J185041_1 Std_Tal_L4 Final Report_Part3.pdf

P ag e o f 1 e o f 1 e o f 1

Reagent

ICPICSABsol1_00007

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MTAG_00031

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MTICP/ICPMS_00063

Page 1416 of 15442

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MTICP/ICPMS_00073

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MTRCRA_00023

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MTZN_00015

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NONRCRA SOL A_00012

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NONRCRA SOL B_00013

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SB 10000PPM_00006

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SPIKE1_00031

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SPIKE2_00023

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14DIOXNEAT_00004

Page 1447 of 15442

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2-CEVEC_00031

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7 Freons_00007

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8260 SURR C_00067

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8260ISNEW_00171

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8260ISNEW_00207

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8260ISNEW_00208

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Acrolein SSH_00040

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ACROLEIN_00025

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Acrylonitrile_00010

Page 1465 of 15442 e o f 1 alpha-Pinene_00001

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EPICHLO(NEAT)_00001

Page 1469 of 15442

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ETHANOL(new)_00025

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Extra Cmpd_00024

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GASES C_00041

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GASES SS_00028

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KetonesC SS_00017

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KetonesC_00030

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LIST2/STD6_00023

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LIST2/STD7_00026

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Mega Mix SS_00022

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Mega Mix_00042

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OP_Ali_st_new_00010

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OP_OTP_00032

Page 1497 of 15442

ISO 17034

Reference Material Certificate

Product Information Sheet o-Terphenyl Surrogate Std - 10,000ug/mL (10mL)

CUS-00004218

Product Name:

Product Number:

Expiration Date:Store at Room Temperature (15° to 30°C).Storage Conditions:

07-Jun-2022Lot Issue Date:

Lot Number:

Traceability:

The balances used for these measurements are calibrated with weights traceable to NIST in compliance with ANSI/NCSL Z540.3, ISO 9001, ISO 17025, and ISO 17034. Calibrated Class A glassware is used for volumetric measurements. Thermometers are calibrated against a NIST traceable thermometer in accordance with NIST Special Publication 1088.

Homogeneity:

This analytical reference standard was unitized according to an in-house procedure and is guaranteed to be homogeneous. There is no minimum sub-sample size required.

Intended Use:

This analytical reference standard is intended for the preparation of working reference samples for use in routine laboratory analyses, calibration of instruments, validation of analytical methods, assessments of measurement methods, and continuing calibration verification.

Instructions for Use:

Sample aliquots for analysis should be withdrawn at 20ºC to 25ºC immediately after opening the container and should be processed without delay for the certified values to be valid within the stated uncertainties.

Safety:

Expiration of Certification:

The certification of this analytical reference standard is valid until the expiration date specified above, provided the material is handled and stored in accordance with the instructions given in this certificate. This certification is nullified if the material is damaged, contaminated, or otherwise modified.

Matrix: methylene chloride (dichloromethane)

Refer to the Safety Data Sheet on www.agilent.com for information regarding this analytical reference material.

This document is prepared in accordance with ISO 17034 and Guide 31. This analytical reference material standard was manufactured and verified in accordance with an ISO 9001 registered quality system and analyte concentrations were verified by an ISO 17025 accredited laboratory. The concentration and uncertainty value at the 95% confidence level for each analyte, determined gravimetrically, is listed above.

Description:

Component Name CAS# Analyte LotConcentration Expanded Uncertainty

CERTIFIED VALUES

o-terphenyl 000084-15-1 NT0161610044 ± 50 µg/mL

1 of 2Page:

CSD-QA-015.1 ISO 17025

31-Jul-2025

0006686252-01

Page 1498 of 15442

Maintenance of Certification:

If substantive changes are noted that affect the certification before the expiration of this certificate, Agilent will notify the purchaser.

Sample lot approver:

ISO 17034 Cert No. AR-1936

RM was produced in accordance with the TUV/SUD registered ISO 9001:2015 Quality Management System. Cert# 951215321

2 of 2Page:

www.agilent.com/quality/

CSD-QA-015.1 ISO 17025

Page 1499 of 15442

OPDIESELFuel2_00018

Page 1500 of 15442

110 Benner Circle

Bellefonte, PA 16823-8812

Tel: (800)356-1688

Fax: (814)353-1309 www.restek.com

Certificate of Analysis

FOR LABORATORY USE ONLY-READ SDS PRIOR TO USE.

This Reference Material is intended for Laboratory Use Only as a standard for the qualitative and/or quantitative determination of the analyte(s) listed.

CERTIFIED REFERENCE MATERIAL

Catalog No. : 31259 Lot No.: A0163966

Diesel Fuel #2 Composite StandardDescription :

Diesel Fuel #2 Composite Standard 50,000µg/mL, Methylene Chloride, 5mL/ampul

Container Size :

Expiration Date : Storage: 25°C nominal

5 mL > 5 mLPkg Amt:

September 30, 2027

Ship: Ambient

Elution

Order Compound Grav. Conc.

(weight/volume)

Expanded Uncertainty

(95% C.L.; K=2)

C E R T I F I E D V A L U E S

1 µg/mL 50,165.8Diesel Fuel #2 Composite

68334-30-5.ACAS #

Purity Stressed

Unstressed

Gravimetric µg/mL+/- 291.6527

+/- 1,493.5921 µg/mL +/- 1,592.9673 µg/mL

(Lot A0160886)

Solvent: Methylene chloride

99%

75-09-2CAS #

Purity

01-Aug-2020 rev. Page 1 of 3

Page 1501 of 15442

Carrier Gas:

Temp. Program:

Inj. Temp:

Det. Type:

Det. Temp:

30m x 0.25mm x 0.25µm

Rtx-5 (cat.#10223)

Column:

hydrogen-constant pressure 10 psi.

40°C (hold 2 min.) to 330°C

@ 10°C/min. (hold 10 min.)

250°C

330°C

FID

1128360905Balance:

04-Sep-2020Date Passed:

Manufactured under Restek's ISO 9001:2015

Registered Quality System

Certificate #FM 80397

27-Aug-2020Date Mixed:

This chromatogram represents a general set of testing conditions chosen for product acceptance. For optimal results in your lab, conditions should be adjusted for your specific instrument, method, and application.

01-Aug-2020 rev. Page 2 of 3

Page 1502 of 15442

Label Conditions Non-Standard Conditions

25°C Nominal (Room Temperature)

10°C or colder (Refrigerate)

0°C or colder (Freezer)

≥ 60°C up to 7 days

≥ 40°C up to 7 days

≥ 25°C up to 7 days

General Certified Reference Material Notes

Expiration Notes:

· Expiration date valid for unopened ampul stored in compliance with the recommended conditions.

· Uncertainty, concentration, and expiration of the CRM are based on the unopened product being stored according to the recommended condition found in the storage field.

Purity Notes:

· Purity and/or chemical identity are determined by one or more of the following techniques: GC/FID, HPLC, GC/µECD, GC/MS, LC/MS, RI, and/or melting point.

· Compounds with a listed purity of less than 99% have been weight corrected to compensate for impurities and/or salts. A correction factor is used to calculate the amount of compound necessary to achieve the desired concentration of the parent compound in solution.

