Appendix B - Environmental Sampling Report.pdf
PDF 2 MB Posted
- Solicitation number
- W912DS26BA020
About this file
This is an Environmental Sampling Report from ALS Environmental for analytical testing services performed on samples submitted on May 20, 2026, under Service Request No. K2605119 for Project No. 40-3458226. The report documents comprehensive per- and polyfluoroalkyl substances (PFAS) analysis conducted on eight samples consisting of sludge, solid, and groundwater matrices collected on May 12, 2026, and received at the laboratory on May 20, 2026. Analyses were performed according to NELAP-approved quality assurance protocols using Method 1633 by LC/MS/MS, with results reported as of June 12, 2026. The laboratory is NELAP-accredited in multiple states and holds certifications from regulatory bodies including Washington Department of Ecology (C544), California Water Resources Board, Florida Department of Health, Texas Commission on Environmental Quality, and others.
The analytical results indicate detected PFAS contamination in groundwater samples, with Perfluorooctane Sulfonic Acid (PFOS) ranging from 1.0 to 15 ng/L across samples, and Perfluorooctanoic Acid (PFOA) detected at 3.3 to 17 ng/L. Sludge and solid samples contained higher concentrations, with PFOS at 0.59 to 5.9 ng/g and PFOA at 0.046 to 0.46 ng/g on a dry weight basis. Several carboxylic acids and sulfonic acids were detected below quantitation limits (marked as "J" for estimated values). Suspended solids testing of groundwater samples showed results ranging from 100 to 120 mg/L. All quality control measures, including surrogate recovery percentages, method blanks, and lab control samples, met or fell within acceptable control limits as specified in the NELAP standards. Manual integration of chromatographic peaks was performed consistent with established protocols; one calibration verification exceeded upper control criteria but did not affect field sample data quality.
View the file
Other files
Show all 12
On GovTribe
Work with this file
- Download the original file
- Contacts named in this file
- Similar government files
- Ask GovTribe AI about this file
Text version
June 12, 2026 Analytical Report for Service Request No: K2605119
Dereck Ciecierski ALS Environmental - Middletown 301 Fulling Mill Road Middletown, PA 17057
Analyses were performed according to our laboratory’s NELAP-approved quality assurance program.
The test results meet requirements of the current NELAP standards, where applicable, and except as noted in the laboratory case narrative provided. For a specific list of NELAP-accredited analytes, refer to the certifications section at www.alsglobal.com. All results are intended to be considered in their entirety, and ALS Group USA Corp. dba ALS Environmental (ALS) is not responsible for use of less than the complete report. Results apply only to the items submitted to the laboratory for analysis and individual items (samples) analyzed, as listed in the report.
For your reference, these analyses have been assigned our service request number Enclosed are the results of the sample(s) submitted to our laboratory May 20, 2026
RE: 40-3458226
Dear Dereck, K2605119.
Please contact me if you have any questions. My extension is 3301. You may also contact me via email at Naomi.Pedersen@alsglobal.com.
Respectfully submitted, ALS Group USA, Corp. dba ALS Environmental
Naomi Pedersen Project Manager
ALS Group USA, Corp 1317 South 13th Avenue Kelso, WA 98626
+1 360 577 7222 +1 360 636 1068
T :
F :
ALS Environmental www.alsglobal.com
RIGHT SOLUTIONS | RIGHT PARTNER
www.alsglobal.com
ALS Environmental
F :
T :
+1 360 636 1068 +1 360 577 7222
Kelso, WA 98626 1317 South 13th Avenue ALS Group USA, Corp
Table of Contents
RIGHT SOLUTIONS | RIGHT PARTNER
Acronyms
Qualifiers
State Certifications, Accreditations, And Licenses
Case Narrative
Chain of Custody
Total Solids
General Chemistry
Per- and Polyfluoroalkyl Substances (PFAS) by LCMSMS
ASTM American Society for Testing and Materials
A2LA American Association for Laboratory Accreditation
CARB California Air Resources Board
CAS Number Chemical Abstract Service registry Number
CFC Chlorofluorocarbon
CFU Colony-Forming Unit
DEC Department of Environmental Conservation
DEQ Department of Environmental Quality
DHS Department of Health Services
DOE Department of Ecology
DOH Department of Health
EPA U. S. Environmental Protection Agency
ELAP Environmental Laboratory Accreditation Program
GC Gas Chromatography
GC/MS Gas Chromatography/Mass Spectrometry
LOD Limit of Detection
LOQ Limit of Quantitation
LUFT Leaking Underground Fuel Tank
M Modified MCL Maximum Contaminant Level is the highest permissible concentration of a substance allowed in drinking water as established by the USEPA.
MDL Method Detection Limit
MPN Most Probable Number
MRL Method Reporting Limit
NA Not Applicable
NC Not Calculated
NCASI National Council of the Paper Industry for Air and Stream Improvement
ND Not Detected
NIOSH National Institute for Occupational Safety and Health
PQL Practical Quantitation Limit
RCRA Resource Conservation and Recovery Act
SIM Selected Ion Monitoring
TPH Total Petroleum Hydrocarbons tr Trace level is the concentration of an analyte that is less than the PQL but greater than or equal to the MDL.
Acronyms
Inorganic Data Qualifiers
* The result is an outlier. See case narrative.
# The control limit criteria is not applicable.
B The analyte was found in the associated method blank at a level that is significant relative to the sample result as defined by the DOD or NELAC standards.
E The result is an estimate amount because the value exceeded the instrument calibration range.
J The result is an estimated value.
