8-PRIVATE WELL SAMPLING - DAVIS.pdf
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- Attached to
- 25B-143 GROUNDWATER SAMPLING AND ANALYSIS
- Solicitation number
- 25B-143
- Issued by
- Marion County, Florida
About this file
The document is a laboratory analytical report from Pace Analytical Services, LLC for water sample testing conducted for the Davis Landfill Pilot Water System (Davis LF PWs) project. The report covers five water samples (DPW-7, DPW-434, DPW-DUP, DPW-435, and a Trip Blank) collected on November 9, 2023, by Aqua Pure W&SS, LLC from various locations. The comprehensive analysis includes testing for multiple parameters such as gross alpha radiation, metals, volatile organic compounds, alkalinity, dissolved solids, chloride, sulfate, ammonia, and nitrate using various Environmental Protection Agency (EPA) and Standard Methods protocols.
The laboratory performed extensive quality control measures, including method blanks, laboratory control samples, matrix spikes, and sample duplicates to ensure data accuracy. The samples were analyzed using multiple techniques like EPA 6010 for metals, EPA 624.1 and 625.1 for volatile organics, SM 7110C-2000 for gross alpha radiation, and other standardized methods. The results were reported with detection limits, uncertainty measurements, and qualifiers to indicate the reliability and precision of each measurement. The testing was conducted across multiple Pace Analytical Services locations, including facilities in Ormond Beach, Charlotte, and Greensburg, and the report was prepared for delivery on December 6, 2023, with a project number of 35840909.
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Text version
#=CL#
December 06, 2023
LIMS USE: FR - LISA SAUPP
LIMS OBJECT ID: 35840909
35840909 Project:
Pace Project No.:
RE:
Lisa Saupp Aqua Pure W&SS, LLC 3855 East Silver Springs Blvd Unit #107 Ocala, FL 34470
Davis LF PWs
Dear Lisa Saupp:
Enclosed are the analytical results for sample(s) received by the laboratory on November 10, 2023. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
• Pace Analytical Services - Ormond Beach
• Pace Analytical Services - Greensburg
If you have any questions concerning this report, please feel free to contact me.
Sincerely, Rossy Guima for jeff.baylor@pacelabs.com
Project Manager
Jeff Baylor
(386)672-5668
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC 8 East Tower Circle
Ormond Beach, FL 32174 (386)672-5668
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
35840909 Davis LF PWs
Pace Analytical Services Pennsylvania 1638 Roseytown Rd Suites 2,3&4, Greensburg, PA 15601 ANAB DOD-ELAP Rad Accreditation #: L2417 ANABISO/IEC 17025:2017 Rad Cert#: L24170 Alabama Certification #: 41590 Arizona Certification #: AZ0734 Arkansas Certification California Certification #: 2950 Colorado Certification #: PA01547 Connecticut Certification #: PH-0694 EPA Region 4 DW Rad Florida/TNI Certification #: E87683 Georgia Certification #: C040 Guam Certification Hawaii Certification Idaho Certification Illinois Certification Indiana Certification Iowa Certification #: 391 Kansas Certification #: E-10358 Kentucky Certification #: KY90133 KY WW Permit #: KY0098221 KY WW Permit #: KY0000221 Louisiana DHH/TNI Certification #: LA010 Louisiana DEQ/TNI Certification #: 04086 Maine Certification #: 2023021 Maryland Certification #: 308 Massachusetts Certification #: M-PA1457 Michigan/PADEP Certification #: 9991
Missouri Certification #: 235 Montana Certification #: Cert0082 Nebraska Certification #: NE-OS-29-14 Nevada Certification #: PA014572023-03 New Hampshire/TNI Certification #: 297622 New Jersey/TNI Certification #: PA051 New Mexico Certification #: PA01457 New York/TNI Certification #: 10888 North Carolina Certification #: 42706 North Dakota Certification #: R-190 Ohio EPA Rad Approval: #41249 Oregon/TNI Certification #: PA200002-015 Pennsylvania/TNI Certification #: 65-00282 Puerto Rico Certification #: PA01457 Rhode Island Certification #: 65-00282 South Dakota Certification Tennessee Certification #: TN02867 Texas/TNI Certification #: T104704188-22-18 Utah/TNI Certification #: PA014572223-14 USDA Soil Permit #: 525-23-67-77263 Vermont Dept. of Health: ID# VT-0282 Virgin Island/PADEP Certification Virginia/VELAP Certification #: 460198 Washington Certification #: C868 West Virginia DEP Certification #: 143 West Virginia DHHR Certification #: 9964C Wisconsin Approve List for Rad
Pace Analytical Services Ormond Beach 8 East Tower Circle, Ormond Beach, FL 32174 Alaska DEC- CS/UST/LUST Alabama Certification #: 41320 Colorado Certification: FL NELAC Reciprocity Connecticut Certification #: PH-0216 Delaware Certification: FL NELAC Reciprocity DoD-ANAB #:ADE-3199 Florida Certification #: E83079 Georgia Certification #: 955 Guam Certification: FL NELAC Reciprocity Hawaii Certification: FL NELAC Reciprocity Illinois Certification #: 200068 Indiana Certification: FL NELAC Reciprocity Kansas Certification #: E-10383 Kentucky Certification #: 90050 Louisiana Certification #: FL NELAC Reciprocity Louisiana Environmental Certificate #: 05007 Maine Certification #: FL01264 Maryland Certification: #346 Massachusetts Certification #: M-FL1264 Michigan Certification #: 9911
Mississippi Certification: FL NELAC Reciprocity Missouri Certification #: 236 Montana Certification #: Cert 0074 Nebraska Certification: NE-OS-28-14 New Hampshire Certification #: 2958 New Jersey Certification #: FL022 New York Certification #: 11608 North Carolina Environmental Certificate #: 667 North Carolina Certification #: 12710 North Dakota Certification #: R-216 Ohio DEP 87780 Oklahoma Certification #: D9947 Pennsylvania Certification #: 68-00547 Puerto Rico Certification #: FL01264 South Carolina Certification: #96042001 Tennessee Certification #: TN02974 Texas Certification: FL NELAC Reciprocity US Virgin Islands Certification: FL NELAC Reciprocity Virginia Environmental Certification #: 460165 West Virginia Certification #: 9962C Wisconsin Certification #: 399079670
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC 8 East Tower Circle
Ormond Beach, FL 32174