· Purity of isomeric compounds is reported as the sum of the isomers.

· Purity values are rounded to the nearest whole number.

Certified Uncertainty Value Notes:

· The uncertainties are determined in accordance with ISO 17034 and Guide 35. The certified combined stressed uncertainty value ( includes gravimetric uncertainty, homogeneity between-ampul uncertainty, storage stability uncertainty and shipping stability uncertainty and were combined using the following formula:

k is a coverage factor of 2, which gives a level of confidence of approximately 95%.

· It is important to note that the shipping stability uncertainty was obtained under temperature extremes for specific time intervals; therefore, the certified combined stressed uncertainty value should only be applied to the product if it was stored at non-standard temperature conditions up to and including 7 days. Contact Restek Technical Service at www.restek.com/Contact-Us for use recommendations if your shipment was in-transit for more than 7 days at non-standard temperature conditions.

· Apply the certified combined unstressed uncertainty value if the product was received under standard shipping conditions. Apply the certified combined stressed uncertainty value if the product was received under non-standard conditions as specified below.

Standard Conditions

< 60°C

< 40°C

< 25°C

· Separate (not combined) uncertainty values for gravimetric uncertainty are also displayed on the certificate, if needed, separate homogeneity between-ampul uncertainty, storage stability uncertainty and shipping stability uncertainty values are available by contacting Restek Technical Service at www.restek.com/Contact-Us.

· The packaged amount is the minimum sample size for which uncertainty is valid. The ampules are over-filled to ensure that the minimum packaged amount can be sufficiently transferred .

Manufacturing Notes:

· Concentration is based upon gravimetric preparation using either a balance whose calibration has been verified daily using NIST traceable weights, and/or dilutions with Class A glassware.

Handling Notes:

· Stability of the unopened product, when stored in compliance with the recommended conditions, is guaranteed through the expiration displayed on the product label and certificate. Contact Restek for additional opened product stability information, with the knowledge/understanding that open product stability is subject to the specific handling and environmental conditions to which the product is exposed. For your convenience Restek supplies deactivated vials with most standards packed in 2mL ampules. Larger volume deactivated vials are available through Restek as a custom ordered item. Additionally, Restek sells DMDCS for the purpose of glassware deactivation as catalog number 31861, which includes complete instructions.

-20°C or colder (Deep Freezer)

01-Aug-2020 rev. Page 3 of 3

Page 1503 of 15442

OPEPH AR_Std_00009

Page 1504 of 15442

Page 1505 of 15442

OPEPH1-Chloro_00033

Page 1506 of 15442

Product Information Sheet

1-Chlorooctadecane Surrogate Std - 10,000ug/mL (10mL)

CUS-00004217

Product Name:

Product Number:

Expiration Date:Store at Room Temperature (15° to 30°C).Storage Conditions:

03-Jun-2022Lot Issue Date:

Lot Number:

Traceability:

The balances used for these measurements are calibrated with weights traceable to NIST in compliance with ANSI/NCSL Z540.3, ISO 9001, ISO 17025, and ISO 17034. Calibrated Class A glassware is used for volumetric measurements. Thermometers are calibrated against a NIST traceable thermometer in accordance with NIST Special Publication 1088.

Homogeneity:

This analytical reference standard was unitized according to an in-house procedure and is guaranteed to be homogeneous. There is no minimum sub-sample size required.

Intended Use:

This analytical reference standard is intended for the preparation of working reference samples for use in routine laboratory analyses, calibration of instruments, validation of analytical methods, assessments of measurement methods, and continuing calibration verification.

Instructions for Use:

Sample aliquots for analysis should be withdrawn at 20ºC to 25ºC immediately after opening the container and should be processed without delay for the certified values to be valid within the stated uncertainties.

Safety:

Expiration of Certification:

The certification of this analytical reference standard is valid until the expiration date specified above, provided the material is handled and stored in accordance with the instructions given in this certificate. This certification is nullified if the material is

Refer to the Safety Data Sheet on www.agilent.com for information regarding this analytical reference material.

This document is prepared in accordance with ISO 17034 and Guide 31. This analytical reference material standard was manufactured and verified in accordance with an ISO 9001 registered quality system and analyte concentrations were verified by an ISO 17025 accredited laboratory. The concentration and uncertainty value at the 95% confidence level for each analyte, determined gravimetrically, is listed above.

Description:

Component Name CAS# Analyte LotConcentration Expanded Uncertainty

CERTIFIED VALUES

1-chlorooctadecane 003386-33-2 RM1777210038 ± 50 µg/mL

1 of 2Page:

CSD-QA-015.1 ISO 17025

31-Jul-2025

0006686253-01

Page 1507 of 15442

If substantive changes are noted that affect the certification before the expiration of this certificate, Agilent will notify the purchaser.

No. AR-1936

RM was produced in accordance with the TUV/SUD registered ISO 9001:2015 Quality Management System. Cert# 951215321

2 of 2Page:

www.agilent.com/quality/

Page 1508 of 15442

POLAR ADD_00030

Page 1509 of 15442 e o f 1

SG_Ali_2nd_00001

Page 1511 of 15442

Product Information Sheet

Aliphatic Std - 20 at 2000ug/mL (5mL)

CUS-00003433

Store at Room Temperature (15° to 30°C).

03-Jun-2022

Traceability:

The balances used for these measurements are calibrated with weights traceable to NIST in compliance with ANSI/NCSL Z540.3, ISO 9001, ISO 17025, and ISO 17034. Calibrated Class A glassware is used for volumetric measurements. Thermometers are calibrated against a NIST traceable thermometer in accordance with NIST Special Publication 1088.

Matrix: hexane/carbon disulfide (4:1)

This document is prepared in accordance with ISO 17034 and Guide 31. This analytical reference material standard was manufactured and verified in accordance with an ISO 9001 registered quality system and analyte concentrations were verified by an ISO 17025 accredited laboratory. The concentration and uncertainty value at the 95% confidence level for each analyte, determined gravimetrically, is listed above.

Description:

Component Name CAS# Analyte LotConcentration Expanded Uncertainty

CERTIFIED VALUES

n-nonane 000111-84-2 RM150362003 ± 10 µg/mL n-decane 000124-18-5 RM051192005 ± 10 µg/mL naphthalene 000091-20-3 RM104452009 ± 10 µg/mL n-dodecane 000112-40-3 RM196372004 ± 10 µg/mL

2-methylnaphthalene 000091-57-6 RM012582004 ± 10 µg/mL n-tetradecane 000629-59-4 RM099972000 ± 10 µg/mL n-hexadecane 000544-76-3 RM174122008 ± 10 µg/mL n-octadecane 000593-45-3 RM099952001 ± 10 µg/mL n-eicosane 000112-95-8 RM041692001 ± 10 µg/mL n-heneicosane 000629-94-7 RM041702002 ± 10 µg/mL n-docosane 000629-97-0 RM121342000 ± 10 µg/mL n-tetracosane 000646-31-1 RM139982002 ± 10 µg/mL n-hexacosane 000630-01-3 RM143952005 ± 10 µg/mL n-octacosane 000630-02-4 RM147152008 ± 10 µg/mL n-triacontane 000638-68-6 RM158672002 ± 10 µg/mL n-dotriacontane 000544-85-4 NT020382006 ± 10 µg/mL n-tetratriacontane 014167-59-0 RM095622000 ± 10 µg/mL n-hexatriacontane 000630-06-8 RM042742002 ± 10 µg/mL n-octatriacontane 007194-85-6 RM161572004 ± 10 µg/mL n-tetracontane 004181-95-7 RM188232008 ± 10 µg/mL

1 of 2Page:

CSD-QA-015.1 ISO 17025

250 Smith Street North Kingstown, Rhode Island 02852 www.agilent.com/quality

31-Jul-2025

0006686255-01

Page 1512 of 15442

Homogeneity:

This analytical reference standard was unitized according to an in-house procedure and is guaranteed to be homogeneous. There is no minimum sub-sample size required.