U The analyte was analyzed for, but was not detected ("Non-detect") at or above the MRL/MDL.
DOD-QSM 4.2 definition : Analyte was not detected and is reported as less than the LOD or as defined by the project. The detection limit is adjusted for dilution.
i The MRL/MDL or LOQ/LOD is elevated due to a matrix interference.
X See case narrative.
Q See case narrative. One or more quality control criteria was outside the limits.
H The holding time for this test is immediately following sample collection. The samples were analyzed as soon as possible after receipt by the laboratory.
Metals Data Qualifiers # The control limit criteria is not applicable.
J The result is an estimated value.
E The percent difference for the serial dilution was greater than 10%, indicating a possible matrix interference in the sample.
M The duplicate injection precision was not met.
N The Matrix Spike sample recovery is not within control limits. See case narrative.
S The reported value was determined by the Method of Standard Additions (MSA).
U The analyte was analyzed for, but was not detected ("Non-detect") at or above the MRL/MDL.
DOD-QSM 4.2 definition : Analyte was not detected and is reported as less than the LOD or as defined by the project. The detection limit is adjusted for dilution.
W The post-digestion spike for furnace AA analysis is out of control limits, while sample absorbance is less than 50% of spike absorbance.
i The MRL/MDL or LOQ/LOD is elevated due to a matrix interference.
X See case narrative.
+ The correlation coefficient for the MSA is less than 0.995.
Q See case narrative. One or more quality control criteria was outside the limits.
Organic Data Qualifiers
* The result is an outlier. See case narrative.
# The control limit criteria is not applicable. See case narrative.
A A tentatively identified compound, a suspected aldol-condensation product.
B The analyte was found in the associated method blank at a level that is significant relative to the sample result as defined by the DOD or NELAC standards.
C The analyte was qualitatively confirmed using GC/MS techniques, pattern recognition, or by comparing to historical data.
D The reported result is from a dilution.
E The result is an estimated value.
J The result is an estimated value.
N The result is presumptive. The analyte was tentatively identified, but a confirmation analysis was not performed.
P The GC or HPLC confirmation criteria was exceeded. The relative percent difference is greater than 40% between the two analytical results.
U The analyte was analyzed for, but was not detected ("Non-detect") at or above the MRL/MDL.
DOD-QSM 4.2 definition : Analyte was not detected and is reported as less than the LOD or as defined by the project. The detection limit is adjusted for dilution.
i The MRL/MDL or LOQ/LOD is elevated due to a chromatographic interference.
X See case narrative.
Q See case narrative. One or more quality control criteria was outside the limits.
Additional Petroleum Hydrocarbon Specific Qualifiers
F The chromatographic fingerprint of the sample matches the elution pattern of the calibration standard.
L The chromatographic fingerprint of the sample resembles a petroleum product, but the elution pattern indicates the presence of a greater amount of lighter molecular weight constituents than the calibration standard.
H The chromatographic fingerprint of the sample resembles a petroleum product, but the elution pattern indicates the presence of a greater amount of heavier molecular weight constituents than the calibration standard.
O The chromatographic fingerprint of the sample resembles an oil, but does not match the calibration standard.
Y The chromatographic fingerprint of the sample resembles a petroleum product eluting in approximately the correct carbon range, but the elution pattern does not match the calibration standard.
Z The chromatographic fingerprint does not resemble a petroleum product.
ALS Group USA Corp. dba ALS Environmental (ALS) - Kelso State Certifications, Accreditations, and Licenses
Agency Website Number
Alaska DEC https://dec.alaska.gov/spar/csp/lab-approval/ 17-004
Arizona DHS https://www.azdhs.gov/preparedness/state-laboratory/lab-licensure-certification/index.php
AZ0339
Arkansas DEQ https://www.adeq.state.ar.us/techsvs/lab_cert/ 88-00637
California WB (ELAP) https://www.waterboards.ca.gov/drinking_water/certlic/labs/index.html 2795
DOD ELAP https://www.denix.osd.mil/edqw/accreditation/accreditedlabs/ 65188
Florida DOH https://www.floridahealth.gov/licensing-regulations/regulated-facilities/environmental-laboratories/
E87412
ISO 17025 https://www.pjlabs.com/ 65188
Louisiana DEQ https://www.deq.louisiana.gov/page/la-lab-accreditation 03016
Maine DHHS https://www.maine.gov/dhhs/mecdc/services/business-services/laboratory-accreditation
WA01276
Minnesota DOH https://www.health.state.mn.us/communities/environment/mnelap 053-999-457
Nevada DEP https://ndep.nv.gov/water/lab-certification WA01276
New Jersey DEP https://dep.nj.gov/dsr/oqa/certified-laboratories/ WA005
New York DOH https://www.wadsworth.org/regulatory/elap 12060
North Carolina DEQ https://www.deq.nc.gov/about/divisions/water-resources/water-sciences/chemistry-laboratory/laboratory-certification-branch/non-field-lab-certification
WA01276
Ohio EPA https://epa.ohio.gov/divisions-and-offices/drinking-and-ground-waters 87776
Oregon DEQ (NELAP) https://www.oregon.gov/oha/PH/LaboratoryServices/ EnvironmentalLaboratoryAccreditation/Pages/index.aspx
WA100010
South Carolina DES https://des.sc.gov/permits-regulations/laws-regulations-regulatory-updates/environmental-regulations/environmental-laboratory-certification
61002
Texas CEQ https://www.tceq.texas.gov/agency/qa/env_lab_accreditation.html T104704427
Washington DOE https://ecology.wa.gov/regulations-permits/permits-certifications/laboratory-accreditation
C544
ALS Solutions https://solutions.alsglobal.com/ NA Analyses were performed in accordance with our laboratory’s NELAP‑approved Quality Assurance Program. A complete listing of NELAP and other certified analytes is available in ALS Solutions. For initial access to ALS Solutions, please contact your ALS Project Manager. If samples are submitted for compliance purposes, please consult the applicable certification and/or accreditation body’s website. States highlighted above require that the specific method/analyte be included on the state certification when used for compliance purposes and when that method/analyte is offered by the state.
