J185041_1 Std_Tal_L4 Final Report_Part2.pdf
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- Solicitation number
- W912DS25BA005
About this file
This file contains multiple Certificates of Analysis for various chemical reagents and standards, primarily from manufacturers like Agilent, Ricca Chemical Company, and Sigma-Aldrich. The certificates provide detailed technical specifications for reference materials and standards, including complex cyanide standards, chromium AA standards, lead(II) chromate, pH buffer solutions, and other laboratory reagents. Each certificate includes critical information such as lot numbers, manufacture and expiration dates, product traceability to NIST standards, concentration details, quality control certifications (ISO 9001, ISO 17025, ISO 17034), and specific chemical composition and purity measurements.
The certificates demonstrate rigorous quality control processes, with measurements performed using calibrated equipment traceable to national standards, precise concentration verifications, and comprehensive documentation of manufacturing and testing procedures. The standards are intended for use in laboratory analyses, instrument calibration, method validation, and other scientific research applications, with specific storage instructions, handling guidelines, and safety considerations provided for each reagent.
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P ag e o f 1
Reagent
SV LST1/STD10_00015
Page 1262 of 15442
SV SS L1/S10_00007
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SV SS L1/S11_00007
Page 1266 of 15442 e o f 1 e o f 1
SV SS L2/S2_00011
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SV SS L2/S2_00013
Page 1272 of 15442 e o f 1 e o f 1
SV SS L2/S2_00014
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SV SS L2/S5_00008
Page 1276 of 15442 e o f 1
SV SS L2/STD1_00013
Page 1278 of 15442 e o f 1 e o f 1 e o f 1
SV SS L3/STD1_00003
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SV SS L3/STD1_00005
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SV2356TCPs_00006
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SV2NAPAMINEs_00014
Page 1287 of 15442 e o f 1 e o f 1 sv712dimbenza_00015
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SVFAMPHURs_00021
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SVKEPONEs_00016
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SVKEPONs_00001
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SVLIST1/STD1_00013
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SVLIST1/STD1_00017
Page 1304 of 15442 e o f 1 e o f 1 e o f 1 e o f 1
SVLIST1/STD1_00019
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SVLIST1/STD1_00022
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SVLIST1/STD11_00010
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SVLIST1/STD11_00012
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SVLIST1/STD11_00013
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SVLIST1/STD11_00015
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SVLIST1/STD11_00016
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SVLIST1/STD9_00010
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SVLIST1/STD9_00012
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SVLIST1/STD9_00014
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SVLIST1/STD9_00015
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SVLIST1/STD9_00016
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SVLIST1/STD9_00017
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SVLVIntstd_00012
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SVLVIntstd_00013
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SVLVSURSPK_00022
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SVLVSURSPK_00028
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SVLVSURSPK_00030
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SVLVSURSPK_00031
Page 1351 of 15442 svmethylmetha_00014
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SVNNITROPYROs_00023
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SVSEC L1/STD1_00007
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SVTUNINGMIXs_00009
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SVTUNINGMIXs_00010
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TECHCHLORDANE_00007
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TECHCHLORDANE_00008
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WCNSoilLCS_00032
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WCNWSTOCK_00012
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ISO 17034
Reference Material Certificate
Product Information Sheet
Complex Cyanide Standard
ICC-009
Product Name:
Product Number:
30-Nov-2025Expiration Date:Store at Room Temperature (15° to 30°C). Light Sensitive.Storage Conditions:
16-Oct-2023Lot Issue Date:
0006766987Lot Number:
Traceability:
The balances used for these measurements are calibrated with weights traceable to NIST in compliance with ANSI/NCSL Z540.3, ISO 9001, ISO 17025, and ISO 17034. Calibrated Class A glassware is used for volumetric measurements. Thermometers are calibrated against a NIST traceable thermometer in accordance with NIST Special Publication 1088.
Homogeneity:
This analytical reference standard was unitized according to an in-house procedure and is guaranteed to be homogeneous. There is no minimum sub-sample size required.
Intended Use:
This analytical reference standard is intended for the preparation of working reference samples for use in routine laboratory analyses, calibration of instruments, validation of analytical methods, assessments of measurement methods, and continuing calibration verification.
Instructions for Use:
Sample aliquots for analysis should be withdrawn at 20ºC to 25ºC immediately after opening the container and should be processed without delay for the certified values to be valid within the stated uncertainties.
Safety:
Expiration of Certification:
The certification of this analytical reference standard is valid until the expiration date specified above, provided the material is handled and stored in accordance with the instructions given in this certificate. This certification is nullified if the material is damaged, contaminated, or otherwise modified.
Matrix: 0.1% sodium hydroxide in water
Refer to the Safety Data Sheet on www.agilent.com for information regarding this analytical reference material.
This document is prepared in accordance with ISO 17034 and Guide 31. This analytical reference material (RM) was manufactured and verified in accordance with an ISO 9001 registered quality system. The analyte concentration(s) were prepared and verified by an ISO 17034 / ISO 17025 accredited laboratory and compared to calibration standards independently prepared using NIST SRM(s) when available. The certified value and uncertainty value at the 95% confidence level for each analyte is determined gravimetrically.
