloride ND ug/L 20.0 11/5/18 12:55 TMP ESW846 8260C

Surrogate Recoveries Flag UnitsResults Limits Prepared By Analyzed By CntrMethod

1,2-Dichloroethane-d4 (S) 81.2 % 62 - 133 11/5/18 12:55 TMP ESW846 8260C 4-Bromofluorobenzene (S) 103 % 79 - 114 11/5/18 12:55 TMP ESW846 8260C Dibromofluoromethane (S) 83.6 % 78 - 116 11/5/18 12:55 TMP ESW846 8260C Toluene-d8 (S) 83.9 % 76 - 127 11/5/18 12:55 TMP ESW846 8260C

GASOLINE RANGE ORGANICS

Gasoline Range Organics ND ug/kg 10600 10/30/18 09:23 DD 10/30/18 14:21 DD A1 SW846 8015D

Surrogate Recoveries Flag UnitsResults Limits Prepared By Analyzed By CntrMethod a,a,a-Trifluorotoluene (S) 120 % 72 - 134 10/30/18 09:23 DD 10/30/18 14:21 DD ASW846 8015D

VOLATILE ORGANICS

Benzene ND ug/kg 53.1 10/30/18 09:23 PDK 10/31/18 06:08 PDK A1SW846 8260B Ethylbenzene ND ug/kg 53.1 10/30/18 09:23 PDK 10/31/18 06:08 PDK A1SW846 8260B Toluene ND ug/kg 53.1 10/30/18 09:23 PDK 10/31/18 06:08 PDK A1SW846 8260B Total Xylenes ND ug/kg 159 10/30/18 09:23 PDK 10/31/18 06:08 PDK A1SW846 8260B

Surrogate Recoveries Flag UnitsResults Limits Prepared By Analyzed By CntrMethod

1,2-Dichloroethane-d4 (S) 93.2 % 71 - 146 10/30/18 09:23 PDK 10/31/18 06:08 PDK A1SW846 8260B 4-Bromofluorobenzene (S) 98.8 % 46 - 138 10/30/18 09:23 PDK 10/31/18 06:08 PDK A1SW846 8260B Dibromofluoromethane (S) 90.3 % 42 - 143 10/30/18 09:23 PDK 10/31/18 06:08 PDK A1SW846 8260B Toluene-d8 (S) 104 % 54 - 141 10/30/18 09:23 PDK 10/31/18 06:08 PDK A1SW846 8260B

LIBRARY SEARCH - VOLATILES

No TIC's Detected . 10/31/18 06:08 CPK ALib Search VOC

PETROLEUM HC's Diesel Range Organics C10- C28

90.6 mg/kg 12.2 10/30/18 19:40 J1H 10/31/18 21:58 BS ASW846 8015D

Report ID: 2346880 - 11/7/2018 Page 5 of 12

ANALYTICAL RESULTS

10/29/2018 21:45CT-1 1-5'

Matrix: Solid

Parameters

Lab ID:

Sample ID:

2346880001

Results Units RDL Prepared By ByAnalyzedFlag

Date Collected:

Date Received:

10/25/2018 10:05

CntrMethod

Surrogate Recoveries Flag UnitsResults Limits Prepared By Analyzed By CntrMethod o-Terphenyl (S) 67.2 % 36 - 122 10/30/18 19:40 J1H 10/31/18 21:58 BS ASW846 8015D

WET CHEMISTRY

Moisture 16.0 % 0.1 10/31/18 12:00 AXDS2540G-11 Total Solids 84.0 % 0.1 10/31/18 12:00 AXDS2540G-11

