J185280_1 Std_Tal_L4 Final Report_Part8.pdf

Report Date: 02-Dec-2024 12:38:37 Chrom Revision: 2.3 12-Nov-2024 16:55:22 Manual Integration/User Assign Peak Report

Eurofins Edison

Data File: \\chromfs\Edison\ChromData\CBNAGC1\20241202-184171.b\1F0017321.D

Injection Date: 02-Dec-2024 10:41:43 Instrument ID: CBNAGC1

Lims ID: IC

Client ID:

Operator ID: ALS Bottle#: 3 Worklist Smp#: 3

Injection Vol: 1.0 ul Dil. Factor: 1.0000

Method: ALEPH1F Limit Group: GC NJEPH ICAL

Column: Rtx Mineral Oil ( 0.32 mm) Detector GC fid1a

7 Hexadecane, CAS: 544-76-3 Signal: 1

Processing Integration Results

RT: 3.16

Area: 659507

Amount: 9.850656

Amount Units: ug/ml

2.8 3.0 3.2 3.4 Min

Y

X

GC FID1A, 1F0017321.D

.1

Manual Integration Results

RT: 3.16

Area: 661592

Amount: 10.113994

Amount Units: ug/ml

2.8 3.0 3.2 3.4 Min

RT

Y

X

Reviewer: OR9X, 02-Dec-2024 11:14:11 -05:00:00 (UTC)

Audit Action: Assigned New Baseline Audit Reason: Peak not integrated

Page 7874 of 21459

Eurofins Edison

Data File: \\chromfs\Edison\ChromData\CBNAGC1\20241202-184171.b\1F0017321.D

Injection Date: 02-Dec-2024 10:41:43 Instrument ID: CBNAGC1

Lims ID: IC

Client ID:

Operator ID: ALS Bottle#: 3 Worklist Smp#: 3

Injection Vol: 1.0 ul Dil. Factor: 1.0000

Method: ALEPH1F Limit Group: GC NJEPH ICAL

Column: Rtx Mineral Oil ( 0.32 mm) Detector GC fid1a

A 25 C9-C40, RT: 3.463, CAS: STL00695

Signal: 1

Processing Integration Results

RT: 3.49

Response: 12850506

Amount: 195.2158

0.6 1.2 1.8 2.4 3.0 3.6 4.2 4.8 5.4 6.0 6.6 Min

Y

X

GC FID1A, 1F0017321.D

o

-T e rp h e n y l(

.6

-C h lo ro o c ta d e c a n e

.1

Manual Integration Results

RT: 3.46

Response: 12888955

Amount: 196.8687

0.6 1.2 1.8 2.4 3.0 3.6 4.2 4.8 5.4 6.0 6.6 Min

Y

X

GC FID1A, 1F0017321.D

o

-T e rp h e n

-C h lo ro o c ta d e c a n e

.1

Reviewer: OR9X, 02-Dec-2024 12:38:13 -05:00:00 (UTC)

Audit Action: Assigned New Baseline Audit Reason: Baseline Smoothing

Page 7875 of 21459

Eurofins Edison

Data File: \\chromfs\Edison\ChromData\CBNAGC1\20241202-184171.b\1F0017321.D

Injection Date: 02-Dec-2024 10:41:43 Instrument ID: CBNAGC1

Lims ID: IC

Client ID:

Operator ID: ALS Bottle#: 3 Worklist Smp#: 3

Injection Vol: 1.0 ul Dil. Factor: 1.0000

Method: ALEPH1F Limit Group: GC NJEPH ICAL

Column: Rtx Mineral Oil ( 0.32 mm) Detector GC fid1a

17 n-Octadecane, CAS: 593-45-3 Signal: 1

Processing Integration Results

RT: 3.60

Area: 688878

Amount: 10.031002

Amount Units: ug/ml

3.3 3.5 3.7 3.9 Min

Y

X

.5

Manual Integration Results

RT: 3.60

Area: 694774

Amount: 10.601605

Amount Units: ug/ml

3.3 3.5 3.7 3.9 Min

RT

Y

X

.5

Reviewer: OR9X, 02-Dec-2024 11:14:13 -05:00:00 (UTC)

Page 7876 of 21459

Report Date: 02-Dec-2024 12:38:38 Chrom Revision: 2.3 12-Nov-2024 16:55:22

Eurofins Edison

Data File: \\chromfs\Edison\ChromData\CBNAGC1\20241202-184171.b\1F0017321.D

Injection Date: 02-Dec-2024 10:41:43 Instrument ID: CBNAGC1

Lims ID: IC

Client ID:

Operator ID: ALS Bottle#: 3 Worklist Smp#: 3

Injection Vol: 1.0 ul Dil. Factor: 1.0000

Method: ALEPH1F Limit Group: GC NJEPH ICAL

Column: Rtx Mineral Oil ( 0.32 mm) Detector GC fid1a

A 26 C16-C21 Aliphatics, RT: 3.766, CAS: STL00950 Signal: 1

Processing Integration Results

RT: 3.78

Response: 2143152

Amount: 29.087686

3.1 4.1 Min

Y

X

GC FID1A, 1F0017321.D

o

-T e rp h e n

-C h lo ro o c ta d e c a n e

.1

Manual Integration Results

RT: 3.77

Response: 2226373

Amount: 31.083875

3.1 4.1 Min

Y

X

GC FID1A, 1F0017321.D

o

-T e rp h e n

-C h lo ro o c ta d e c a n e

.1

Reviewer: OR9X, 02-Dec-2024 11:14:11 -05:00:00 (UTC)

Page 7877 of 21459

Eurofins Edison

Data File: \\chromfs\Edison\ChromData\CBNAGC1\20241202-184171.b\1F0017321.D

Injection Date: 02-Dec-2024 10:41:43 Instrument ID: CBNAGC1

Lims ID: IC

Client ID:

Operator ID: ALS Bottle#: 3 Worklist Smp#: 3

Injection Vol: 1.0 ul Dil. Factor: 1.0000

Method: ALEPH1F Limit Group: GC NJEPH ICAL

Column: Rtx Mineral Oil ( 0.32 mm) Detector GC fid1a

22 icosane, CAS: 112-95-8 Signal: 1

Processing Integration Results

RT: 3.98

Area: 695213

Amount: 10.136792

Amount Units: ug/ml

3.7 3.9 4.1 4.3 Min

Y

X

.9

Manual Integration Results

RT: 3.98

Area: 697136

Amount: 10.842706

Amount Units: ug/ml

3.7 3.9 4.1 4.3 Min

RT

Y

X

Reviewer: OR9X, 02-Dec-2024 11:14:13 -05:00:00 (UTC)

Page 7878 of 21459

Eurofins Edison

Data File: \\chromfs\Edison\ChromData\CBNAGC1\20241202-184171.b\1F0017321.D

Injection Date: 02-Dec-2024 10:41:43 Instrument ID: CBNAGC1

Lims ID: IC

Client ID:

Operator ID: ALS Bottle#: 3 Worklist Smp#: 3

Injection Vol: 1.0 ul Dil. Factor: 1.0000

Method: ALEPH1F Limit Group: GC NJEPH ICAL

Column: Rtx Mineral Oil ( 0.32 mm) Detector GC fid1a

8 C21, CAS: 629-94-7

Signal: 1

Processing Integration Results

RT: 4.16

Area: 705533

Amount: 10.119413

Amount Units: ug/ml

3.8 4.0 4.2 4.4 Min

Y

X

Manual Integration Results

RT: 4.16

Area: 708108

Amount: 10.890930

Amount Units: ug/ml

3.8 4.0 4.2 4.4 Min

RT

Y

X

Reviewer: OR9X, 02-Dec-2024 11:14:13 -05:00:00 (UTC)

Page 7879 of 21459

Eurofins Edison

Data File: \\chromfs\Edison\ChromData\CBNAGC1\20241202-184171.b\1F0017321.D

Injection Date: 02-Dec-2024 10:41:43 Instrument ID: CBNAGC1

Lims ID: IC

Client ID:

Operator ID: ALS Bottle#: 3 Worklist Smp#: 3

Injection Vol: 1.0 ul Dil. Factor: 1.0000

Method: ALEPH1F Limit Group: GC NJEPH ICAL

Column: Rtx Mineral Oil ( 0.32 mm) Detector GC fid1a

21 n-Docosane, CAS: 629-97-0 Signal: 1

Processing Integration Results

RT: 4.33

Area: 682461

Amount: 10.164190

Amount Units: ug/ml

4.0 4.2 4.4 4.6 Min

Y

X

.3

Manual Integration Results

RT: 4.33

Area: 684503

Amount: 10.856832

Amount Units: ug/ml

4.0 4.2 4.4 4.6 Min

RT

Y

X

.3

Reviewer: OR9X, 02-Dec-2024 11:14:13 -05:00:00 (UTC)

Page 7880 of 21459

Report Date: 02-Dec-2024 12:38:38 Chrom Revision: 2.3 12-Nov-2024 16:55:22

Eurofins Edison

Data File: \\chromfs\Edison\ChromData\CBNAGC1\20241202-184171.b\1F0017321.D

Injection Date: 02-Dec-2024 10:41:43 Instrument ID: CBNAGC1

Lims ID: IC

Client ID:

Operator ID: ALS Bottle#: 3 Worklist Smp#: 3

Injection Vol: 1.0 ul Dil. Factor: 1.0000

Method: ALEPH1F Limit Group: GC NJEPH ICAL

Column: Rtx Mineral Oil ( 0.32 mm) Detector GC fid1a

A 27 C21-C40 Aliphatics, RT: 5.292, CAS: STL01059 Signal: 1

Processing Integration Results

RT: 5.32

Response: 5455281

Amount: 96.794007

4.0 4.2 4.4 4.6 4.8 5.0 5.2 5.4 5.6 5.8 6.0 6.2 6.4 6.6 Min

Y

X

GC FID1A, 1F0017321.D

Manual Integration Results

RT: 5.29

Response: 5458285

Amount: 94.588624

4.0 4.2 4.4 4.6 4.8 5.0 5.2 5.4 5.6 5.8 6.0 6.2 6.4 6.6 Min

Y

X

GC FID1A, 1F0017321.D

Reviewer: OR9X, 02-Dec-2024 11:14:13 -05:00:00 (UTC)