Intended Use:

This analytical reference standard is intended for the preparation of working reference samples for use in routine laboratory analyses, calibration of instruments, validation of analytical methods, assessments of measurement methods, and continuing calibration verification.

Instructions for Use:

Sample aliquots for analysis should be withdrawn at 20ºC to 25ºC immediately after opening the container and should be processed without delay for the certified values to be valid within the stated uncertainties.

Safety:

Expiration of Certification:

The certification of this analytical reference standard is valid until the expiration date specified above, provided the material is handled and stored in accordance with the instructions given in this certificate. This certification is nullified if the material is damaged, contaminated, or otherwise modified.

Maintenance of Certification:

If substantive changes are noted that affect the certification before the expiration of this certificate, Agilent will notify the purchaser.

Refer to the Safety Data Sheet on www.agilent.com for information regarding this analytical reference material.

Sample lot approver:

ISO 17034 Cert No. AR-1936

RM was produced in accordance with the TUV/SUD registered ISO 9001:2015 Quality Management System. Cert# 951215321

2 of 2Page:

www.agilent.com/quality/

250 Smith Street North Kingstown, Rhode Island 02852 www.agilent.com/qualityPage 1513 of 15442

SGEPH 1-CODst_00009

Page 1514 of 15442

Tel: (800)356-1688

Fax: (814)353-1309 www.restek.com

Certificate of Analysis

FOR LABORATORY USE ONLY-READ SDS PRIOR TO USE.

This Reference Material is intended for Laboratory Use Only as a standard for the qualitative and/or quantitative determination of the analyte(s) listed.

CERTIFIED REFERENCE MATERIAL

Catalog No. : 31098 Lot No.: A0183404

1-Chlorooctadecane StandardDescription :

1-Chlorooctadecane Standard 10,000µg/mL, Methylene Chloride, 1mL/ampul

Container Size :

Expiration Date : Storage: 10°C or colder

2 mL > 1 mLPkg Amt:

April 30, 2029

Ship: Ambient

Elution

Order Compound Grav. Conc.

(weight/volume)

Expanded Uncertainty

(95% C.L.; K=2)

C E R T I F I E D V A L U E S

99%

1 µg/mL 10,051.01-Chlorooctadecane

3386-33-2CAS #

Purity Stressed

Unstressed

Gravimetric µg/mL+/- 58.4374

+/- 563.5496 µg/mL +/- 576.7359 µg/mL

(Lot 12882200)

Solvent: Methylene chloride

99%

75-09-2CAS #

Purity

01-Aug-2020 rev. Page 1 of 3

Page 1515 of 15442

Inj. Temp:

Det. Type:

Det. Temp:

30m x 0.25mm x 0.25µm

Rtx-5 (cat.#10223)

Column:

hydrogen-constant pressure 10 psi.

75°C (hold 1 min.) to 330°C

@ 20°C/min. (hold 10 min.)

250°C

330°C

FID

1128353505Balance:

31-Mar-2022Date Passed:

Manufactured under Restek's ISO 9001:2015

Registered Quality System

Certificate #FM 80397

28-Mar-2022Date Mixed:

This chromatogram represents a general set of testing conditions chosen for product acceptance. For optimal results in your lab, conditions should be adjusted for your specific instrument, method, and application.

01-Aug-2020 rev. Page 2 of 3

Page 1516 of 15442

10°C or colder (Refrigerate)

0°C or colder (Freezer)

≥ 60°C up to 7 days

≥ 40°C up to 7 days

≥ 25°C up to 7 days

General Certified Reference Material Notes

Expiration Notes:

· Expiration date valid for unopened ampul stored in compliance with the recommended conditions.

· Uncertainty, concentration, and expiration of the CRM are based on the unopened product being stored according to the recommended condition found in the storage field.

Purity Notes:

· Purity and/or chemical identity are determined by one or more of the following techniques: GC/FID, HPLC, GC/µECD, GC/MS, LC/MS, RI, and/or melting point.

· Compounds with a listed purity of less than 99% have been weight corrected to compensate for impurities and/or salts. A correction factor is used to calculate the amount of compound necessary to achieve the desired concentration of the parent compound in solution.

· Purity of isomeric compounds is reported as the sum of the isomers.

· Purity values are rounded to the nearest whole number.

Certified Uncertainty Value Notes:

· The uncertainties are determined in accordance with ISO 17034 and Guide 35. The certified combined stressed uncertainty value ( includes gravimetric uncertainty, homogeneity between-ampul uncertainty, storage stability uncertainty and shipping stability uncertainty and were combined using the following formula:

k is a coverage factor of 2, which gives a level of confidence of approximately 95%.

· It is important to note that the shipping stability uncertainty was obtained under temperature extremes for specific time intervals; therefore, the certified combined stressed uncertainty value should only be applied to the product if it was stored at non-standard temperature conditions up to and including 7 days. Contact Restek Technical Service at www.restek.com/Contact-Us for use recommendations if your shipment was in-transit for more than 7 days at non-standard temperature conditions.

· Apply the certified combined unstressed uncertainty value if the product was received under standard shipping conditions. Apply the certified combined stressed uncertainty value if the product was received under non-standard conditions as specified below.

Standard Conditions

< 60°C

< 40°C

< 25°C

· Separate (not combined) uncertainty values for gravimetric uncertainty are also displayed on the certificate, if needed, separate homogeneity between-ampul uncertainty, storage stability uncertainty and shipping stability uncertainty values are available by contacting Restek Technical Service at www.restek.com/Contact-Us.

· The packaged amount is the minimum sample size for which uncertainty is valid. The ampules are over-filled to ensure that the minimum packaged amount can be sufficiently transferred .

Manufacturing Notes:

· Concentration is based upon gravimetric preparation using either a balance whose calibration has been verified daily using NIST traceable weights, and/or dilutions with Class A glassware.

Handling Notes:

· Stability of the unopened product, when stored in compliance with the recommended conditions, is guaranteed through the expiration displayed on the product label and certificate. Contact Restek for additional opened product stability information, with the knowledge/understanding that open product stability is subject to the specific handling and environmental conditions to which the product is exposed. For your convenience Restek supplies deactivated vials with most standards packed in 2mL ampules. Larger volume deactivated vials are available through Restek as a custom ordered item. Additionally, Restek sells DMDCS for the purpose of glassware deactivation as catalog number 31861, which includes complete instructions.

