AMENDMENT 0005 - Drum Disposal Characterization Composite Sample Results.pdf

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Design-Bid-Build (DBB), Building 633 River Water Cooling System, Philadelphia Naval Business Center (PNBC), Philadelphia, PA
Solicitation number
N4008520R0079
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This federal contract opportunity solicitation seeks design-bid-build services to replace an aging river water cooling system at the Philadelphia Naval Business Center in Philadelphia, Pennsylvania. The project involves replacing an existing 50,000 gallon per minute river water cooling system that is 77 years old with a new 8,200 gallon per minute cooling tower capable of rejecting up to 75 million British Thermal Units per hour of heat. The new cooling water system must reliably provide cooling water on demand to support research, development, test and evaluation activities performed in Building 633, including testing of the Columbia Class Program Integrated Power System. The solicitation is seeking firms to provide design services followed by construction bids to implement the replacement of the cooling system. The contracting agency is the Naval Facilities Engineering Command of the Department of the Navy.

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TABLE 2

SUMMARY OF DETECTED COMPOUNDS - DISPOSAL COMPOSITE

PHILADELPHIA NAVY YARD

Building 633 Cooling Tower

Drum

Comp

10/26/2018

Volatile Organic Compounds

Acetone ug/kg 63.2

2-Butanone ug/kg 16.8

TCLP Volatile Organic Compounds (None Detected)

Metals

Arsenic mg/kg 4.5

Barium mg/kg 69.4

Chromium mg/kg 23.7

Lead mg/kg 29.8

Mercury mg/kg 0.28

TCLP Metals

Lead mg/L 0.055

Semi-Volatile Organic Compounds

Anthracene ug/kg 69.2

Benzo(a)anthracene ug/kg 216

Benzo(a)pyrene ug/kg 210

Benzo(b)fluoranthene ug/kg 277

Benzo(g,h,i)perylene ug/kg 125

Benzo(k)fluoranthene ug/kg 103

Chrysene ug/kg 214

Fluoranthene ug/kg 452

Indeno(1,2,3-cd)pyrene ug/kg 136

Phenanthrene ug/kg 285

Pyrene ug/kg 381

TCLP Semi-Volatile Organic Compounds (None Detected)

TCLP Pesticides (None Detected)

TCLP Herbicides (None Detected)

PCBs (None Detected)

Asbestos (None Detected)

NOTES:

mg/kg = milligrams per kilogram ug/kg = micrograms per kilogram ug/L = micrograms per Liter mg/L = milligrams per Liter

ND = Not Detected (the Reporting Limit is in parentheses)

Bold cell = Analyte reported.

Analyte Units

Report ID: 2346875 - 11/7/2018 Page 1 of 13

Mr. David Leety ARC Environmental 1311 Haubert St Baltimore, MD 21230

November 7, 2018

Dear Mr. Leety:

Certificate of Analysis Project Name:

Purchase Order:

Philadelphia Navy Yard Workorder:

Workorder ID:

2346875 PNY-Bldg 633 Cooling

This page is included as part of the Analytical Report and must be retained as a permanent record thereof. Project Coordinator

Mrs. Kelli L Wolfgang

Enclosed are the analytical results for samples received by the laboratory on Monday, October 29, 2018.

The ALS Environmental laboratory in Middletown, Pennsylvania is a National Environmental Laboratory Accreditation Program (NELAP) accredited laboratory and as such, certifies that all applicable test results meet the requirements of NELAP.

If you have any questions regarding this certificate of analysis, please contact Mrs. Kelli L Wolfgang (Project Coordinator) at (717) 944-5541.

Analyses were performed according to our laboratory’s NELAP-approved quality assurance program and any applicable state requirements. The test results meet requirements of the current NELAP standards or state requirements, where applicable. For a specific list of accredited analytes, refer to the certifications section of the ALS website at www.alsglobal.com/en/Our-Services/Life-Sciences/Environmental/Downloads.

This laboratory report may not be reproduced, except in full, without the written approval of ALS Environmental.

ALS Spring City: 10 Riverside Drive, Spring City, PA 19475 610-948-4903

NELAP Certifications: NJ PA010 , NY 11759 , PA 22-293 DoD ELAP: A2LA 0818.01 State Certifications: DE ID 11 , MA PA0102 , MD 128 , VA 460157 , WV 343

DL ID - 69377, QC - 0

Report ID: 2346875 - 11/7/2018 Page 2 of 13

Workorder: 2346875 PNY-Bldg 633 Cooling

SAMPLE SUMMARY

Lab ID Sample ID Matrix Date Collected Date Received Collected By

2346875001 Drum Comp Solid 10/26/2018 05:39 10/29/2018 21:45 Collected by Client

Report ID: 2346875 - 11/7/2018 Page 3 of 13

SAMPLE SUMMARY

Standard Acronyms/Flags

Notes

-- All Waste Water analyses comply with methodology requirements of 40 CFR Part 136.

-- All Drinking Water analyses comply with methodology requirements of 40 CFR Part 141.

-- Unless otherwise noted, all quantitative results for soils are reported on a dry weight basis.

-- The Chain of Custody document is included as part of this report.

Indicates an estimated value between the Method Detection Limit (MDL) and the Practical Quantitation Limit (PQL) for the analyte Indicates that the analyte was Not Detected (ND)

Method Detection Limit Practical Quantitation Limit

J U

MDL

PQL

Reporting Detection Limit Not Detected - indicates that the analyte was Not Detected at the RDL Analysis was performed using this container Regulatory Limit

RDL

ND

Cntr

RegLmt Laboratory Control Sample Matrix Spike

LCS

MS

Matrix Spike Duplicate Sample Duplicate Percent Recovery

MSD

DUP

%Rec Relative Percent DifferenceRPD

-- Samples collected by ALS personnel are done so in accordance with the procedures set forth in the ALS Field Sampling Plan (20 - Field Services Sampling Plan).