TCLP METALS

Arsenic, Total ND mg/L 0.14 11/1/18 14:40 BMK 11/2/18 10:00 SRT A1SW846 6010C Barium, Total ND mg/L 2.8 11/1/18 14:40 BMK 11/2/18 10:00 SRT A1SW846 6010C Cadmium, Total ND mg/L 0.011 11/1/18 14:40 BMK 11/2/18 10:00 SRT A1SW846 6010C Chromium, Total ND mg/L 0.028 11/1/18 14:40 BMK 11/2/18 10:00 SRT A1SW846 6010C Lead, Total 0.62 mg/L 0.033 11/1/18 14:40 BMK 11/2/18 10:00 SRT A1SW846 6010C Mercury, Total ND mg/L 0.0020 11/2/18 08:30 AXC 11/2/18 11:21 AXC A2SW846 7470A Selenium, Total ND mg/L 0.11 11/1/18 14:40 BMK 11/2/18 10:00 SRT A1SW846 6010C Silver, Total ND mg/L 0.022 11/1/18 14:40 BMK 11/2/18 10:00 SRT A1SW846 6010C

TCLP SEMI-VOLATILES

mp-Cresol ND ug/L 60.0 11/1/18 11:00 CAC 11/1/18 21:49 DHF ASW846 8270D o-Cresol ND ug/L 60.0 11/1/18 11:00 CAC 11/1/18 21:49 DHF ASW846 8270D 1,4-Dichlorobenzene ND ug/L 60.0 11/1/18 11:00 CAC 11/1/18 21:49 DHF ASW846 8270D 2,4-Dinitrotoluene ND ug/L 60.0 11/1/18 11:00 CAC 11/1/18 21:49 DHF ASW846 8270D Hexachlorobenzene ND ug/L 60.0 11/1/18 11:00 CAC 11/1/18 21:49 DHF ASW846 8270D Hexachlorobutadiene ND ug/L 60.0 11/1/18 11:00 CAC 11/1/18 21:49 DHF ASW846 8270D Hexachloroethane ND ug/L 60.0 11/1/18 11:00 CAC 11/1/18 21:49 DHF ASW846 8270D Nitrobenzene ND ug/L 60.0 11/1/18 11:00 CAC 11/1/18 21:49 DHF ASW846 8270D Pentachlorophenol ND ug/L 120 11/1/18 11:00 CAC 11/1/18 21:49 DHF ASW846 8270D Pyridine ND ug/L 60.0 11/1/18 11:00 CAC 11/1/18 21:49 DHF ASW846 8270D 2,4,5-Trichlorophenol ND ug/L 60.0 11/1/18 11:00 CAC 11/1/18 21:49 DHF ASW846 8270D 2,4,6-Trichlorophenol ND ug/L 60.0 11/1/18 11:00 CAC 11/1/18 21:49 DHF ASW846 8270D

Surrogate Recoveries Flag UnitsResults Limits Prepared By Analyzed By CntrMethod

2,4,6-Tribromophenol (S) 84 % 47 - 128 11/1/18 11:00 CAC 11/1/18 21:49 DHF ASW846 8270D 2-Fluorobiphenyl (S) 84.8 % 52 - 118 11/1/18 11:00 CAC 11/1/18 21:49 DHF ASW846 8270D 2-Fluorophenol (S) 59.7 % 20 - 87 11/1/18 11:00 CAC 11/1/18 21:49 DHF ASW846 8270D Nitrobenzene-d5 (S) 93.8 % 27 - 139 11/1/18 11:00 CAC 11/1/18 21:49 DHF ASW846 8270D Phenol-d5 (S) 40.6 % 10 - 81 11/1/18 11:00 CAC 11/1/18 21:49 DHF ASW846 8270D Terphenyl-d14 (S) 106 % 46 - 133 11/1/18 11:00 CAC 11/1/18 21:49 DHF ASW846 8270D

TCLP PESTICIDES

gamma-BHC ND ug/L 0.40 11/1/18 23:10 DXL 11/2/18 16:47 RWS ASW846 8081B

Report ID: 2346880 - 11/7/2018 Page 6 of 12

ANALYTICAL RESULTS

10/29/2018 21:45CT-1 1-5'

Matrix: Solid

Parameters

Lab ID:

Sample ID:

2346880001

Results Units RDL Prepared By ByAnalyzedFlag

Date Collected:

Date Received:

10/25/2018 10:05

CntrMethod

Chlordane ND ug/L 10.0 11/1/18 23:10 DXL 11/2/18 16:47 RWS ASW846 8081B Endrin ND ug/L 0.40 11/1/18 23:10 DXL 11/2/18 16:47 RWS ASW846 8081B Heptachlor ND ug/L 0.40 11/1/18 23:10 DXL 11/2/18 16:47 RWS ASW846 8081B Heptachlor Epoxide ND ug/L 0.40 11/1/18 23:10 DXL 11/2/18 16:47 RWS ASW846 8081B Methoxychlor ND ug/L 0.40 11/1/18 23:10 DXL 11/2/18 16:47 RWS ASW846 8081B Toxaphene ND ug/L 20.0 11/1/18 23:10 DXL 11/2/18 16:47 RWS ASW846 8081B

Surrogate Recoveries Flag UnitsResults Limits Prepared By Analyzed By CntrMethod

Decachlorobiphenyl (S) 65.2 % 30 - 140 11/1/18 23:10 DXL 11/2/18 16:47 RWS ASW846 8081B Tetrachloro-m-xylene (S) 69.3 % 30 - 123 11/1/18 23:10 DXL 11/2/18 16:47 RWS ASW846 8081B

TCLP HERBICIDES

2,4-D ND ug/L 4.0 11/1/18 19:05 DXL 11/2/18 09:48 KJH ASW846 8151A 2,4,5-TP ND ug/L 6.0 11/1/18 19:05 DXL 11/2/18 09:48 KJH ASW846 8151A

Surrogate Recoveries Flag UnitsResults Limits Prepared By Analyzed By CntrMethod

2,4-Dichlorophenylacetic acid (S)

94.2 % 14 - 172 11/1/18 19:05 DXL 11/2/18 09:48 KJH ASW846 8151A

Project Coordinator Mrs. Kelli L Wolfgang

Report ID: 2346880 - 11/7/2018 Page 7 of 12

ANALYTICAL RESULTS

10/29/2018 21:45CT-2 1-5'

Matrix: Solid

Parameters

Lab ID:

Sample ID:

2346880002

Results Units RDL Prepared By ByAnalyzedFlag

Date Collected:

Date Received:

10/25/2018 15:15

CntrMethod

TCLP VOLATILE ORGANICS

Benzene ND ug/L 20.0 11/5/18 13:17 TMP ESW846 8260C 2-Butanone ND ug/L 200 11/5/18 13:17 TMP ESW846 8260C Carbon Tetrachloride ND ug/L 20.0 11/5/18 13:17 TMP ESW846 8260C Chlorobenzene ND ug/L 20.0 11/5/18 13:17 TMP ESW846 8260C Chloroform ND ug/L 20.0 11/5/18 13:17 TMP ESW846 8260C 1,2-Dichloroethane ND ug/L 20.0 11/5/18 13:17 TMP ESW846 8260C 1,1-Dichloroethene ND ug/L 20.0 11/5/18 13:17 TMP ESW846 8260C Tetrachloroethene ND ug/L 20.0 11/5/18 13:17 TMP ESW846 8260C Trichloroethene ND ug/L 20.0 11/5/18 13:17 TMP ESW846 8260C Vinyl Chloride ND ug/L 20.0 11/5/18 13:17 TMP ESW846 8260C

Surrogate Recoveries Flag UnitsResults Limits Prepared By Analyzed By CntrMethod

1,2-Dichloroethane-d4 (S) 83.3 % 62 - 133 11/5/18 13:17 TMP ESW846 8260C 4-Bromofluorobenzene (S) 99.5 % 79 - 114 11/5/18 13:17 TMP ESW846 8260C Dibromofluoromethane (S) 84.3 % 78 - 116 11/5/18 13:17 TMP ESW846 8260C Toluene-d8 (S) 83.9 % 76 - 127 11/5/18 13:17 TMP ESW846 8260C