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
35840909 Davis LF PWs
Pace Analytical Services Ormond Beach Wyoming (EPA Region 8): FL NELAC Reciprocity
Pace Analytical Services Charlotte South Carolina Laboratory ID: 99006 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001 South Carolina Drinking Water Cert. #: 99006003 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Louisiana DoH Drinking Water #: LA029 Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC 8 East Tower Circle
Ormond Beach, FL 32174
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
35840909 Davis LF PWs
Lab ID Sample ID Matrix Date Collected Date Received
35840909001 DPW-7 Water 11/09/23 10:15 11/10/23 12:22
35840909002 DPW-434 Water 11/09/23 10:55 11/10/23 12:22
35840909003 DPW-DUP Water 11/09/23 10:55 11/10/23 12:22
35840909004 DPW-435 Water 11/09/23 11:35 11/10/23 12:22
35840909005 Trip Blank Water 11/09/23 00:01 11/10/23 12:22
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC 8 East Tower Circle
Ormond Beach, FL 32174
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
35840909 Davis LF PWs
Lab ID Sample ID Method Analytes Reported LaboratoryAnalysts
35840909001 DPW-7 EPA 6010 10 PASI-OAME
EPA 6020 1 PASI-OEAP
EPA 7470 1 PASI-OJNK
EPA 625.1 61 PASI-CPKS
EPA 624.1 34 PASI-OJIF
SM 7110C-2000 1 PASI-PAKET
SM 2320B 1 PASI-OSAH
SM 2540C 1 PASI-OWW1
EPA 300.0 2 PASI-OCMB
EPA 350.1 1 PASI-OCLL
EPA 353.2 1 PASI-OKW1
35840909002 DPW-434 EPA 6010 10 PASI-OTMA
EPA 6020 1 PASI-OEAP
EPA 7470 1 PASI-OJNK
EPA 625.1 61 PASI-CPKS
EPA 624.1 34 PASI-OJIF
SM 7110C-2000 1 PASI-PAKET
SM 2320B 1 PASI-OSAH
SM 2540C 1 PASI-OWW1
EPA 300.0 2 PASI-OCMB
EPA 350.1 1 PASI-OCLL
EPA 353.2 1 PASI-OKW1
35840909003 DPW-DUP EPA 6010 10 PASI-OAME
EPA 6020 1 PASI-OEAP
EPA 7470 1 PASI-OJNK
EPA 625.1 61 PASI-CPKS
EPA 624.1 34 PASI-OJIF
SM 7110C-2000 1 PASI-PAKET
SM 2320B 1 PASI-OSAH
SM 2540C 1 PASI-OWW1
EPA 300.0 2 PASI-OCMB
EPA 350.1 1 PASI-OCLL
EPA 353.2 1 PASI-OKW1
35840909004 DPW-435 EPA 6010 10 PASI-OAME
EPA 6020 1 PASI-OEAP
EPA 7470 1 PASI-OJNK
EPA 625.1 61 PASI-CPKS
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC 8 East Tower Circle
Ormond Beach, FL 32174
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
35840909 Davis LF PWs
Lab ID Sample ID Method Analytes Reported LaboratoryAnalysts
EPA 624.1 34 PASI-OJIF
SM 7110C-2000 1 PASI-PAKET
SM 2320B 1 PASI-OSAH
SM 2540C 1 PASI-OWW1
EPA 300.0 2 PASI-OCMB
EPA 350.1 1 PASI-OCLL
EPA 353.2 1 PASI-OKW1
35840909005 Trip Blank EPA 624.1 34 PASI-OJIF
PASI-C = Pace Analytical Services - Charlotte PASI-O = Pace Analytical Services - Ormond Beach PASI-PA = Pace Analytical Services - Greensburg
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC 8 East Tower Circle
Ormond Beach, FL 32174
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
35840909 Davis LF PWs
Parameters AnalyzedResult Lab Sample ID
Report Limit QualifiersUnitsMethod Client Sample ID
35840909001 DPW-7
Field pH 7.74 Std. Units 11/09/23 10:15 Field Temperature 22.4 deg C 11/09/23 10:15 Field Specific Conductance 251 umhos/cm 11/09/23 10:15 Oxygen, Dissolved 1.61 mg/L 11/09/23 10:15 REDOX 88.00 mV 11/09/23 10:15 Turbidity .10 NTU 11/09/23 10:15 Sodium 55.6 mg/L 11/27/23 01:112.0EPA 6010 Gross Alpha 3.16U ±
1.84 (3.16)
C:NA T:NA
pCi/L 12/05/23 18:28SM 7110C-2000
Alkalinity, Total as CaCO3 111 mg/L 11/18/23 20:525.0SM 2320B Total Dissolved Solids 218 mg/L 11/13/23 21:30 J(D6)5.0SM 2540C Chloride 10.1 mg/L 11/30/23 14:115.0EPA 300.0 Sulfate 4.7 I mg/L 11/30/23 14:115.0EPA 300.0 Nitrogen, Nitrate 0.95 mg/L 11/10/23 21:460.050EPA 353.2
35840909002 DPW-434
Field pH 7.95 Std. Units 11/09/23 10:55 Field Temperature 22.5 deg C 11/09/23 10:55 Field Specific Conductance 256 umhos/cm 11/09/23 10:55 Oxygen, Dissolved 2.02 mg/L 11/09/23 10:55 REDOX -142.00 mV 11/09/23 10:55 Turbidity 12.6 NTU 11/09/23 10:55 Calcium 35400 ug/L 11/26/23 14:25500EPA 6010 Chromium 1.8 I ug/L 11/26/23 14:255.0EPA 6010 Iron 2750 ug/L 11/26/23 14:2540.0EPA 6010 Lead 6.2 I ug/L 11/26/23 14:2510.0EPA 6010 Magnesium 8360 ug/L 11/26/23 14:25500EPA 6010 Manganese 22.0 ug/L 11/26/23 14:255.0EPA 6010 Potassium 1100 ug/L 11/26/23 14:251000EPA 6010 Sodium 7.3 mg/L 11/26/23 14:252.0EPA 6010 Zinc 695 ug/L 11/26/23 14:2520.0EPA 6010 Arsenic 0.65 I ug/L 11/21/23 18:501.0EPA 6020 1,1-Dichloroethane 0.71 I ug/L 11/14/23 15:161.0EPA 624.1 1,1-Dichloroethene 2.6 ug/L 11/14/23 15:161.0EPA 624.1 Gross Alpha 3.63U ±
1.92 (3.63)
C:NA T:NA
pCi/L 12/05/23 18:28SM 7110C-2000
Alkalinity, Total as CaCO3 105 mg/L 11/18/23 22:105.0SM 2320B Total Dissolved Solids 231 mg/L 11/13/23 21:305.0SM 2540C Chloride 10.6 mg/L 11/29/23 18:015.0EPA 300.0 Sulfate 5.5 mg/L 11/29/23 18:015.0EPA 300.0 Nitrogen, Ammonia 0.40 mg/L 11/12/23 19:310.050EPA 350.1 Nitrogen, Nitrate 0.38 mg/L 11/10/23 21:500.050EPA 353.2
35840909003 DPW-DUP
Calcium 38200 ug/L 11/27/23 01:15500EPA 6010 Iron 1780 ug/L 11/27/23 01:1540.0EPA 6010 Lead 2.9 I ug/L 11/27/23 01:1510.0EPA 6010
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC 8 East Tower Circle
Ormond Beach, FL 32174
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
35840909 Davis LF PWs
Parameters AnalyzedResult Lab Sample ID
Report Limit QualifiersUnitsMethod Client Sample ID
35840909003 DPW-DUP
Magnesium 8500 ug/L 11/27/23 01:15500EPA 6010 Manganese 15.1 ug/L 11/27/23 01:155.0EPA 6010 Potassium 971 I ug/L 11/27/23 01:151000EPA 6010 Sodium 7.0 mg/L 11/27/23 01:152.0EPA 6010 Zinc 492 ug/L 11/27/23 01:1520.0EPA 6010 Arsenic 0.58 I ug/L 11/21/23 18:521.0EPA 6020 1,1-Dichloroethane 0.75 I ug/L 11/14/23 16:021.0EPA 624.1 1,1-Dichloroethene 2.9 ug/L 11/14/23 16:021.0EPA 624.1 Gross Alpha 3.54 ± 1.80
(2.66) C:NA
T:NA
pCi/L 12/05/23 18:28SM 7110C-2000
Alkalinity, Total as CaCO3 116 mg/L 11/18/23 22:215.0SM 2320B Total Dissolved Solids 170 mg/L 11/13/23 21:305.0SM 2540C Chloride 11.8 mg/L 11/29/23 18:235.0EPA 300.0 Sulfate 6.8 mg/L 11/29/23 18:23 J(M1)5.0EPA 300.0 Nitrogen, Ammonia 0.24 mg/L 11/12/23 19:320.050EPA 350.1 Nitrogen, Nitrate 1.1 mg/L 11/10/23 21:540.050EPA 353.2
35840909004 DPW-435