Description:
Component Name CAS# Analyte LotConcentration Uncertainty potassium ferricyanide (as cyanide) 013746-66-2 RM194461001 ± 5 µg/mL
1 of 2Page:
CSD-QA-040.1 ISO 17025
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Maintenance of Certification:
If substantive changes are noted that affect the certification before the expiration of this certificate, Agilent will notify the purchaser.
Sample lot approver:
ISO 17034 Cert No. AR-1936
RM was produced in accordance with the TUV/SUD registered ISO 9001:2015 Quality Management System. Cert# 951215321
2 of 2Page:
www.agilent.com/quality/
CSD-QA-040.1 ISO 17025
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WCr1000S_00014
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Certificate of Analysis
Lot Number: 44020249
Manufacture Date: February 26, 2024LC131207
Chromium AA Standard 1000 ppm (1ml = 1mg Cr)
Product Code:
Expiration Date: February 26, 2026
Test Specification Result clear solutionclear solutionAppearance (clarity) orangeorangeAppearance (color)
0.999mg Cr/mL0.995 - 1.005mg Cr/mLChromium (Cr)
999ppm995 - 1,005ppmChromium (Cr)
136fReportTraceable to NIST K2Cr2O7
Intended Use - Product is intended for use in manufacturing procedures and laboratory procedures and protocols.
Storage Information - Unless noted on the product label, store the product under normal lab conditions in its tightly closed, original container. Do not pipet directly from the container or return unused portions to the container.
Instructions for Handling and Use - Please refer to the associated product label and Safety Data Sheet (SDS) for information regarding safety and handling of this product.
Preparation - All products are manufactured and tested according to established, documented procedures and methodology.
Production documentation records manufacturing data, raw material traceability and testing history on a per lot basis. Balances, thermometers, and glassware are calibrated before first use and on a regular schedule with references traceable to NIST standards.
Quality Control
ISO9001:2015 Registration #0306-01 Michael Monteleone
Chemistry Supervisor
2024032114:40:11ahoffman-0-0 Page 1375 of 15442
WCr6InsolSP_00005
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BEANTOWN CHEMICAL CORPORATION, 9 SAGAMORE PARK ROAD, HUDSON NH 03051
WWW.BEANTOWNCHEM.COM TOLL FREE: 1-844-891-6306 EMAIL: TECHNICAL@BEANTOWNCHEM.COM
Catalog Number 211075 Product Description Lead(II) chromate, ACS, 98.0% min.
CAS Number 7758-97-6
Lot Number 50105919
Test Results
Results Assay, PbCrO4 99.28% Appearance Orange/red powder Soluble matter <0.15% Carbon compounds (as C) <0.01%
This certificate of analysis has been electronically generated and is valid without a signature.
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WHemPSP_00314
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WK2CrO7P_00021
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Product Number: 207802
Batch Number: MKCT4740
Brand: SIGALD
CAS Number: 7778-50-9
MDL Number: MFCD00011367
Formula: Cr2K2O7
Formula Weight: 294.18 g/mol
Quality Release Date: 02 MAY 2023
Test Specification Result________________________________________________________________________
Appearance (Color) Conforms to Requirements Orange
Orange
Appearance (Form) Crystals Crystals
X-Ray Diffraction Conforms to Structure Conforms
Titration by Na2S2O3 > 99.0 % > 99.5 %_
Loss on Drying < 0.05 % 0.02 %_
Calcium (Ca) < 0.003 % 0.002 %_
Chloride Content < 0.001 % < 0.001 %_
Iron (Fe) < 0.001 % < 0.001 %_
Insoluble Matter < 0.005 % 0.003 %_
C = 10%, H2O
Sodium (Na) < 0.02 % < 0.02 %_
Sulfate (SO4) < 0.005 % 0.002 %_
Meets ACS Requirements Current ACS Specification Conforms ________________________________________________________________________
Larry Coers, Director
Quality Control
Milwaukee, WI US
Certificate of Analysis
Version Number: 1
3050 Spruce Street, Saint Louis, MO 63103, USA
Website: www.sigmaaldrich.com
Email USA: techserv@sial.com
Outside USA: eurtechserv@sial.com
Product Name:
Sigma-Aldrich warrants, that at the time of the quality release or subsequent retest date this product conformed to the information contained in this publication. The current Specification sheet may be available at Sigma-Aldrich.com. For further inquiries, please contact
Technical Service. Purchaser must determine the suitability of the product for its particular use. See reverse side of invoice or packing slip for additional terms and conditions of sale.
Page 1381 of 15442
WKCN_ACS_00002
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Order our products online thermofisher.com/chemicals
This document has been electronically generated and does not require a signature.
Products are processed under ISO 9001:2015 quality management systems and samples are tested for conformance to the noted specifications. Certain data may have been supplied by third parties. We disclaim the implied warranties of merchantability and fitness for a particular purpose, and the accuracy of third party data or information associated with the product. Products are for research and development use only. Products are not for direct administration to humans or animals. It is the responsibility of the final formulator or end user to determine suitability, and to qualify and/or validate each product for its intended use.