-20°C or colder (Deep Freezer)

01-Aug-2020 rev. Page 3 of 3

Page 1517 of 15442

SGEPH AR_Std_00007

Page 1518 of 15442 e o f 1

SGEPH_OTP_00001

Page 1520 of 15442

Product Information Sheet o-Terphenyl Surrogate Std - 10,000ug/mL (10mL)

CUS-00004218

Product Name:

Product Number:

Expiration Date:Store at Room Temperature (15° to 30°C).Storage Conditions:

Lot Issue Date:

Lot Number:

Traceability:

The balances used for these measurements are calibrated with weights traceable to NIST in compliance with ANSI/NCSL Z540.3, ISO 9001, ISO 17025, and ISO 17034. Calibrated Class A glassware is used for volumetric measurements. Thermometers are calibrated against a NIST traceable thermometer in accordance with NIST Special Publication 1088.

Homogeneity:

This analytical reference standard was unitized according to an in-house procedure and is guaranteed to be homogeneous. There is no minimum sub-sample size required.

Intended Use:

This analytical reference standard is intended for the preparation of working reference samples for use in routine laboratory analyses, calibration of instruments, validation of analytical methods, assessments of measurement methods, and continuing calibration verification.

Instructions for Use:

Sample aliquots for analysis should be withdrawn at 20ºC to 25ºC immediately after opening the container and should be processed without delay for the certified values to be valid within the stated uncertainties.

Safety:

Expiration of Certification:

The certification of this analytical reference standard is valid until the expiration date specified above, provided the material is handled and stored in accordance with the instructions given in this certificate. This certification is nullified if the material is

Refer to the Safety Data Sheet on www.agilent.com for information regarding this analytical reference material.

This document is prepared in accordance with ISO 17034 and Guide 31. This analytical reference material standard was manufactured and verified in accordance with an ISO 9001 registered quality system and analyte concentrations were verified by an ISO 17025 accredited laboratory. The concentration and uncertainty value at the 95% confidence level for each analyte, determined gravimetrically, is listed above.

Description:

Component Name CAS# Analyte LotConcentration Expanded Uncertainty

CERTIFIED VALUES

o-terphenyl 000084-15-1 NT0161610044 ± 50 µg/mL

1 of 2Page:

CSD-QA-015.1 ISO 17025

31-Jun-2027

07-M ay-2024

0006686252-01

Page 1521 of 15442

If substantive changes are noted that affect the certification before the expiration of this certificate, Agilent will notify the purchaser.

No. AR-1936

RM was produced in accordance with the TUV/SUD registered ISO 9001:2015 Quality Management System. Cert# 951215321

2 of 2Page:

www.agilent.com/quality/

Page 1522 of 15442

SGEPHAR_SS_00003

Page 1523 of 15442

Tel: (800)356-1688

Fax: (814)353-1309 www.restek.com

Certificate of Analysis

FOR LABORATORY USE ONLY-READ SDS PRIOR TO USE.

This Reference Material is intended for Laboratory Use Only as a standard for the qualitative and/or quantitative determination of the analyte(s) listed.

CERTIFIED REFERENCE MATERIAL

Catalog No. : 31469 Lot No.: A0156231

WA EPH Aromatic Hydrocarbon StdDescription :

WA EPH Aromatic HYDRO. Std 1000µg/mL, Methylene Chloride, 1mL/ampul

Container Size :

Expiration Date : Storage: 25°C nominal

2 mL > 1 mLPkg Amt:

Handling: Sonication required. Mix is photosensitive.

December 31, 2025

Elution

Order Compound Grav. Conc.

(weight/volume)

Expanded Uncertainty

(95% C.L.; K=2)

C E R T I F I E D V A L U E S

99%

1 µg/mL 999.51,2,3-Trimethylbenzene

526-73-8CAS #

Purity Stressed

Unstressed

Gravimetric µg/mL+/- 5.9367

+/- 45.0345 µg/mL +/- 49.9679 µg/mL

(Lot 8776.10-14)

99%

2 µg/mL 1,004.0Naphthalene

91-20-3CAS #

Purity Stressed

Unstressed

Gravimetric µg/mL+/- 5.8920

+/- 45.2279 µg/mL +/- 50.1844 µg/mL

(Lot MKBZ8680V)

96%

3 µg/mL 1,006.62-Methylnaphthalene

91-57-6CAS #

Purity Stressed

Unstressed

Gravimetric µg/mL+/- 5.9071

+/- 45.3432 µg/mL +/- 50.3124 µg/mL

(Lot STBG8884)

98%

4 µg/mL 1,007.0Acenaphthylene

208-96-8CAS #

Purity Stressed

Unstressed

Gravimetric µg/mL+/- 5.9093

+/- 45.3607 µg/mL +/- 50.3319 µg/mL

(Lot R22T)

99%

5 µg/mL 1,000.5Acenaphthene

83-32-9CAS #

Purity Stressed

Unstressed

Gravimetric µg/mL+/- 5.8715

+/- 45.0702 µg/mL +/- 50.0095 µg/mL

(Lot MKCG4614)

99%

6 µg/mL 1,000.5Fluorene

86-73-7CAS #

Purity Stressed

Unstressed

Gravimetric µg/mL+/- 5.8715

+/- 45.0702 µg/mL +/- 50.0095 µg/mL

(Lot 10215869)

99%

7 µg/mL 997.5Phenanthrene

85-01-8CAS #

Purity Stressed

Unstressed

Gravimetric µg/mL+/- 5.9248

+/- 44.9443 µg/mL +/- 49.8679 µg/mL

(Lot MKCG6676)

Page 1524 of 15442

99%

8 µg/mL 1,003.5Anthracene

120-12-7CAS #

Purity Stressed

Unstressed

Gravimetric µg/mL+/- 5.8891

+/- 45.2053 µg/mL +/- 50.1594 µg/mL

(Lot MKCG5026)

98%

9 µg/mL 996.2Fluoranthene

206-44-0CAS #

Purity Stressed

Unstressed

Gravimetric µg/mL+/- 5.8461

+/- 44.8751 µg/mL +/- 49.7930 µg/mL

(Lot MKBQ6360V)

99%

10 µg/mL 1,001.5Pyrene

129-00-0CAS #

Purity Stressed

Unstressed

Gravimetric µg/mL+/- 5.8774

+/- 45.1152 µg/mL +/- 50.0595 µg/mL

(Lot BCBW7698)

96%

11 µg/mL 997.9Benz(a)anthracene

56-55-3CAS #

Purity Stressed

Unstressed

Gravimetric µg/mL+/- 5.8564

+/- 44.9540 µg/mL +/- 49.8805 µg/mL

(Lot 0022018)

99%

12 µg/mL 1,008.5Chrysene

218-01-9CAS #

Purity Stressed

Unstressed

Gravimetric µg/mL+/- 5.9184

+/- 45.4306 µg/mL +/- 50.4093 µg/mL

(Lot 012015)

97%

13 µg/mL 1,009.3Benzo(b)fluoranthene

205-99-2CAS #

Purity Stressed

Unstressed

Gravimetric µg/mL+/- 5.9230

+/- 45.4659 µg/mL +/- 50.4486 µg/mL

(Lot 012012B)