https://dec.alaska.gov/spar/csp/lab-approval/ https://www.azdhs.gov/preparedness/state-laboratory/lab-licensure-certification/index.php https://www.azdhs.gov/preparedness/state-laboratory/lab-licensure-certification/index.php https://www.adeq.state.ar.us/techsvs/lab_cert/ https://www.waterboards.ca.gov/drinking_water/certlic/labs/index.html https://www.denix.osd.mil/edqw/accreditation/accreditedlabs/ https://www.floridahealth.gov/licensing-regulations/regulated-facilities/environmental-laboratories/ https://www.floridahealth.gov/licensing-regulations/regulated-facilities/environmental-laboratories/ https://www.pjlabs.com/ https://www.deq.louisiana.gov/page/la-lab-accreditation https://www.maine.gov/dhhs/mecdc/services/business-services/laboratory-accreditation https://www.maine.gov/dhhs/mecdc/services/business-services/laboratory-accreditation https://www.health.state.mn.us/communities/environment/mnelap https://ndep.nv.gov/water/lab-certification https://dep.nj.gov/dsr/oqa/certified-laboratories/ https://www.wadsworth.org/regulatory/elap https://www.deq.nc.gov/about/divisions/water-resources/water-sciences/chemistry-laboratory/laboratory-certification-branch/non-field-lab-certification https://www.deq.nc.gov/about/divisions/water-resources/water-sciences/chemistry-laboratory/laboratory-certification-branch/non-field-lab-certification https://www.deq.nc.gov/about/divisions/water-resources/water-sciences/chemistry-laboratory/laboratory-certification-branch/non-field-lab-certification https://epa.ohio.gov/divisions-and-offices/drinking-and-ground-waters https://www.oregon.gov/oha/PH/LaboratoryServices/EnvironmentalLaboratoryAccreditation/Pages/index.aspx https://www.oregon.gov/oha/PH/LaboratoryServices/EnvironmentalLaboratoryAccreditation/Pages/index.aspx https://des.sc.gov/permits-regulations/laws-regulations-regulatory-updates/environmental-regulations/environmental-laboratory-certification https://des.sc.gov/permits-regulations/laws-regulations-regulatory-updates/environmental-regulations/environmental-laboratory-certification https://www.tceq.texas.gov/agency/qa/env_lab_accreditation.html https://ecology.wa.gov/regulations-permits/permits-certifications/laboratory-accreditation https://ecology.wa.gov/regulations-permits/permits-certifications/laboratory-accreditation https://solutions.alsglobal.com/
Case Narrative
ALS Environmental—Kelso Laboratory 1317 South 13th Avenue, Kelso, WA 98626 Phone (360)577-7222 Fax (360)636-1068 www.alsglobal.com
Client:
Project:
Sample Matrix:
Service Request:
Date Received:
ALS Environmental - Middletown
Sludge, Solid, Ground Water
K2605119 05/20/2026
CASE NARRATIVE
All analyses were performed consistent with the quality assurance program of ALS Environmental. This report contains analytical results for samples for the Tier level II requested by the client.
Sample Receipt:
Eight sludge, solid, ground water samples were received for analysis at ALS Environmental on 05/20/2026. Any discrepancies upon initial sample inspection are annotated on the sample receipt and preservation form included within this report. The samples were stored at minimum in accordance with the analytical method requirements.
General Chemistry:
No significant anomalies were noted with this analysis.
Organic LC:
Method 1633final, 06/10/2026:The upper control criterion was exceeded for 11-Chloroeicosafluoro-3-oxaundecane-1-sulfonic acid (11-Cl-PF3OUdS) in Continuing Calibration Verification (CCV) KQ2609462-09. The field samples analyzed in this sequence did not contain the analyte in question. Since the apparent problem indicated a potential high bias, the data quality was not affected. No further corrective action was required.
Method 1633final, 06/10/2026:Manual integration of one or more chromatographic peaks in several samples was required to correct the integration performed by the automated data processing program. The manual integration was performed in accordance with ALS policy, which is consistent with the National Environmental Laboratory Accreditation Program (NELAP), Department of Defense (DOD), and other certifying agencies. Refer to the raw data for the compounds impacted by the manual integration.
1317 South 13th Ave, Kelso, WA 98626 | 1-360-577-7222 | www.alsglobal.com
Approved by Date 06/12/2026
Chain of Custody
1317 South 13th Avenue, Kelso, WA 98626 Phone (360)577-7222 Fax (360)636-1068 www.alsglobal.com
A 301 '""'"' MW Rd CHAIN OF CUSTODY/ J:;' f {_1 /41 I 4 I ~i~1d~~~~;~si4~ 17057 REQUEST FOR ANALYSIS '!IIT:ll:'!Wr:r ~ ~,5« 1 • of F.717-944-1430 iiN• ALS Quote#:.. . ·. •. · 4
Enuiranmenl:-al
Client Name: ALS Middletown I Receipt Information (completed by Receiving Lab)
• , Container Address: 301 Fulling Mill Rd Size Cooler Temp: __ Therm ID: ____ _
Middletown, PA 1705,7 Preservative UNP No.of Coolers: __ _ y
Contact: Dereck Ciecierski ANALYSES/METHOD REQUESTED
Phone#: 717-944-5541 Project Name/#: 40-3458226 .,,.