GASOLINE RANGE ORGANICS

Gasoline Range Organics ND ug/kg 11700 10/30/18 09:22 DD 10/30/18 13:51 DD A1 SW846 8015D

Surrogate Recoveries Flag UnitsResults Limits Prepared By Analyzed By CntrMethod a,a,a-Trifluorotoluene (S) 119 % 72 - 134 10/30/18 09:22 DD 10/30/18 13:51 DD ASW846 8015D

VOLATILE ORGANICS

Benzene ND ug/kg 58.4 10/30/18 09:22 PDK 10/31/18 06:31 PDK A1SW846 8260B Ethylbenzene ND ug/kg 58.4 10/30/18 09:22 PDK 10/31/18 06:31 PDK A1SW846 8260B Toluene ND ug/kg 58.4 10/30/18 09:22 PDK 10/31/18 06:31 PDK A1SW846 8260B Total Xylenes ND ug/kg 175 10/30/18 09:22 PDK 10/31/18 06:31 PDK A1SW846 8260B

Surrogate Recoveries Flag UnitsResults Limits Prepared By Analyzed By CntrMethod

1,2-Dichloroethane-d4 (S) 88.5 % 71 - 146 10/30/18 09:22 PDK 10/31/18 06:31 PDK A1SW846 8260B 4-Bromofluorobenzene (S) 89.3 % 46 - 138 10/30/18 09:22 PDK 10/31/18 06:31 PDK A1SW846 8260B Dibromofluoromethane (S) 88.3 % 42 - 143 10/30/18 09:22 PDK 10/31/18 06:31 PDK A1SW846 8260B Toluene-d8 (S) 98.2 % 54 - 141 10/30/18 09:22 PDK 10/31/18 06:31 PDK A1SW846 8260B

LIBRARY SEARCH - VOLATILES

No TIC's Detected . 10/31/18 06:31 CPK ALib Search VOC

PETROLEUM HC's Diesel Range Organics C10- C28

20.0 mg/kg 12.6 10/30/18 19:40 J1H 10/31/18 22:33 BS ASW846 8015D

Report ID: 2346880 - 11/7/2018 Page 8 of 12

ANALYTICAL RESULTS

10/29/2018 21:45CT-2 1-5'

Matrix: Solid

Parameters

Lab ID:

Sample ID:

2346880002

Results Units RDL Prepared By ByAnalyzedFlag

Date Collected:

Date Received:

10/25/2018 15:15

CntrMethod

Surrogate Recoveries Flag UnitsResults Limits Prepared By Analyzed By CntrMethod o-Terphenyl (S) 69.1 % 36 - 122 10/30/18 19:40 J1H 10/31/18 22:33 BS ASW846 8015D

WET CHEMISTRY

Moisture 18.7 % 0.1 10/31/18 12:00 AXDS2540G-11 Total Solids 81.3 % 0.1 10/31/18 12:00 AXDS2540G-11

TCLP METALS

Arsenic, Total ND mg/L 0.14 11/1/18 14:40 BMK 11/2/18 10:04 SRT A1SW846 6010C Barium, Total ND mg/L 2.8 11/1/18 14:40 BMK 11/2/18 10:04 SRT A1SW846 6010C Cadmium, Total ND mg/L 0.011 11/1/18 14:40 BMK 11/2/18 10:04 SRT A1SW846 6010C Chromium, Total ND mg/L 0.028 11/1/18 14:40 BMK 11/2/18 10:04 SRT A1SW846 6010C Lead, Total 2.3 mg/L 0.033 11/1/18 14:40 BMK 11/2/18 10:04 SRT A1SW846 6010C Mercury, Total ND mg/L 0.0020 11/2/18 08:30 AXC 11/2/18 11:22 AXC A2SW846 7470A Selenium, Total ND mg/L 0.11 11/1/18 14:40 BMK 11/2/18 10:04 SRT A1SW846 6010C Silver, Total ND mg/L 0.022 11/1/18 14:40 BMK 11/2/18 10:04 SRT A1SW846 6010C