99%

14 µg/mL 1,004.0Benzo(k)fluoranthene

207-08-9CAS #

Purity Stressed

Unstressed

Gravimetric µg/mL+/- 5.8920

+/- 45.2279 µg/mL +/- 50.1844 µg/mL

(Lot 012017K)

99%

15 µg/mL 1,001.5Benzo(a)pyrene

50-32-8CAS #

Purity Stressed

Unstressed

Gravimetric µg/mL+/- 5.8774

+/- 45.1152 µg/mL +/- 50.0595 µg/mL

(Lot 6-SCZ-51-1)

99%

16 µg/mL 1,007.5Indeno(1,2,3-cd)pyrene

193-39-5CAS #

Purity Stressed

Unstressed

Gravimetric µg/mL+/- 5.9126

+/- 45.3855 µg/mL +/- 50.3594 µg/mL

(Lot ER082107-02)

99%

17 µg/mL 999.0Dibenz(a,h)anthracene

53-70-3CAS #

Purity Stressed

Unstressed

Gravimetric µg/mL+/- 5.9338

+/- 45.0119 µg/mL +/- 49.9429 µg/mL

(Lot ER032211-01)

99%

18 µg/mL 1,002.5Benzo(g,h,i)perylene

191-24-2CAS #

Purity Stressed

Unstressed

Gravimetric µg/mL+/- 5.8832

+/- 45.1603 µg/mL +/- 50.1094 µg/mL

(Lot TBJ4J)

Solvent: Methylene chloride

99%

75-09-2CAS #

Purity

Page 1525 of 15442

Inj. Temp:

Det. Type:

Det. Temp:

30m x 0.25mm x 0.25µm

Rtx-5 (cat.#10223)

Column:

hydrogen-constant pressure 10 psi.

100°C (hold 1 min.) to 330°C

@ 4°C/min. (hold 5 min.)

250°C

330°C

FID

B345965662Balance:

03-Jan-2020Date Passed:

Manufactured under Restek's ISO 9001:2015

Registered Quality System

Certificate #FM 80397

02-Jan-2020Date Mixed:

This chromatogram represents a general set of testing conditions chosen for product acceptance. For optimal results in your lab, conditions should be adjusted for your specific instrument, method, and application.

Page 1526 of 15442

10°C or colder (Refrigerate)

0°C or colder (Freezer)

≥ 60°C up to 7 days

≥ 40°C up to 7 days

≥ 25°C up to 7 days

General Certified Reference Material Notes

Expiration Notes:

· Expiration date valid for unopened ampul stored in compliance with the recommended conditions.

· Uncertainty, concentration, and expiration of the CRM are based on the unopened product being stored according to the recommended condition found in the storage field.

Purity Notes:

· Purity and/or chemical identity are determined by one or more of the following techniques: GC/FID, HPLC, GC/µECD, GC/MS, LC/MS, RI, and/or melting point.

· Compounds with a listed purity of less than 99% have been weight corrected to compensate for impurities and/or salts. A correction factor is used to calculate the amount of compound necessary to achieve the desired concentration of the parent compound in solution.

· Purity of isomeric compounds is reported as the sum of the isomers.

· Purity values are rounded to the nearest whole number.

Certified Uncertainty Value Notes:

· The uncertainties are determined in accordance with ISO 17034 and Guide 35. The certified combined stressed uncertainty value ( includes gravimetric uncertainty, homogeneity between-ampul uncertainty, storage stability uncertainty and shipping stability uncertainty and were combined using the following formula:

k is a coverage factor of 2, which gives a level of confidence of approximately 95%.

· It is important to note that the shipping stability uncertainty was obtained under temperature extremes for specific time intervals; therefore, the certified combined stressed uncertainty value should only be applied to the product if it was stored at non-standard temperature conditions up to and including 7 days. Contact Restek Technical Service at www.restek.com/Contact-Us for use recommendations if your shipment was in-transit for more than 7 days at non-standard temperature conditions.

· Apply the certified combined unstressed uncertainty value if the product was received under standard shipping conditions. Apply the certified combined stressed uncertainty value if the product was received under non-standard conditions as specified below.

Standard Conditions

< 60°C

< 40°C

< 25°C

· Separate (not combined) uncertainty values for gravimetric uncertainty are also displayed on the certificate, if needed, separate homogeneity between-ampul uncertainty, storage stability uncertainty and shipping stability uncertainty values are available by contacting Restek Technical Service at www.restek.com/Contact-Us.

· The packaged amount is the minimum sample size for which uncertainty is valid. The ampules are over-filled to ensure that the minimum packaged amount can be sufficiently transferred .

Manufacturing Notes:

· Concentration is based upon gravimetric preparation using either a balance whose calibration has been verified daily using NIST traceable weights, and/or dilutions with Class A glassware.

Handling Notes:

· Stability of the unopened product, when stored in compliance with the recommended conditions, is guaranteed through the expiration displayed on the product label and certificate. Contact Restek for additional opened product stability information, with the knowledge/understanding that open product stability is subject to the specific handling and environmental conditions to which the product is exposed. For your convenience Restek supplies deactivated vials with most standards packed in 2mL ampules. Larger volume deactivated vials are available through Restek as a custom ordered item. Additionally, Restek sells DMDCS for the purpose of glassware deactivation as catalog number 31861, which includes complete instructions.

· If any undissolved material is visible inside the ampul, sonicate the unopened ampul until the material is completely dissolved.