Bill To: ALS Middletown
TAT []]Normal-Standard TAT is 10-12 business days.
□Rush-Subject to ALS approval and surcharges.
v~ •1 I I I I I I I I ~ w I
C I
Custody Seals Present? I--
(if present) Seals Intact? I--
Received on Ice?
I--
CCC/Labels Complete/Accurate?
I--
Cont. in Good Cond.?
I--
Correct Containers?
I--
Correct Sample Volumes?
I--
Correct Preservation? Email? L!J·Y NAMU I ;::iUbcontract(a)AL::it:ilobal.COIJI I I ~·· . . . . . -r-, V ··~. I I ~ I I I I I !? I I--
<T)
I ~ ~ HeadspaceNolatiles?
~ ~ Courier/Tracking#: 1--c:i
N
Sample/C0C Comments
MW702-12052026 5/12/2026 I 11:40 I G IGW 3 3458226001 - .,..
MW701-12052026 5/1212026 I 12:03 I G IGW 3 3458226002
MW301-1205W26 5/1212026 I 12:35 I G IGW 3458226003
MW601-12052026 5/1212026 I 13:06 I G IGW 3458226004
MW602-12052026 5/1212026 I 13.;28 I G IGW 3458226005
MW201-12052026 5/1212026 13:55 G.IGW 3458226006
SS-HLLA 1-0-12 5/1212026 14:12 GIS I 3458226007 -
SS-HLLA2-O-12 .51.1212026 I 14:39 I G I S 2 3458226008
Initial
T
ALS Field Services: _Pickup _Labor _Composite Sampling _Rental Equipment _Other: __________ _
LOGGED BY(slgnature): ~ ll
~ □standard Special Processing State Samples
REVIEWED BY(signature): ~ ~ QcLP~like USAGE 0 Collected In
Date Time Received B / om an Name [!]USAGE Navy D D NY
1 □ 0NJ
3 Reportable to PADEP? Sample Disposal □ PA
5 6 YesO Lab 0 ONc 7 8 PWSID# Special □ nMo
9 10 EDDS: Format Type,
• G=Grab; C=Composite __ ''Matrix -Al=Air; DW=Drinking Water; GW=Groundwater; Ol=Oil; OL=Other Liquid; SL=Sludge-' SO=Soil; WP:Wipe; WW=Wastew_ater
ALS ENVIRONMENTAL SHIPPING ADDRESS: 34 DOGWOOD LANE, MIDDLETOWN, PA 17057 Rev 10/14
Cooler Receipt and Preservation Form
Clien1Prl.0 ~~~ W~l AJ'U . Service Request K26 .cJ):l/ L2...
PMU
Recei~~ IJ. LjY)(8~pene;510,oJQ(o By: \hM Unloaded: E:2110] ijCo By:
I. Snmples were rcccivccl vin? USPS e UPS DH!, PDX Co11ri!J1• f/1111(1 Delivel'ed
2. Snmplcs were received in: (circle) ~- ~ Envelope
}. Were euslody seals on coolers? YA Y ~ If yes, how many ;ind where? ____________ _ fl' present, were custody sen ls intncl? Y N If present, were they signed nnd dnlcd?
Other __________ _ NA y N
PM
Notified Out of temp
Tomp Blank Samole Temp IR Gun Cooler 11/COC ID/ NA Indicate with "X" If out of tomP Tracklm1 Number NA rJ.~ ti>Cl1- YL19:: \L\f)ILDLA C t\
4. W;is n Tempernturc Glnnk present in cooler? NA Y ~ lt'yes, notate lhe lempernture in lhc npproprintc column below:
11'110, Inkc the tcmpcrntmc ofn representative sillnplc bottle contnined within tl1c cooler; notntc in the col11mn "Snmplc Temp",Q
5. Were snmplcs received within the method specified tcmpcrnllll'C rnngcs? ~ Y lfno, were they rcccivccl on ice ond snrnc dny ns collected? [fnot, notate the cooler I/ below nnd notify the PM. ~, Y
N
N
Ir nppl_ienblc, tissue snmplcs were rec ·vcd: Fl'oten Pr11•t/11/ly Tlimvc:d Tlunvc:d .
6. Pncking mntcrinl: fll,1·e1·t.1· 1ggi11.I' fJubbfu JVmp Gel P11c:k.l' Ye Dl'y lc:e Sle11ve.1· _________ _,,.."---½----
7. Were custody pnpcrs properly 111 out (ink, signed, etc.)?
8. Were snmplcs received in good condition (unbroken)
9. Were nil snmplc lnbcls complete (ie. onolysis, prcservotion, etc.)?
I 0. Did nll sample lnbcls nnd togs ngrcc with euslody pn11crs?
11. Were npproprintc bottlcs/contnincrs ond volumes received for the tests indicntcd?
12, Were the pH-preserved bollles (sec SMO GEN SOP) received nt lhe appropriate pH? fndicMe in the table below
I J. Were V01\ vinls received without hcndspncc? Indicate in tire tabla below.