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WKCN_ACS_P_00001
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WpHBuffer7CCV_00096
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1490 Lammers Pike Batesville, IN 47006 http://www.riccachemical.com
1-888-GO-RICCA
customerservice@riccachemical.com
Buffer, Reference Standard, pH 7.00 ± 0.01 at 25°C (Color Coded Green)
Manufacture Date: SEP 20, 2024
Expiration Date: SEP 2026Lot Number: 4409M13 Product Number: 1551.4
The certified value for this product is confirmed in independent testing by a second qualified chemist.
pH
7.12 7.09 °C 5 10 15 20 25 30 35 40 45 50
7.06 7.04 7.02 7.00 6.99 6.98 6.98 6.97 6.97
Name CAS# Grade
ACS/ASTM/USP/EP7732-18-5Water
ACS7558-79-4Sodium Phosphate Dibasic
ACS7778-77-0Potassium Dihydrogen Phosphate
ProprietaryPreservative
ProprietaryYellow Dye
ProprietaryBlue Dye
Reagent1310-73-2Sodium Hydroxide
Test Specification Result
Appearance Passed Green liquid *Not a certified value.
Test Certified Value NIST SRM#Uncertainty pH at 25°C (Method: SQCP027, SQCP033) 7.005 186-I-g, 186-II-g, 191d0.02 pH measurements were performed in our Batesville, IN laboratory under ISO/IEC 17025 accreditation (ANAB Certificate L2387.02) and are certified traceable to National Institute of Standards and Technology (NIST) Standard Reference Material as indicated above via an unbroken chain of comparisons. The uncertainty is calculated from the uncertainty of the measurement variation from sample to sample, the uncertainty in the NIST Standard Reference Material, and the uncertainty of the measurement process. The uncertainty is multiplied by k=2, corresponding to
95% coverage in a normal distribution. Volumetric glassware complies with Class A tolerance requirements of ASTM E 288 and NIST Circular 434;
it is calibrated before first use and recalibrated regularly in accordance with ASTM E 542 and NIST Procedure NBSIR 74-461. Balances are calibrated regularly with weights certified traceable to the NIST national mass standard. Thermometers and temperature probes are calibrated before first use and recalibrated regularly with a thermometer traceable to NIST standards. All products are prepared according to master documents that assure manufacture according to validated methods. Batch records document raw material traceability and production and testing history for each lot manufactured.
Part Number Shelf Life (Unopened Container)Size / Package Type
1551.4-1 24 months4 L natural poly
1551.4-32 24 months1 L natural poly
1551.4-5 24 months20 L Cubitainer®
Recommended Storage: 15°C - 30°C (59°F - 86°F)
Version: 1.3 Product Number: 1551.4Lot Number: 4409M13 Page 1 of 2
Page 1387 of 15442
Production Manager
Paul Brandon (09/20/2024)
This test report shall not be reproduced, except in full, without the written approval of Ricca Chemical Company.
This product was tested in an ISO 17025 Accredited Laboratory
Version: 1.3 Product Number: 1551.4Lot Number: 4409M13 Page 2 of 2
Page 1388 of 15442
WpHBuffer7P_00058
Page 1389 of 15442
Lot Number: 44020056
Manufacture Date: February 21, 2024LC123701
Buffer Solution pH 7.0
Product Code:
Expiration Date: February 21, 2026
Test Specification Result clear solutionclear solutionAppearance (clarity) colorlesscolorlessAppearance (color)
186g, 187fReportVerified against NIST Buffer
7.006.99 - 7.01pH @ 25°C
Intended Use - Product is intended for use in manufacturing procedures and laboratory procedures and protocols.
Storage Information - Unless noted on the product label, store the product under normal lab conditions in its tightly closed, original container. Do not pipet directly from the container or return unused portions to the container.
Instructions for Handling and Use - Please refer to the associated product label and Safety Data Sheet (SDS) for information regarding safety and handling of this product.
Preparation - All products are manufactured and tested according to established, documented procedures and methodology.
Production documentation records manufacturing data, raw material traceability and testing history on a per lot basis. Balances, thermometers, and glassware are calibrated before first use and on a regular schedule with references traceable to NIST standards.
Quality Control
ISO9001:2015 Registration #0306-01 Michael Monteleone
Chemistry Supervisor
2024031910:36:15ahoffman-0-0 Page 1390 of 15442
WTKN1000P_00008
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WTKN1000S_00006
Page 1393 of 15442 e o f 1
B 10000PPM_00005
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ICP ICVL/CCVL_00014
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ICPICSA_00014
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ICPICSA_00015
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| Data Summaries |
| Sample Container Check |
| Organic Sample Data |
| GC/MS VOA |
| 8260D |
| 8260D QC Summary |
| 8260D Sample Data |
| Standards Data |
| 8260D ICAL Data |
File details come from the government source that posted it. Updated .