Page 1527 of 15442

TBA AB_00007

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Vinyl Acetate_00098

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Vinyl Acetate_00101

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Vinyl Acetate_00102

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VMC21SU_00011

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HRM_1613STK_00028

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HRM_1613STK_00030

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HRM_1613STKSS_00009

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HRM_DFLCSC_00111

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HRM_MDD1234_00013

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HRM_MDD123468_00013

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HRM_TDTFWD_00036

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HRM_TDTFWD_00037

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MT_1KV_PIV_00008

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MT_H2O2_Baker_00004

Page 1628 of 15442

Hydrogen Peroxide, 30%

ULTREX® II Ultrapure Reagent

Material No.: 5155-01 Batch No.: 24I2461017

Certificate of Analysis

Retest Date:2031-04-23 Manufactured Date: 2024-04-24

Revision No.: 0

ResultTest Specification Assay (H₂O₂) 25.0 - 35.0 % 31.0 %

Appearance Passes Test Passes Test

Free Acid (µeq/g) <= 0.5 0.1

Chloride (Cl) <= 1 ppm <1 ppm

Nitrate (NO₃) <= 2 ppm <1 ppm

Phosphate (PO₄) <= 2 ppm <1 ppm

ACS - Sulfate (SO₄) <= 5 ppm <2 ppm

Trace Impurities - Aluminum (Al) <= 100 ppt 5 ppt

Trace Impurities - Antimony (Sb) <= 1000 ppt <5 ppt

Trace Impurities - Arsenic (As) <= 1000 ppt <5 ppt

Trace Impurities - Barium (Ba) <= 50 ppt <5 ppt

Trace Impurities - Beryllium (Be) <= 1000 ppt <5 ppt

Trace Impurities - Bismuth (Bi) <= 1000 ppt <5 ppt

Trace Impurities - Boron (B) <= 1000 ppt <100 ppt

Trace Impurities - Cadmium (Cd) <= 50 ppt <5 ppt

Trace Impurities - Calcium (Ca) <= 100 ppt <50 ppt

Trace Impurities - Chromium (Cr) <= 50 ppt <5 ppt

Trace Impurities - Cobalt (Co) <= 50 ppt <5 ppt

Trace Impurities - Copper (Cu) <= 50 ppt <5 ppt

Trace Impurities - Gallium (Ga) <= 1000 ppt <5 ppt

Trace Impurities - Iron (Fe) <= 100 ppt <50 ppt

Trace Impurities - Lead (Pb) <= 100 ppt <5 ppt

Trace Impurities - Lithium (Li) <= 50 ppt <5 ppt

Trace Impurities - Magnesium (Mg) <= 50 ppt <5 ppt

Trace Impurities - Manganese (Mn) <= 50 ppt <5 ppt

Trace Impurities - Mercury (Hg) <= 1000 ppt <100 ppt

Trace Impurities - Molybdenum (Mo) <= 1000 ppt <5 ppt

Trace Impurities - Nickel (Ni) <= 50 ppt <5 ppt

Page 21 of

For questions on this Certificate of Analysis please contact Technical Services at 855.282.6867 or +1.610.386.1700

Avantor Performance Materials,LLC

100 Matsonford Rd, Suite 200,Radnor,PA,19087.U.S.A.Phone 610.386.1700

Page 1629 of 15442

Hydrogen Peroxide, 30%

ULTREX® II Ultrapure Reagent

Material No.: 5155-01 Batch No.: 24I2461017

ResultTest Specification Trace Impurities - Potassium (K) <= 100 ppt <50 ppt

Trace Impurities - Silicon (Si) <= 5000 ppt <5000 ppt

Trace Impurities - Silver (Ag) <= 50 ppt <5 ppt

Trace Impurities - Sodium (Na) <= 100 ppt <50 ppt

Trace Impurities - Strontium (Sr) <= 50 ppt <5 ppt

Trace Impurities - Tin (Sn) <= 50 ppt <5 ppt

Trace Impurities - Titanium (Ti) <= 1000 ppt <5 ppt

Trace Impurities - Vanadium (V) <= 1000 ppt <5 ppt

Trace Impurities - Zinc (Zn) <= 50 ppt <5 ppt

Trace Impurities - Zirconium (Zr) <= 1000 ppt <5 ppt

Certificate Provided Reports Actual Lot Analysis

For Laboratory,Research,or Manufacturing Use

Country of Origin: United States Packaging Site: Paris Mfg Ctr & DC

100 Matsonford Rd, Suite 200,Radnor,PA,19087.U.S.A.Phone 610.386.1700

Avantor Performance Materials,LLC

For questions on this Certificate of Analysis please contact Technical Services at 855.282.6867 or +1.610.386.1700

Page 2 of 2Page 1630 of 15442

MT_H3NO_Fishe_00061

Page 1631 of 15442

Certificate of Analysis 1 Reagent Lane Fair Lawn, NJ 07410

201.796.7100 tel

201.796.1329 fax

Thermo Fisher Scientific's Quality System has been found to conform to Quality Management System Standard ISO9001:2015 by SAI Global Certificate Number CERT – 0120633

Certificate of Analysis

This is to certify that units of the lot number below were tested and found to comply with the specifications of the grade listed. Certain data have been supplied by third parties. Thermo Fisher Scientific expressly disclaims all warranties, expressed or implied, including the implied warranties of merchantability and fitness for a particular purpose. Products are for research use or further manufacturing. Not for direct administration to humans or animals. It is the responsibility of the final formulator and end user to determine suitability based upon the intended use of the end product. Products are tested to meet the analytical requirements of the noted grade. The following information is the actual analytical results obtained.

Catalog Number H330 Quality Test / Release Date 08/21/2024

Lot Number 243373

Description HYDROXYLAMINE HYDROCHLORIDE, A.C.S.

Country of Origin India Suggested Retest Date Feb/2027

Result Name Specifications Test ValueUnits

N/A

Colorless to white crystalsAPPEARANCE REPORT

AMMONIUM (NH4) PASS/FAIL = PASS TEST PASS TEST

ASSAY % >= 96 98.6

CLARITY OF ALCOHOL SOLUTION PASS/FAIL = PASS TEST PASS TEST

HEAVY METALS BY ICP-OES ppm <= 5 <5

IDENTIFICATION PASS/FAIL = PASS TEST PASS TEST

IGNITION RESIDUE % <= 0.05 0.03

IRON (Fe) ppm <= 5 <5

MERCURY (Hg) ppm <= 0.05 <0.05

SULFUR COMPOUNDS % <= 0.005 <0.005

TITRATABLE FREE ACID MEQ/G <= 0.25 <0.25

Harout Sahagian - Quality Control Manager - Fair Lawn

Note: The data listed is valid for all package sizes of this lot of this product, expressed as an extension of this catalog number listed above.

If there are any questions with this certificate, please call at (800) 227-6701.

*Based on suggested storage condition.

Page 1632 of 15442

MT_HCl_JT_00017

Page 1633 of 15442

Test Specification Result

Certificate of Analysis

For questions on this Certificate of Analysis please contact Technical Services at 855.282.6867 or +1.610.386.1700