Page 7881 of 21459

Report Date: 02-Dec-2024 12:38:39 Chrom Revision: 2.3 12-Nov-2024 16:55:22

Eurofins Edison

Target Compound Quantitation Report

Data File: \\chromfs\Edison\ChromData\CBNAGC1\20241202-184171.b\1F0017322.D

Lims ID: IC

Client ID:

Sample Type: ICRT Calib Level: 3

Inject. Date: 02-Dec-2024 10:55:33 ALS Bottle#: 4 Worklist Smp#: 4

Injection Vol: 1.0 ul Dil. Factor: 1.0000

Sample Info: 460-0184171-004

Operator ID: Instrument ID: CBNAGC1

Sublist: chrom-ALEPH1F*sub7

Method: \\chromfs\Edison\ChromData\CBNAGC1\20241202-184171.b\ALEPH1F.m

Limit Group: GC NJEPH ICAL

Last Update: 02-Dec-2024 12:38:38 Calib Date: 02-Dec-2024 11:23:14

Integrator: Falcon

Quant Method: External Standard Quant By: Initial Calibration

Last ICal File: \\chromfs\Edison\ChromData\CBNAGC1\20241202-184171.b\1F0017324.D

Column 1 : Rtx Mineral Oil ( 0.32 mm) Det: GC fid1a

Process Host: CTX1673

First Level Reviewer: OR9X Date: 02-Dec-2024 11:13:49

Compound

RT

(min.)

Exp RT (min.)

Dlt RT (min.) Response

Cal Amt ug/ml

OnCol Amt ug/ml Flags

$ 1 o-Terphenyl 3.668 3.668 0.000 3856265 50.0 51.6

$ 2 1-Chlorooctadecane 4.111 4.111 0.000 2592337 50.0 49.5

3 n-Nonane 0.710 0.710 0.000 3663037 50.0 49.8

19 n-Decane 1.175 1.175 0.000 3651835 50.0 51.6

4 Naphthalene 1.804 1.804 0.000 3857566 50.0 50.5

5 Dodecane 2.035 2.035 0.000 3645671 50.0 49.8

6 2-Methylnaphthalene 2.208 2.208 0.000 3757337 50.0 50.9

18 n-Tetradecane 2.656 2.656 0.000 3565940 50.0 51.9

7 Hexadecane 3.165 3.165 0.000 3507710 50.0 53.6

17 n-Octadecane 3.605 3.605 0.000 3224254 50.0 49.2

22 icosane 3.988 3.988 0.000 3081836 50.0 47.9

8 C21 4.167 4.167 0.000 3106677 50.0 47.8

21 n-Docosane 4.335 4.335 0.000 2989965 50.0 47.4

20 n-Tetracosane 4.641 4.641 0.000 3009160 50.0 48.0

16 n-Hexacosane 4.898 4.898 0.000 3031817 50.0 48.6

12 n-Octacosane 5.125 5.125 0.000 3080035 50.0 49.2

11 Triacontane 5.330 5.330 0.000 3116091 50.0 49.9

10 Dotriacontane 5.524 5.524 0.000 3185099 50.0 51.5

15 Tetratriacontane 5.707 5.707 0.000 3255568 50.0 54.1

14 n-Hexatriacontane 5.882 5.882 0.000 3023505 50.0 57.5

13 C38 6.051 6.051 0.000 2602687 50.0 58.5

9 C40 6.216 6.216 0.000 1939385 50.0 55.1

A 23 C9-C12 Aliphatics 1.373 (0.610-2.135) 15079911 200.0 201.5

A 24 C12-C16 Aliphatics 2.700 (2.135-3.265) 11031989 150.0 141.0

A 25 C9-C40 3.463 (0.610-6.316) 66208142 1000.0 1011.3

A 26 C16-C21 Aliphatics 3.766 (3.265-4.267) 10322616 150.0 144.1

A 27 C21-C40 Aliphatics 5.292 (4.267-6.316) 29826142 500.0 516.9

Page 7882 of 21459

QC Flag Legend Processing Flags

Reagents:

SGEPH_ALIL3_00030 Amount Added: 1.00 Units: mL

Page 7883 of 21459

Data File: \\chromfs\Edison\ChromData\CBNAGC1\20241202-184171.b\1F0017322.D

Injection Date: 02-Dec-2024 10:55:33 Instrument ID: CBNAGC1 Operator ID:

Lims ID: IC Worklist Smp#: 4

Client ID:

Injection Vol: 1.0 ul Dil. Factor: 1.0000 ALS Bottle#: 4

Method: ALEPH1F Limit Group: GC NJEPH ICAL

Column: Rtx Mineral Oil ( 0.32 mm)

0.6 1.0 1.4 1.8 2.2 2.6 3.0 3.4 3.8 4.2 4.6 5.0 5.4 5.8 6.2 6.6 7.0 7.4 7.8 8.2 8.6 Min

Y

X

GC FID1A, 1F0017322.D

n

-N o n a n e

.7

-D e c a n e

.1

N a p h th a le n e

.8

D o d e c a n e

.0

-M e th y ln a p h th a le n e

.2

-T e tr a d e c a n e

.6

H e x a d e c a n e

.1

-O c ta d e c a n e

.6 o

-T e rp h e n ic s a n e

.9

-C h lo ro o c ta d e c a n e

.1

C

.1 o c o s a n e

.3 e tr a c o s a n e

.6

-H e x a c o s a n e

.8 c ta c o s a n e

.1

T ri a c o n ta n e

.3 tr ia c o n ta n e

.5 tr a tr ia c o n ta n e

.7 e x a tr ia c o n ta n e

.8

.0

.2

Page 7884 of 21459

Data File: \\chromfs\Edison\ChromData\CBNAGC1\20241202-184171.b\1F0017322.D

Injection Date: 02-Dec-2024 10:55:33 Instrument ID: CBNAGC1

Lims ID: IC

Client ID:

Operator ID: ALS Bottle#: 4 Worklist Smp#: 4

Injection Vol: 1.0 ul Dil. Factor: 1.0000

Method: ALEPH1F Limit Group: GC NJEPH ICAL

Column: Rtx Mineral Oil ( 0.32 mm) Detector GC fid1a

A 23 C9-C12 Aliphatics, CAS: STL00191

0.6 1.6 Min

Y

X

Page 7885 of 21459

Data File: \\chromfs\Edison\ChromData\CBNAGC1\20241202-184171.b\1F0017322.D

Injection Date: 02-Dec-2024 10:55:33 Instrument ID: CBNAGC1

Lims ID: IC

Client ID:

Operator ID: ALS Bottle#: 4 Worklist Smp#: 4

Injection Vol: 1.0 ul Dil. Factor: 1.0000

Method: ALEPH1F Limit Group: GC NJEPH ICAL

Column: Rtx Mineral Oil ( 0.32 mm) Detector GC fid1a

A 24 C12-C16 Aliphatics, CAS: STL00159

2.0 3.0 Min

Y

X

Page 7886 of 21459

Data File: \\chromfs\Edison\ChromData\CBNAGC1\20241202-184171.b\1F0017322.D

Injection Date: 02-Dec-2024 10:55:33 Instrument ID: CBNAGC1

Lims ID: IC

Client ID:

Operator ID: ALS Bottle#: 4 Worklist Smp#: 4

Injection Vol: 1.0 ul Dil. Factor: 1.0000

Method: ALEPH1F Limit Group: GC NJEPH ICAL

Column: Rtx Mineral Oil ( 0.32 mm) Detector GC fid1a

A 25 C9-C40, CAS: STL00695

0.6 0.9 1.2 1.5 1.8 2.1 2.4 2.7 3.0 3.3 3.6 3.9 4.2 4.5 4.8 5.1 5.4 5.7 6.0 6.3 6.6 6.9 Min

Y

X

GC FID1A, 1F0017322.D

o

-T e rp h e n

-C h lo ro o c ta d e c a n e

.1

Page 7887 of 21459

Data File: \\chromfs\Edison\ChromData\CBNAGC1\20241202-184171.b\1F0017322.D

Injection Date: 02-Dec-2024 10:55:33 Instrument ID: CBNAGC1

Lims ID: IC

Client ID:

Operator ID: ALS Bottle#: 4 Worklist Smp#: 4

Injection Vol: 1.0 ul Dil. Factor: 1.0000

Method: ALEPH1F Limit Group: GC NJEPH ICAL

Column: Rtx Mineral Oil ( 0.32 mm) Detector GC fid1a

A 26 C16-C21 Aliphatics, CAS: STL00950

3.1 4.1 Min

Y

X

GC FID1A, 1F0017322.D

o

-T e rp h e n

-C h lo ro o c ta d e c a n e

.1

Page 7888 of 21459

Data File: \\chromfs\Edison\ChromData\CBNAGC1\20241202-184171.b\1F0017322.D

Injection Date: 02-Dec-2024 10:55:33 Instrument ID: CBNAGC1

Lims ID: IC

Client ID:

Operator ID: ALS Bottle#: 4 Worklist Smp#: 4

Injection Vol: 1.0 ul Dil. Factor: 1.0000

Method: ALEPH1F Limit Group: GC NJEPH ICAL

Column: Rtx Mineral Oil ( 0.32 mm) Detector GC fid1a

A 27 C21-C40 Aliphatics, CAS: STL01059

4.0 4.2 4.4 4.6 4.8 5.0 5.2 5.4 5.6 5.8 6.0 6.2 6.4 6.6 Min

Y

X

Page 7889 of 21459

Report Date: 02-Dec-2024 12:38:40 Chrom Revision: 2.3 12-Nov-2024 16:55:22

Target Compound Quantitation Report

Data File: \\chromfs\Edison\ChromData\CBNAGC1\20241202-184171.b\1F0017323.D

Lims ID: IC

Client ID:

Sample Type: IC Calib Level: 4

Inject. Date: 02-Dec-2024 11:09:25 ALS Bottle#: 5 Worklist Smp#: 5

Injection Vol: 1.0 ul Dil. Factor: 1.0000

Sample Info: 460-0184171-005

Operator ID: Instrument ID: CBNAGC1

Sublist: chrom-ALEPH1F*sub7

Method: \\chromfs\Edison\ChromData\CBNAGC1\20241202-184171.b\ALEPH1F.m

Limit Group: GC NJEPH ICAL

Last Update: 02-Dec-2024 12:38:40 Calib Date: 02-Dec-2024 11:23:14

Integrator: Falcon

Quant Method: External Standard Quant By: Initial Calibration

Last ICal File: \\chromfs\Edison\ChromData\CBNAGC1\20241202-184171.b\1F0017324.D

Column 1 : Rtx Mineral Oil ( 0.32 mm) Det: GC fid1a

Process Host: CTX1673

Compound

RT

(min.)

