B19011633-01-22-19.pdf

ANALYTICAL SUMMARY REPORT

The analyses presented in this report were performed by Energy Laboratories, Inc., 1120 S 27th St., Billings, MT 59101, unless otherwise noted. Any exceptions or problems with the analyses are noted in the Laboratory Analytical Report, the QA/QC Summary Report, or the Case Narrative.

The results as reported relate only to the item(s) submitted for testing.

If you have any questions regarding these test results, please call.

Lab ID Client Sample ID Collect Date Receive Date Matrix Test

Report Approved By:

B19011633-001 24 Hr Composite 01/22/19 8:00 01/23/19 Waste Water Biochemical Oxygen Demand, 5 Day

B19011633-002 Grab 01/22/19 8:00 01/23/19 Waste Water Oil & Grease, Gravimetric

SIA Solutions

Project Name: Malmstrom AFB (Lift Station Bldg 1995)

Work Order: B19011633

15115 Park Row Ste 125

Houston, TX 77084-4945

February 01, 2019

Energy Laboratories Inc Billings MT received the following 2 samples for SIA Solutions on 1/23/2019 for analysis.

Project: Malmstrom AFB (Lift Station Bldg 1995)

CLIENT: SIA Solutions

Work Order: B19011633 CASE NARRATIVE

02/01/19Report Date:

Tests associated with analyst identified as ELI-G were subcontracted to Energy Laboratories, 400 W Boxelder Rd, Gillette, WY, EPA Number WY00006.

The LCS (GGA3) from the Biochemical Oxygen Demand (BOD) analysis on 1/23/2019 did not get seeded correctly resulting in the LCS recovering outside of the EPA recommended control limits of 85-115%.

The LCS (GGA2) from the Carbonaceous Biochemical Oxygen Demand (CBOD) analysis was performed on the same day and falls within the EPA recommended control limits and will be included in the QA/QC report.

LABORATORY ANALYTICAL REPORT

Client: SIA Solutions

Project: Malmstrom AFB (Lift Station Bldg 1995)

Lab ID: B19011633-001

Client Sample ID: 24 Hr Composite

Collection Date: 01/22/19 08:00

Matrix: Waste Water

Report Date: 02/01/19

DateReceived: 01/23/19

Prepared by Billings, MT Branch

Analyses Result Units Analysis Date / ByRL Method

MCL/

QCLQualifiers

AGGREGATE ORGANICS

01/23/19 18:19 / ean86mg/L150Oxygen Demand, Biochemical (BOD) A5210 B

Report

Definitions:

RL - Analyte reporting limit. MCL - Maximum contaminant level.

QCL - Quality control limit. ND - Not detected at the reporting limit.

LABORATORY ANALYTICAL REPORT

Project: Malmstrom AFB (Lift Station Bldg 1995)

Lab ID: B19011633-002

Client Sample ID: Grab

Collection Date: 01/22/19 08:00

Matrix: Waste Water

Report Date: 02/01/19

DateReceived: 01/23/19

Prepared by Billings, MT Branch

Analyses Result Units Analysis Date / ByRL Method

MCL/

QCLQualifiers

ORGANIC CHARACTERISTICS

01/25/19 08:21 / eli-g1mg/L13Oil & Grease (HEM) E1664A

Report

Definitions:

RL - Analyte reporting limit. MCL - Maximum contaminant level.

QCL - Quality control limit. ND - Not detected at the reporting limit.

Project: Malmstrom AFB (Lift Station Bldg 1995)

Work Order: B19011633

QA/QC Summary Report

02/01/19Report Date:

Analyte Result %REC RPDLow Limit High Limit RPDLimitRLUnits QualCount

Prepared by Billings, MT Branch

Method: A5210 B Batch: 190123_1_BOD5-W

Lab ID: Dil-H201_190123 01/23/19 11:38Dilution Water Blank Run: BOD-SP2000_190123A

Oxygen Demand, Biochemical (BOD) 0 0.20 mg/L

Lab ID: GGA3_190123 01/23/19 11:55Laboratory Control Sample Run: BOD-SP2000_190123A

Oxygen Demand, Biochemical (BOD) 21 85 1154141 mg/L S

No BOD dilution depleted greater than 2.0 mg/L DO.

All glucose-glutamic acid check standard(s) fall outside quality control advisory limits.

Lab ID: B19011591-001ADUP 01/23/19 12:07Sample Duplicate Run: BOD-SP2000_190123A

Oxygen Demand, Biochemical (BOD) 152 0.913 mg/L

Lab ID: GGA2_190123 01/23/19 17:57Laboratory Control Sample Run: BOD-SP2000_190123A

Oxygen Demand, Biochemical (BOD) 92 85 11528180 mg/L

This LCS is from the Carbonaceous BOD analysis performed on the same day.

Qualifiers:

RL - Analyte reporting limit. ND - Not detected at the reporting limit.

S - Spike recovery outside of advisory limits.

Shipping container/cooler in good condition?

Custody seals intact on all shipping container(s)/cooler(s)?

Custody seals intact on all sample bottles?

Chain of custody present?

Chain of custody signed when relinquished and received?

Chain of custody agrees with sample labels?

Samples in proper container/bottle?

Sample containers intact?

Sufficient sample volume for indicated test?

All samples received within holding time?

(Exclude analyses that are considered field parameters such as pH, DO, Res Cl, Sulfite, Ferrous Iron, etc.)

Container/Temp Blank temperature:

Water - VOA vials have zero headspace?

Water - pH acceptable upon receipt?

Yes

Yes

Yes

Yes

Yes

Yes

Yes

Yes

Yes

Yes

Yes

Yes

No

No

No

No

No

No

No

No

No

No

No

No

R £

R

R

R

R

R

R

R

R

R

R

Not Present

Not Present

Not Present

No VOA vials submitted

Not Applicable £

R

0.5°C On Ice

1/23/2019Darcy Chirrick

Return-UPS Ground se

Date Received:

Received by:

Login completed by:

Carrier name:

BL2000\gmccartney

1/23/2019

Reviewed by:

Reviewed Date:

Contact and Corrective Action Comments:

None

Temp Blank received in all shipping container(s)/cooler(s)? Yes NoR £ Not Applicable £

Lab measurement of analytes considered field parameters that require analysis within 15 minutes of sampling such as pH, Dissolved Oxygen and Residual Chlorine, are qualified as being analyzed outside of recommended holding time.

Solid/soil samples are reported on a wet weight basis (as received) unless specifically indicated. If moisture corrected, data units are typically noted as –dry. For agricultural and mining soil parameters/characteristics, all samples are dried and ground prior to sample analysis.

Standard Reporting Procedures:

Work Order Receipt Checklist

SIA Solutions B19011633