Avantor Performance Materials, LLC

100 Matsonford Rd, Suite 200, Radnor, PA 19087. U.S.A. Phone 610.386.1700

Material No.: 9530-33 Batch No.: 24D1562005

Manufactured Date: 2024-03-18 Retest Date: 2029-03-17

Revision No.: 0

ACS - Assay (as HCl) (by acid-base titrn) 36.5 - 38.0 % 37.6 %

ACS - Color (APHA) ≤ 10 5

ACS - Residue after Ignition ≤ 3 ppm < 1 ppm

ACS - Specific Gravity at 60°/60°F 1.185 - 1.192 1.192

ACS - Bromide (Br) ≤ 0.005 % < 0.005 %

ACS - Extractable Organic Substances ≤ 5 ppm < 1 ppm

ACS - Free Chlorine (as Cl₂) ≤ 0.5 ppm < 0.5 ppm

Phosphate (PO₄) ≤ 0.05 ppm 0.03 ppm

Sulfate (SO₄) ≤ 0.5 ppm < 0.3 ppm

Sulfite (SO₃) ≤ 0.8 ppm 0.3 ppm

Ammonium (NH₄) ≤ 3 ppm < 1 ppm

Trace Impurities - Arsenic (As) ≤ 0.010 ppm < 0.003 ppm

Trace Impurities - Aluminum (Al) ≤ 10.0 ppb < 5.0 ppb

Arsenic and Antimony (as As) ≤ 5.0 ppb < 3.0 ppb

Trace Impurities - Barium (Ba) ≤ 1.0 ppb < 1.0 ppb

Trace Impurities - Beryllium (Be) ≤ 1.0 ppb < 1.0 ppb

Trace Impurities - Bismuth (Bi) ≤ 10.0 ppb < 10.0 ppb

Trace Impurities - Boron (B) ≤ 20.0 ppb 2.2 ppb

Trace Impurities - Cadmium (Cd) ≤ 1.0 ppb < 1.0 ppb

Trace Impurities - Calcium (Ca) ≤ 50.0 ppb 31.0 ppb

Trace Impurities - Chromium (Cr) ≤ 1.0 ppb 0.5 ppb

Trace Impurities - Cobalt (Co) ≤ 1.0 ppb 0.2 ppb

Trace Impurities - Copper (Cu) ≤ 1.0 ppb < 0.1 ppb

Trace Impurities - Gallium (Ga) ≤ 1.0 ppb < 0.2 ppb

Trace Impurities - Germanium (Ge) ≤ 3.0 ppb < 2.0 ppb

Trace Impurities - Gold (Au) ≤ 4.0 ppb < 0.2 ppb

Heavy Metals (as Pb) ≤ 100 ppb < 50 ppb

Trace Impurities - Iron (Fe) ≤ 15 ppb 3 ppb

>>> Continued on page 2 >>>

Hydrochloric Acid, 36.5-38.0%

BAKER INSTRA-ANALYZED® Reagent

For Trace Metal Analysis

Page 1634 of 15442

Material No.: 9530-33 Batch No.: 24D1562005

Test Specification Result

For questions on this Certificate of Analysis please contact Technical Services at 855.282.6867 or +1.610.386.1700

Avantor Performance Materials, LLC

100 Matsonford Rd, Suite 200, Radnor, PA 19087. U.S.A. Phone 610.386.1700

Trace Impurities - Magnesium (Mg) ≤ 10.0 ppb 2.2 ppb

Trace Impurities - Manganese (Mn) ≤ 1.0 ppb < 0.2 ppb

Trace Impurities - Mercury (Hg) ≤ 0.5 ppb

< 5.0 ppbTrace Impurities - Molybdenum (Mo) ≤ 10.0 ppb

0.2 ppbTrace Impurities - Nickel (Ni) ≤ 4.0 ppb

< 0.2 ppbTrace Impurities - Niobium (Nb) ≤ 1.0 ppb

< 1.0 ppbTrace Impurities - Potassium (K) ≤ 9.0 ppb

< 1.0 ppbTrace Impurities - Selenium (Se), For Information Only

< 0.1 ppb

Trace Impurities - Silicon (Si) ≤ 100.0 ppb < 10.0 ppb

Trace Impurities - Silver (Ag) ≤ 1.0 ppb < 0.3 ppb

Trace Impurities - Sodium (Na) ≤ 100.0 ppb 2.0 ppb

Trace Impurities - Strontium (Sr) ≤ 1.0 ppb < 0.2 ppb

Trace Impurities - Tantalum (Ta) ≤ 1.0 ppb < 0.9 ppb

Trace Impurities - Thallium (Tl) ≤ 5.0 ppb < 2.0 ppb

Trace Impurities - Tin (Sn) ≤ 5.0 ppb < 0.4 ppb

Trace Impurities - Titanium (Ti) ≤ 1.0 ppb 0.2 ppb

Trace Impurities - Vanadium (V) ≤ 1.0 ppb < 0.2 ppb

Trace Impurities - Zinc (Zn) ≤ 5.0 ppb < 0.2 ppb

Trace Impurities - Zirconium (Zr) ≤ 1.0 ppb < 0.1 ppb

Trace Impurities - Lead (Pb) ≤ 1.0 ppb < 0.2 ppb

Trace Impurities - Lithium (Li) ≤ 1.0 ppb < 0.1 ppb

>>> Continued on page 3 >>>

Hydrochloric Acid, 36.5-38.0%

BAKER INSTRA-ANALYZED® Reagent

Page 2 of 3Page 1635 of 15442

Batch No.: 24D1562005

For questions on this Certificate of Analysis please contact Technical Services at 855.282.6867 or +1.610.386.1700

Avantor Performance Materials, LLC

100 Matsonford Rd, Suite 200, Radnor, PA 19087. U.S.A. Phone 610.386.1700

Test Specification Result

Hydrochloric Acid, 36.5-38.0%

BAKER INSTRA-ANALYZED® Reagent

For Trace Metal Analysis

For Laboratory,Research,or Manufacturing Use Product Information (not specifications):

Appearance (clear, fuming liquid) Meets ACS Specifications Storage Condition: Store below 25 °C.

Country of Origin: USA Packaging Site: Phillipsburg Mfg Ctr & DC

Page 1636 of 15442

MT_HCl_JT_00018

Page 1637 of 15442

Certificate of Analysis

For questions on this Certificate of Analysis please contact Technical Services at 855.282.6867 or +1.610.386.1700

Avantor Performance Materials, LLC

100 Matsonford Rd, Suite 200, Radnor, PA 19087. U.S.A. Phone 610.386.1700

Material No.: 9530-33 Batch No.: 24H1262004

Manufactured Date: 2024-07-19 Retest Date: 2029-07-18

Revision No.: 0

ACS - Assay (as HCl) (by acid-base titrn) 36.5 - 38.0 % 37.7 %

ACS - Color (APHA) ≤ 10 5

ACS - Residue after Ignition ≤ 3 ppm < 1 ppm

ACS - Specific Gravity at 60°/60°F 1.185 - 1.192 1.192

ACS - Bromide (Br) ≤ 0.005 % < 0.005 %

ACS - Extractable Organic Substances ≤ 5 ppm < 1 ppm

ACS - Free Chlorine (as Cl₂) ≤ 0.5 ppm < 0.5 ppm

Phosphate (PO₄) ≤ 0.05 ppm < 0.03 ppm

Sulfate (SO₄) ≤ 0.5 ppm < 0.3 ppm

Sulfite (SO₃) ≤ 0.8 ppm 0.3 ppm

Ammonium (NH₄) ≤ 3 ppm < 1 ppm

Trace Impurities - Arsenic (As) ≤ 0.010 ppm < 0.003 ppm

Trace Impurities - Aluminum (Al) ≤ 10.0 ppb 0.4 ppb

Arsenic and Antimony (as As) ≤ 5.0 ppb < 3.0 ppb

Trace Impurities - Barium (Ba) ≤ 1.0 ppb < 0.2 ppb

Trace Impurities - Beryllium (Be) ≤ 1.0 ppb < 0.2 ppb

Trace Impurities - Bismuth (Bi) ≤ 10.0 ppb < 1.0 ppb

Trace Impurities - Boron (B) ≤ 20.0 ppb 2.8 ppb

Trace Impurities - Cadmium (Cd) ≤ 1.0 ppb < 0.3 ppb

Trace Impurities - Calcium (Ca) ≤ 50.0 ppb 43.0 ppb

Trace Impurities - Chromium (Cr) ≤ 1.0 ppb < 0.4 ppb

Trace Impurities - Cobalt (Co) ≤ 1.0 ppb < 0.3 ppb

Trace Impurities - Copper (Cu) ≤ 1.0 ppb < 0.1 ppb

Trace Impurities - Gallium (Ga) ≤ 1.0 ppb < 0.2 ppb

Trace Impurities - Germanium (Ge) ≤ 3.0 ppb < 2.0 ppb

Trace Impurities - Gold (Au) ≤ 4.0 ppb < 0.2 ppb

Heavy Metals (as Pb) ≤ 100 ppb < 50 ppb

Trace Impurities - Iron (Fe) ≤ 15 ppb < 1 ppb

>>> Continued on page 2 >>>

Hydrochloric Acid, 36.5-38.0%

BAKER INSTRA-ANALYZED® Reagent

Page 1638 of 15442

Batch No.: 24H1262004

Test Specification Result

For questions on this Certificate of Analysis please contact Technical Services at 855.282.6867 or +1.610.386.1700