14. Wns Cl2/Rcs negntivc?
15. Were snniplcs received within method specified time limit? If not, notate the ~low nnd notify the PM.
NA
NA
NA
NA
16. Were 100ml, sterile microbiology bottles f11lcd cxnctly to the [00ml, mnrk?{ Ni Y N Underfillcd
Sample ID on Bottle Sample ID on COG Identified by:
Bottlo Count Hoad. Volumo Roagont Loi SamQfO ID Botllo TVPO SQaCe Broke l)H Roaoont added Number
Notes, Discrepancies, Resolutions:
N
N N N
N
N y N y N y N
Overfilled
Initials
~Hod
Tlmo
Q:\ENVIRONMENTAL\1 SOP & Policy Statements\SMO\CRF Update 2025-05-06.docx Updated: NP 01/07/26
Total Solids
1317 South 13th Avenue, Kelso, WA 98626 Phone (360)577-7222 Fax (360)636-1068 www.alsglobal.com
05/20/26
K2605119
Date Received:
Date Collected:
Service Request:
Sludge, Solid 40-3458226 ALS Environmental - Middletown
Sample Matrix:
Project: 05/12/26
Solids, Total
Basis:
Units: Percent
As Received
160.3 Modified
NonePrep Method:
Analysis Method:
Lab CodeSample Name Date
AnalyzedDil.MDLMRLResult Q
SS-HLLA1-O-12 05/22/26 12:161--74.8K2605119-007
SS-HLLA2-O-12 05/22/26 12:161--85.6K2605119-008
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
Printed 5/27/2026 3:36:49 PM 26-0000772926 rev 00Superset Reference:
ALS Group USA, Corp.
QA/QC Report
Client:
Project Sample Matrix: Sludge, Solid
40-3458226 ALS Environmental - Middletown Service Request: K2605119
05/12/26Date Collected:
Date Received: 05/20/26
05/22/26Date Analyzed:
Replicate Sample Summary Inorganic Parameters
SS-HLLA1-O-12 Percent Basis:
Units:
K2605119-007 As ReceivedLab Code:
Sample Name:
RPD LimitMRLAnalysis Method RPD
Duplicate Sample
K2605119-
007DUP
Result Average
Sample ResultAnalyte Name dba ALS Environmental
Solids, Total 3 - 74.8 77.2 76.0 20160.3 Modified
Results flagged with an asterisk (*) indicate values outside control criteria.
Results flagged with a pound (#) indicate the control criteria is not applicable.
Percent recoveries and relative percent differences (RPD) are determined by the software using values in the calculation which have not been rounded.
Printed 5/27/2026 3:36:49 PM 26-0000772926 rev 00Superset Reference:
General Chemistry
1317 South 13th Avenue, Kelso, WA 98626 Phone (360)577-7222 Fax (360)636-1068 www.alsglobal.com
05/20/26
K2605119
Date Received:
Date Collected:
Service Request:
Ground Water 40-3458226 ALS Environmental - Middletown
Sample Matrix:
Project: 05/12/26
Solids, Total Suspended (TSS)
Basis:
Units: mg/L
NA
SM 2540 D Modified NonePrep Method:
Analysis Method:
Lab CodeSample Name LOD Date
AnalyzedDil.MDLLOQResult Q
MW702-12052026 05/26/26 14:411--100120K2605119-001
MW701-12052026 06/01/26 15:521--100 UNDK2605119-002
MW201-12052026 05/26/26 14:411--100 UNDK2605119-006
Method Blank 05/26/26 14:411--100 UNDK2605119-MB1 Method Blank 05/26/26 14:411--100 UNDK2605119-MB2 Method Blank 06/01/26 15:521--100 UNDK2605119-MB3 Method Blank 06/01/26 15:521--100 UNDK2605119-MB4
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
Printed 6/2/2026 5:11:50 PM 26-0000772926 rev 00Superset Reference:
Per and Polyfluoroalkyl Substances
(PFAS) by LC/MS/MS
ALS Environmental—Kelso Laboratory
1317 South 13th Avenue, Kelso, WA 98626
Phone (360)577-7222 Fax (360)636-1068 www.alsglobal.com
K2605119-001Lab Code:
Sample Name: MW702-12052026
Per- and Polyfluoroalkyl Substances (PFAS) by LC/MS/MS
05/12/26 11:40
NA
ng/L
Basis:
Units:
1633Analysis Method:
MethodPrep Method:
05/20/26 10:45
K2605119
Date Received:
Date Collected:
Service Request:
Ground Water
ALS Environmental - Middletown
Sample Matrix:
Project:
Client:
Analyte Name LOD QDate Analyzed Date
ExtractedDil.MDLLOQResult