Exp RT (min.)

Dlt RT (min.) Response

Cal Amt ug/ml

OnCol Amt ug/ml Flags

$ 1 o-Terphenyl 3.674 3.668 0.006 7281022 100.0 97.4

$ 2 1-Chlorooctadecane 4.118 4.111 0.007 4928054 100.0 94.2

3 n-Nonane 0.712 0.710 0.002 7103806 100.0 96.7

19 n-Decane 1.181 1.175 0.006 7113850 100.0 100.5

4 Naphthalene 1.812 1.804 0.008 7633281 100.0 99.9

5 Dodecane 2.040 2.035 0.005 7073287 100.0 96.7

6 2-Methylnaphthalene 2.213 2.208 0.005 7444482 100.0 100.9

18 n-Tetradecane 2.661 2.656 0.005 6929031 100.0 100.8

7 Hexadecane 3.171 3.165 0.006 6486894 100.0 99.2

17 n-Octadecane 3.612 3.605 0.007 5979531 100.0 91.2

22 icosane 3.995 3.988 0.007 5809241 100.0 90.4

8 C21 4.172 4.167 0.005 5841270 100.0 89.8

21 n-Docosane 4.341 4.335 0.006 5740663 100.0 91.1

20 n-Tetracosane 4.650 4.641 0.009 5814588 100.0 92.8

16 n-Hexacosane 4.906 4.898 0.008 5901739 100.0 94.5

12 n-Octacosane 5.133 5.125 0.008 6001809 100.0 96.0

11 Triacontane 5.339 5.330 0.009 6065571 100.0 97.2

10 Dotriacontane 5.531 5.524 0.007 6195839 100.0 100.1

15 Tetratriacontane 5.714 5.707 0.007 6412894 100.0 106.5

14 n-Hexatriacontane 5.891 5.882 0.009 6171513 100.0 117.3

13 C38 6.061 6.051 0.010 5738706 100.0 129.1

9 C40 6.226 6.216 0.010 4792518 100.0 136.3

A 23 C9-C12 Aliphatics 1.373 (0.610-2.135) 29194902 400.0 390.1

A 24 C12-C16 Aliphatics 2.700 (2.135-3.265) 21478842 300.0 274.5

A 25 C9-C40 3.463 (0.610-6.316) 131021757 2000.0 2001.3

A 26 C16-C21 Aliphatics 3.766 (3.265-4.267) 20235403 300.0 282.5

A 27 C21-C40 Aliphatics 5.292 (4.267-6.316) 60113882 1000.0 1041.7

Reagents:

SGEPH_ALIL4_00021 Amount Added: 1.00 Units: mL

Page 7890 of 21459

Data File: \\chromfs\Edison\ChromData\CBNAGC1\20241202-184171.b\1F0017323.D

Injection Date: 02-Dec-2024 11:09:25 Instrument ID: CBNAGC1 Operator ID:

Lims ID: IC Worklist Smp#: 5

Client ID:

Injection Vol: 1.0 ul Dil. Factor: 1.0000 ALS Bottle#: 5

Method: ALEPH1F Limit Group: GC NJEPH ICAL

Column: Rtx Mineral Oil ( 0.32 mm)

0.6 1.0 1.4 1.8 2.2 2.6 3.0 3.4 3.8 4.2 4.6 5.0 5.4 5.8 6.2 6.6 7.0 7.4 7.8 8.2 8.6 Min

Y

X

GC FID1A, 1F0017323.D

o n a n e

.7 e c a n e

.1 p h th a le n e

.8 d e c a n e

.0 e th y ln a p h th a le n e

.2 e tr a d e c a n e

.6 x a d e c a n e

.1 c ta d e c a n e

.6 o

-T e rp h e n s a n e

.9

-C h lo ro o c ta d e c a n e

.1

.1 o c o s a n e

.3 e tr a c o s a n e

.6 e x a c o s a n e

.9 c ta c o s a n e

.1 a c o n ta n e

.3 tr ia c o n ta n e

.5 tr a tr ia c o n ta n e

.7 e x a tr ia c o n ta n e

.8

.0

.2

Page 7891 of 21459

Data File: \\chromfs\Edison\ChromData\CBNAGC1\20241202-184171.b\1F0017323.D

Injection Date: 02-Dec-2024 11:09:25 Instrument ID: CBNAGC1

Lims ID: IC

Client ID:

Operator ID: ALS Bottle#: 5 Worklist Smp#: 5

Injection Vol: 1.0 ul Dil. Factor: 1.0000

Method: ALEPH1F Limit Group: GC NJEPH ICAL

Column: Rtx Mineral Oil ( 0.32 mm) Detector GC fid1a

A 23 C9-C12 Aliphatics, CAS: STL00191

0.6 1.6 Min

Y

X

Page 7892 of 21459

Data File: \\chromfs\Edison\ChromData\CBNAGC1\20241202-184171.b\1F0017323.D

Injection Date: 02-Dec-2024 11:09:25 Instrument ID: CBNAGC1

Lims ID: IC

Client ID:

Operator ID: ALS Bottle#: 5 Worklist Smp#: 5

Injection Vol: 1.0 ul Dil. Factor: 1.0000

Method: ALEPH1F Limit Group: GC NJEPH ICAL

Column: Rtx Mineral Oil ( 0.32 mm) Detector GC fid1a

A 24 C12-C16 Aliphatics, CAS: STL00159

2.0 3.0 Min

Y

X

Page 7893 of 21459

Data File: \\chromfs\Edison\ChromData\CBNAGC1\20241202-184171.b\1F0017323.D

Injection Date: 02-Dec-2024 11:09:25 Instrument ID: CBNAGC1

Lims ID: IC

Client ID:

Operator ID: ALS Bottle#: 5 Worklist Smp#: 5

Injection Vol: 1.0 ul Dil. Factor: 1.0000

Method: ALEPH1F Limit Group: GC NJEPH ICAL

Column: Rtx Mineral Oil ( 0.32 mm) Detector GC fid1a

A 25 C9-C40, CAS: STL00695

0.6 0.9 1.2 1.5 1.8 2.1 2.4 2.7 3.0 3.3 3.6 3.9 4.2 4.5 4.8 5.1 5.4 5.7 6.0 6.3 6.6 6.9 Min

Y

X

GC FID1A, 1F0017323.D

o

-T e rp h e n

-C h lo ro o c ta d e c a n e

.1

Page 7894 of 21459

Data File: \\chromfs\Edison\ChromData\CBNAGC1\20241202-184171.b\1F0017323.D

Injection Date: 02-Dec-2024 11:09:25 Instrument ID: CBNAGC1

Lims ID: IC

Client ID:

Operator ID: ALS Bottle#: 5 Worklist Smp#: 5

Injection Vol: 1.0 ul Dil. Factor: 1.0000

Method: ALEPH1F Limit Group: GC NJEPH ICAL

Column: Rtx Mineral Oil ( 0.32 mm) Detector GC fid1a

A 26 C16-C21 Aliphatics, CAS: STL00950

3.1 4.1 Min

Y

X

GC FID1A, 1F0017323.D

o

-T e rp h e n

-C h lo ro o c ta d e c a n e

.1

Page 7895 of 21459

Data File: \\chromfs\Edison\ChromData\CBNAGC1\20241202-184171.b\1F0017323.D

Injection Date: 02-Dec-2024 11:09:25 Instrument ID: CBNAGC1

Lims ID: IC

Client ID:

Operator ID: ALS Bottle#: 5 Worklist Smp#: 5

Injection Vol: 1.0 ul Dil. Factor: 1.0000

Method: ALEPH1F Limit Group: GC NJEPH ICAL

Column: Rtx Mineral Oil ( 0.32 mm) Detector GC fid1a

A 27 C21-C40 Aliphatics, CAS: STL01059

4.0 4.2 4.4 4.6 4.8 5.0 5.2 5.4 5.6 5.8 6.0 6.2 6.4 6.6 Min

Y

X

Page 7896 of 21459

Report Date: 02-Dec-2024 12:38:41 Chrom Revision: 2.3 12-Nov-2024 16:55:22

Target Compound Quantitation Report

Data File: \\chromfs\Edison\ChromData\CBNAGC1\20241202-184171.b\1F0017324.D

Lims ID: IC

Client ID:

Sample Type: IC Calib Level: 5

Inject. Date: 02-Dec-2024 11:23:14 ALS Bottle#: 6 Worklist Smp#: 6

Injection Vol: 1.0 ul Dil. Factor: 1.0000

Sample Info: 460-0184171-006

Operator ID: Instrument ID: CBNAGC1

Sublist: chrom-ALEPH1F*sub7

Method: \\chromfs\Edison\ChromData\CBNAGC1\20241202-184171.b\ALEPH1F.m

Limit Group: GC NJEPH ICAL

Last Update: 02-Dec-2024 12:38:41 Calib Date: 02-Dec-2024 11:23:14

Integrator: Falcon

Quant Method: External Standard Quant By: Initial Calibration

Last ICal File: \\chromfs\Edison\ChromData\CBNAGC1\20241202-184171.b\1F0017324.D

Column 1 : Rtx Mineral Oil ( 0.32 mm) Det: GC fid1a

Process Host: CTX1673

First Level Reviewer: OR9X Date: 02-Dec-2024 11:51:43

Compound

RT

(min.)

