A18_Rpt_WO_12061908_ver_1_000.pdf

Certificate of Analysis No.: 12061908

Clean Venture - Bethesda

Project Manager: Harvey Neuman Project Name : Vault + Transformer

June 26, 2012

6630 Baltimore National Pike Baltimore, MD 21228

Phone: (410) 747-8770 Fax: (410) 788-8723

Analytical Report for

Project Location: Bldg 10, Vault 11 Feeder 80 Transformer

Phase Separation Science, Inc.

Page 1 of 9 Final 1.000. WO#: 12061908

OFFICES:

6630 BALTIMORE NATIONAL PIKE

ROUTE 40 WEST

BALTIMORE, MD 21228

410-747-8770 800-932-9047

FAX 410-788-8723

PHASE

SEPARATION

SCIENCE,

INC.

Harvey Neuman Clean Venture - Bethesda 9000 Rockville Pk. Bldg 21 1N-102 Bethesda, MD 20892

Reference: PSS Work Order No: 12061908 Project Name: Vault + Transformer Project Location: Bldg 10, Vault 11 Feeder 80 Transformer

Dear Harvey Neuman :

This report includes the analytical results from the analyses performed on the samples received under the project name referenced above and identified with the Phase Separation Science (PSS) Work Order numbered 12061908.

All work reported herein has been performed in accordance with current NELAP standards, referenced methodologies, PSS Standard Operating Procedures and the PSS Quality Assurance Manual unless otherwise noted in the Case Narrative Summary. PSS is limited in liability to the actual cost of the sample analysis done.

PSS reserves the right to return any unused samples, extracts or related solutions. Otherwise, the samples are scheduled for disposal, without any further notice, on July 24, 2012. This includes any samples that were received with a request to be held but lacked a specific hold period. It is your responsibility to provide a written request defining a specific disposal date if additional storage is required. Upon receipt , the request will be acknowledged by PSS, thus extending the storage period.

This report shall not be reproduced except in full, without the written approval of an authorized PSS representative. A copy of this report will be retained by PSS for at least 5 years, after which time it will be disposed of without further notice, unless prior arrangements have been made.

We thank you for selecting Phase Separation Science, Inc. to serve your analytical needs. If you have any questions concerning this report, do not hesitate to contact us at 410-747-8770 or info@phaseonline.com.

June 26, 2012

Dan Prucnal Laboratory Manager

Page 2 of 9 Final 1.000. WO#: 12061908

Sample Summary

Client Name: Clean Venture - Bethesda Project Name: Vault + Transformer

Sample Id 14348 Bldg 10 Vault 11 14350 Bldg 10 Vault 11

06/15/2012 08:15 06/15/2012 08:15

Date/Time Collected Lab Sample Id 12061908-001 12061908-002

OIL

OIL

Matrix

Standard Flags/Abbreviations:

B A target analyte or common laboratory contaminant was identified in the method blank. Its presence indicates possible field or laboratory contamination.

C Results Pending Final Confirmation.

E The data exceeds the upper calibration limit; therefore, the concentration is reported as estimated.

Fail The result exceeds the regulatory level for Toxicity Characteristic (TCLP) as cited in 40 CFR 261.24 Table 1.

J The target analyte was positively identified below the reporting limit but greater than the LOD.

LOD Limit of Detection. An estimate of the minimum amount of a substance that an analytical process can reliably detect.

An LOD is analyte and matrix specific.

ND Not Detected at or above the reporting limit.

RL PSS Reporting Limit.

U Not detected.

Please reference the Chain of Custody and Sample Receipt Checklist for specific container counts and preservatives. Any sample conditions not in compliance with sample acceptance criteria are described in Case Narrative Summary.

Notes:

1. The presence of common laboratory contaminants such as acetone, methylene chloride and phthalates, may be considered a possible laboratory artifact. Where observed, appropriate consideration of data should be taken.

2. The following analytical results are never reported on a dry weight basis: pH, flashpoint, moisture and paint filter test.