Perfluoroalkyl Sulfonic Acids (PFSAs) 4.1Perfluorobutane sulfonic acid (PFBS) 0.840.89 1 06/09/26 04:16 6/8/261.7 3.4Perfluoropentane sulfonic acid (PFPeS) 0.500.94 1 06/09/26 04:16 6/8/261.7 35Perfluorohexane sulfonic acid (PFHxS) 0.530.91 1 06/09/26 04:16 6/8/261.7
NDPerfluoroheptane sulfonic acid (PFHpS) 0.500.95 1 06/09/26 04:16 6/8/261.7 U 1.4Perfluorooctane sulfonic acid (PFOS) 0.500.93 1 06/09/26 04:16 6/8/261.7 J NDPerfluorononane sulfonic acid (PFNS) 0.500.96 1 06/09/26 04:16 6/8/261.7 U NDPerfluorodecane sulfonic acid (PFDS) 0.500.97 1 06/09/26 04:16 6/8/261.7 U NDPerfluorododecane sulfonic acid (PFDoS) 0.500.97 1 06/09/26 04:16 6/8/261.7 U
Perfluoroalkyl Carboxylic Acids (PFCAs) 6.1Perfluorobutanoic acid (PFBA) 1.32.0 1 06/09/26 04:16 6/8/262.0 5.8Perfluoropentanoic acid (PFPeA) 0.501.0 1 06/09/26 04:16 6/8/261.7 5.0Perfluorohexanoic acid (PFHxA) 0.501.0 1 06/09/26 04:16 6/8/261.7
0.99Perfluoroheptanoic acid (PFHpA) 0.501.0 1 06/09/26 04:16 6/8/261.7 J 3.3Perfluorooctanoic acid (PFOA) 0.501.0 1 06/09/26 04:16 6/8/261.7 NDPerfluorononanoic acid (PFNA) 0.501.0 1 06/09/26 04:16 6/8/261.7 U NDPerfluorodecanoic acid (PFDA) 0.751.0 1 06/09/26 04:16 6/8/261.7 U NDPerfluoroundecanoic acid (PFUnDA) 0.501.0 1 06/09/26 04:16 6/8/261.7 U NDPerfluorododecanoic acid (PFDOA) 0.501.0 1 06/09/26 04:16 6/8/261.7 U NDPerfluorotridecanoic acid (PFTrDA) 0.701.0 1 06/09/26 04:16 6/8/261.7 U NDPerfluorotetradecanoic acid (PFTDA) 0.501.0 1 06/09/26 04:16 6/8/261.7 U
Perfluoroalkyl Sulfonamido Substances NDPerfluorooctane sulfonamide (PFOSAm) 0.501.0 1 06/09/26 04:16 6/8/261.7 U NDN-Methylperfluorooctane sulfonamide
(MeFOSA)
0.501.0 1 06/09/26 04:16 6/8/261.7 U
NDN-Ethylperfluorooctane sulfonamide (EtFOSAm)
0.501.0 1 06/09/26 04:16 6/8/261.7 U
NDN-Methylperfluorooctane sulfonamido ethanol (MeFOSE)
0.531.0 1 06/09/26 04:16 6/8/261.7 U
NDN-Ethylperfluorooctane sulfonamido ethanol (EtFOSE)
0.541.0 1 06/09/26 04:16 6/8/261.7 U
NDN-Methylperfluorooctane sulfonamido acetic acid (NMeFOSAA)
0.501.0 1 06/09/26 04:16 6/8/261.7 U
NDN-Ethylperfluorooctane sulfonamido acetic acid (NEtFOSAA)
0.611.0 1 06/09/26 04:16 6/8/261.7 U
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
Printed 6/12/2026 11:53:11 AM 26-0000772926 rev 00Superset Reference:
Per- and Polyfluoroalkyl Substances (PFAS) by LC/MS/MS
05/12/26 11:40
NA
ng/L
Basis:
Units:
1633Analysis Method:
MethodPrep Method:
05/20/26 10:45
K2605119
Date Received:
Date Collected:
Service Request:
Ground Water
ALS Environmental - Middletown
Sample Matrix:
Project:
Client:
Analyte Name LOD QDate Analyzed Date
ExtractedDil.MDLLOQResult
Fluorotelomer Sulfonic Acids (FTSAs) ND1H, 1H, 2H, 2H-Perfluorohexanesulfonic acid (4:2 FTS)
0.500.94 1 06/09/26 04:16 6/8/261.7 U
ND1H, 1H, 2H, 2H-Perfluorooctanesulfonic acid (6:2 FTS)
0.501.4 1 06/09/26 04:16 6/8/261.7 U
ND1H, 1H, 2H, 2H-Perfluorodecanesulfonic acid (8:2 FTS)
0.500.96 1 06/09/26 04:16 6/8/261.7 U
Fluorotelomer Carboxylic Acids (FTCAs) ND4,4,5,5,6,6,6-Heptafluorohexanoic acid
(3:3 FTCA)
4.210 1 06/09/26 04:16 6/8/2617 U
ND2H,2H,3H,3H-Perfluorooctanoic acid (5:3
FTCA)
8.210 1 06/09/26 04:16 6/8/2617 U
ND2H,2H,3H,3H-Perfluorodecanoic acid (7:3
FTCA)
7.010 1 06/09/26 04:16 6/8/2617 U
Perfluoroalkyl Ether Sulfonic Acids (PFESAs) NDPerfluoro(2-ethoxyethane) sulfonic acid
(PFEESA)
0.500.89 1 06/09/26 04:16 6/8/261.7 U
ND9-Chlorohexadecafluoro-3-oxanonane-1-sulfonic acid (9-Cl-PF3ONS)
0.500.93 1 06/09/26 04:16 6/8/261.7 U
ND11-Chloroeicosafluoro-3-oxaundecane-1-sulfonic acid (11-Cl-PF3OUdS)
0.500.94 1 06/09/26 04:16 6/8/261.7 U
Perfluoroalkyl Ether Carboxylic Acids (PFECAs) NDPerfluoro-3-methoxypropanoic acid