TCLP SEMI-VOLATILES

mp-Cresol ND ug/L 60.0 11/1/18 11:00 CAC 11/1/18 22:40 DHF ASW846 8270D o-Cresol ND ug/L 60.0 11/1/18 11:00 CAC 11/1/18 22:40 DHF ASW846 8270D 1,4-Dichlorobenzene ND ug/L 60.0 11/1/18 11:00 CAC 11/1/18 22:40 DHF ASW846 8270D 2,4-Dinitrotoluene ND ug/L 60.0 11/1/18 11:00 CAC 11/1/18 22:40 DHF ASW846 8270D Hexachlorobenzene ND ug/L 60.0 11/1/18 11:00 CAC 11/1/18 22:40 DHF ASW846 8270D Hexachlorobutadiene ND ug/L 60.0 11/1/18 11:00 CAC 11/1/18 22:40 DHF ASW846 8270D Hexachloroethane ND ug/L 60.0 11/1/18 11:00 CAC 11/1/18 22:40 DHF ASW846 8270D Nitrobenzene ND ug/L 60.0 11/1/18 11:00 CAC 11/1/18 22:40 DHF ASW846 8270D Pentachlorophenol ND ug/L 120 11/1/18 11:00 CAC 11/1/18 22:40 DHF ASW846 8270D Pyridine ND ug/L 60.0 11/1/18 11:00 CAC 11/1/18 22:40 DHF ASW846 8270D 2,4,5-Trichlorophenol ND ug/L 60.0 11/1/18 11:00 CAC 11/1/18 22:40 DHF ASW846 8270D 2,4,6-Trichlorophenol ND ug/L 60.0 11/1/18 11:00 CAC 11/1/18 22:40 DHF ASW846 8270D

Surrogate Recoveries Flag UnitsResults Limits Prepared By Analyzed By CntrMethod

2,4,6-Tribromophenol (S) 84.8 % 47 - 128 11/1/18 11:00 CAC 11/1/18 22:40 DHF ASW846 8270D 2-Fluorobiphenyl (S) 87.3 % 52 - 118 11/1/18 11:00 CAC 11/1/18 22:40 DHF ASW846 8270D 2-Fluorophenol (S) 57 % 20 - 87 11/1/18 11:00 CAC 11/1/18 22:40 DHF ASW846 8270D Nitrobenzene-d5 (S) 96.8 % 27 - 139 11/1/18 11:00 CAC 11/1/18 22:40 DHF ASW846 8270D Phenol-d5 (S) 37.3 % 10 - 81 11/1/18 11:00 CAC 11/1/18 22:40 DHF ASW846 8270D Terphenyl-d14 (S) 109 % 46 - 133 11/1/18 11:00 CAC 11/1/18 22:40 DHF ASW846 8270D

TCLP PESTICIDES

gamma-BHC ND ug/L 0.40 11/1/18 23:10 DXL 11/2/18 17:18 RWS ASW846 8081B

Report ID: 2346880 - 11/7/2018 Page 9 of 12

ANALYTICAL RESULTS

10/29/2018 21:45CT-2 1-5'

Matrix: Solid

Parameters

Lab ID:

Sample ID:

2346880002

Results Units RDL Prepared By ByAnalyzedFlag

Date Collected:

Date Received:

10/25/2018 15:15

CntrMethod

Chlordane ND ug/L 10.0 11/1/18 23:10 DXL 11/2/18 17:18 RWS ASW846 8081B Endrin ND ug/L 0.40 11/1/18 23:10 DXL 11/2/18 17:18 RWS ASW846 8081B Heptachlor ND ug/L 0.40 11/1/18 23:10 DXL 11/2/18 17:18 RWS ASW846 8081B Heptachlor Epoxide ND ug/L 0.40 11/1/18 23:10 DXL 11/2/18 17:18 RWS ASW846 8081B Methoxychlor ND ug/L 0.40 11/1/18 23:10 DXL 11/2/18 17:18 RWS ASW846 8081B Toxaphene ND ug/L 20.0 11/1/18 23:10 DXL 11/2/18 17:18 RWS ASW846 8081B