Field pH 7.16 Std. Units 11/09/23 11:35 Field Temperature 19.1 deg C 11/09/23 11:35 Field Specific Conductance 503 umhos/cm 11/09/23 11:35 Oxygen, Dissolved 9.10 mg/L 11/09/23 11:35 REDOX -109.00 mV 11/09/23 11:35 Turbidity 1.6 NTU 11/09/23 11:35 Calcium 75300 ug/L 11/27/23 01:18500EPA 6010 Iron 2290 ug/L 11/27/23 01:1840.0EPA 6010 Magnesium 15300 ug/L 11/27/23 01:18500EPA 6010 Manganese 155 ug/L 11/27/23 01:185.0EPA 6010 Potassium 1320 ug/L 11/27/23 01:181000EPA 6010 Sodium 14.3 mg/L 11/27/23 01:182.0EPA 6010 Zinc 486 ug/L 11/27/23 01:1820.0EPA 6010 Arsenic 3.3 ug/L 11/21/23 18:551.0EPA 6020 1,4-Dichlorobenzene 0.46 I ug/L 11/14/23 16:251.0EPA 624.1 1,1-Dichloroethane 1.5 ug/L 11/14/23 16:251.0EPA 624.1 1,1-Dichloroethene 3.5 ug/L 11/14/23 16:251.0EPA 624.1 Vinyl chloride 1.4 ug/L 11/14/23 16:251.0EPA 624.1 Gross Alpha 7.16 ± 2.32
(2.66) C:NA
T:NA
pCi/L 12/05/23 18:28SM 7110C-2000
Alkalinity, Total as CaCO3 232 mg/L 11/18/23 22:335.0SM 2320B Total Dissolved Solids 359 mg/L 11/13/23 21:305.0SM 2540C Chloride 25.6 mg/L 11/29/23 19:305.0EPA 300.0 Sulfate 5.6 mg/L 11/29/23 19:305.0EPA 300.0 Nitrogen, Ammonia 0.22 mg/L 11/12/23 19:390.050EPA 350.1 Nitrogen, Nitrate 0.034 I mg/L 11/10/23 21:570.050EPA 353.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC 8 East Tower Circle
Ormond Beach, FL 32174
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
35840909 Davis LF PWs
Sample: DPW-7 Lab ID: 35840909001 Collected: 11/09/23 10:15 Received: 11/10/23 12:22 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLPQL
Analytical Method:
Pace Analytical Services - Ormond Beach
Field Data
Field pH 7.74 Std. Units 11/09/23 10:151 Field Temperature 22.4 deg C 11/09/23 10:151 Field Specific Conductance 251 umhos/cm 11/09/23 10:151 Oxygen, Dissolved 1.61 mg/L 11/09/23 10:15 7782-44-71 REDOX 88.00 mV 11/09/23 10:151 Turbidity .10 NTU 11/09/23 10:151
Analytical Method: EPA 6010 Preparation Method: EPA 3010 Pace Analytical Services - Ormond Beach
6010 MET ICP
Cadmium 0.33 U ug/L 11/27/23 01:11 7440-43-911/21/23 09:451.0 0.33 1 Calcium 190 U ug/L 11/27/23 01:11 7440-70-211/21/23 09:45500 190 1 Chromium 1.7 U ug/L 11/27/23 01:11 7440-47-311/21/23 09:455.0 1.7 1 Iron 25.0 U ug/L 11/27/23 01:11 7439-89-611/21/23 09:4540.0 25.0 1 Lead 2.1 U ug/L 11/27/23 01:11 7439-92-111/21/23 09:4510.0 2.1 1 Magnesium 84.0 U ug/L 11/27/23 01:11 7439-95-411/21/23 09:45500 84.0 1 Manganese 1.1 U ug/L 11/27/23 01:11 7439-96-511/21/23 09:455.0 1.1 1 Potassium 270 U ug/L 11/27/23 01:11 7440-09-711/21/23 09:451000 270 1 Sodium 55.6 mg/L 11/27/23 01:11 7440-23-511/21/23 09:452.0 0.54 1 Zinc 11.0 U ug/L 11/27/23 01:11 7440-66-611/21/23 09:4520.0 11.0 1
Analytical Method: EPA 6020 Preparation Method: EPA 3010 Pace Analytical Services - Ormond Beach
6020 MET ICPMS
Arsenic 0.50 U ug/L 11/21/23 18:42 7440-38-211/21/23 09:451.0 0.50 1
Analytical Method: EPA 7470 Preparation Method: EPA 7470 Pace Analytical Services - Ormond Beach
7470 Mercury
Mercury 0.14 U ug/L 12/04/23 12:29 7439-97-611/29/23 13:440.20 0.14 1
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1 Pace Analytical Services - Charlotte
625 RVE
Acenaphthene 1.7 U ug/L 11/17/23 04:01 83-32-911/15/23 07:574.2 1.7 1 Acenaphthylene 1.6 U ug/L 11/17/23 04:01 208-96-811/15/23 07:574.2 1.6 1 Anthracene 1.9 U ug/L 11/17/23 04:01 120-12-711/15/23 07:574.2 1.9 1 Benzidine 11.2 U ug/L 11/17/23 04:01 92-87-511/15/23 07:5741.7 11.2 1 Benzo(a)anthracene 2.2 U ug/L 11/17/23 04:01 56-55-311/15/23 07:574.2 2.2 1 Benzo(a)pyrene 2.3 U ug/L 11/17/23 04:01 50-32-811/15/23 07:574.2 2.3 1 Benzo(b)fluoranthene 2.2 U ug/L 11/17/23 04:01 205-99-211/15/23 07:574.2 2.2 1 Benzo(g,h,i)perylene 2.4 U ug/L 11/17/23 04:01 191-24-211/15/23 07:574.2 2.4 1 Benzo(k)fluoranthene 2.3 U ug/L 11/17/23 04:01 207-08-911/15/23 07:574.2 2.3 1 4-Bromophenylphenyl ether 1.5 U ug/L 11/17/23 04:01 101-55-311/15/23 07:574.2 1.5 1 Butylbenzylphthalate 2.6 U ug/L 11/17/23 04:01 85-68-711/15/23 07:574.2 2.6 1 bis(2-Chloroethoxy)methane 1.5 U ug/L 11/17/23 04:01 111-91-111/15/23 07:578.3 1.5 1 bis(2-Chloroethyl) ether 1.6 U ug/L 11/17/23 04:01 111-44-411/15/23 07:574.2 1.6 1 2-Chloronaphthalene 1.4 U ug/L 11/17/23 04:01 91-58-711/15/23 07:574.2 1.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 12/06/2023 04:57 PM
Pace Analytical Services, LLC 8 East Tower Circle
Ormond Beach, FL 32174
Pace Project No.:
Project:
35840909 Davis LF PWs
Sample: DPW-7 Lab ID: 35840909001 Collected: 11/09/23 10:15 Received: 11/10/23 12:22 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLPQL
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1 Pace Analytical Services - Charlotte
625 RVE
2-Chlorophenol 1.0 U ug/L 11/17/23 04:01 95-57-811/15/23 07:574.2 1.0 1 4-Chlorophenylphenyl ether 1.7 U ug/L 11/17/23 04:01 7005-72-311/15/23 07:574.2 1.7 1 Chrysene 2.3 U ug/L 11/17/23 04:01 218-01-911/15/23 07:574.2 2.3 1 Dibenz(a,h)anthracene 2.5 U ug/L 11/17/23 04:01 53-70-311/15/23 07:574.2 2.5 1 3,3'-Dichlorobenzidine 6.8 U ug/L 11/17/23 04:01 91-94-111/15/23 07:578.3 6.8 1 2,4-Dichlorophenol 1.2 U ug/L 11/17/23 04:01 120-83-211/15/23 07:574.2 1.2 1 Diethylphthalate 1.7 U ug/L 11/17/23 04:01 84-66-211/15/23 07:574.2 1.7 1 2,4-Dimethylphenol 1.4 U ug/L 11/17/23 04:01 105-67-9 J(L1)11/15/23 07:578.3 1.4 1 Dimethylphthalate 1.8 U ug/L 11/17/23 04:01 131-11-311/15/23 07:574.2 1.8 1 Di-n-butylphthalate 1.8 U ug/L 11/17/23 04:01 84-74-2 J(L1)11/15/23 07:574.2 1.8 1 4,6-Dinitro-2-methylphenol 6.5 U ug/L 11/17/23 04:01 534-52-111/15/23 07:578.3 6.5 1 2,4-Dinitrophenol 21.7 U ug/L 11/17/23 04:01 51-28-511/15/23 07:5741.7 21.7 1 2,4-Dinitrotoluene 1.4 U ug/L 11/17/23 04:01 121-14-211/15/23 07:574.2 1.4 1 2,6-Dinitrotoluene 1.4 U ug/L 11/17/23 04:01 606-20-211/15/23 07:574.2 1.4 1 Di-n-octylphthalate 3.3 U ug/L 11/17/23 04:01 117-84-011/15/23 07:574.2 3.3 1 1,2-Diphenylhydrazine 1.3 U ug/L 11/17/23 04:01 122-66-711/15/23 07:574.2 1.3 1 bis(2-Ethylhexyl)phthalate 3.1 U ug/L 11/17/23 04:01 117-81-711/15/23 07:574.2 3.1 1 Fluoranthene 1.8 U ug/L 11/17/23 04:01 206-44-011/15/23 07:574.2 1.8 1 Fluorene 1.7 U ug/L 11/17/23 04:01 86-73-711/15/23 07:574.2 1.7 1 Hexachloro-1,3-butadiene 1.5 U ug/L 11/17/23 04:01 87-68-311/15/23 07:574.2 1.5 1 Hexachlorobenzene 1.8 U ug/L 11/17/23 04:01 