Exp RT (min.)

Dlt RT (min.) Response

Cal Amt ug/ml

OnCol Amt ug/ml Flags

$ 1 o-Terphenyl 3.685 3.668 0.017 13474250 200.0 180.2

$ 2 1-Chlorooctadecane 4.126 4.111 0.015 9696423 200.0 185.3

3 n-Nonane 0.718 0.710 0.008 13872654 200.0 188.8

19 n-Decane 1.190 1.175 0.015 13935035 200.0 196.8

4 Naphthalene 1.820 1.804 0.016 15034124 200.0 196.8

5 Dodecane 2.048 2.035 0.013 13828899 200.0 189.0

6 2-Methylnaphthalene 2.225 2.208 0.017 14689971 200.0 199.2

18 n-Tetradecane 2.670 2.656 0.014 13539792 200.0 197.0

7 Hexadecane 3.176 3.165 0.011 12227698 200.0 186.9

17 n-Octadecane 3.623 3.605 0.018 12252874 200.0 187.0

22 icosane 4.004 3.988 0.016 11488564 200.0 178.7

8 C21 4.185 4.167 0.018 11451649 200.0 176.1

21 n-Docosane 4.349 4.335 0.014 11239769 200.0 178.3

20 n-Tetracosane 4.656 4.641 0.015 11413384 200.0 182.1

16 n-Hexacosane 4.914 4.898 0.016 11496103 200.0 184.1

12 n-Octacosane 5.143 5.125 0.018 11634153 200.0 186.0

11 Triacontane 5.352 5.330 0.022 11713597 200.0 187.7

10 Dotriacontane 5.546 5.524 0.022 11941308 200.0 192.9

15 Tetratriacontane 5.734 5.707 0.027 12381623 200.0 205.7

14 n-Hexatriacontane 5.912 5.882 0.030 12103224 200.0 230.0 a

13 C38 6.084 6.051 0.033 11702497 200.0 263.2 a

9 C40 6.248 6.216 0.032 10503440 200.0 298.6 a

A 23 C9-C12 Aliphatics 1.373 (0.610-2.135) 57067330 800.0 762.6

A 24 C12-C16 Aliphatics 2.700 (2.135-3.265) 42032438 600.0 537.1

A 25 C9-C40 3.463 (0.610-6.316) 257820124 4000.0 3938.0 a

A 26 C16-C21 Aliphatics 3.766 (3.265-4.267) 40116630 600.0 560.1

A 27 C21-C40 Aliphatics 5.292 (4.267-6.316) 118609088 2000.0 2055.4 a

Page 7897 of 21459

Processing Flags

Review Flags a - User Assigned ID

Reagents:

SGEPH_ALIL5_00029 Amount Added: 1.00 Units: mL

Page 7898 of 21459

Data File: \\chromfs\Edison\ChromData\CBNAGC1\20241202-184171.b\1F0017324.D

Injection Date: 02-Dec-2024 11:23:14 Instrument ID: CBNAGC1 Operator ID:

Lims ID: IC Worklist Smp#: 6

Client ID:

Injection Vol: 1.0 ul Dil. Factor: 1.0000 ALS Bottle#: 6

Method: ALEPH1F Limit Group: GC NJEPH ICAL

Column: Rtx Mineral Oil ( 0.32 mm)

0.6 1.0 1.4 1.8 2.2 2.6 3.0 3.4 3.8 4.2 4.6 5.0 5.4 5.8 6.2 6.6 7.0 7.4 7.8 8.2 8.6 Min

Y

X

GC FID1A, 1F0017324.D

o n a n e

.7 e c a n e

.1 p h th a le n e

.8 d e c a n e

.0 e th y ln a p h th a le n e

.2 e tr a d e c a n e

.6 x a d e c a n e

.1 c ta d e c a n e

.6 o

-T e rp h e n s a n e

.0

-C h lo ro o c ta d e c a n e

.1

.1 o c o s a n e

.3 e tr a c o s a n e

.6 e x a c o s a n e

.9 c ta c o s a n e

.1 a c o n ta n e

.3 tr ia c o n ta n e

.5 tr a tr ia c o n ta n e

.7 e x a tr ia c o n ta n e

.9

.0

.2

Page 7899 of 21459

Data File: \\chromfs\Edison\ChromData\CBNAGC1\20241202-184171.b\1F0017324.D

Injection Date: 02-Dec-2024 11:23:14 Instrument ID: CBNAGC1

Lims ID: IC

Client ID:

Operator ID: ALS Bottle#: 6 Worklist Smp#: 6

Injection Vol: 1.0 ul Dil. Factor: 1.0000

Method: ALEPH1F Limit Group: GC NJEPH ICAL

Column: Rtx Mineral Oil ( 0.32 mm) Detector GC fid1a

A 23 C9-C12 Aliphatics, CAS: STL00191

0.6 1.6 Min

Y

X

Page 7900 of 21459

Data File: \\chromfs\Edison\ChromData\CBNAGC1\20241202-184171.b\1F0017324.D

Injection Date: 02-Dec-2024 11:23:14 Instrument ID: CBNAGC1

Lims ID: IC

Client ID:

Operator ID: ALS Bottle#: 6 Worklist Smp#: 6

Injection Vol: 1.0 ul Dil. Factor: 1.0000

Method: ALEPH1F Limit Group: GC NJEPH ICAL

Column: Rtx Mineral Oil ( 0.32 mm) Detector GC fid1a

A 24 C12-C16 Aliphatics, CAS: STL00159

2.0 3.0 Min

Y

X

Page 7901 of 21459

Data File: \\chromfs\Edison\ChromData\CBNAGC1\20241202-184171.b\1F0017324.D

Injection Date: 02-Dec-2024 11:23:14 Instrument ID: CBNAGC1

Lims ID: IC

Client ID:

Operator ID: ALS Bottle#: 6 Worklist Smp#: 6

Injection Vol: 1.0 ul Dil. Factor: 1.0000

Method: ALEPH1F Limit Group: GC NJEPH ICAL

Column: Rtx Mineral Oil ( 0.32 mm) Detector GC fid1a

A 25 C9-C40, CAS: STL00695

0.6 0.9 1.2 1.5 1.8 2.1 2.4 2.7 3.0 3.3 3.6 3.9 4.2 4.5 4.8 5.1 5.4 5.7 6.0 6.3 6.6 6.9 Min

Y

X

GC FID1A, 1F0017324.D

o

-T e rp h e n

-C h lo ro o c ta d e c a n e

.1

Page 7902 of 21459

Report Date: 02-Dec-2024 12:38:42 Chrom Revision: 2.3 12-Nov-2024 16:55:22

Data File: \\chromfs\Edison\ChromData\CBNAGC1\20241202-184171.b\1F0017324.D

Injection Date: 02-Dec-2024 11:23:14 Instrument ID: CBNAGC1

Lims ID: IC

Client ID:

Operator ID: ALS Bottle#: 6 Worklist Smp#: 6

Injection Vol: 1.0 ul Dil. Factor: 1.0000

Method: ALEPH1F Limit Group: GC NJEPH ICAL

Column: Rtx Mineral Oil ( 0.32 mm) Detector GC fid1a

A 26 C16-C21 Aliphatics, CAS: STL00950

3.1 4.1 Min

Y

X

GC FID1A, 1F0017324.D

o

-T e rp h e n

-C h lo ro o c ta d e c a n e

.1

Page 7903 of 21459

Data File: \\chromfs\Edison\ChromData\CBNAGC1\20241202-184171.b\1F0017324.D

Injection Date: 02-Dec-2024 11:23:14 Instrument ID: CBNAGC1

Lims ID: IC

Client ID:

Operator ID: ALS Bottle#: 6 Worklist Smp#: 6

Injection Vol: 1.0 ul Dil. Factor: 1.0000

Method: ALEPH1F Limit Group: GC NJEPH ICAL

Column: Rtx Mineral Oil ( 0.32 mm) Detector GC fid1a

A 27 C21-C40 Aliphatics, CAS: STL01059

4.0 4.2 4.4 4.6 4.8 5.0 5.2 5.4 5.6 5.8 6.0 6.2 6.4 6.6 Min

Y

X

Page 7904 of 21459

Eurofins Edison

Data File: \\chromfs\Edison\ChromData\CBNAGC1\20241202-184171.b\1F0017324.D

Injection Date: 02-Dec-2024 11:23:14 Instrument ID: CBNAGC1

Lims ID: IC

Client ID:

Operator ID: ALS Bottle#: 6 Worklist Smp#: 6

Injection Vol: 1.0 ul Dil. Factor: 1.0000

Method: ALEPH1F Limit Group: GC NJEPH ICAL

Column: Rtx Mineral Oil ( 0.32 mm) Detector GC fid1a

A 25 C9-C40, RT: 3.463, CAS: STL00695

Signal: 1

Processing Integration Results

RT: 3.46

Response: 257820124

Amount: 3930.9180

0.6 1.2 1.8 2.4 3.0 3.6 4.2 4.8 5.4 6.0 6.6 Min

Y

X

GC FID1A, 1F0017324.D

o

-T e rp h e n

-C h lo ro o c ta d e c a n e

.1

Manual Integration Results

RT: 3.46

Response: 257820124

Amount: 3938.0001

0.6 1.2 1.8 2.4 3.0 3.6 4.2 4.8 5.4 6.0 6.6 Min

Y

X

GC FID1A, 1F0017324.D

o

-T e rp h e n

-C h lo ro o c ta d e c a n e

.1

Reviewer: OR9X, 02-Dec-2024 11:51:37 -05:00:00 (UTC)

Audit Action: Assigned Compound ID Audit Reason: Peak assignment corrected

Page 7905 of 21459

Eurofins Edison

Data File: \\chromfs\Edison\ChromData\CBNAGC1\20241202-184171.b\1F0017324.D

Injection Date: 02-Dec-2024 11:23:14 Instrument ID: CBNAGC1

Lims ID: IC

Client ID:

Operator ID: ALS Bottle#: 6 Worklist Smp#: 6

Injection Vol: 1.0 ul Dil. Factor: 1.0000

Method: ALEPH1F Limit Group: GC NJEPH ICAL

Column: Rtx Mineral Oil ( 0.32 mm) Detector GC fid1a

A 27 C21-C40 Aliphatics, RT: 5.292, CAS: STL01059 Signal: 1

Processing Integration Results

RT: 5.29

Response: 118609088

Amount: 2055.4204

4.0 4.2 4.4 4.6 4.8 5.0 5.2 5.4 5.6 5.8 6.0 6.2 6.4 6.6 Min

Y

X

GC FID1A, 1F0017324.D

Manual Integration Results

RT: 5.29

Response: 118609088

Amount: 2055.4204

4.0 4.2 4.4 4.6 4.8 5.0 5.2 5.4 5.6 5.8 6.0 6.2 6.4 6.6 Min

Y

X

GC FID1A, 1F0017324.D

Reviewer: OR9X, 02-Dec-2024 11:51:37 -05:00:00 (UTC)

Audit Action: Assigned Compound ID Audit Reason: Peak assignment corrected

Page 7906 of 21459

Eurofins Edison

Data File: \\chromfs\Edison\ChromData\CBNAGC1\20241202-184171.b\1F0017324.D

Injection Date: 02-Dec-2024 11:23:14 Instrument ID: CBNAGC1

Lims ID: IC

Client ID:

Operator ID: ALS Bottle#: 6 Worklist Smp#: 6

Injection Vol: 1.0 ul Dil. Factor: 1.0000

Method: ALEPH1F Limit Group: GC NJEPH ICAL

Column: Rtx Mineral Oil ( 0.32 mm) Detector GC fid1a

14 n-Hexatriacontane, CAS: 630-06-8 Signal: 1

Processing Integration Results

RT: 5.87

Area: 10896

Amount: 0.268881

Amount Units: ug/ml

5.6 5.8 6.0 6.2 Min

Y

X

.8

Manual Integration Results

RT: 5.91

Area: 12103224

Amount: 230.0298

Amount Units: ug/ml

5.6 5.8 6.0 6.2 Min

RT

Y

X

Reviewer: OR9X, 02-Dec-2024 11:51:37 -05:00:00 (UTC)

Audit Action: Assigned Compound ID Audit Reason: Peak not integrated

Page 7907 of 21459

Eurofins Edison

Data File: \\chromfs\Edison\ChromData\CBNAGC1\20241202-184171.b\1F0017324.D

Injection Date: 02-Dec-2024 11:23:14 Instrument ID: CBNAGC1

Lims ID: IC

Client ID:

Operator ID: ALS Bottle#: 6 Worklist Smp#: 6

Injection Vol: 1.0 ul Dil. Factor: 1.0000

Method: ALEPH1F Limit Group: GC NJEPH ICAL

Column: Rtx Mineral Oil ( 0.32 mm) Detector GC fid1a

13 C38, CAS: 7194-85-6

Signal: 1

Processing Integration Results

RT: 6.02

Area: 4775

Amount: 0.145743

Amount Units: ug/ml

5.7 5.9 6.1 6.3 Min

Y

X

.0

Manual Integration Results

RT: 6.08

Area: 11702497

Amount: 263.2092

Amount Units: ug/ml

5.7 5.9 6.1 6.3 Min

RT

Y

X

.0

Reviewer: OR9X, 02-Dec-2024 11:51:34 -05:00:00 (UTC)

Page 7908 of 21459

Eurofins Edison

Data File: \\chromfs\Edison\ChromData\CBNAGC1\20241202-184171.b\1F0017324.D

Injection Date: 02-Dec-2024 11:23:14 Instrument ID: CBNAGC1

Lims ID: IC

Client ID:

Operator ID: ALS Bottle#: 6 Worklist Smp#: 6

Injection Vol: 1.0 ul Dil. Factor: 1.0000

Method: ALEPH1F Limit Group: GC NJEPH ICAL

Column: Rtx Mineral Oil ( 0.32 mm) Detector GC fid1a

9 C40, CAS: 4181-95-7

Signal: 1

Processing Integration Results

RT: 6.21

Area: 128086

Amount: 5.165424

Amount Units: ug/ml

5.9 6.1 6.3 6.5 Min

Y

X

.2

Manual Integration Results

RT: 6.25

Area: 10503440

Amount: 298.6294

Amount Units: ug/ml

5.9 6.1 6.3 6.5 Min

RT

Y

X

.2

Reviewer: OR9X, 02-Dec-2024 11:51:30 -05:00:00 (UTC)

Page 7909 of 21459

Calibration / n-Nonane

Curve Type: Average

Weighting: Conc_Sq

Origin: Force

Dependency: Response

Calib Mode: ESTD

Response Base: AREA

RF Rounding: 0

Curve Coefficients

Intercept: 0

Slope: 7.348E+04

Error Coefficients

Relative Standard Deviation: 4.8

ID Level Concentration Response IS Amount IS Response RF Used

1 IC 460-1009900/2 5.0 391354.0 78270.8 Y

2 IC 460-1009900/3 10.0 754795.0 75479.5 Y

3 IC 460-1009900/4 50.0 3663037.0 73260.74 Y

4 IC 460-1009900/5 100.0 7103806.0 71038.06 Y

5 IC 460-1009900/6 200.0 13872654.0 69363.27 Y

Response = [7.348E+04]x

Concentration

0 100 200 0.0

0.2

0.4

0.6

0.8

1.0

1.2

1.4

R esponse ( X

10000000)

IC 460-1009900/2

IC 460-1009900/3

IC 460-1009900/4

IC 460-1009900/5

Page 7910 of 21459

Calibration / n-Decane

Weighting: Conc_Sq

Origin: Force

Dependency: Response

Calib Mode: ESTD

Response Base: AREA

RF Rounding: 0

Curve Coefficients

Intercept: 0

Slope: 7.082E+04

Error Coefficients

Relative Standard Deviation: 2.0

ID Level Concentration Response IS Amount IS Response RF Used

1 IC 460-1009900/2 5.0 353956.0 70791.2 Y

2 IC 460-1009900/3 10.0 694376.0 69437.6 Y

3 IC 460-1009900/4 50.0 3651835.0 73036.7 Y

4 IC 460-1009900/5 100.0 7113850.0 71138.5 Y

5 IC 460-1009900/6 200.0 13935035.0 69675.175 Y

Response = [7.082E+04]x

Concentration

0 100 200 0.0

0.2

0.4

0.6

0.8

1.0

1.2

1.4

R esponse ( X

10000000)

IC 460-1009900/2

IC 460-1009900/3

IC 460-1009900/4

Page 7911 of 21459

Calibration / C9-C12 Aliphatics

Weighting: Conc_Sq

Origin: Force

Dependency: Response

Calib Mode: ESTD

Response Base: AREA

RF Rounding: 0

Curve Coefficients

Intercept: 0

Slope: 7.483E+04

Error Coefficients

Relative Standard Deviation: 3.9

ID Level Concentration Response IS Amount IS Response RF Used

1 IC 460-1009900/2 20.0 1578663.0 78933.15 Y

2 IC 460-1009900/3 40.0 3020258.0 75506.45 Y

3 IC 460-1009900/4 200.0 15079911.0 75399.555 Y

4 IC 460-1009900/5 400.0 29194902.0 72987.255 Y

5 IC 460-1009900/6 800.0 57067330.0 71334.1625 Y

Response = [7.483E+04]x

Concentration

0 100 200 300 400 500 600 700 800 0.0

0.5

1.0

1.5

2.0

2.5

3.0

3.5

4.0

4.5

5.0

5.5

R esponse ( X

10000000)

IC 460-1009900/2

IC 460-1009900/3

IC 460-1009900/4

Page 7912 of 21459

Calibration / Naphthalene

Weighting: Conc_Sq

Origin: Force

Dependency: Response

Calib Mode: ESTD

Response Base: AREA

RF Rounding: 0

Curve Coefficients

Intercept: 0

Slope: 7.64E+04

Error Coefficients

Relative Standard Deviation: 1.0

ID Level Concentration Response IS Amount IS Response RF Used

1 IC 460-1009900/2 5.0 384647.0 76929.4 Y

2 IC 460-1009900/3 10.0 764285.0 76428.5 Y

3 IC 460-1009900/4 50.0 3857566.0 77151.32 Y

4 IC 460-1009900/5 100.0 7633281.0 76332.81 Y

5 IC 460-1009900/6 200.0 15034124.0 75170.62 Y

Response = [7.64E+04]x

Concentration

0 100 200 0.0

0.5

1.0

1.5

R esponse ( X

10000000)

IC 460-1009900/2

IC 460-1009900/3

IC 460-1009900/4

Page 7913 of 21459

Calibration / Dodecane

Weighting: Conc_Sq

Origin: Force

Dependency: Response

Calib Mode: ESTD

Response Base: AREA

RF Rounding: 0

Curve Coefficients

Intercept: 0

Slope: 7.317E+04

Error Coefficients

Relative Standard Deviation: 5.0

ID Level Concentration Response IS Amount IS Response RF Used

1 IC 460-1009900/2 5.0 393075.0 78615.0 Y

2 IC 460-1009900/3 10.0 744640.0 74464.0 Y

3 IC 460-1009900/4 50.0 3645671.0 72913.42 Y

4 IC 460-1009900/5 100.0 7073287.0 70732.87 Y

5 IC 460-1009900/6 200.0 13828899.0 69144.495 Y

Response = [7.317E+04]x

Concentration

0 100 200 0.0

0.2

0.4

0.6

0.8

1.0

1.2

1.4

R esponse ( X

10000000)

IC 460-1009900/2

IC 460-1009900/3

IC 460-1009900/4

Page 7914 of 21459

Calibration / 2-Methylnaphthalene

Weighting: Conc_Sq

Origin: Force

Dependency: Response

Calib Mode: ESTD

Response Base: AREA

RF Rounding: 0

Curve Coefficients

Intercept: 0

Slope: 7.375E+04

Error Coefficients

Relative Standard Deviation: 2.0

ID Level Concentration Response IS Amount IS Response RF Used

1 IC 460-1009900/2 5.0 356733.0 71346.6 Y

2 IC 460-1009900/3 10.0 743797.0 74379.7 Y

3 IC 460-1009900/4 50.0 3757337.0 75146.74 Y

4 IC 460-1009900/5 100.0 7444482.0 74444.82 Y

5 IC 460-1009900/6 200.0 14689971.0 73449.855 Y

Response = [7.375E+04]x

Concentration

0 100 200 0.0

0.5

1.0

1.5

R esponse ( X

10000000)