N Indicates presumptive evidence of the presence of a compound

-- All Library Search analytes should be regarded as tentative identifications based on the presumptive evidence of the mass spectra.

Concentrations reported are estimated values.

-- Parameters identified as "analyze immediately" require analysis within 15 minutes of collection. Any "analyze immediately" parameters not listed under the header "Field Parameters" are preformed in the laboratory and are therefore analyzed out of hold time.

LOD DoD Limit of Detection LOQ DoD Limit of Quantitation DL DoD Detection Limit

-- Method references listed on this report beginning with the prefix “S” followed by a method number (such as S2310B-97) refer to methods from “Standard Methods for the Examination of Water and Wastewater”.

I Indicates reported value is greater than or equal to the Method Detection Limit (MDL) but less than the Report Detection Limit (RDL)

(S) Surrogate Compound NC Not Calculated

* Result outside of QC limits

-- For microbiological analyses, the "Prepared" value is the date/time into the incurbator and the "Analyzed" value is the date/time out the incubator.

Report ID: 2346875 - 11/7/2018 Page 4 of 13

ANALYTICAL RESULTS

10/29/2018 21:45Drum Comp

Matrix: Solid

Parameters

Lab ID:

Sample ID:

2346875001

Results Units RDL Prepared By ByAnalyzedFlag

Date Collected:

Date Received:

10/26/2018 05:39

CntrMethod

TCLP VOLATILE ORGANICS

Benzene ND ug/L 20.0 11/5/18 12:33 TMP ASW846 8260C 2-Butanone ND ug/L 200 11/5/18 12:33 TMP ASW846 8260C Carbon Tetrachloride ND ug/L 20.0 11/5/18 12:33 TMP ASW846 8260C Chlorobenzene ND ug/L 20.0 11/5/18 12:33 TMP ASW846 8260C Chloroform ND ug/L 20.0 11/5/18 12:33 TMP ASW846 8260C 1,2-Dichloroethane ND ug/L 20.0 11/5/18 12:33 TMP ASW846 8260C 1,1-Dichloroethene ND ug/L 20.0 11/5/18 12:33 TMP ASW846 8260C Tetrachloroethene ND ug/L 20.0 11/5/18 12:33 TMP ASW846 8260C Trichloroethene ND ug/L 20.0 11/5/18 12:33 TMP ASW846 8260C Vinyl Chloride ND ug/L 20.0 11/5/18 12:33 TMP ASW846 8260C

Surrogate Recoveries Flag UnitsResults Limits Prepared By Analyzed By CntrMethod

1,2-Dichloroethane-d4 (S) 81.4 % 62 - 133 11/5/18 12:33 TMP ASW846 8260C 4-Bromofluorobenzene (S) 98.8 % 79 - 114 11/5/18 12:33 TMP ASW846 8260C Dibromofluoromethane (S) 83.3 % 78 - 116 11/5/18 12:33 TMP ASW846 8260C Toluene-d8 (S) 83.6 % 76 - 127 11/5/18 12:33 TMP ASW846 8260C

VOLATILE ORGANICS

Acetone 63.2 ug/kg 12.5 10/30/18 09:20 TMP 10/30/18 20:42 TMP A2SW846 8260B Benzene ND ug/kg 2.5 10/30/18 09:20 TMP 10/30/18 20:42 TMP A2SW846 8260B Bromochloromethane ND ug/kg 2.5 10/30/18 09:20 TMP 10/30/18 20:42 TMP A2SW846 8260B Bromodichloromethane ND ug/kg 2.5 10/30/18 09:20 TMP 10/30/18 20:42 TMP A2SW846 8260B Bromoform ND ug/kg 2.5 10/30/18 09:20 TMP 10/30/18 20:42 TMP A2SW846 8260B Bromomethane ND ug/kg 2.5 10/30/18 09:20 TMP 10/30/18 20:42 TMP A2SW846 8260B 2-Butanone 16.8 ug/kg 12.5 10/30/18 09:20 TMP 10/30/18 20:42 TMP A2SW846 8260B Carbon Disulfide ND ug/kg 2.5 10/30/18 09:20 TMP 10/30/18 20:42 TMP A2SW846 8260B Carbon Tetrachloride ND ug/kg 2.5 10/30/18 09:20 TMP 10/30/18 20:42 TMP A2SW846 8260B Chlorobenzene ND ug/kg 2.5 10/30/18 09:20 TMP 10/30/18 20:42 TMP A2SW846 8260B Chlorodibromomethane ND ug/kg 2.5 10/30/18 09:20 TMP 10/30/18 20:42 TMP A2SW846 8260B Chloroethane ND ug/kg 6.2 10/30/18 09:20 TMP 10/30/18 20:42 TMP A2SW846 8260B Chloroform ND ug/kg 2.5 10/30/18 09:20 TMP 10/30/18 20:42 TMP A2SW846 8260B Chloromethane ND ug/kg 2.5 10/30/18 09:20 TMP 10/30/18 20:42 TMP A2SW846 8260B Cyclohexane ND ug/kg 2.5 10/30/18 09:20 TMP 10/30/18 20:42 TMP A2SW846 8260B 1,2-Dibromo-3-chloropropane