118-74-111/15/23 07:574.2 1.8 1 Hexachlorocyclopentadiene 1.3 U ug/L 11/17/23 04:01 77-47-411/15/23 07:578.3 1.3 1 Hexachloroethane 1.2 U ug/L 11/17/23 04:01 67-72-111/15/23 07:574.2 1.2 1 Indeno(1,2,3-cd)pyrene 2.4 U ug/L 11/17/23 04:01 193-39-511/15/23 07:574.2 2.4 1 Isophorone 1.4 U ug/L 11/17/23 04:01 78-59-111/15/23 07:578.3 1.4 1 2-Methylphenol(o-Cresol) 1.6 U ug/L 11/17/23 04:01 95-48-711/15/23 07:574.2 1.6 1 3&4-Methylphenol(m&p Cresol) 1.0 U ug/L 11/17/23 04:01 15831-10-411/15/23 07:578.3 1.0 1 Naphthalene 1.7 U ug/L 11/17/23 04:01 91-20-311/15/23 07:574.2 1.7 1 Nitrobenzene 1.6 U ug/L 11/17/23 04:01 98-95-311/15/23 07:574.2 1.6 1 2-Nitrophenol 1.2 U ug/L 11/17/23 04:01 88-75-511/15/23 07:574.2 1.2 1 4-Nitrophenol 5.5 U ug/L 11/17/23 04:01 100-02-711/15/23 07:578.3 5.5 1 N-Nitrosodimethylamine 1.6 U ug/L 11/17/23 04:01 62-75-911/15/23 07:574.2 1.6 1 N-Nitroso-di-n-propylamine 1.1 U ug/L 11/17/23 04:01 621-64-711/15/23 07:574.2 1.1 1 N-Nitrosodiphenylamine 2.5 U ug/L 11/17/23 04:01 86-30-611/15/23 07:578.3 2.5 1 2,2'-Oxybis(1-chloropropane) 0.96 U ug/L 11/17/23 04:01 108-60-111/15/23 07:574.2 0.96 1 Pentachlorophenol 3.1 U ug/L 11/17/23 04:01 87-86-511/15/23 07:578.3 3.1 1 Phenanthrene 1.7 U ug/L 11/17/23 04:01 85-01-811/15/23 07:574.2 1.7 1 Phenol 1.1 U ug/L 11/17/23 04:01 108-95-211/15/23 07:574.2 1.1 1 Pyrene 1.8 U ug/L 11/17/23 04:01 129-00-0 J(L1)11/15/23 07:574.2 1.8 1 1,2,4-Trichlorobenzene 1.4 U ug/L 11/17/23 04:01 120-82-111/15/23 07:574.2 1.4 1 2,4,6-Trichlorophenol 1.3 U ug/L 11/17/23 04:01 88-06-211/15/23 07:578.3 1.3 1 Surrogates Nitrobenzene-d5 (S) 93 % 11/17/23 04:01 4165-60-011/15/23 07:5710-120 1 2-Fluorobiphenyl (S) 87 % 11/17/23 04:01 321-60-811/15/23 07:5715-120 1 Terphenyl-d14 (S) 121 % 11/17/23 04:01 1718-51-011/15/23 07:5711-131 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 12/06/2023 04:57 PM
Pace Analytical Services, LLC 8 East Tower Circle
Ormond Beach, FL 32174
Pace Project No.:
Project:
35840909 Davis LF PWs
Sample: DPW-7 Lab ID: 35840909001 Collected: 11/09/23 10:15 Received: 11/10/23 12:22 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLPQL
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1 Pace Analytical Services - Charlotte
625 RVE
Surrogates Phenol-d6 (S) 64 % 11/17/23 04:01 13127-88-311/15/23 07:5710-120 1 2-Fluorophenol (S) 88 % 11/17/23 04:01 367-12-411/15/23 07:5710-120 1 2,4,6-Tribromophenol (S) 134 % 11/17/23 04:01 118-79-611/15/23 07:5710-137 1
Analytical Method: EPA 624.1 Pace Analytical Services - Ormond Beach
624.1 Volatile Organics Unpres
Benzene 0.30 U ug/L 11/14/23 14:29 71-43-21.0 0.30 1 Bromodichloromethane 0.19 U ug/L 11/14/23 14:29 75-27-41.0 0.19 1 Bromoform 0.48 U ug/L 11/14/23 14:29 75-25-23.0 0.48 1 Bromomethane 3.9 U ug/L 11/14/23 14:29 74-83-910.0 3.9 1 Carbon tetrachloride 0.44 U ug/L 11/14/23 14:29 56-23-53.0 0.44 1 Chlorobenzene 0.35 U ug/L 11/14/23 14:29 108-90-71.0 0.35 1 Chloroethane 3.7 U ug/L 11/14/23 14:29 75-00-310.0 3.7 1 2-Chloroethylvinyl ether 6.1 U ug/L 11/14/23 14:29 110-75-840.0 6.1 1 Chloroform 0.56 U ug/L 11/14/23 14:29 67-66-31.0 0.56 1 Chloromethane 0.43 U ug/L 11/14/23 14:29 74-87-31.0 0.43 1 Dibromochloromethane 0.45 U ug/L 11/14/23 14:29 124-48-12.0 0.45 1 1,2-Dichlorobenzene 0.60 U ug/L 11/14/23 14:29 95-50-11.0 0.60 1 1,3-Dichlorobenzene 0.33 U ug/L 11/14/23 14:29 541-73-11.0 0.33 1 1,4-Dichlorobenzene 0.28 U ug/L 11/14/23 14:29 106-46-71.0 0.28 1 1,1-Dichloroethane 0.34 U ug/L 11/14/23 14:29 75-34-31.0 0.34 1 1,2-Dichloroethane 0.27 U ug/L 11/14/23 14:29 107-06-21.0 0.27 1 1,1-Dichloroethene 0.59 U ug/L 11/14/23 14:29 75-35-41.0 0.59 1 trans-1,2-Dichloroethene 0.23 U ug/L 11/14/23 14:29 156-60-51.0 0.23 1 1,2-Dichloropropane 0.23 U ug/L 11/14/23 14:29 78-87-51.0 0.23 1 cis-1,3-Dichloropropene 0.17 U ug/L 11/14/23 14:29 10061-01-51.0 0.17 1 trans-1,3-Dichloropropene 0.37 U ug/L 11/14/23 14:29 10061-02-61.0 0.37 1 Ethylbenzene 0.30 U ug/L 11/14/23 14:29 100-41-41.0 0.30 1 Methylene Chloride 1.7 U ug/L 11/14/23 14:29 75-09-25.0 1.7 1 1,1,2,2-Tetrachloroethane 0.59 U ug/L 11/14/23 14:29 79-34-51.0 0.59 1 Tetrachloroethene 0.38 U ug/L 11/14/23 14:29 127-18-41.0 0.38 1 Toluene 0.33 U ug/L 11/14/23 14:29 108-88-31.0 0.33 1 1,1,1-Trichloroethane 0.30 U ug/L 11/14/23 14:29 71-55-61.0 0.30 1 1,1,2-Trichloroethane 0.30 U ug/L 11/14/23 14:29 79-00-51.0 0.30 1 Trichloroethene 0.36 U ug/L 11/14/23 14:29 79-01-61.0 0.36 1 Trichlorofluoromethane 0.72 U ug/L 11/14/23 14:29 75-69-41.0 0.72 1 Vinyl chloride 0.39 U ug/L 11/14/23 14:29 75-01-41.0 0.39 1 Surrogates 1,2-Dichlorobenzene-d4 (S) 100 % 11/14/23 14:29 2199-69-160-140 1 4-Bromofluorobenzene (S) 93 % 11/14/23 14:29 460-00-460-140 1 Toluene-d8 (S) 99 % 11/14/23 14:29 2037-26-560-140 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 12/06/2023 04:57 PM
Pace Analytical Services, LLC 8 East Tower Circle
Ormond Beach, FL 32174
Pace Project No.:
Project:
35840909 Davis LF PWs
Sample: DPW-7 Lab ID: 35840909001 Collected: 11/09/23 10:15 Received: 11/10/23 12:22 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLPQL
Analytical Method: SM 2320B Pace Analytical Services - Ormond Beach
2320B Alkalinity
Alkalinity, Total as CaCO3 111 mg/L 11/18/23 20:525.0 5.0 1
Analytical Method: SM 2540C Pace Analytical Services - Ormond Beach
2540C Total Dissolved Solids
Total Dissolved Solids 218 mg/L 11/13/23 21:30 J(D6)5.0 5.0 1
Analytical Method: EPA 300.0 Pace Analytical Services - Ormond Beach
300.0 IC Anions 28 Days
Chloride 10.1 mg/L 11/30/23 14:11 16887-00-65.0 2.5 1 Sulfate 4.7 I mg/L 11/30/23 14:11 14808-79-85.0 2.5 1
Analytical Method: EPA 350.1 Pace Analytical Services - Ormond Beach
350.1 Ammonia
Nitrogen, Ammonia 0.035 U mg/L 11/12/23 19:29 7664-41-70.050 0.035 1
Analytical Method: EPA 353.2 Pace Analytical Services - Ormond Beach
353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate 0.95 mg/L 11/10/23 21:46 14797-55-80.050 0.025 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 12/06/2023 04:57 PM
Pace Analytical Services, LLC 8 East Tower Circle
Ormond Beach, FL 32174
Pace Project No.:
Project:
35840909 Davis LF PWs