(PFMPA)
0.501.0 1 06/09/26 04:16 6/8/261.7 U
NDPerfluoro-4-methoxybutanoic acid
(PFMBA)
0.501.0 1 06/09/26 04:16 6/8/261.7 U
NDHexafluoropropyleneoxide dimer acid (HFPO-DA) (GenX)
0.501.0 1 06/09/26 04:16 6/8/261.7 U
NDNonafluoro-3,6-dioxaheptanoic acid
(NFDHA)
0.501.0 1 06/09/26 04:16 6/8/261.7 U
ND4,8-Dioxa-3H-perfluorononanoic acid
(DONA)
0.500.95 1 06/09/26 04:16 6/8/261.7 U
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
Printed 6/12/2026 11:53:12 AM 26-0000772926 rev 00Superset Reference:
Per- and Polyfluoroalkyl Substances (PFAS) by LC/MS/MS
05/12/26 11:40
NA
ng/L
Basis:
Units:
1633Analysis Method:
MethodPrep Method:
05/20/26 10:45
K2605119
Date Received:
Date Collected:
Service Request:
Ground Water
ALS Environmental - Middletown
Sample Matrix:
Project:
Client:
Surrogate Name Q% Rec Control Limits Date Analyzed
06/09/26 04:1640 - 1357913C3-PFBS
06/09/26 04:1640 - 1306913C3-PFHxS
06/09/26 04:1640 - 1306513C8-PFOS
06/09/26 04:165 - 1307613C4-PFBA
06/09/26 04:1640 - 1307413C5-PFPeA 06/09/26 04:1640 - 1307313C5-PFHxA 06/09/26 04:1640 - 1306713C4-PFHpA
06/09/26 04:1640 - 1306813C8-PFOA
06/09/26 04:1640 - 1306713C9-PFNA
06/09/26 04:1640 - 1306213C6-PFDA
06/09/26 04:1630 - 1305513C7-PFUnDA 06/09/26 04:1610 - 1305013C2-PFDoDA 06/09/26 04:1610 - 1304713C2-PFTeDA
06/09/26 04:1640 - 1305013C8-FOSA
06/09/26 04:1610 - 13051D3-MeFOSA 06/09/26 04:1610 - 13051D5-EtFOSA 06/09/26 04:1610 - 13044D7-MeFOSE 06/09/26 04:1610 - 13042D9-EtFOSE 06/09/26 04:1640 - 17051D3-MeFOSAA 06/09/26 04:1625 - 13549D5-EtFOSAA
06/09/26 04:1640 - 2007513C2-4:2 FTS
06/09/26 04:1640 - 2006913C2-6:2 FTS
06/09/26 04:1640 - 3006613C2-8:2 FTS
06/09/26 04:1640 - 1306413C3-HFPO-DA
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
K2605119-002Lab Code:
Sample Name: MW701-12052026
Per- and Polyfluoroalkyl Substances (PFAS) by LC/MS/MS
05/12/26 12:03
NA
ng/L
Basis:
Units:
1633Analysis Method:
MethodPrep Method:
05/20/26 10:45
K2605119
Date Received:
Date Collected:
Service Request:
Ground Water
ALS Environmental - Middletown
Sample Matrix:
Project:
Client:
Analyte Name LOD QDate Analyzed Date
ExtractedDil.MDLLOQResult
Perfluoroalkyl Sulfonic Acids (PFSAs) 5.6Perfluorobutane sulfonic acid (PFBS) 0.840.89 1 06/09/26 04:33 6/8/261.7 4.7Perfluoropentane sulfonic acid (PFPeS) 0.500.94 1 06/09/26 04:33 6/8/261.7 97Perfluorohexane sulfonic acid (PFHxS) 0.530.91 1 06/09/26 04:33 6/8/261.7 1.0Perfluoroheptane sulfonic acid (PFHpS) 0.500.95 1 06/09/26 04:33 6/8/261.7 J 15Perfluorooctane sulfonic acid (PFOS) 0.500.93 1 06/09/26 04:33 6/8/261.7
NDPerfluorononane sulfonic acid (PFNS) 0.500.96 1 06/09/26 04:33 6/8/261.7 U NDPerfluorodecane sulfonic acid (PFDS) 0.500.97 1 06/09/26 04:33 6/8/261.7 U NDPerfluorododecane sulfonic acid (PFDoS) 0.500.97 1 06/09/26 04:33 6/8/261.7 U
Perfluoroalkyl Carboxylic Acids (PFCAs) 18Perfluorobutanoic acid (PFBA) 1.32.0 1 06/09/26 04:33 6/8/262.0 14Perfluoropentanoic acid (PFPeA) 0.501.0 1 06/09/26 04:33 6/8/261.7 18Perfluorohexanoic acid (PFHxA) 0.501.0 1 06/09/26 04:33 6/8/261.7 3.7Perfluoroheptanoic acid (PFHpA) 0.501.0 1 06/09/26 04:33 6/8/261.7 17Perfluorooctanoic acid (PFOA) 0.501.0 1 06/09/26 04:33 6/8/261.7 1.4Perfluorononanoic acid (PFNA) 0.501.0 1 06/09/26 04:33 6/8/261.7 J NDPerfluorodecanoic acid (PFDA) 0.751.0 1 06/09/26 04:33 6/8/261.7 U NDPerfluoroundecanoic acid (PFUnDA) 0.501.0 1 06/09/26 04:33 6/8/261.7 U NDPerfluorododecanoic acid (PFDOA) 0.501.0 1 06/09/26 04:33 6/8/261.7 U NDPerfluorotridecanoic acid (PFTrDA) 0.701.0 1 06/09/26 04:33 6/8/261.7 U NDPerfluorotetradecanoic acid (PFTDA) 0.501.0 1 06/09/26 04:33 6/8/261.7 U