ND ug/kg 6.2 10/30/18 09:20 TMP 10/30/18 20:42 TMP A2SW846 8260B

1,2-Dibromoethane ND ug/kg 2.5 10/30/18 09:20 TMP 10/30/18 20:42 TMP A2SW846 8260B 1,2-Dichlorobenzene ND ug/kg 2.5 10/30/18 09:20 TMP 10/30/18 20:42 TMP A2SW846 8260B 1,3-Dichlorobenzene ND ug/kg 2.5 10/30/18 09:20 TMP 10/30/18 20:42 TMP A2SW846 8260B

Report ID: 2346875 - 11/7/2018 Page 5 of 13

ANALYTICAL RESULTS

10/29/2018 21:45Drum Comp

Matrix: Solid

Parameters

Lab ID:

Sample ID:

2346875001

Results Units RDL Prepared By ByAnalyzedFlag

Date Collected:

Date Received:

10/26/2018 05:39

CntrMethod

1,4-Dichlorobenzene ND ug/kg 2.5 10/30/18 09:20 TMP 10/30/18 20:42 TMP A2SW846 8260B Dichlorodifluoromethane ND ug/kg 2.5 10/30/18 09:20 TMP 10/30/18 20:42 TMP A2SW846 8260B 1,1-Dichloroethane ND ug/kg 2.5 10/30/18 09:20 TMP 10/30/18 20:42 TMP A2SW846 8260B 1,2-Dichloroethane ND ug/kg 2.5 10/30/18 09:20 TMP 10/30/18 20:42 TMP A2SW846 8260B 1,1-Dichloroethene ND ug/kg 2.5 10/30/18 09:20 TMP 10/30/18 20:42 TMP A2SW846 8260B cis-1,2-Dichloroethene ND ug/kg 2.5 10/30/18 09:20 TMP 10/30/18 20:42 TMP A2SW846 8260B trans-1,2-Dichloroethene ND ug/kg 2.5 10/30/18 09:20 TMP 10/30/18 20:42 TMP A2SW846 8260B 1,2-Dichloropropane ND ug/kg 2.5 10/30/18 09:20 TMP 10/30/18 20:42 TMP A2SW846 8260B cis-1,3-Dichloropropene ND ug/kg 2.5 10/30/18 09:20 TMP 10/30/18 20:42 TMP A2SW846 8260B trans-1,3-Dichloropropene ND ug/kg 2.5 10/30/18 09:20 TMP 10/30/18 20:42 TMP A2SW846 8260B 1,4-Dioxane ND ug/kg 93.5 10/30/18 09:20 TMP 10/30/18 20:42 TMP A2SW846 8260B Ethylbenzene ND ug/kg 2.5 10/30/18 09:20 TMP 10/30/18 20:42 TMP A2SW846 8260B Freon 113 ND ug/kg 2.5 10/30/18 09:20 TMP 10/30/18 20:42 TMP A2SW846 8260B 2-Hexanone ND ug/kg 12.5 10/30/18 09:20 TMP 10/30/18 20:42 TMP A2SW846 8260B Isopropylbenzene ND ug/kg 2.5 10/30/18 09:20 TMP 10/30/18 20:42 TMP A2SW846 8260B Methyl acetate ND ug/kg 2.5 10/30/18 09:20 TMP 10/30/18 20:42 TMP A2SW846 8260B Methyl cyclohexane ND ug/kg 2.5 10/30/18 09:20 TMP 10/30/18 20:42 TMP A2SW846 8260B Methyl t-Butyl Ether ND ug/kg 2.5 10/30/18 09:20 TMP 10/30/18 20:42 TMP A2SW846 8260B 4-Methyl-2- Pentanone(MIBK)

ND ug/kg 12.5 10/30/18 09:20 TMP 10/30/18 20:42 TMP A2SW846 8260B

Methylene Chloride ND ug/kg 2.5 10/30/18 09:20 TMP 10/30/18 20:42 TMP A2SW846 8260B Styrene ND ug/kg 2.5 10/30/18 09:20 TMP 10/30/18 20:42 TMP A2SW846 8260B 1,1,2,2-Tetrachloroethane ND ug/kg 2.5 10/30/18 09:20 TMP 10/30/18 20:42 TMP A2SW846 8260B Tetrachloroethene ND ug/kg 2.5 10/30/18 09:20 TMP 10/30/18 20:42 TMP A2SW846 8260B Toluene ND ug/kg 2.5 10/30/18 09:20 TMP 10/30/18 20:42 TMP A2SW846 8260B Total Xylenes ND ug/kg 7.5 10/30/18 09:20 TMP 10/30/18 20:42 TMP A2SW846 8260B 1,2,3-Trichlorobenzene ND ug/kg 6.2 10/30/18 09:20 TMP 10/30/18 20:42 TMP A2SW846 8260B 1,2,4-Trichlorobenzene ND ug/kg 6.2 10/30/18 09:20 TMP 10/30/18 20:42 TMP A2SW846 8260B 1,1,1-Trichloroethane ND ug/kg 2.5 10/30/18 09:20 TMP 10/30/18 20:42 TMP A2SW846 8260B 1,1,2-Trichloroethane ND ug/kg 2.5 10/30/18 09:20 TMP 10/30/18 20:42 TMP A2SW846 8260B Trichloroethene ND ug/kg 2.5 10/30/18 09:20 TMP 10/30/18 20:42 TMP A2SW846 8260B Trichlorofluoromethane ND ug/kg 2.5 10/30/18 09:20 TMP 10/30/18 20:42 TMP A2SW846 8260B Vinyl Chloride ND ug/kg 2.5 10/30/18 09:20 TMP 10/30/18 20:42 TMP A2SW846 8260B o-Xylene ND ug/kg 2.5 10/30/18 09:20 TMP 10/30/18 20:42 TMP A2SW846 8260B mp-Xylene ND ug/kg 5.0 10/30/18 09:20 TMP 10/30/18 20:42 TMP A2SW846 8260B