Sample: DPW-434 Lab ID: 35840909002 Collected: 11/09/23 10:55 Received: 11/10/23 12:22 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLPQL
Analytical Method:
Pace Analytical Services - Ormond Beach
Field Data
Field pH 7.95 Std. Units 11/09/23 10:551 Field Temperature 22.5 deg C 11/09/23 10:551 Field Specific Conductance 256 umhos/cm 11/09/23 10:551 Oxygen, Dissolved 2.02 mg/L 11/09/23 10:55 7782-44-71 REDOX -142.00 mV 11/09/23 10:551 Turbidity 12.6 NTU 11/09/23 10:551
Analytical Method: EPA 6010 Preparation Method: EPA 3010 Pace Analytical Services - Ormond Beach
6010 MET ICP
Cadmium 0.33 U ug/L 11/26/23 14:25 7440-43-911/21/23 09:451.0 0.33 1 Calcium 35400 ug/L 11/26/23 14:25 7440-70-211/21/23 09:45500 190 1 Chromium 1.8 I ug/L 11/26/23 14:25 7440-47-311/21/23 09:455.0 1.7 1 Iron 2750 ug/L 11/26/23 14:25 7439-89-611/21/23 09:4540.0 25.0 1 Lead 6.2 I ug/L 11/26/23 14:25 7439-92-111/21/23 09:4510.0 2.1 1 Magnesium 8360 ug/L 11/26/23 14:25 7439-95-411/21/23 09:45500 84.0 1 Manganese 22.0 ug/L 11/26/23 14:25 7439-96-511/21/23 09:455.0 1.1 1 Potassium 1100 ug/L 11/26/23 14:25 7440-09-711/21/23 09:451000 270 1 Sodium 7.3 mg/L 11/26/23 14:25 7440-23-511/21/23 09:452.0 0.54 1 Zinc 695 ug/L 11/26/23 14:25 7440-66-611/21/23 09:4520.0 11.0 1
Analytical Method: EPA 6020 Preparation Method: EPA 3010 Pace Analytical Services - Ormond Beach
6020 MET ICPMS
Arsenic 0.65 I ug/L 11/21/23 18:50 7440-38-211/21/23 09:451.0 0.50 1
Analytical Method: EPA 7470 Preparation Method: EPA 7470 Pace Analytical Services - Ormond Beach
7470 Mercury
Mercury 0.14 U ug/L 12/04/23 14:07 7439-97-611/29/23 13:440.20 0.14 1
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1 Pace Analytical Services - Charlotte
625 RVE
Acenaphthene 1.7 U ug/L 11/17/23 04:26 83-32-911/15/23 07:574.2 1.7 1 Acenaphthylene 1.6 U ug/L 11/17/23 04:26 208-96-811/15/23 07:574.2 1.6 1 Anthracene 1.9 U ug/L 11/17/23 04:26 120-12-711/15/23 07:574.2 1.9 1 Benzidine 11.2 U ug/L 11/17/23 04:26 92-87-511/15/23 07:5741.7 11.2 1 Benzo(a)anthracene 2.2 U ug/L 11/17/23 04:26 56-55-311/15/23 07:574.2 2.2 1 Benzo(a)pyrene 2.3 U ug/L 11/17/23 04:26 50-32-811/15/23 07:574.2 2.3 1 Benzo(b)fluoranthene 2.2 U ug/L 11/17/23 04:26 205-99-211/15/23 07:574.2 2.2 1 Benzo(g,h,i)perylene 2.4 U ug/L 11/17/23 04:26 191-24-211/15/23 07:574.2 2.4 1 Benzo(k)fluoranthene 2.3 U ug/L 11/17/23 04:26 207-08-911/15/23 07:574.2 2.3 1 4-Bromophenylphenyl ether 1.5 U ug/L 11/17/23 04:26 101-55-311/15/23 07:574.2 1.5 1 Butylbenzylphthalate 2.6 U ug/L 11/17/23 04:26 85-68-711/15/23 07:574.2 2.6 1 bis(2-Chloroethoxy)methane 1.5 U ug/L 11/17/23 04:26 111-91-111/15/23 07:578.3 1.5 1 bis(2-Chloroethyl) ether 1.6 U ug/L 11/17/23 04:26 111-44-411/15/23 07:574.2 1.6 1 2-Chloronaphthalene 1.4 U ug/L 11/17/23 04:26 91-58-711/15/23 07:574.2 1.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 12/06/2023 04:57 PM
Pace Analytical Services, LLC 8 East Tower Circle
Ormond Beach, FL 32174
Pace Project No.:
Project:
35840909 Davis LF PWs
Sample: DPW-434 Lab ID: 35840909002 Collected: 11/09/23 10:55 Received: 11/10/23 12:22 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLPQL
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1 Pace Analytical Services - Charlotte
625 RVE
2-Chlorophenol 1.0 U ug/L 11/17/23 04:26 95-57-811/15/23 07:574.2 1.0 1 4-Chlorophenylphenyl ether 1.7 U ug/L 11/17/23 04:26 7005-72-311/15/23 07:574.2 1.7 1 Chrysene 2.3 U ug/L 11/17/23 04:26 218-01-911/15/23 07:574.2 2.3 1 Dibenz(a,h)anthracene 2.5 U ug/L 11/17/23 04:26 53-70-311/15/23 07:574.2 2.5 1 3,3'-Dichlorobenzidine 6.8 U ug/L 11/17/23 04:26 91-94-111/15/23 07:578.3 6.8 1 2,4-Dichlorophenol 1.2 U ug/L 11/17/23 04:26 120-83-211/15/23 07:574.2 1.2 1 Diethylphthalate 1.7 U ug/L 11/17/23 04:26 84-66-211/15/23 07:574.2 1.7 1 2,4-Dimethylphenol 1.4 U ug/L 11/17/23 04:26 105-67-9 J(L1)11/15/23 07:578.3 1.4 1 Dimethylphthalate 1.8 U ug/L 11/17/23 04:26 131-11-311/15/23 07:574.2 1.8 1 Di-n-butylphthalate 1.8 U ug/L 11/17/23 04:26 84-74-2 J(L1)11/15/23 07:574.2 1.8 1 4,6-Dinitro-2-methylphenol 6.5 U ug/L 11/17/23 04:26 534-52-111/15/23 07:578.3 6.5 1 2,4-Dinitrophenol 21.7 U ug/L 11/17/23 04:26 51-28-511/15/23 07:5741.7 21.7 1 2,4-Dinitrotoluene 1.4 U ug/L 11/17/23 04:26 121-14-211/15/23 07:574.2 1.4 1 2,6-Dinitrotoluene 1.4 U ug/L 11/17/23 04:26 606-20-211/15/23 07:574.2 1.4 1 Di-n-octylphthalate 3.3 U ug/L 11/17/23 04:26 117-84-011/15/23 07:574.2 3.3 1 1,2-Diphenylhydrazine 1.3 U ug/L 11/17/23 04:26 122-66-711/15/23 07:574.2 1.3 1 bis(2-Ethylhexyl)phthalate 3.1 U ug/L 11/17/23 04:26 117-81-711/15/23 07:574.2 3.1 1 Fluoranthene 1.8 U ug/L 11/17/23 04:26 206-44-011/15/23 07:574.2 1.8 1 Fluorene 1.7 U ug/L 11/17/23 04:26 86-73-711/15/23 07:574.2 1.7 1 Hexachloro-1,3-butadiene 1.5 U ug/L 11/17/23 04:26 87-68-311/15/23 07:574.2 1.5 1 Hexachlorobenzene 1.8 U ug/L 11/17/23 04:26 118-74-111/15/23 07:574.2 1.8 1 Hexachlorocyclopentadiene 1.3 U ug/L 11/17/23 04:26 77-47-411/15/23 07:578.3 1.3 1 Hexachloroethane 1.2 U ug/L 11/17/23 04:26 67-72-111/15/23 07:574.2 1.2 1 Indeno(1,2,3-cd)pyrene 2.4 U ug/L 11/17/23 04:26 193-39-511/15/23 07:574.2 2.4 1 Isophorone 1.4 U ug/L 11/17/23 04:26 78-59-111/15/23 07:578.3 1.4 1 2-Methylphenol(o-Cresol) 1.6 U ug/L 11/17/23 04:26 95-48-711/15/23 07:574.2 1.6 1 3&4-Methylphenol(m&p Cresol) 1.0 U ug/L 11/17/23 04:26 15831-10-411/15/23 07:578.3 1.0 1 Naphthalene 1.7 U ug/L 11/17/23 04:26 91-20-311/15/23 07:574.2 1.7 1 Nitrobenzene 1.6 U ug/L 11/17/23 04:26 98-95-311/15/23 07:574.2 1.6 1 2-Nitrophenol 1.2 U ug/L 11/17/23 04:26 88-75-511/15/23 07:574.2 1.2 1 4-Nitrophenol 5.5 U ug/L 11/17/23 04:26 100-02-711/15/23 07:578.3 5.5 1 N-Nitrosodimethylamine 1.6 U ug/L 11/17/23 04:26 62-75-911/15/23 07:574.2 1.6 1 N-Nitroso-di-n-propylamine 1.1 U ug/L 11/17/23 04:26 621-64-711/15/23 07:574.2 1.1 1 N-Nitrosodiphenylamine 2.5 U ug/L 11/17/23 04:26 86-30-611/15/23 07:578.3 2.5 1 2,2'-Oxybis(1-chloropropane) 0.96 U ug/L 11/17/23 04:26 108-60-111/15/23 07:574.2 0.96 1 Pentachlorophenol 3.1 U ug/L 11/17/23 04:26 87-86-511/15/23 07:578.3 3.1 1 Phenanthrene 1.7 U ug/L 11/17/23 04:26 85-01-811/15/23 07:574.2 1.7 1 Phenol 1.1 U ug/L 11/17/23 04:26 108-95-211/15/23 07:574.2 1.1 1 Pyrene 1.8 U ug/L 11/17/23 04:26 129-00-0 J(L1)11/15/23 07:574.2 1.8 1 1,2,4-Trichlorobenzene 1.4 U ug/L 11/17/23 04:26 120-82-111/15/23 07:574.2 1.4 1 2,4,6-Trichlorophenol 1.3 U ug/L 11/17/23 04:26 88-06-211/15/23 07:578.3 1.3 1 Surrogates Nitrobenzene-d5 (S) 48 % 11/17/23 04:26 4165-60-011/15/23 07:5710-120 1 2-Fluorobiphenyl (S) 48 % 11/17/23 04:26 321-60-811/15/23 07:5715-120 1 Terphenyl-d14 (S) 77 % 11/17/23 04:26 1718-51-011/15/23 07:5711-131 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 12/06/2023 04:57 PM