3. Drinking water samples collected for the purpose of compliance with SDWA may not be suitable for their intended use unless collected by a certified sampler [COMAR 26.08.05.07.C.2].

Project ID: N/A 12061908Work Order Number:

The following samples were received under chain of custody by Phase Separation Science (PSS) on 06/19/2012 at 11:26 am

Page 3 of 9 Final 1.000. WO#: 12061908

Case Narrative Summary

12061908Work Order Number:N/AProject ID:

Project Name: Vault + Transformer

Client Name: Clean Venture - Bethesda

All sample receipt conditions were acceptable.

Sample Receipt:

NELAP accreditation was held for all analyses performed unless noted below. See www.phaseonline.com for complete PSS scope of accreditation.

Any holding time exceedances, deviations from the method specifications, regulatory requirements or variations to the procedures outlined in the PSS Quality Assurance Manual are outlined below.

Page 4 of 9 Final 1.000. WO#: 12061908

No: 12061908 Clean Venture - Bethesda, Bethesda, MD June 26, 2012

CERTIFICATE OF ANALYSIS

PHASE

SEPARATION

SCIENCE,

INC.

OFFICES:

6630 BALTIMORE NATIONAL PIKE

ROUTE 40 WEST

BALTIMORE, MD 21228

410-747-8770 800-932-9047

FAX 410-788-8723

Project Name: Vault + Transformer Project Location: Bldg 10, Vault 11 Feeder 80 Transformer

06/19/2012 11:26

06/19/2012 11:26

Date/Time Received:

Date/Time Received:

06/15/2012 08:15

06/15/2012 08:15

Date/Time Sampled:

Date/Time Sampled:

12061908-001

12061908-002

PSS Sample ID:

PSS Sample ID:

OIL

OIL

Matrix:

Matrix:

14348 Bldg 10 Vault 11

14350 Bldg 10 Vault 11

Sample ID:

Sample ID:

Polychlorinated Biphenyls

Polychlorinated Biphenyls

Analytical Method:

Analytical Method:

06/20/12 15:17

06/20/12 15:17

06/20/12 15:17

06/20/12 15:17

06/20/12 15:17

06/20/12 15:17

06/20/12 15:17

06/20/12 15:46

06/20/12 15:46

06/20/12 15:46

06/20/12 15:46

06/20/12 15:46

06/20/12 15:46

06/20/12 15:46

3580A

3580A

Preparation Method:

Preparation Method:

06/20/12

06/20/12

06/20/12

06/20/12

06/20/12

06/20/12

06/20/12

06/20/12

06/20/12

06/20/12

06/20/12

06/20/12

06/20/12

06/20/12

PCB-1016

PCB-1221

PCB-1232

PCB-1242

PCB-1248

PCB-1254

PCB-1260

PCB-1016

PCB-1221

PCB-1232

PCB-1242

PCB-1248

PCB-1254

PCB-1260

Result

Result

0.98

0.98

0.98

0.98

0.98

0.98

0.98

0.98

0.98

0.98

0.98

0.98

0.98

0.98

Flag

Flag mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg

Units

Units

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

SW-846 8082 A

SW-846 8082 A

Analyst

Analyst

Prepared

Prepared

Analyzed

Analyzed

Clean up Method: SW846 3665A

Clean up Method: SW846 3665A

Dil

Dil

RL

RL

Page 5 of 9 Final 1.000. WO#: 12061908 b

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L# Page 6 of 9 Final 1.000. WO#: 12061908

SAMPLE DESCRIPTION AND CUSTODY RECORD

NIH SampleN,: t435o

Attachment 8 Page 1 of I

Drum No:

ProfileNo. (where applicable): 6NIH-

Process Generating Waste:

l,abel Information:

Sa:rple Volume: Sample Method Sampletyp.r 6t(

Collection Site (specifi c) :

Description, color,ttl# uyot/Uvt^'Qz consistency €('J

Phpical State: Solid % [f() riquiau Semisotd %

Other Information:

a

Expected Chemical Composition:

Solid Phase gamFle Taken By:

Authorization:

Transporterl:

Receiverl:

LiquidPhase . I Crl,rq-r,q Drl bo o^t",d fr1lrc'ri^., ([6 f* our.,Tft f /v,r^", \6,,o ; A^ D^t", (lAl > r-,": t b I t S. 4kt o^t , bf iT'f rt xm., ii Lbku

Transporter2:

Receiver2:

Datq Time:

Date: Time:

(Note:Include

Analyses Requested:

panyrnrne on receiver and transporter line) cg €pt+ (d(z r-. r'ield Results: Flash Point: Exact---__-__--,__ <60F _ 61-100F

141-140F 141-200F_>200F

101-140F

Page 7 of 9 Final 1.000. WO#: 12061908

SAMPLE DESCRIPTION AND CUSTODY RECORD Attachment 8

NIH sampl "*r, /'13 4$

Profiie No. (where applicable): 6NIH--

Process Generating Waste:

l,abel Information:

Drum No:

SampleVolume: 40 tuQ- Sample 76"rao6tC ro.b Sample tW", Ot f

Collection Site (specific):

Description: cotor:d-&uf I-ayer: '' Consistency:

Physical State:

Other Information:

Ifrl i iqsi6Y" _Serrisolid %Sotid %

Expected Chemical Composition:

Solid Phase % Liouid Phase /' Sil,'.o-q 0i I lo'a

Time:

(Note:hrclude conrpany name on receiver and transporter line)

Sample Taken By

Transporterl:

oate'6 ( t5/lz trr,", lOi /S 4,1't r e. l i 'ZL rtq

Dats Time:

Date:_Time:

Analyses Requested:

,- rield Resr"rlts: Flash Point: Exact____-_._ <60F _- 61-100F 101-140F

141-140F 141-200F_>200F pH:-

Page 8 of 9 Final 1.000. WO#: 12061908

Sample Receipt Checklist

Phase Separation Science, Inc

06/26/2012 09:02 AMPrinted:

12061908Work Order #

06/19/2012 11:26:00 AMDate Received

Trans Time ExpressDelivered By

Clean Venture - Bethesda Client Name

N/AProject Number

Vault + TransformerProject Name

Rachel DavisReceived By

Not ApplicableTracking No

Shipping Container(s)

No. of Coolers Ice Temp (deg C) Temp Blank Present

Total No. of Samples Received

Preservation

No

For any improper preservation conditions, list sample ID, preservative added (reagent ID number) below as well as documentation of any client notification as well as client instructions. Samples for pH, chlorine and dissolved oxygen should be analyzed as soon as possible, preferably in the field at the time of sampling. Samples which require thermal preservation shall be considered acceptable when received at a temperature above freezing to 6°C. Samples that are hand delivered on the day that they are collected may not meet these criteria but shall be considered acceptable if there is evidence that the chilling process has begun such as arrival on ice.

Comments: (Any "No" response must be detailed in the comments section below.)

Samples Inspected/Checklist Completed By: Date:

PM Review and Approval: Date:

Logged In By Rachel Davis

Absent

Disposal Date 07/24/2012

Rachel Davis

Simon Crisp

06/19/2012

06/19/2012

Metals Cyanides Sulfide TOC, COD, Phenols TOX, TKN, NH3, Total Phos VOC, BTEX (VOA Vials Rcvd Preserved) Do VOA vials have zero headspace?

(pH<2) (pH>12) (pH>9) (ph<2) (pH<2) (pH<2)

N/A N/A N/A N/A N/A N/A N/A

Appropriate for Specified Analysis?

Intact?

Labeled and Labels Legible?

Yes Yes Yes

Sample Container

COC agrees with sample labels?

Chain of Custody

Yes Yes

Documentation Brian KimSampler Name MD DW Cert. No.

Custody Seal(s) Intact?

Seal(s) Signed / Dated

Total No. of Containers Received 2

Not Applicable

Not Applicable

N/A

Custody Seal(s) Intact?

Seal(s) Signed / Dated?

N/A N/A

Page 9 of 9 Final 1.000. WO#: 12061908