Surrogate Recoveries Flag UnitsResults Limits Prepared By Analyzed By CntrMethod

1,2-Dichloroethane-d4 (S) 102 % 56 - 124 10/30/18 09:20 TMP 10/30/18 20:42 TMP A2SW846 8260B 4-Bromofluorobenzene (S) 99.7 % 51 - 128 10/30/18 09:20 TMP 10/30/18 20:42 TMP A2SW846 8260B

Report ID: 2346875 - 11/7/2018 Page 6 of 13

ANALYTICAL RESULTS

10/29/2018 21:45Drum Comp

Matrix: Solid

Parameters

Lab ID:

Sample ID:

2346875001

Results Units RDL Prepared By ByAnalyzedFlag

Date Collected:

Date Received:

10/26/2018 05:39

CntrMethod

Dibromofluoromethane (S) 105 % 62 - 123 10/30/18 09:20 TMP 10/30/18 20:42 TMP A2SW846 8260B Toluene-d8 (S) 97.5 % 59 - 131 10/30/18 09:20 TMP 10/30/18 20:42 TMP A2SW846 8260B

Library Search - Volatiles Benzene, 2-ethyl-1,4-dimeth 11.8 ug/kg 10/30/18 09:20 TMP 10/30/18 20:42 TMP A2J N SW846 8260B Tridecane, 7-methyl- 20.5 ug/kg 10/30/18 09:20 TMP 10/30/18 20:42 TMP A2J N SW846 8260B Unknown 20.7 ug/kg 10/30/18 09:20 TMP 10/30/18 20:42 TMP A2J SW846 8260B Naphthalene, 1,2,3,4-tetrah 22.9 ug/kg 10/30/18 09:20 TMP 10/30/18 20:42 TMP A2J N SW846 8260B Dodecane, 2,7,10-trimethyl- 32.5 ug/kg 10/30/18 09:20 TMP 10/30/18 20:42 TMP A2J N SW846 8260B

SEMIVOLATILES

Acenaphthene ND ug/kg 68.6 10/31/18 19:35 J1H 11/1/18 15:39 CGS ASW846 8270D Acenaphthylene ND ug/kg 68.6 10/31/18 19:35 J1H 11/1/18 15:39 CGS ASW846 8270D Acetophenone ND ug/kg 137 10/31/18 19:35 J1H 11/1/18 15:39 CGS ASW846 8270D Anthracene 69.2 ug/kg 68.6 10/31/18 19:35 J1H 11/1/18 15:39 CGS ASW846 8270D Atrazine ND ug/kg 137 10/31/18 19:35 J1H 11/1/18 15:39 CGS ASW846 8270D Benzaldehyde ND ug/kg 274 10/31/18 19:35 J1H 11/1/18 15:39 CGS ASW846 8270D Benzo(a)anthracene 216 ug/kg 68.6 10/31/18 19:35 J1H 11/1/18 15:39 CGS ASW846 8270D Benzo(a)pyrene 210 ug/kg 68.6 10/31/18 19:35 J1H 11/1/18 15:39 CGS ASW846 8270D Benzo(b)fluoranthene 277 ug/kg 68.6 10/31/18 19:35 J1H 11/1/18 15:39 CGS ASW846 8270D Benzo(g,h,i)perylene 125 ug/kg 68.6 10/31/18 19:35 J1H 11/1/18 15:39 CGS ASW846 8270D Benzo(k)fluoranthene 103 ug/kg 68.6 10/31/18 19:35 J1H 11/1/18 15:39 CGS ASW846 8270D Biphenyl ND ug/kg 137 10/31/18 19:35 J1H 11/1/18 15:39 CGS ASW846 8270D 4-Bromophenyl-phenylether ND ug/kg 137 10/31/18 19:35 J1H 11/1/18 15:39 CGS ASW846 8270D Butylbenzylphthalate ND ug/kg 137 10/31/18 19:35 J1H 11/1/18 15:39 CGS ASW846 8270D Caprolactam ND ug/kg 274 10/31/18 19:35 J1H 11/1/18 15:39 CGS A1 SW846 8270D Carbazole ND ug/kg 137 10/31/18 19:35 J1H 11/1/18 15:39 CGS ASW846 8270D 4-Chloro-3-methylphenol ND ug/kg 274 10/31/18 19:35 J1H 11/1/18 15:39 CGS ASW846 8270D 4-Chloroaniline ND ug/kg 274 10/31/18 19:35 J1H 11/1/18 15:39 CGS ASW846 8270D bis(2-Chloroethoxy)methane ND ug/kg 137 10/31/18 19:35 J1H 11/1/18 15:39 CGS ASW846 8270D bis(2-Chloroethyl)ether ND ug/kg 137 10/31/18 19:35 J1H 11/1/18 15:39 CGS ASW846 8270D bis(2-Chloroisopropyl)ether ND ug/kg 137 10/31/18 19:35 J1H 11/1/18 15:39 CGS ASW846 8270D 2-Chloronaphthalene ND ug/kg 137 10/31/18 19:35 J1H 11/1/18 15:39 CGS ASW846 8270D 2-Chlorophenol ND ug/kg 274 10/31/18 19:35 J1H 11/1/18 15:39 CGS ASW846 8270D 4-Chlorophenyl-phenylether ND ug/kg 137 10/31/18 19:35 J1H 11/1/18 15:39 CGS ASW846 8270D Chrysene 214 ug/kg 68.6 10/31/18 19:35 J1H 11/1/18 15:39 CGS ASW846 8270D mp-Cresol ND ug/kg 274 10/31/18 19:35 J1H 11/1/18 15:39 CGS ASW846 8270D o-Cresol ND ug/kg 274 10/31/18 19:35 J1H 11/1/18 15:39 CGS ASW846 8270D Di-n-Butylphthalate ND ug/kg 137 10/31/18 19:35 J1H 11/1/18 15:39 CGS ASW846 8270D Di-n-Octylphthalate ND ug/kg 137 10/31/18 19:35 J1H 11/1/18 15:39 CGS ASW846 8270D