Pace Analytical Services, LLC 8 East Tower Circle
Ormond Beach, FL 32174
Pace Project No.:
Project:
35840909 Davis LF PWs
Sample: DPW-434 Lab ID: 35840909002 Collected: 11/09/23 10:55 Received: 11/10/23 12:22 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLPQL
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1 Pace Analytical Services - Charlotte
625 RVE
Surrogates Phenol-d6 (S) 31 % 11/17/23 04:26 13127-88-311/15/23 07:5710-120 1 2-Fluorophenol (S) 44 % 11/17/23 04:26 367-12-411/15/23 07:5710-120 1 2,4,6-Tribromophenol (S) 68 % 11/17/23 04:26 118-79-611/15/23 07:5710-137 1
Analytical Method: EPA 624.1 Pace Analytical Services - Ormond Beach
624.1 Volatile Organics Unpres
Benzene 0.30 U ug/L 11/14/23 15:16 71-43-21.0 0.30 1 Bromodichloromethane 0.19 U ug/L 11/14/23 15:16 75-27-41.0 0.19 1 Bromoform 0.48 U ug/L 11/14/23 15:16 75-25-23.0 0.48 1 Bromomethane 3.9 U ug/L 11/14/23 15:16 74-83-910.0 3.9 1 Carbon tetrachloride 0.44 U ug/L 11/14/23 15:16 56-23-53.0 0.44 1 Chlorobenzene 0.35 U ug/L 11/14/23 15:16 108-90-71.0 0.35 1 Chloroethane 3.7 U ug/L 11/14/23 15:16 75-00-310.0 3.7 1 2-Chloroethylvinyl ether 6.1 U ug/L 11/14/23 15:16 110-75-840.0 6.1 1 Chloroform 0.56 U ug/L 11/14/23 15:16 67-66-31.0 0.56 1 Chloromethane 0.43 U ug/L 11/14/23 15:16 74-87-31.0 0.43 1 Dibromochloromethane 0.45 U ug/L 11/14/23 15:16 124-48-12.0 0.45 1 1,2-Dichlorobenzene 0.60 U ug/L 11/14/23 15:16 95-50-11.0 0.60 1 1,3-Dichlorobenzene 0.33 U ug/L 11/14/23 15:16 541-73-11.0 0.33 1 1,4-Dichlorobenzene 0.28 U ug/L 11/14/23 15:16 106-46-71.0 0.28 1 1,1-Dichloroethane 0.71 I ug/L 11/14/23 15:16 75-34-31.0 0.34 1 1,2-Dichloroethane 0.27 U ug/L 11/14/23 15:16 107-06-21.0 0.27 1 1,1-Dichloroethene 2.6 ug/L 11/14/23 15:16 75-35-41.0 0.59 1 trans-1,2-Dichloroethene 0.23 U ug/L 11/14/23 15:16 156-60-51.0 0.23 1 1,2-Dichloropropane 0.23 U ug/L 11/14/23 15:16 78-87-51.0 0.23 1 cis-1,3-Dichloropropene 0.17 U ug/L 11/14/23 15:16 10061-01-51.0 0.17 1 trans-1,3-Dichloropropene 0.37 U ug/L 11/14/23 15:16 10061-02-61.0 0.37 1 Ethylbenzene 0.30 U ug/L 11/14/23 15:16 100-41-41.0 0.30 1 Methylene Chloride 1.7 U ug/L 11/14/23 15:16 75-09-25.0 1.7 1 1,1,2,2-Tetrachloroethane 0.59 U ug/L 11/14/23 15:16 79-34-51.0 0.59 1 Tetrachloroethene 0.38 U ug/L 11/14/23 15:16 127-18-41.0 0.38 1 Toluene 0.33 U ug/L 11/14/23 15:16 108-88-31.0 0.33 1 1,1,1-Trichloroethane 0.30 U ug/L 11/14/23 15:16 71-55-61.0 0.30 1 1,1,2-Trichloroethane 0.30 U ug/L 11/14/23 15:16 79-00-51.0 0.30 1 Trichloroethene 0.36 U ug/L 11/14/23 15:16 79-01-61.0 0.36 1 Trichlorofluoromethane 0.72 U ug/L 11/14/23 15:16 75-69-41.0 0.72 1 Vinyl chloride 0.39 U ug/L 11/14/23 15:16 75-01-41.0 0.39 1 Surrogates 1,2-Dichlorobenzene-d4 (S) 99 % 11/14/23 15:16 2199-69-160-140 1 4-Bromofluorobenzene (S) 97 % 11/14/23 15:16 460-00-460-140 1 Toluene-d8 (S) 101 % 11/14/23 15:16 2037-26-560-140 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 12/06/2023 04:57 PM
Pace Analytical Services, LLC 8 East Tower Circle
Ormond Beach, FL 32174
Pace Project No.:
Project:
35840909 Davis LF PWs
Sample: DPW-434 Lab ID: 35840909002 Collected: 11/09/23 10:55 Received: 11/10/23 12:22 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLPQL
Analytical Method: SM 2320B Pace Analytical Services - Ormond Beach
2320B Alkalinity
Alkalinity, Total as CaCO3 105 mg/L 11/18/23 22:105.0 5.0 1
Analytical Method: SM 2540C Pace Analytical Services - Ormond Beach
2540C Total Dissolved Solids
Total Dissolved Solids 231 mg/L 11/13/23 21:305.0 5.0 1
Analytical Method: EPA 300.0 Pace Analytical Services - Ormond Beach
300.0 IC Anions 28 Days
Chloride 10.6 mg/L 11/29/23 18:01 16887-00-65.0 2.5 1 Sulfate 5.5 mg/L 11/29/23 18:01 14808-79-85.0 2.5 1
Analytical Method: EPA 350.1 Pace Analytical Services - Ormond Beach
350.1 Ammonia
Nitrogen, Ammonia 0.40 mg/L 11/12/23 19:31 7664-41-70.050 0.035 1
Analytical Method: EPA 353.2 Pace Analytical Services - Ormond Beach
353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate 0.38 mg/L 11/10/23 21:50 14797-55-80.050 0.025 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 12/06/2023 04:57 PM
Pace Analytical Services, LLC 8 East Tower Circle
Ormond Beach, FL 32174
Pace Project No.:
Project:
35840909 Davis LF PWs
Sample: DPW-DUP Lab ID: 35840909003 Collected: 11/09/23 10:55 Received: 11/10/23 12:22 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLPQL
Analytical Method: EPA 6010 Preparation Method: EPA 3010 Pace Analytical Services - Ormond Beach
6010 MET ICP
Cadmium 0.33 U ug/L 11/27/23 01:15 7440-43-911/21/23 09:451.0 0.33 1 Calcium 38200 ug/L 11/27/23 01:15 7440-70-211/21/23 09:45500 190 1 Chromium 1.7 U ug/L 11/27/23 01:15 7440-47-311/21/23 09:455.0 1.7 1 Iron 1780 ug/L 11/27/23 01:15 7439-89-611/21/23 09:4540.0 25.0 1 Lead 2.9 I ug/L 11/27/23 01:15 7439-92-111/21/23 09:4510.0 2.1 1 Magnesium 8500 ug/L 11/27/23 01:15 7439-95-411/21/23 09:45500 84.0 1 Manganese 15.1 ug/L 11/27/23 01:15 7439-96-511/21/23 09:455.0 1.1 1 Potassium 971 I ug/L 11/27/23 01:15 7440-09-711/21/23 09:451000 270 1 Sodium 7.0 mg/L 11/27/23 01:15 7440-23-511/21/23 09:452.0 0.54 1 Zinc 492 ug/L 11/27/23 01:15 7440-66-611/21/23 09:4520.0 11.0 1
Analytical Method: EPA 6020 Preparation Method: EPA 3010 Pace Analytical Services - Ormond Beach
6020 MET ICPMS
Arsenic 0.58 I ug/L 11/21/23 18:52 7440-38-211/21/23 09:451.0 0.50 1
Analytical Method: EPA 7470 Preparation Method: EPA 7470 Pace Analytical Services - Ormond Beach
7470 Mercury
Mercury 0.14 U ug/L 12/04/23 14:09 7439-97-611/29/23 13:440.20 0.14 1
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1 Pace Analytical Services - Charlotte
625 RVE