IC 460-1009900/2

IC 460-1009900/3 IC 460-1009900/4

Page 7915 of 21459

Calibration / n-Tetradecane

Weighting: Conc_Sq

Origin: Force

Dependency: Response

Calib Mode: ESTD

Response Base: AREA

RF Rounding: 0

Curve Coefficients

Intercept: 0

Slope: 6.873E+04

Error Coefficients

Relative Standard Deviation: 4.1

ID Level Concentration Response IS Amount IS Response RF Used

1 IC 460-1009900/2 5.0 321818.0 64363.6 Y

2 IC 460-1009900/3 10.0 709620.0 70962.0 Y

3 IC 460-1009900/4 50.0 3565940.0 71318.8 Y

4 IC 460-1009900/5 100.0 6929031.0 69290.31 Y

5 IC 460-1009900/6 200.0 13539792.0 67698.96 Y

Response = [6.873E+04]x

Concentration

0 100 200 0.0

0.2

0.4

0.6

0.8

1.0

1.2

1.4

R esponse ( X

10000000)

IC 460-1009900/2

Page 7916 of 21459

Calibration / C12-C16 Aliphatics

Weighting: Conc_Sq

Origin: Force

Dependency: Response

Calib Mode: ESTD

Response Base: AREA

RF Rounding: 0

Curve Coefficients

Intercept: 0

Slope: 7.825E+04

Error Coefficients

Relative Standard Deviation: 15.2

ID Level Concentration Response IS Amount IS Response RF Used

1 IC 460-1009900/2 15.0 1155116.0 77007.733333 Y

2 IC 460-1009900/3 30.0 2971664.0 99055.466667 Y

3 IC 460-1009900/4 150.0 11031989.0 73546.593333 Y

4 IC 460-1009900/5 300.0 21478842.0 71596.14 Y

5 IC 460-1009900/6 600.0 42032438.0 70054.063333 Y

Response = [7.825E+04]x

Concentration

0 100 200 300 400 500 600 0.0

0.5

1.0

1.5

2.0

2.5

3.0

3.5

4.0

R esponse ( X

10000000)

IC 460-1009900/2

IC 460-1009900/3

IC 460-1009900/4

Page 7917 of 21459

Calibration / Hexadecane

Weighting: Conc_Sq

Origin: Force

Dependency: Response

Calib Mode: ESTD

Response Base: AREA

RF Rounding: 0

Curve Coefficients

Intercept: 0

Slope: 6.541E+04

Error Coefficients

Relative Standard Deviation: 5.0

ID Level Concentration Response IS Amount IS Response RF Used

1 IC 460-1009900/2 5.0 323734.0 64746.8 Y

2 IC 460-1009900/3 10.0 661592.0 66159.2 Y

3 IC 460-1009900/4 50.0 3507710.0 70154.2 Y

4 IC 460-1009900/5 100.0 6486894.0 64868.94 Y

5 IC 460-1009900/6 200.0 12227698.0 61138.49 Y

Response = [6.541E+04]x

Concentration

0 100 200 0.0

0.2

0.4

0.6

0.8

1.0

1.2

R esponse ( X

10000000)

IC 460-1009900/2

IC 460-1009900/3 IC 460-1009900/4

Page 7918 of 21459

Calibration / C9-C40

Weighting: Conc_Sq

Origin: Force

Dependency: Response

Calib Mode: ESTD

Response Base: AREA

RF Rounding: 0

Curve Coefficients

Intercept: 0

Slope: 6.547E+04

Error Coefficients

Relative Standard Deviation: 1.6

ID Level Concentration Response IS Amount IS Response RF Used

1 IC 460-1009900/2 100.0 6673023.0 66730.23 Y

2 IC 460-1009900/3 200.0 12888955.0 64444.775 Y

3 IC 460-1009900/4 1000.0 66208142.0 66208.142 Y

4 IC 460-1009900/5 2000.0 131021757.0 65510.8785 Y

5 IC 460-1009900/6 4000.0 257820124.0 64455.031 Y

Response = [6.547E+04]x

Concentration

0 1000 2000 3000 4000 0.0

0.5

1.0

1.5

2.0

2.5

R esponse ( X

100000000)

IC 460-1009900/2

IC 460-1009900/3

IC 460-1009900/4

Page 7919 of 21459

Calibration / n-Octadecane

Weighting: Conc_Sq

Origin: Force

Dependency: Response

Calib Mode: ESTD

Response Base: AREA

RF Rounding: 0

Curve Coefficients

Intercept: 0

Slope: 6.553E+04

Error Coefficients

Relative Standard Deviation: 8.3

ID Level Concentration Response IS Amount IS Response RF Used

1 IC 460-1009900/2 5.0 363259.0 72651.8 Y

2 IC 460-1009900/3 10.0 694774.0 69477.4 Y

3 IC 460-1009900/4 50.0 3224254.0 64485.08 Y

4 IC 460-1009900/5 100.0 5979531.0 59795.31 Y

5 IC 460-1009900/6 200.0 12252874.0 61264.37 Y

Response = [6.553E+04]x

Concentration

0 100 200 0.0

0.2

0.4

0.6

0.8

1.0

1.2

R esponse ( X

10000000)

IC 460-1009900/2

IC 460-1009900/3

IC 460-1009900/4

Page 7920 of 21459

Calibration / o-Terphenyl

Weighting: Conc_Sq

Origin: Force

Dependency: Response

Calib Mode: ESTD

Response Base: AREA

RF Rounding: 0

Curve Coefficients

Intercept: 0

Slope: 7.475E+04

Error Coefficients

Relative Standard Deviation: 6.3

ID Level Concentration Response IS Amount IS Response RF Used

1 IC 460-1009900/2 5.0 393407.0 78681.4 Y

2 IC 460-1009900/3 10.0 777829.0 77782.9 Y

3 IC 460-1009900/4 50.0 3856265.0 77125.3 Y

4 IC 460-1009900/5 100.0 7281022.0 72810.22 Y

5 IC 460-1009900/6 200.0 13474250.0 67371.25 Y

Response = [7.475E+04]x

Concentration

0 100 200 0.0

0.2

0.4

0.6

0.8

1.0

1.2

1.4

R esponse ( X

10000000)

IC 460-1009900/2

IC 460-1009900/3

IC 460-1009900/4

Page 7921 of 21459

Calibration / C16-C21 Aliphatics

Weighting: Conc_Sq

Origin: Force

Dependency: Response

Calib Mode: ESTD

Response Base: AREA

RF Rounding: 0

Curve Coefficients

Intercept: 0

Slope: 7.162E+04

Error Coefficients

Relative Standard Deviation: 8.2

ID Level Concentration Response IS Amount IS Response RF Used

1 IC 460-1009900/2 15.0 1211718.0 80781.2 Y

2 IC 460-1009900/3 30.0 2226373.0 74212.433333 Y

3 IC 460-1009900/4 150.0 10322616.0 68817.44 Y

4 IC 460-1009900/5 300.0 20235403.0 67451.343333 Y

5 IC 460-1009900/6 600.0 40116630.0 66861.05 Y

Response = [7.162E+04]x

Concentration

0 100 200 300 400 500 600 0.0

0.5

1.0

1.5

2.0

2.5

3.0

3.5

4.0

R esponse ( X

10000000)

IC 460-1009900/2

IC 460-1009900/3

IC 460-1009900/4

Page 7922 of 21459

Calibration / icosane

Weighting: Conc_Sq

Origin: Force

Dependency: Response

Calib Mode: ESTD

Response Base: AREA

RF Rounding: 0

Curve Coefficients

Intercept: 0

Slope: 6.43E+04

Error Coefficients

Relative Standard Deviation: 11.7

ID Level Concentration Response IS Amount IS Response RF Used

1 IC 460-1009900/2 5.0 372957.0 74591.4 Y

2 IC 460-1009900/3 10.0 697136.0 69713.6 Y

3 IC 460-1009900/4 50.0 3081836.0 61636.72 Y

4 IC 460-1009900/5 100.0 5809241.0 58092.41 Y

5 IC 460-1009900/6 200.0 11488564.0 57442.82 Y

Response = [6.43E+04]x

Concentration

0 100 200 0.0

0.2

0.4

0.6

0.8

1.0

1.2

R esponse ( X

10000000)

IC 460-1009900/2

IC 460-1009900/3

IC 460-1009900/4

Page 7923 of 21459

Calibration / 1-Chlorooctadecane

Weighting: Conc_Sq

Origin: Force

Dependency: Response

Calib Mode: ESTD

Response Base: AREA

RF Rounding: 0

Curve Coefficients

Intercept: 0

Slope: 5.234E+04

Error Coefficients

Relative Standard Deviation: 7.0

ID Level Concentration Response IS Amount IS Response RF Used

1 IC 460-1009900/2 5.0 283898.0 56779.6 Y

2 IC 460-1009900/3 10.0 553074.0 55307.4 Y

3 IC 460-1009900/4 50.0 2592337.0 51846.74 Y

4 IC 460-1009900/5 100.0 4928054.0 49280.54 Y

5 IC 460-1009900/6 200.0 9696423.0 48482.115 Y

Response = [5.234E+04]x

Concentration

0 100 200 0.0

1.0

2.0

3.0

4.0

5.0

6.0

7.0

8.0

9.0

R esponse ( X

1000000)