Report ID: 2346875 - 11/7/2018 Page 7 of 13

ANALYTICAL RESULTS

10/29/2018 21:45Drum Comp

Matrix: Solid

Parameters

Lab ID:

Sample ID:

2346875001

Results Units RDL Prepared By ByAnalyzedFlag

Date Collected:

Date Received:

10/26/2018 05:39

CntrMethod

Dibenzo(a,h)anthracene ND ug/kg 68.6 10/31/18 19:35 J1H 11/1/18 15:39 CGS ASW846 8270D Dibenzofuran ND ug/kg 137 10/31/18 19:35 J1H 11/1/18 15:39 CGS ASW846 8270D 3,3-Dichlorobenzidine ND ug/kg 274 10/31/18 19:35 J1H 11/1/18 15:39 CGS ASW846 8270D 2,4-Dichlorophenol ND ug/kg 274 10/31/18 19:35 J1H 11/1/18 15:39 CGS ASW846 8270D Diethylphthalate ND ug/kg 137 10/31/18 19:35 J1H 11/1/18 15:39 CGS ASW846 8270D 2,4-Dimethylphenol ND ug/kg 274 10/31/18 19:35 J1H 11/1/18 15:39 CGS ASW846 8270D Dimethylphthalate ND ug/kg 137 10/31/18 19:35 J1H 11/1/18 15:39 CGS ASW846 8270D 2,4-Dinitrophenol ND ug/kg 548 10/31/18 19:35 J1H 11/1/18 15:39 CGS ASW846 8270D 2,4-Dinitrotoluene ND ug/kg 137 10/31/18 19:35 J1H 11/1/18 15:39 CGS ASW846 8270D 2,6-Dinitrotoluene ND ug/kg 137 10/31/18 19:35 J1H 11/1/18 15:39 CGS ASW846 8270D 1,4-Dioxane ND ug/kg 137 10/31/18 19:35 J1H 11/1/18 15:39 CGS ASW846 8270D bis(2-Ethylhexyl)phthalate ND ug/kg 137 10/31/18 19:35 J1H 11/1/18 15:39 CGS ASW846 8270D Fluoranthene 452 ug/kg 68.6 10/31/18 19:35 J1H 11/1/18 15:39 CGS ASW846 8270D Fluorene ND ug/kg 68.6 10/31/18 19:35 J1H 11/1/18 15:39 CGS ASW846 8270D Hexachlorobenzene ND ug/kg 137 10/31/18 19:35 J1H 11/1/18 15:39 CGS ASW846 8270D Hexachlorobutadiene ND ug/kg 137 10/31/18 19:35 J1H 11/1/18 15:39 CGS ASW846 8270D Hexachlorocyclopentadiene ND ug/kg 274 10/31/18 19:35 J1H 11/1/18 15:39 CGS A2 SW846 8270D Hexachloroethane ND ug/kg 137 10/31/18 19:35 J1H 11/1/18 15:39 CGS ASW846 8270D Indeno(1,2,3-cd)pyrene 136 ug/kg 68.6 10/31/18 19:35 J1H 11/1/18 15:39 CGS ASW846 8270D Isophorone ND ug/kg 137 10/31/18 19:35 J1H 11/1/18 15:39 CGS ASW846 8270D 2-Methyl-4,6-dinitrophenol ND ug/kg 274 10/31/18 19:35 J1H 11/1/18 15:39 CGS ASW846 8270D 2-Methylnaphthalene ND ug/kg 137 10/31/18 19:35 J1H 11/1/18 15:39 CGS ASW846 8270D Naphthalene ND ug/kg 68.6 10/31/18 19:35 J1H 11/1/18 15:39 CGS ASW846 8270D 2-Nitroaniline ND ug/kg 274 10/31/18 19:35 J1H 11/1/18 15:39 CGS ASW846 8270D 3-Nitroaniline ND ug/kg 274 10/31/18 19:35 J1H 11/1/18 15:39 CGS ASW846 8270D 4-Nitroaniline ND ug/kg 274 10/31/18 19:35 J1H 11/1/18 15:39 CGS ASW846 8270D Nitrobenzene ND ug/kg 137 10/31/18 19:35 J1H 11/1/18 15:39 CGS ASW846 8270D 2-Nitrophenol ND ug/kg 274 10/31/18 19:35 J1H 11/1/18 15:39 CGS ASW846 8270D 4-Nitrophenol ND ug/kg 274 10/31/18 19:35 J1H 11/1/18 15:39 CGS ASW846 8270D N-Nitroso-di-n-propylamine ND ug/kg 137 10/31/18 19:35 J1H 11/1/18 15:39 CGS ASW846 8270D N-Nitrosodiphenylamine ND ug/kg 137 10/31/18 19:35 J1H 11/1/18 15:39 CGS ASW846 8270D n-Nonane ND ug/kg 274 10/31/18 19:35 J1H 11/1/18 15:39 CGS A3 SW846 8270D Pentachlorophenol ND ug/kg 274 10/31/18 19:35 J1H 11/1/18 15:39 CGS ASW846 8270D Phenanthrene 285 ug/kg 68.6 10/31/18 19:35 J1H 11/1/18 15:39 CGS ASW846 8270D Phenol ND ug/kg 274 10/31/18 19:35 J1H 11/1/18 15:39 CGS ASW846 8270D Pyrene 381 ug/kg 68.6 10/31/18 19:35 J1H 11/1/18 15:39 CGS ASW846 8270D 1,2,4,5-Tetrachlorobenzene ND ug/kg 137 10/31/18 19:35 J1H 11/1/18 15:39 CGS ASW846 8270D 2,3,4,6-Tetrachlorophenol ND ug/kg 274 10/31/18 19:35 J1H 11/1/18 15:39 CGS ASW846 8270D