Acenaphthene 1.7 U ug/L 11/17/23 04:51 83-32-911/15/23 07:574.2 1.7 1 Acenaphthylene 1.6 U ug/L 11/17/23 04:51 208-96-811/15/23 07:574.2 1.6 1 Anthracene 1.9 U ug/L 11/17/23 04:51 120-12-711/15/23 07:574.2 1.9 1 Benzidine 11.2 U ug/L 11/17/23 04:51 92-87-511/15/23 07:5741.7 11.2 1 Benzo(a)anthracene 2.2 U ug/L 11/17/23 04:51 56-55-311/15/23 07:574.2 2.2 1 Benzo(a)pyrene 2.3 U ug/L 11/17/23 04:51 50-32-811/15/23 07:574.2 2.3 1 Benzo(b)fluoranthene 2.2 U ug/L 11/17/23 04:51 205-99-211/15/23 07:574.2 2.2 1 Benzo(g,h,i)perylene 2.4 U ug/L 11/17/23 04:51 191-24-211/15/23 07:574.2 2.4 1 Benzo(k)fluoranthene 2.3 U ug/L 11/17/23 04:51 207-08-911/15/23 07:574.2 2.3 1 4-Bromophenylphenyl ether 1.5 U ug/L 11/17/23 04:51 101-55-311/15/23 07:574.2 1.5 1 Butylbenzylphthalate 2.6 U ug/L 11/17/23 04:51 85-68-711/15/23 07:574.2 2.6 1 bis(2-Chloroethoxy)methane 1.5 U ug/L 11/17/23 04:51 111-91-111/15/23 07:578.3 1.5 1 bis(2-Chloroethyl) ether 1.6 U ug/L 11/17/23 04:51 111-44-411/15/23 07:574.2 1.6 1 2-Chloronaphthalene 1.4 U ug/L 11/17/23 04:51 91-58-711/15/23 07:574.2 1.4 1 2-Chlorophenol 1.0 U ug/L 11/17/23 04:51 95-57-811/15/23 07:574.2 1.0 1 4-Chlorophenylphenyl ether 1.7 U ug/L 11/17/23 04:51 7005-72-311/15/23 07:574.2 1.7 1 Chrysene 2.3 U ug/L 11/17/23 04:51 218-01-911/15/23 07:574.2 2.3 1 Dibenz(a,h)anthracene 2.5 U ug/L 11/17/23 04:51 53-70-311/15/23 07:574.2 2.5 1 3,3'-Dichlorobenzidine 6.8 U ug/L 11/17/23 04:51 91-94-111/15/23 07:578.3 6.8 1 2,4-Dichlorophenol 1.2 U ug/L 11/17/23 04:51 120-83-211/15/23 07:574.2 1.2 1 Diethylphthalate 1.7 U ug/L 11/17/23 04:51 84-66-211/15/23 07:574.2 1.7 1 2,4-Dimethylphenol 1.4 U ug/L 11/17/23 04:51 105-67-9 J(L1)11/15/23 07:578.3 1.4 1 Dimethylphthalate 1.8 U ug/L 11/17/23 04:51 131-11-311/15/23 07:574.2 1.8 1 Di-n-butylphthalate 1.8 U ug/L 11/17/23 04:51 84-74-2 J(L1)11/15/23 07:574.2 1.8 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 12/06/2023 04:57 PM
Pace Analytical Services, LLC 8 East Tower Circle
Ormond Beach, FL 32174
Pace Project No.:
Project:
35840909 Davis LF PWs
Sample: DPW-DUP Lab ID: 35840909003 Collected: 11/09/23 10:55 Received: 11/10/23 12:22 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLPQL
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1 Pace Analytical Services - Charlotte
625 RVE
4,6-Dinitro-2-methylphenol 6.5 U ug/L 11/17/23 04:51 534-52-111/15/23 07:578.3 6.5 1 2,4-Dinitrophenol 21.7 U ug/L 11/17/23 04:51 51-28-511/15/23 07:5741.7 21.7 1 2,4-Dinitrotoluene 1.4 U ug/L 11/17/23 04:51 121-14-211/15/23 07:574.2 1.4 1 2,6-Dinitrotoluene 1.4 U ug/L 11/17/23 04:51 606-20-211/15/23 07:574.2 1.4 1 Di-n-octylphthalate 3.3 U ug/L 11/17/23 04:51 117-84-011/15/23 07:574.2 3.3 1 1,2-Diphenylhydrazine 1.3 U ug/L 11/17/23 04:51 122-66-711/15/23 07:574.2 1.3 1 bis(2-Ethylhexyl)phthalate 3.1 U ug/L 11/17/23 04:51 117-81-711/15/23 07:574.2 3.1 1 Fluoranthene 1.8 U ug/L 11/17/23 04:51 206-44-011/15/23 07:574.2 1.8 1 Fluorene 1.7 U ug/L 11/17/23 04:51 86-73-711/15/23 07:574.2 1.7 1 Hexachloro-1,3-butadiene 1.5 U ug/L 11/17/23 04:51 87-68-311/15/23 07:574.2 1.5 1 Hexachlorobenzene 1.8 U ug/L 11/17/23 04:51 118-74-111/15/23 07:574.2 1.8 1 Hexachlorocyclopentadiene 1.3 U ug/L 11/17/23 04:51 77-47-411/15/23 07:578.3 1.3 1 Hexachloroethane 1.2 U ug/L 11/17/23 04:51 67-72-111/15/23 07:574.2 1.2 1 Indeno(1,2,3-cd)pyrene 2.4 U ug/L 11/17/23 04:51 193-39-511/15/23 07:574.2 2.4 1 Isophorone 1.4 U ug/L 11/17/23 04:51 78-59-111/15/23 07:578.3 1.4 1 2-Methylphenol(o-Cresol) 1.6 U ug/L 11/17/23 04:51 95-48-711/15/23 07:574.2 1.6 1 3&4-Methylphenol(m&p Cresol) 1.0 U ug/L 11/17/23 04:51 15831-10-411/15/23 07:578.3 1.0 1 Naphthalene 1.7 U ug/L 11/17/23 04:51 91-20-311/15/23 07:574.2 1.7 1 Nitrobenzene 1.6 U ug/L 11/17/23 04:51 98-95-311/15/23 07:574.2 1.6 1 2-Nitrophenol 1.2 U ug/L 11/17/23 04:51 88-75-511/15/23 07:574.2 1.2 1 4-Nitrophenol 5.5 U ug/L 11/17/23 04:51 100-02-711/15/23 07:578.3 5.5 1 N-Nitrosodimethylamine 1.6 U ug/L 11/17/23 04:51 62-75-911/15/23 07:574.2 1.6 1 N-Nitroso-di-n-propylamine 1.1 U ug/L 11/17/23 04:51 621-64-711/15/23 07:574.2 1.1 1 N-Nitrosodiphenylamine 2.5 U ug/L 11/17/23 04:51 86-30-611/15/23 07:578.3 2.5 1 2,2'-Oxybis(1-chloropropane) 0.96 U ug/L 11/17/23 04:51 108-60-111/15/23 07:574.2 0.96 1 Pentachlorophenol 3.1 U ug/L 11/17/23 04:51 87-86-511/15/23 07:578.3 3.1 1 Phenanthrene 1.7 U ug/L 11/17/23 04:51 85-01-811/15/23 07:574.2 1.7 1 Phenol 1.1 U ug/L 11/17/23 04:51 108-95-211/15/23 07:574.2 1.1 1 Pyrene 1.8 U ug/L 11/17/23 04:51 129-00-0 J(L1)11/15/23 07:574.2 1.8 1 1,2,4-Trichlorobenzene 1.4 U ug/L 11/17/23 04:51 120-82-111/15/23 07:574.2 1.4 1 2,4,6-Trichlorophenol 1.3 U ug/L 11/17/23 04:51 88-06-211/15/23 07:578.3 1.3 1 Surrogates Nitrobenzene-d5 (S) 75 % 11/17/23 04:51 4165-60-011/15/23 07:5710-120 1 2-Fluorobiphenyl (S) 75 % 11/17/23 04:51 321-60-811/15/23 07:5715-120 1 Terphenyl-d14 (S) 103 % 11/17/23 04:51 1718-51-011/15/23 07:5711-131 1 Phenol-d6 (S) 47 % 11/17/23 04:51 13127-88-311/15/23 07:5710-120 1 2-Fluorophenol (S) 68 % 11/17/23 04:51 367-12-411/15/23 07:5710-120 1 2,4,6-Tribromophenol (S) 103 % 11/17/23 04:51 118-79-611/15/23 07:5710-137 1
Analytical Method: EPA 624.1 Pace Analytical Services - Ormond Beach
624.1 Volatile Organics Unpres
Benzene 0.30 U ug/L 11/14/23 16:02 71-43-21.0 0.30 1 Bromodichloromethane 0.19 U ug/L 11/14/23 16:02 75-27-41.0 0.19 1 Bromoform 0.48 U ug/L 11/14/23 16:02 75-25-23.0 0.48 1 Bromomethane 3.9 U ug/L 11/14/23 16:02 74-83-910.0 3.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 12/06/2023 04:57 PM
Pace Analytical Services, LLC 8 East Tower Circle
Ormond Beach, FL 32174
Pace Project No.:
Project:
35840909 Davis LF PWs
Sample: DPW-DUP Lab ID: 35840909003 Collected: 11/09/23 10:55 Received: 11/10/23 12:22 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLPQL
Analytical Method: EPA 624.1 Pace Analytical Services - Ormond Beach
624.1 Volatile Organics Unpres