Avantor Performance Materials, LLC

100 Matsonford Rd, Suite 200, Radnor, PA 19087. U.S.A. Phone 610.386.1700

Trace Impurities - Magnesium (Mg) ≤ 10.0 ppb 1.1 ppb

Trace Impurities - Manganese (Mn) ≤ 1.0 ppb < 0.4 ppb

Trace Impurities - Mercury (Hg) ≤ 0.5 ppb

< 3.0 ppbTrace Impurities - Molybdenum (Mo) ≤ 10.0 ppb

< 0.3 ppbTrace Impurities - Nickel (Ni) ≤ 4.0 ppb

0.2 ppbTrace Impurities - Niobium (Nb) ≤ 1.0 ppb

< 2.0 ppbTrace Impurities - Potassium (K) ≤ 9.0 ppb

< 1.0 ppbTrace Impurities - Selenium (Se), For Information Only

0.1 ppb

Trace Impurities - Silicon (Si) ≤ 100.0 ppb 0.7 ppb

Trace Impurities - Silver (Ag) ≤ 1.0 ppb < 0.3 ppb

Trace Impurities - Sodium (Na) ≤ 100.0 ppb 1.3 ppb

Trace Impurities - Strontium (Sr) ≤ 1.0 ppb < 0.2 ppb

Trace Impurities - Tantalum (Ta) ≤ 1.0 ppb < 0.9 ppb

Trace Impurities - Thallium (Tl) ≤ 5.0 ppb < 2.0 ppb

Trace Impurities - Tin (Sn) ≤ 5.0 ppb < 0.8 ppb

Trace Impurities - Titanium (Ti) ≤ 1.0 ppb 1.0 ppb

Trace Impurities - Vanadium (V) ≤ 1.0 ppb < 0.2 ppb

Trace Impurities - Zinc (Zn) ≤ 5.0 ppb < 0.3 ppb

Trace Impurities - Zirconium (Zr) ≤ 1.0 ppb 0.4 ppb

Trace Impurities - Lead (Pb) ≤ 1.0 ppb < 0.5 ppb

Trace Impurities - Lithium (Li) ≤ 1.0 ppb < 0.2 ppb

>>> Continued on page 3 >>>

Hydrochloric Acid, 36.5-38.0%

BAKER INSTRA-ANALYZED® Reagent

Page 2 of 3Page 1639 of 15442

Batch No.: 24H1262004

For questions on this Certificate of Analysis please contact Technical Services at 855.282.6867 or +1.610.386.1700

Avantor Performance Materials, LLC

100 Matsonford Rd, Suite 200, Radnor, PA 19087. U.S.A. Phone 610.386.1700

Test Specification Result

Hydrochloric Acid, 36.5-38.0%

BAKER INSTRA-ANALYZED® Reagent

For Trace Metal Analysis

For Laboratory,Research,or Manufacturing Use Product Information (not specifications):

Appearance (clear, fuming liquid) Meets ACS Specifications Storage Condition: Store below 25 °C.

Country of Origin: USA Packaging Site: Phillipsburg Mfg Ctr & DC

Page 1640 of 15442

MT_HNO3_FI_00015

Page 1641 of 15442

1 Reagent Lane Fair Lawn, NJ 07410

201.796.7100 tel

201.796.1329 fax

Thermo Fisher Scientific's Quality System has been found to conform to Quality Management System Standard ISO9001:2015 by SAI Global Certificate Number CERT – 0120633

Certificate of Analysis

This is to certify that units of the lot number below were tested and found to comply with the specifications of the grade listed. Certain data have been supplied by third parties. Thermo Fisher Scientific expressly disclaims all warranties, expressed or implied, including the implied warranties of merchantability and fitness for a particular purpose. Products are for research use or further manufacturing. Not for direct administration to humans or animals. It is the responsibility of the final formulator and end user to determine suitability based upon the intended use of the end product. Products are tested to meet the analytical requirements of the noted grade. The following information is the actual analytical results obtained.

Catalog Number A200 Quality Test / Release Date 05/13/2024

Lot Number 241938

Description NITRIC ACID, CERTIFIED ACS

Country of Origin Canada Suggested Retest Date May/2029

Chemical Origin Inorganic-non animal

BSE/TSE Comment No animal products are used as starting raw material ingredients, or used in processing, including lubricants, processing aids, or any other material that might migrate to the finished product.

Result Name Specifications Test ValueUnits

N/A

Clear, colorless free from suspended matter

APPEARANCE REPORT

ALUMINUM ppm <= 0.2 <0.2

ARSENIC (As) ppm <= 0.004 <0.004

ASSAY w/w % Inclusive Between 68.0 - 70.0 69.4

BORON (B) ppm <= 0.1 <0.1

CALCIUM (Ca) ppm <= 0.2 <0.2

CHLORIDE ppm <= 0.08 <0.08

CHROMIUM (Cr) ppm <= 0.1 <0.1

COLOR APHA <= 10 <10

COPPER (Cu) ppm <= 0.05 <0.05

GOLD (Au) ppm <= 0.3 <0.3

HEAVY METALS (as Pb) ppm <= 0.2 <0.2

IDENTIFICATION PASS/FAIL = PASS TEST PASS TEST

IRON (Fe) ppm <= 0.2 <0.2

LEAD (Pb) ppm <= 0.1 <0.1

MAGNESIUM (Mg) ppm <= 0.3 <0.3

NICKEL (Ni) ppm <= 0.05 <0.05

PHOSPHATE (PO4) ppm <= 0.2 <0.2

POTASSIUM (K) ppm <= 0.3 <0.3

RESIDUE AFTER IGNITION ppm <= 2 <2

SODIUM (Na) ppm <= 0.3 <0.3

SULFATE (SO4) ppm <= 0.5 <0.5

TIN (Sn) ppm <= 0.3 <0.3

TITANIUM (Ti) ppm <= 0.3 <0.3

Note: The data listed is valid for all package sizes of this lot of this product, expressed as an extension of this catalog number listed above.

If there are any questions with this certificate, please call at (800) 227-6701.

Page 1642 of 15442

1 Reagent Lane Fair Lawn, NJ 07410

201.796.7100 tel

201.796.1329 fax

Thermo Fisher Scientific's Quality System has been found to conform to Quality Management System Standard ISO9001:2015 by SAI Global Certificate Number CERT – 0120633

Certificate of Analysis

ZINC (Zn) ppm <= 0.3 <0.3

Kalyan Paruchuri - Quality Control Supervisor - Bridgewater

Note: The data listed is valid for all package sizes of this lot of this product, expressed as an extension of this catalog number listed above.

If there are any questions with this certificate,…