IC 460-1009900/2

IC 460-1009900/3

IC 460-1009900/4

Page 7924 of 21459

Calibration / C21

Weighting: Conc_Sq

Origin: Force

Dependency: Response

Calib Mode: ESTD

Response Base: AREA

RF Rounding: 0

Curve Coefficients

Intercept: 0

Slope: 6.502E+04

Error Coefficients

Relative Standard Deviation: 12.8

ID Level Concentration Response IS Amount IS Response RF Used

1 IC 460-1009900/2 5.0 382377.0 76475.4 Y

2 IC 460-1009900/3 10.0 708108.0 70810.8 Y

3 IC 460-1009900/4 50.0 3106677.0 62133.54 Y

4 IC 460-1009900/5 100.0 5841270.0 58412.7 Y

5 IC 460-1009900/6 200.0 11451649.0 57258.245 Y

Response = [6.502E+04]x

Concentration

0 100 200 0.0

0.2

0.4

0.6

0.8

1.0

1.2

R esponse ( X

10000000)

IC 460-1009900/2

IC 460-1009900/3

IC 460-1009900/4

Page 7925 of 21459

Calibration / n-Docosane

Weighting: Conc_Sq

Origin: Force

Dependency: Response

Calib Mode: ESTD

Response Base: AREA

RF Rounding: 0

Curve Coefficients

Intercept: 0

Slope: 6.305E+04

Error Coefficients

Relative Standard Deviation: 11.9

ID Level Concentration Response IS Amount IS Response RF Used

1 IC 460-1009900/2 5.0 366928.0 73385.6 Y

2 IC 460-1009900/3 10.0 684503.0 68450.3 Y

3 IC 460-1009900/4 50.0 2989965.0 59799.3 Y

4 IC 460-1009900/5 100.0 5740663.0 57406.63 Y

5 IC 460-1009900/6 200.0 11239769.0 56198.845 Y

Response = [6.305E+04]x

Concentration

0 100 200 0.0

0.2

0.4

0.6

0.8

1.0

1.2

R esponse ( X

10000000)

IC 460-1009900/2

IC 460-1009900/3

IC 460-1009900/4

Page 7926 of 21459

Calibration / n-Tetracosane

Weighting: Conc_Sq

Origin: Force

Dependency: Response

Calib Mode: ESTD

Response Base: AREA

RF Rounding: 0

Curve Coefficients

Intercept: 0

Slope: 6.268E+04

Error Coefficients

Relative Standard Deviation: 9.6

ID Level Concentration Response IS Amount IS Response RF Used

1 IC 460-1009900/2 5.0 353430.0 70686.0 Y

2 IC 460-1009900/3 10.0 673355.0 67335.5 Y

3 IC 460-1009900/4 50.0 3009160.0 60183.2 Y

4 IC 460-1009900/5 100.0 5814588.0 58145.88 Y

5 IC 460-1009900/6 200.0 11413384.0 57066.92 Y

Response = [6.268E+04]x

Concentration

0 100 200 0.0

0.2

0.4

0.6

0.8

1.0

1.2

R esponse ( X

10000000)

IC 460-1009900/2

IC 460-1009900/3

IC 460-1009900/4

Page 7927 of 21459

Calibration / n-Hexacosane

Weighting: Conc_Sq

Origin: Force

Dependency: Response

Calib Mode: ESTD

Response Base: AREA

RF Rounding: 0

Curve Coefficients

Intercept: 0

Slope: 6.244E+04

Error Coefficients

Relative Standard Deviation: 7.8

ID Level Concentration Response IS Amount IS Response RF Used

1 IC 460-1009900/2 5.0 343957.0 68791.4 Y

2 IC 460-1009900/3 10.0 662607.0 66260.7 Y

3 IC 460-1009900/4 50.0 3031817.0 60636.34 Y

4 IC 460-1009900/5 100.0 5901739.0 59017.39 Y

5 IC 460-1009900/6 200.0 11496103.0 57480.515 Y

Response = [6.244E+04]x

Concentration

0 100 200 0.0

0.2

0.4

0.6

0.8

1.0

1.2

R esponse ( X

10000000)

IC 460-1009900/2

IC 460-1009900/3

IC 460-1009900/4

Page 7928 of 21459

Calibration / n-Octacosane

Weighting: Conc_Sq

Origin: Force

Dependency: Response

Calib Mode: ESTD

Response Base: AREA

RF Rounding: 0

Curve Coefficients

Intercept: 0

Slope: 6.255E+04

Error Coefficients

Relative Standard Deviation: 6.2

ID Level Concentration Response IS Amount IS Response RF Used

1 IC 460-1009900/2 5.0 338592.0 67718.4 Y

2 IC 460-1009900/3 10.0 652386.0 65238.6 Y

3 IC 460-1009900/4 50.0 3080035.0 61600.7 Y

4 IC 460-1009900/5 100.0 6001809.0 60018.09 Y

5 IC 460-1009900/6 200.0 11634153.0 58170.765 Y

Response = [6.255E+04]x

Concentration

0 100 200 0.0

0.2

0.4

0.6

0.8

1.0

1.2

R esponse ( X

10000000)

IC 460-1009900/2

IC 460-1009900/3

IC 460-1009900/4

Page 7929 of 21459

Calibration / C21-C40 Aliphatics

Weighting: Conc_Sq

Origin: Force

Dependency: Response

Calib Mode: ESTD

Response Base: AREA

RF Rounding: 0

Curve Coefficients

Intercept: 0

Slope: 5.771E+04

Error Coefficients

Relative Standard Deviation: 4.7

ID Level Concentration Response IS Amount IS Response RF Used

1 IC 460-1009900/2 50.0 2743700.0 54874.0 Y

2 IC 460-1009900/3 100.0 5458285.0 54582.85 Y

3 IC 460-1009900/4 500.0 29826142.0 59652.284 Y

4 IC 460-1009900/5 1000.0 60113882.0 60113.882 Y

5 IC 460-1009900/6 2000.0 118609088.0 59304.544 Y

Response = [5.771E+04]x

Concentration

0 1000 2000 0.0

0.2

0.4

0.6

0.8

1.0

1.2

R esponse ( X

100000000)

IC 460-1009900/2

IC 460-1009900/3

IC 460-1009900/4

IC 460-1009900/6

Page 7930 of 21459

Calibration / Triacontane

Weighting: Conc_Sq

Origin: Force

Dependency: Response

Calib Mode: ESTD

Response Base: AREA

RF Rounding: 0

Curve Coefficients

Intercept: 0

Slope: 6.24E+04

Error Coefficients

Relative Standard Deviation: 4.7

ID Level Concentration Response IS Amount IS Response RF Used

1 IC 460-1009900/2 5.0 330147.0 66029.4 Y

2 IC 460-1009900/3 10.0 644111.0 64411.1 Y

3 IC 460-1009900/4 50.0 3116091.0 62321.82 Y

4 IC 460-1009900/5 100.0 6065571.0 60655.71 Y

5 IC 460-1009900/6 200.0 11713597.0 58567.985 Y

Response = [6.24E+04]x

Concentration

0 100 200 0.0

0.2

0.4

0.6

0.8

1.0

1.2

R esponse ( X

10000000)

IC 460-1009900/2

IC 460-1009900/3

IC 460-1009900/4

Page 7931 of 21459

Calibration / Dotriacontane

Weighting: Conc_Sq

Origin: Force

Dependency: Response

Calib Mode: ESTD

Response Base: AREA

RF Rounding: 0

Curve Coefficients

Intercept: 0

Slope: 6.189E+04

Error Coefficients

Relative Standard Deviation: 2.4

ID Level Concentration Response IS Amount IS Response RF Used

1 IC 460-1009900/2 5.0 308082.0 61616.4 Y

2 IC 460-1009900/3 10.0 624673.0 62467.3 Y

3 IC 460-1009900/4 50.0 3185099.0 63701.98 Y

4 IC 460-1009900/5 100.0 6195839.0 61958.39 Y

5 IC 460-1009900/6 200.0 11941308.0 59706.54 Y

Response = [6.189E+04]x

Concentration

0 100 200 0.0

0.2

0.4

0.6

0.8

1.0

1.2

R esponse ( X

10000000)

IC 460-1009900/2

Page 7932 of 21459

Calibration / Tetratriacontane

Weighting: Conc_Sq

Origin: Force

Dependency: Response

Calib Mode: ESTD

Response Base: AREA

RF Rounding: 0

Curve Coefficients

Intercept: 0

Slope: 6.02E+04

Error Coefficients

Relative Standard Deviation: 8.6

ID Level Concentration Response IS Amount IS Response RF Used

1 IC 460-1009900/2 5.0 263715.0 52743.0 Y

2 IC 460-1009900/3 10.0 571195.0 57119.5 Y

3 IC 460-1009900/4 50.0 3255568.0 65111.36 Y

4 IC 460-1009900/5 100.0 6412894.0 64128.94 Y

5 IC 460-1009900/6 200.0 12381623.0 61908.115 Y

Response = [6.02E+04]x

Concentration

0 100 200 0.0

0.2

0.4

0.6

0.8

1.0

1.2

R esponse ( X

10000000)

IC 460-1009900/2

IC 460-1009900/3

IC 460-1009900/4 IC 460-1009900/6

Page 7933 of 21459

Calibration / n-Hexatriacontane

Weighting: Conc_Sq

Origin: Force

Dependency: Response

Calib Mode: ESTD

Response Base: AREA

RF Rounding: 0

Curve Coefficients

Intercept: 0

Slope: 5.262E+04

Error Coefficients

Relative Standard Deviation: 22.0

ID Level Concentration Response IS Amount IS Response RF Used

1 IC 460-1009900/2 5.0 184992.0 36998.4 Y

2 IC 460-1009900/3 10.0 433797.0 43379.7 Y

3 IC 460-1009900/4 50.0 3023505.0 60470.1 Y

4 IC 460-1009900/5 100.0 6171513.0 61715.13 Y

5 IC 460-1009900/6 200.0 12103224.0 60516.12 Y

Response = [5.262E+04]x

Concentration

0 100 200 0.0

0.2

0.4

0.6

0.8

1.0

1.2

R esponse ( X

10000000)