Carbon tetrachloride 0.44 U ug/L 11/14/23 16:02 56-23-53.0 0.44 1 Chlorobenzene 0.35 U ug/L 11/14/23 16:02 108-90-71.0 0.35 1 Chloroethane 3.7 U ug/L 11/14/23 16:02 75-00-310.0 3.7 1 2-Chloroethylvinyl ether 6.1 U ug/L 11/14/23 16:02 110-75-840.0 6.1 1 Chloroform 0.56 U ug/L 11/14/23 16:02 67-66-31.0 0.56 1 Chloromethane 0.43 U ug/L 11/14/23 16:02 74-87-31.0 0.43 1 Dibromochloromethane 0.45 U ug/L 11/14/23 16:02 124-48-12.0 0.45 1 1,2-Dichlorobenzene 0.60 U ug/L 11/14/23 16:02 95-50-11.0 0.60 1 1,3-Dichlorobenzene 0.33 U ug/L 11/14/23 16:02 541-73-11.0 0.33 1 1,4-Dichlorobenzene 0.28 U ug/L 11/14/23 16:02 106-46-71.0 0.28 1 1,1-Dichloroethane 0.75 I ug/L 11/14/23 16:02 75-34-31.0 0.34 1 1,2-Dichloroethane 0.27 U ug/L 11/14/23 16:02 107-06-21.0 0.27 1 1,1-Dichloroethene 2.9 ug/L 11/14/23 16:02 75-35-41.0 0.59 1 trans-1,2-Dichloroethene 0.23 U ug/L 11/14/23 16:02 156-60-51.0 0.23 1 1,2-Dichloropropane 0.23 U ug/L 11/14/23 16:02 78-87-51.0 0.23 1 cis-1,3-Dichloropropene 0.17 U ug/L 11/14/23 16:02 10061-01-51.0 0.17 1 trans-1,3-Dichloropropene 0.37 U ug/L 11/14/23 16:02 10061-02-61.0 0.37 1 Ethylbenzene 0.30 U ug/L 11/14/23 16:02 100-41-41.0 0.30 1 Methylene Chloride 1.7 U ug/L 11/14/23 16:02 75-09-25.0 1.7 1 1,1,2,2-Tetrachloroethane 0.59 U ug/L 11/14/23 16:02 79-34-51.0 0.59 1 Tetrachloroethene 0.38 U ug/L 11/14/23 16:02 127-18-41.0 0.38 1 Toluene 0.33 U ug/L 11/14/23 16:02 108-88-31.0 0.33 1 1,1,1-Trichloroethane 0.30 U ug/L 11/14/23 16:02 71-55-61.0 0.30 1 1,1,2-Trichloroethane 0.30 U ug/L 11/14/23 16:02 79-00-51.0 0.30 1 Trichloroethene 0.36 U ug/L 11/14/23 16:02 79-01-61.0 0.36 1 Trichlorofluoromethane 0.72 U ug/L 11/14/23 16:02 75-69-41.0 0.72 1 Vinyl chloride 0.39 U ug/L 11/14/23 16:02 75-01-41.0 0.39 1 Surrogates 1,2-Dichlorobenzene-d4 (S) 100 % 11/14/23 16:02 2199-69-160-140 1 4-Bromofluorobenzene (S) 99 % 11/14/23 16:02 460-00-460-140 1 Toluene-d8 (S) 99 % 11/14/23 16:02 2037-26-560-140 1
Analytical Method: SM 2320B Pace Analytical Services - Ormond Beach
2320B Alkalinity
Alkalinity, Total as CaCO3 116 mg/L 11/18/23 22:215.0 5.0 1
Analytical Method: SM 2540C Pace Analytical Services - Ormond Beach
2540C Total Dissolved Solids
Total Dissolved Solids 170 mg/L 11/13/23 21:305.0 5.0 1
Analytical Method: EPA 300.0 Pace Analytical Services - Ormond Beach
300.0 IC Anions 28 Days
Chloride 11.8 mg/L 11/29/23 18:23 16887-00-65.0 2.5 1 Sulfate 6.8 mg/L 11/29/23 18:23 14808-79-8 J(M1)5.0 2.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 12/06/2023 04:57 PM
Pace Analytical Services, LLC 8 East Tower Circle
Ormond Beach, FL 32174
Pace Project No.:
Project:
35840909 Davis LF PWs
Sample: DPW-DUP Lab ID: 35840909003 Collected: 11/09/23 10:55 Received: 11/10/23 12:22 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLPQL
Analytical Method: EPA 350.1 Pace Analytical Services - Ormond Beach
350.1 Ammonia
Nitrogen, Ammonia 0.24 mg/L 11/12/23 19:32 7664-41-70.050 0.035 1
Analytical Method: EPA 353.2 Pace Analytical Services - Ormond Beach
353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate 1.1 mg/L 11/10/23 21:54 14797-55-80.050 0.025 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 12/06/2023 04:57 PM
Pace Analytical Services, LLC 8 East Tower Circle
Ormond Beach, FL 32174
Pace Project No.:
Project:
35840909 Davis LF PWs
Sample: DPW-435 Lab ID: 35840909004 Collected: 11/09/23 11:35 Received: 11/10/23 12:22 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLPQL
Analytical Method:
Pace Analytical Services - Ormond Beach
Field Data
Field pH 7.16 Std. Units 11/09/23 11:351 Field Temperature 19.1 deg C 11/09/23 11:351 Field Specific Conductance 503 umhos/cm 11/09/23 11:351 Oxygen, Dissolved 9.10 mg/L 11/09/23 11:35 7782-44-71 REDOX -109.00 mV 11/09/23 11:351 Turbidity 1.6 NTU 11/09/23 11:351
Analytical Method: EPA 6010 Preparation Method: EPA 3010 Pace Analytical Services - Ormond Beach
6010 MET ICP
Cadmium 0.33 U ug/L 11/27/23 01:18 7440-43-911/21/23 09:451.0 0.33 1 Calcium 75300 ug/L 11/27/23 01:18 7440-70-211/21/23 09:45500 190 1 Chromium 1.7 U ug/L 11/27/23 01:18 7440-47-311/21/23 09:455.0 1.7 1 Iron 2290 ug/L 11/27/23 01:18 7439-89-611/21/23 09:4540.0 25.0 1 Lead 2.1 U ug/L 11/27/23 01:18 7439-92-111/21/23 09:4510.0 2.1 1 Magnesium 15300 ug/L 11/27/23 01:18 7439-95-411/21/23 09:45500 84.0 1 Manganese 155 ug/L 11/27/23 01:18 7439-96-511/21/23 09:455.0 1.1 1 Potassium 1320 ug/L 11/27/23 01:18 7440-09-711/21/23 09:451000 270 1 Sodium 14.3 mg/L 11/27/23 01:18 7440-23-511/21/23 09:452.0 0.54 1 Zinc 486 ug/L 11/27/23 01:18 7440-66-611/21/23 09:4520.0 11.0 1
Analytical Method: EPA 6020 Preparation Method: EPA 3010 Pace Analytical Services - Ormond Beach
6020 MET ICPMS
Arsenic 3.3 ug/L 11/21/23 18:55 7440-38-211/21/23 09:451.0 0.50 1
Analytical Method: EPA 7470 Preparation Method: EPA 7470 Pace Analytical Services - Ormond Beach
7470 Mercury
Mercury 0.14 U ug/L 12/04/23 14:12 7439-97-611/29/23 13:440.20 0.14 1
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1 Pace Analytical Services - Charlotte
625 RVE
Acenaphthene 1.7 U ug/L 11/17/23 05:16 83-32-911/15/23 07:574.2 1.7 1 Acenaphthylene 1.6 U ug/L 11/17/23 05:16 208-96-811/15/23 07:574.2 1.6 1 Anthracene 1.9 U ug/L 11/17/23 05:16 120-12-711/15/23 07:574.2 1.9 1 Benzidine 11.2 U ug/L 11/17/23 05:16 92-87-511/15/23 07:5741.7 11.2 1 Benzo(a)anthracene 2.2 U ug/L 11/17/23 05:16 56-55-311/15/23 07:574.2 2.2 1 Benzo(a)pyrene 2.3 U ug/L 11/17/23 05:16 50-32-811/15/23 07:574.2 2.3 1 Benzo(b)fluoranthene 2.2 U ug/L 11/17/23 05:16 205-99-211/15/23 07:574.2 2.2 1 Benzo(g,h,i)perylene 2.4 U ug/L 11/17/23 05:16 191-24-211/15/23 07:574.2 2.4 1 Benzo(k)fluoranthene 2.3 U ug/L 11/17/23 05:16 207-08-911/15/23 07:574.2 2.3 1 4-Bromophenylphenyl ether 1.5 U ug/L 11/17/23 05:16 101-55-311/15/23 07:574.2 1.5 1 Butylbenzylphthalate 2.6 U ug/L 11/17/23 05:16 85-68-711/15/23 07:574.2 2.6 1 bis(2-Chloroethoxy)methane 1.5 U ug/L 11/17/23 05:16 111-91-111/15/23 07:578.3 1.5 1 bis(2-Chloroethyl) ether 1.6 U ug/L 11/17/23 05:16 111-44-411/15/23 07:574.2 1.6 1 2-Chloronaphthalene 1.4 U ug/L 11/17/23 05:16 91-58-711/15/23 07:574.2 1.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 12/06/2023 04:57 PM
Pace Analytical Services, LLC 8 East Tower Circle
Ormond Beach, FL 32174
Pace Project No.:
Project:
35840909 Davis LF PWs
Sample: DPW-435 Lab ID: 35840909004 Collected: 11/09/23 11:35 Received:…
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