Report ID: 2346875 - 11/7/2018 Page 8 of 13

ANALYTICAL RESULTS

10/29/2018 21:45Drum Comp

Matrix: Solid

Parameters

Lab ID:

Sample ID:

2346875001

Results Units RDL Prepared By ByAnalyzedFlag

Date Collected:

Date Received:

10/26/2018 05:39

CntrMethod

2,4,5-Trichlorophenol ND ug/kg 274 10/31/18 19:35 J1H 11/1/18 15:39 CGS ASW846 8270D 2,4,6-Trichlorophenol ND ug/kg 274 10/31/18 19:35 J1H 11/1/18 15:39 CGS ASW846 8270D

Surrogate Recoveries Flag UnitsResults Limits Prepared By Analyzed By CntrMethod

2,4,6-Tribromophenol (S) 93.6 % 19 - 132 10/31/18 19:35 J1H 11/1/18 15:39 CGS ASW846 8270D 2-Fluorobiphenyl (S) 73.9 % 40 - 110 10/31/18 19:35 J1H 11/1/18 15:39 CGS ASW846 8270D 2-Fluorophenol (S) 84.2 % 26 - 116 10/31/18 19:35 J1H 11/1/18 15:39 CGS ASW846 8270D Nitrobenzene-d5 (S) 82.5 % 38 - 112 10/31/18 19:35 J1H 11/1/18 15:39 CGS ASW846 8270D Phenol-d5 (S) 84.3 % 35 - 111 10/31/18 19:35 J1H 11/1/18 15:39 CGS ASW846 8270D Terphenyl-d14 (S) 84.8 % 45 - 126 10/31/18 19:35 J1H 11/1/18 15:39 CGS ASW846 8270D

Library Search - SemiVolatiles Dodecane, 2,6,11-trimethyl- 450 ug/kg 10/31/18 19:35 J1H 11/1/18 15:39 CGS AJ N SW846 8270D Hexadecanoic acid 408 ug/kg 10/31/18 19:35 J1H 11/1/18 15:39 CGS AJ N SW846 8270D

PCBs Total Polychlorinated Biphenyl

ND mg/kg 0.39 10/30/18 04:00 JTH 11/3/18 14:27 EGO ASW846 8082A

Aroclor-1016 ND mg/kg 0.043 10/30/18 04:00 JTH 11/3/18 14:27 EGO ASW846 8082A Aroclor-1221 ND mg/kg 0.043 10/30/18 04:00 JTH 11/3/18 14:27 EGO ASW846 8082A Aroclor-1232 ND mg/kg 0.043 10/30/18 04:00 JTH 11/3/18 14:27 EGO ASW846 8082A Aroclor-1242 ND mg/kg 0.043 10/30/18 04:00 JTH 11/3/18 14:27 EGO ASW846 8082A Aroclor-1248 ND mg/kg 0.043 10/30/18 04:00 JTH 11/3/18 14:27 EGO ASW846 8082A Aroclor-1254 ND mg/kg 0.043 10/30/18 04:00 JTH 11/3/18 14:27 EGO ASW846 8082A Aroclor-1260 ND mg/kg 0.043 10/30/18 04:00 JTH 11/3/18 14:27 EGO ASW846 8082A Aroclor-1262 ND mg/kg 0.043 10/30/18 04:00 JTH 11/3/18 14:27 EGO ASW846 8082A Aroclor-1268 ND mg/kg 0.043 10/30/18 04:00 JTH 11/3/18 14:27 EGO ASW846 8082A

Surrogate Recoveries Flag UnitsResults Limits Prepared By Analyzed By CntrMethod

Decachlorobiphenyl (S) 65.1 % 49 - 115 10/30/18 04:00 JTH 11/3/18 14:27 EGO ASW846 8082A Tetrachloro-m-xylene (S) 67.4 % 27 - 137 10/30/18 04:00 JTH 11/3/18 14:27 EGO ASW846 8082A

WET CHEMISTRY

Moisture 27.1 % 0.1 10/30/18 13:13 AXDS2540G-11 Total Solids 72.9 % 0.1 10/30/18 13:13 AXDS2540G-11

TCLP METALS

Arsenic, Total ND mg/L 0.14 11/1/18 14:40 BMK 11/2/18 09:56 SRT A3SW846 6010C Barium, Total ND mg/L 2.8 11/1/18 14:40 BMK 11/2/18 09:56 SRT A3SW846 6010C Cadmium, Total ND mg/L 0.011 11/1/18 14:40 BMK 11/2/18 09:56 SRT A3SW846 6010C Chromium, Total ND mg/L 0.028 11/1/18 14:40 BMK 11/2/18 09:56 SRT A3SW846 6010C Lead, Total 0.055 mg/L 0.033 11/1/18 14:40 BMK 11/2/18 09:56 SRT A3SW846 6010C

Report ID: 2346875 - 11/7/2018 Page 9 of 13

ANALYTICAL RESULTS

10/29/2018 21:45Drum Comp

Matrix: Solid

Parameters

Lab ID:

Sample ID:

2346875001

Results Units RDL Prepared By ByAnalyzedFlag

Date Collected:

Date Received:

10/26/2018 05:39

CntrMethod

Mercury, Total ND mg/L 0.0020 11/2/18 08:30 AXC 11/2/18 11:20 AXC A4SW846 7470A Selenium, Total ND mg/L 0.11 11/1/18 14:40 BMK 11/2/18 09:56 SRT A3SW846 6010C Silver, Total ND mg/L 0.022 11/1/18 14:40 BMK 11/2/18 09:56 SRT A3SW846 6010C

METALS

Arsenic, Total 4.5 mg/kg 2.0 10/31/18 14:40 AHI 11/2/18 05:23 LXC A2SW846 6020A Barium, Total 69.4 mg/kg 3.3 10/31/18 14:40 AHI 11/2/18 05:23 LXC A2SW846 6020A Cadmium, Total ND mg/kg 0.66 10/31/18 14:40 AHI 11/2/18 05:23 LXC A2SW846 6020A Chromium, Total 23.7 mg/kg 1.3 10/31/18 14:40 AHI 11/2/18 05:23 LXC A2SW846 6020A Lead, Total 29.8 mg/kg 1.3 10/31/18 14:40 AHI 11/2/18 05:23 LXC A2SW846 6020A Mercury, Total 0.28 mg/kg 0.061 10/31/18 10:05 AXC 10/31/18 12:25 AXC A1SW846 7471B Selenium, Total ND mg/kg 3.3 10/31/18 14:40 AHI 11/2/18 05:23 LXC A2SW846 6020A Silver, Total ND mg/kg 1.3 10/31/18 14:40 AHI 11/2/18 05:23 LXC A2SW846 6020A

TCLP SEMI-VOLATILES

mp-Cresol ND ug/L 60.0 11/1/18 11:00 CAC 11/1/18 23:31 DHF ASW846 8270D o-Cresol ND ug/L 60.0 11/1/18 11:00 CAC 11/1/18 23:31 DHF ASW846 8270D 1,4-Dichlorobenzene ND ug/L 60.0 11/1/18 11:00 CAC 11/1/18 23:31 DHF ASW846 8270D 2,4-Dinitrotoluene ND ug/L 60.0 11/1/18 11:00 CAC 11/1/18 23:31 DHF ASW846 8270D Hexachlorobenzene ND ug/L 60.0 11/1/18 11:00 CAC 11/1/18 23:31 DHF ASW846 8270D Hexachlorobutadiene ND ug/L 60.0 11/1/18 11:00 CAC 11/1/18 23:31 DHF ASW846 8270D Hexachloroethane ND ug/L 60.0 11/1/18 11:00 CAC 11/1/18 23:31 DHF ASW846 8270D Nitrobenzene ND ug/L 60.0 11/1/18 11:00 CAC 11/1/18 23:31 DHF ASW846 8270D Pentachlorophenol ND ug/L 120 11/1/18 11:00 CAC 11/1/18 23:31 DHF ASW846 8270D Pyridine ND ug/L 60.0 11/1/18 11:00 CAC 11/1/18 23:31 DHF ASW846 8270D 2,4,5-Trichlorophenol ND ug/L 60.0 11/1/18 11:00 CAC 11/1/18 23:31 DHF ASW846 8270D 2,4,6-Trichlorophenol ND ug/L 60.0 11/1/18 11:00 CAC 11/1/18 23:31 DHF ASW846 8270D

Surrogate Recoveries Flag UnitsResults Limits Prepared By Analyzed By CntrMethod

2,4,6-Tribromophenol (S) 81.6 % 47 - 128 11/1/18 11:00 CAC 11/1/18 23:31 DHF ASW846 8270D 2-Fluorobiphenyl (S) 81.6 % 52 - 118 11/1/18 11:00 CAC 11/1/18 23:31 DHF ASW846 8270D 2-Fluorophenol (S) 54.3 % 20 - 87 11/1/18 11:00 CAC 11/1/18 23:31 DHF ASW846 8270D Nitrobenzene-d5 (S) 90.3 % 27 - 139 11/1/18 11:00 CAC 11/1/18 23:31 DHF ASW846 8270D Phenol-d5 (S) 35.7 % 10 - 81 11/1/18 11:00 CAC 11/1/18 23:31 DHF ASW846 8270D Terphenyl-d14 (S) 105 % 46 - 133 11/1/18 11:00 CAC 11/1/18 23:31 DHF ASW846 8270D

TCLP PESTICIDES

gamma-BHC ND ug/L 0.40 11/1/18 23:10 DXL 11/2/18 17:33 RWS ASW846 8081B Chlordane ND ug/L 10.0 11/1/18 23:10 DXL 11/2/18 17:33 RWS ASW846 8081B Endrin ND ug/L 0.40 11/1/18 23:10 DXL 11/2/18 17:33 RWS ASW846 8081B Heptachlor ND ug/L 0.40 11/1/18 23:10 DXL 11/2/18 17:33 RWS ASW846 8081B

Report ID: 2346875 - 11/7/2018 Page 10 of 13

ANALYTICAL RESULTS

10/29/2018 21:45Drum Comp

Matrix: Solid

Parameters

Lab ID:

Sample ID:

2346875001

Results Units RDL Prepared By ByAnalyzedFlag

Date Collected:

Date Received:

10/26/2018 05:39

CntrMethod

Heptachlor Epoxide ND ug/L 0.40 11/1/18 23:10 DXL 11/2/18 17:33 RWS ASW846 8081B Methoxychlor ND ug/L 0.40 11/1/18 23:10 DXL 11/2/18 17:33 RWS ASW846 8081B Toxaphene ND ug/L 20.0 11/1/18 23:10 DXL 11/2/18 17:33 RWS ASW846 8081B