IC 460-1009900/2

IC 460-1009900/3

IC 460-1009900/4 IC 460-1009900/6

Page 7934 of 21459

Calibration / C38

Weighting: Conc_Sq

Origin: Force

Dependency: Response

Calib Mode: ESTD

Response Base: AREA

RF Rounding: 0

Curve Coefficients

Intercept: 0

Slope: 4.446E+04

Error Coefficients

Relative Standard Deviation: 36.1

ID Level Concentration Response IS Amount IS Response RF Used

1 IC 460-1009900/2 5.0 123404.0 24680.8 Y

2 IC 460-1009900/3 10.0 296700.0 29670.0 Y

3 IC 460-1009900/4 50.0 2602687.0 52053.74 Y

4 IC 460-1009900/5 100.0 5738706.0 57387.06 Y

5 IC 460-1009900/6 200.0 11702497.0 58512.485 Y

Response = [4.446E+04]x

Concentration

0 100 200 0.0

0.2

0.4

0.6

0.8

1.0

1.2

R esponse ( X

10000000)

IC 460-1009900/2

IC 460-1009900/3

IC 460-1009900/4

Page 7935 of 21459

Calibration / C40

Weighting: Conc_Sq

Origin: Force

Dependency: Response

Calib Mode: ESTD

Response Base: AREA

RF Rounding: 0

Curve Coefficients

Intercept: 0

Slope: 3.517E+04

Error Coefficients

Relative Standard Deviation: 46.0

ID Level Concentration Response IS Amount IS Response RF Used

1 IC 460-1009900/2 5.0 89657.0 17931.4 Y

2 IC 460-1009900/3 10.0 186993.0 18699.3 Y

3 IC 460-1009900/4 50.0 1939385.0 38787.7 Y

4 IC 460-1009900/5 100.0 4792518.0 47925.18 Y

5 IC 460-1009900/6 200.0 10503440.0 52517.2 Y

Response = [3.517E+04]x

Concentration

0 100 200 0.0

0.2

0.4

0.6

0.8

1.0

R esponse ( X

10000000)

IC 460-1009900/2

IC 460-1009900/3

IC 460-1009900/4

Page 7936 of 21459

FORM VI

Lab Name: Job No.:

HYDROCARBONS BY EXTERNAL STANDARD - INITIAL CALIBRATION DATA

Eurofins Edison 180-185280-1 Analy Batch No.: 1013895

RETENTION TIME SUMMARY

SDG No.:

Calibration ID:

Instrument ID: Heated Purge: (Y/N)CBNAGC4

99688Calibration Start Date: Calibration End Date:12/24/2024 16:23

N

12/24/2024 17:25

0.32(mm)GC Column: Rtx-Mineral OilID:

Calibration Files:

LEVEL: LAB SAMPLE ID: LAB FILE ID:

Level 1 IC 460-1013895/2 4F0019804.D Level 2 IC 460-1013895/3 4F0019805.D Level 3 IC 460-1013895/4 4F0019806.D Level 4 IC 460-1013895/5 4F0019807.D Level 5 IC 460-1013895/6 4F0019808.D

ANALYTE LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 AVG RTRT WINDOW

n-Nonane 1.2741.223 - 1.3231.270 1.269 1.273 1.276 1.283 n-Decane 1.7401.488 - 1.9881.734 1.736 1.738 1.742 1.750 C9-C12 Aliphatics 1.8891.173 - 2.6081.888 1.888 1.890 1.890 1.890 Naphthalene 2.3142.263 - 2.3632.309 2.308 2.313 2.317 2.323 Dodecane 2.5072.458 - 2.5582.501 2.501 2.508 2.510 2.517 2-Methylnaphthalene 2.6942.644 - 2.7442.688 2.687 2.694 2.698 2.704 n-Tetradecane 3.1222.872 - 3.3723.116 3.116 3.122 3.124 3.130 C12-C16 Aliphatics 3.1702.608 - 3.7353.169 3.169 3.171 3.171 3.171 Hexadecane 3.6363.585 - 3.6853.630 3.631 3.635 3.640 3.646 n-Octadecane 4.0804.029 - 4.1294.070 4.073 4.079 4.084 4.094 Total EPH (C9-C40) 4.1611.173 - 7.1534.159 4.159 4.163 4.163 4.163 C16-C21 Aliphatics 4.2423.735 - 4.7484.241 4.241 4.242 4.242 4.242 icosane 4.4694.418 - 4.5184.460 4.462 4.468 4.472 4.481 n-Heneicosane 4.6494.598 - 4.6984.640 4.641 4.648 4.653 4.665 n-Docosane 4.8214.570 - 5.0704.811 4.813 4.820 4.824 4.838 n-Tetracosane 5.1424.891 - 5.3915.131 5.134 5.141 5.147 5.158 n-Hexacosane 5.4395.188 - 5.6885.428 5.429 5.438 5.443 5.455 n-Octacosane 5.7145.463 - 5.9635.703 5.704 5.713 5.719 5.731 C21-C40 Aliphatics 5.9484.748 - 7.1535.946 5.946 5.950 5.950 5.950 Triacontane 5.9705.720 - 6.2205.958 5.961 5.970 5.975 5.988 Dotriacontane 6.2115.960 - 6.4606.199 6.203 6.210 6.217 6.228 Tetratriacontane 6.4386.188 - 6.6886.425 6.429 6.438 6.444 6.456 n-Hexatriacontane 6.6536.401 - 6.9016.640 6.643 6.651 6.658 6.671 n-Octatriacontane 6.8566.605 - 7.1056.845 6.845 6.855 6.862 6.875 n-Tetracontane 7.0557.003 - 7.1037.043 7.042 7.053 7.062 7.076 o-Terphenyl 4.1614.110 - 4.2104.151 4.154 4.160 4.165 4.174 1-Chlorooctadecane 4.5974.546 - 4.6464.587 4.589 4.596 4.600 4.611

FORM VI NJDEP EPH Page 7937 of 21459

HYDROCARBONS BY EXTERNAL STANDARD - INITIAL CALIBRATION DATA

Eurofins Edison 180-185280-1 Analy Batch No.: 1013895

CURVE EVALUATION

SDG No.:

Calibration ID:

Instrument ID: GC Column: Heated Purge: (Y/N)CBNAGC4

99688Calibration Start Date: Calibration End Date:12/24/2024 16:23

N

12/24/2024 17:25

0.32(mm)Rtx-Mineral OilID:

Calibration Files

LEVEL: LAB SAMPLE ID: LAB FILE ID:

1Level IC 460-1013895/2 4F0019804.D 2Level IC 460-1013895/3 4F0019805.D 3Level IC 460-1013895/4 4F0019806.D 4Level IC 460-1013895/5 4F0019807.D 5Level IC 460-1013895/6 4F0019808.D

MIN R^2

OR COD

#R^2

OR COD

MAX

%RSD

#%RSD#COEFFICIENT

M2M1B

CURVE

TYPE

LVL 4LVL 3LVL 2LVL 1

CFANALYTE MIN CF

/RSE

/RSE

LVL 5

n-Nonane Ave 2.3 100.063245 64859 61058 61943 62724

62765.939 n-Decane Ave 2.0 100.063710 65799 62381 63326

64155 63874.039

C9-C12 Aliphatics Ave 2.2 25.066566 68051 64222 65175

65954 65993.795

Naphthalene Ave 2.1 25.066168 69360 67275 68555

69511 68173.694

Dodecane Ave 1.8 100.065568 67624 64356 65183

65887 65723.735

2-Methylnaphthalene Ave 6.4 25.059053 66831 67310 68715

69865 66354.787 n-Tetradecane Ave 1.8 100.066373 69136 66085 66723

67499 67162.991

C12-C16 Aliphatics Ave 1.9 25.068114 71353 68161 68804

69409 69168.174

Hexadecane Ave 11.7 100.067923 70763 68117 58988

53008 63759.728 n-Octadecane Ave 12.1 100.070418 71770 59344 55599

57294 62885.010

Total EPH (C9-C40) Ave 1.8 25.067340 70113 68509 70064

70198 69244.859

C16-C21 Aliphatics Ave 2.9 25.074287 77200 76810 79970

74810 76615.783 icosane Ave 8.0 100.071198 70176 60395 60935

62638 65068.365 n-Heneicosane Ave 7.6 100.073197 71799 62212 63042

64936 67037.114

FORM VI NJDEP EPH

Note: The M1 coefficient is the same as Ave CF for an Ave curve type. RSD is calculated for Ave curve types. RSE is used for all other types.

Page 7938 of 21459

HYDROCARBONS BY EXTERNAL STANDARD - INITIAL CALIBRATION DATA

Eurofins Edison 180-185280-1 Analy Batch No.: 1013895

CURVE EVALUATION

SDG No.:

Calibration ID:

Instrument ID: GC Column: Heated Purge: (Y/N)CBNAGC4

99688Calibration Start Date: Calibration End Date:12/24/2024 16:23

N

12/24/2024 17:25

0.32(mm)Rtx-Mineral OilID:

MIN R^2

OR COD

#R^2

OR COD

MAX

%RSD

#%RSD#COEFFICIENT

M2M1B

CURVE

TYPE

LVL 4LVL 3LVL 2LVL 1

CFANALYTE MIN CF

/RSE

/RSE

LVL 5

n-Docosane Ave 6.2 100.071270 70163 61859 63520 65655

66493.596 n-Tetracosane Ave 4.2 100.071909 71664 65291 66850

68575 68857.822 n-Hexacosane Ave 3.2 100.071965 72600 67309 68590

69828 70058.115 n-Octacosane Ave 2.4 100.072023 72970 68692 69847

70943 70895.010

C21-C40 Aliphatics Ave 3.0 25.065337 68444 67842 69491

70786 68379.865

Triacontane Ave 1.9 100.071016 72322 68775 69983

70999 70618.913

Dotriacontane Ave 1.6 100.070087 72161 69284 70378

71279 70637.754

Tetratriacontane Ave 2.2 100.068583 71796 70377 71560

72634 70990.056 n-Hexatriacontane Ave 5.1 100.061400 66171 67480 68905

70323 66855.993 n-Octatriacontane Ave 11.4 100.051614 57966 64194 66606

68951 61866.369 n-Tetracontane Ave 23.2 100.036319 44334 57013 61515

65655…