Surrogate Recoveries Flag UnitsResults Limits Prepared By Analyzed By CntrMethod

Decachlorobiphenyl (S) 67.8 % 30 - 140 11/1/18 23:10 DXL 11/2/18 17:18 RWS ASW846 8081B Tetrachloro-m-xylene (S) 73.3 % 30 - 123 11/1/18 23:10 DXL 11/2/18 17:18 RWS ASW846 8081B

TCLP HERBICIDES

2,4-D ND ug/L 4.0 11/1/18 19:05 DXL 11/2/18 12:14 KJH ASW846 8151A 2,4,5-TP ND ug/L 6.0 11/1/18 19:05 DXL 11/2/18 12:14 KJH ASW846 8151A

Surrogate Recoveries Flag UnitsResults Limits Prepared By Analyzed By CntrMethod

2,4-Dichlorophenylacetic acid (S)

94.4 % 14 - 172 11/1/18 19:05 DXL 11/2/18 12:14 KJH ASW846 8151A

Project Coordinator Mrs. Kelli L Wolfgang

Report ID: 2346880 - 11/7/2018 Page 10 of 12

ANALYTICAL RESULTS

PARAMETER QUALIFIERS

#Lab ID Analytical MethodSample ID Analyte

This sample was collected in a soil jar for the volatile analysis. The sample was received and prepared by Method 5035 after the 48-hour holding time.

2346880001 SW846 8015DCT-1 1-5' Gasoline Range Organics

This sample was collected in a soil jar for the volatile analysis. The sample was received and prepared by Method 5035 after the 48-hour holding time.

2346880002 SW846 8015DCT-2 1-5' Gasoline Range Organics

Report ID: 2346880 - 11/7/2018 Page 11 of 12

ANALYSIS - PREP METHOD CROSS REFERENCE TABLE

Lab ID Sample ID Analysis Method Prep Method

Workorder: 2346880 PNY-Bldg 633 Cooling

2346880001 CT-1 1-5' Lib Search VOC

2346880001 CT-1 1-5' S2540G-11

2346880001 CT-1 1-5' SW846 6010C SW846 3015

2346880001 CT-1 1-5' SW846 7470A SW846 7470A

2346880001 CT-1 1-5' SW846 8015D SW846 3546

2346880001 CT-1 1-5' SW846 8015D SW846 5035

2346880001 CT-1 1-5' SW846 8081B SW846 3510C

2346880001 CT-1 1-5' SW846 8151A SW846 8151A

2346880001 CT-1 1-5' SW846 8260B SW846 5035

2346880001 CT-1 1-5' SW846 8260C

2346880001 CT-1 1-5' SW846 8270D SW846 3510C

2346880002 CT-2 1-5' Lib Search VOC

2346880002 CT-2 1-5' S2540G-11

2346880002 CT-2 1-5' SW846 6010C SW846 3015

2346880002 CT-2 1-5' SW846 7470A SW846 7470A

2346880002 CT-2 1-5' SW846 8015D SW846 3546

2346880002 CT-2 1-5' SW846 8015D SW846 5035

2346880002 CT-2 1-5' SW846 8081B SW846 3510C

2346880002 CT-2 1-5' SW846 8151A SW846 8151A

2346880002 CT-2 1-5' SW846 8260B SW846 5035

2346880002 CT-2 1-5' SW846 8260C

2346880002 CT-2 1-5' SW846 8270D SW846 3510C

Wednesday, November 07, 2018 6:32:40 AM

File details come from the government source that posted it. Updated .