Surrogate Recoveries Flag UnitsResults Limits Prepared By Analyzed By CntrMethod

Decachlorobiphenyl (S) 66.2 % 30 - 140 11/1/18 23:10 DXL 11/2/18 17:33 RWS ASW846 8081B Tetrachloro-m-xylene (S) 71.1 % 30 - 123 11/1/18 23:10 DXL 11/2/18 17:33 RWS ASW846 8081B

TCLP HERBICIDES

2,4-D ND ug/L 4.0 11/1/18 19:05 DXL 11/2/18 14:41 KJH ASW846 8151A 2,4,5-TP ND ug/L 6.0 11/1/18 19:05 DXL 11/2/18 14:41 KJH ASW846 8151A

Surrogate Recoveries Flag UnitsResults Limits Prepared By Analyzed By CntrMethod

2,4-Dichlorophenylacetic acid (S)

86.3 % 14 - 172 11/1/18 19:05 DXL 11/2/18 14:41 KJH ASW846 8151A

Project Coordinator Mrs. Kelli L Wolfgang

Report ID: 2346875 - 11/7/2018 Page 11 of 13

ANALYTICAL RESULTS

PARAMETER QUALIFIERS

#Lab ID Analytical MethodSample ID Analyte

The QC sample type CCV for method SW846 8270D was outside the control limits for the analyte Caprolactam. The % Recovery was reported as 74 and the control limits were 80 to 120.

2346875001 SW846 8270DDrum Comp Caprolactam

The QC sample type CCV for method SW846 8270D was outside the control limits for the analyte Hexachlorocyclopentadiene. The % Recovery was reported as 78.3 and the control limits were 80 to 120.

2346875001 SW846 8270DDrum Comp Hexachlorocyclopentadiene

ALS-Middletown does not hold PADEP NELAP accreditation for this analyte by this method of analysis.

2346875001 SW846 8270DDrum Comp n-Nonane

Report ID: 2346875 - 11/7/2018 Page 12 of 13

ANALYSIS - PREP METHOD CROSS REFERENCE TABLE

Lab ID Sample ID Analysis Method Prep Method

Workorder: 2346875 PNY-Bldg 633 Cooling

2346875001 Drum Comp Lib Search SV 2346875001 Drum Comp Lib Search VOC 2346875001 Drum Comp S2540G-11 2346875001 Drum Comp SW846 6010C SW846 3015 2346875001 Drum Comp SW846 6020A SW846 3051 2346875001 Drum Comp SW846 7470A SW846 7470A 2346875001 Drum Comp SW846 7471B SW846 7471B 2346875001 Drum Comp SW846 8081B SW846 3510C 2346875001 Drum Comp SW846 8082A SW846 3546 2346875001 Drum Comp SW846 8151A SW846 8151A 2346875001 Drum Comp SW846 8260B SW846 5035 2346875001 Drum Comp SW846 8260C 2346875001 Drum Comp SW846 8270D SW846 3510C 2346875001 Drum Comp SW846 8270D SW846 3546

P age 13 of 13

W ednesday, N ovem ber 07, 2018 6:32:30 A

M

EMSL Analytical, Inc.

200 Route 130 North Cinnaminson, NJ 08077

Tel/Fax: (800) 220-3675 / (856) 786-5974 http://www.EMSL.com / cinnasblab@EMSL.com

041832570EMSL Order:

Customer ID: ARCE78

Customer PO: 865-8

Project ID:

Attention: Phone:Dave Leety (410) 365-6457

Fax:Arc Environmental (410) 962-1065

Received Date:1311 Haubert Street 10/30/2018 9:25 AM

Analysis Date:Baltimore, MD 21230 11/13/2018

Collected Date: 10/29/2018

Project: 865-8

Test Report: Asbestos Analysis of Bulk Materials via EPA 600/R-93/116 Method using Polarized

Light Microscopy

Sample Description Appearance % Fibrous % Non-Fibrous

Non-Asbestos Asbestos

% Type

Drum Comp

041832570-0001

None DetectedNon-fibrous (Other)100%Brown

Non-Fibrous

Homogeneous

Soil

Sample milled prior to analysis

Analyst(s)

Andrew Castellano (1) Benjamin Ellis, Laboratory Manager or Other Approved Signatory

EMSL maintains liability limited to cost of analysis . The above analyses were performed in general compliance with Appendix E to Subpart E of 40 CFR (previously EPA 600/M4-82-020 "Interim

Method"), but augmented with procedures outlined in the 1993 ("final") version of the method. This report relates only to the samples reported above, and may not be reproduced, except in full, without written approval by EMSL. EMSL bears no responsibility for sample collection activities or analytical method limitations . Interpretation and use of test results are the responsibility of the client. All samples received in acceptable condition unless otherwise noted. This report must not be used by the client to claim product certification, approval, or endorsement by NVLAP, NIST or any agency of the federal government. EMSL recommends gravimetric reduction for all non -friable organically bound materials prior to analysis. Estimation of uncertainty is available on request.

Samples analyzed by EMSL Analytical, Inc. Cinnaminson, NJ NVLAP Lab Code 101048-0, AIHA-LAP, LLC-IHLAP Lab 100194, NYS ELAP 10872, NJ DEP 03036, PA ID# 68-00367

Initial report from: 11/13/2018 15:34:54

Page 1 of 1ASB_PLM_0008_0001 - 1.78 Printed: 11/13/2018 3:34 PM

OrderID: 041832570

File details come from the government source that posted it. Updated .