Perfluoroalkyl Sulfonamido Substances NDPerfluorooctane sulfonamide (PFOSAm) 0.501.0 1 06/09/26 04:33 6/8/261.7 U NDN-Methylperfluorooctane sulfonamide
(MeFOSA)
0.501.0 1 06/09/26 04:33 6/8/261.7 U
NDN-Ethylperfluorooctane sulfonamide (EtFOSAm)
0.501.0 1 06/09/26 04:33 6/8/261.7 U
NDN-Methylperfluorooctane sulfonamido ethanol (MeFOSE)
0.531.0 1 06/09/26 04:33 6/8/261.7 U
NDN-Ethylperfluorooctane sulfonamido ethanol (EtFOSE)
0.541.0 1 06/09/26 04:33 6/8/261.7 U
NDN-Methylperfluorooctane sulfonamido acetic acid (NMeFOSAA)
0.501.0 1 06/09/26 04:33 6/8/261.7 U
NDN-Ethylperfluorooctane sulfonamido acetic acid (NEtFOSAA)
0.611.0 1 06/09/26 04:33 6/8/261.7 U
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
Per- and Polyfluoroalkyl Substances (PFAS) by LC/MS/MS
05/12/26 12:03
NA
ng/L
Basis:
Units:
1633Analysis Method:
MethodPrep Method:
05/20/26 10:45
K2605119
Date Received:
Date Collected:
Service Request:
Ground Water
ALS Environmental - Middletown
Sample Matrix:
Project:
Client:
Analyte Name LOD QDate Analyzed Date
ExtractedDil.MDLLOQResult
Fluorotelomer Sulfonic Acids (FTSAs) ND1H, 1H, 2H, 2H-Perfluorohexanesulfonic acid (4:2 FTS)
0.500.94 1 06/09/26 04:33 6/8/261.7 U
ND1H, 1H, 2H, 2H-Perfluorooctanesulfonic acid (6:2 FTS)
0.501.4 1 06/09/26 04:33 6/8/261.7 U
ND1H, 1H, 2H, 2H-Perfluorodecanesulfonic acid (8:2 FTS)
0.500.96 1 06/09/26 04:33 6/8/261.7 U
Fluorotelomer Carboxylic Acids (FTCAs) ND4,4,5,5,6,6,6-Heptafluorohexanoic acid
(3:3 FTCA)
4.210 1 06/09/26 04:33 6/8/2617 U
ND2H,2H,3H,3H-Perfluorooctanoic acid (5:3
FTCA)
8.210 1 06/09/26 04:33 6/8/2617 U
ND2H,2H,3H,3H-Perfluorodecanoic acid (7:3
FTCA)
7.010 1 06/09/26 04:33 6/8/2617 U
Perfluoroalkyl Ether Sulfonic Acids (PFESAs) NDPerfluoro(2-ethoxyethane) sulfonic acid
(PFEESA)
0.500.89 1 06/09/26 04:33 6/8/261.7 U
ND9-Chlorohexadecafluoro-3-oxanonane-1-sulfonic acid (9-Cl-PF3ONS)
0.500.93 1 06/09/26 04:33 6/8/261.7 U
ND11-Chloroeicosafluoro-3-oxaundecane-1-sulfonic acid (11-Cl-PF3OUdS)
0.500.94 1 06/09/26 04:33 6/8/261.7 U
Perfluoroalkyl Ether Carboxylic Acids (PFECAs) NDPerfluoro-3-methoxypropanoic acid
(PFMPA)
0.501.0 1 06/09/26 04:33 6/8/261.7 U
NDPerfluoro-4-methoxybutanoic acid
(PFMBA)
0.501.0 1 06/09/26 04:33 6/8/261.7 U
NDHexafluoropropyleneoxide dimer acid (HFPO-DA) (GenX)
0.501.0 1 06/09/26 04:33 6/8/261.7 U
NDNonafluoro-3,6-dioxaheptanoic acid
(NFDHA)
0.501.0 1 06/09/26 04:33 6/8/261.7 U
ND4,8-Dioxa-3H-perfluorononanoic acid
(DONA)
0.500.95 1 06/09/26 04:33 6/8/261.7 U
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
Per- and Polyfluoroalkyl Substances (PFAS) by LC/MS/MS
05/12/26 12:03
NA
ng/L
Basis:
Units:
1633Analysis Method:
MethodPrep Method:
05/20/26 10:45
K2605119
Date Received:
Date Collected:
Service Request:
Ground Water
ALS Environmental - Middletown
Sample Matrix:
Project:
Client:
Surrogate Name Q% Rec Control Limits Date Analyzed
06/09/26 04:3340 - 13510213C3-PFBS
06/09/26 04:3340 - 1308813C3-PFHxS
06/09/26 04:3340 - 1309013C8-PFOS
06/09/26 04:335 - 1309713C4-PFBA
06/09/26 04:3340 - 1309013C5-PFPeA 06/09/26 04:3340 - 1309313C5-PFHxA 06/09/26 04:3340 - 1308913C4-PFHpA
06/09/26 04:3340 - 1308913C8-PFOA
06/09/26 04:3340 - 1309013C9-PFNA
06/09/26 04:3340 - 1308513C6-PFDA
06/09/26 04:3330 - 1307813C7-PFUnDA 06/09/26 04:3310 - 1307113C2-PFDoDA 06/09/26 04:3310 - 1306213C2-PFTeDA
06/09/26 04:3340 - 1306813C8-FOSA
06/09/26 04:3310 - 13070D3-MeFOSA 06/09/26 04:3310 - 13068D5-EtFOSA 06/09/26 04:3310 - 13063D7-MeFOSE 06/09/26 04:3310 - 13061D9-EtFOSE 06/09/26 04:3340 - 17070D3-MeFOSAA 06/09/26 04:3325 - 13570D5-EtFOSAA
06/09/26 04:3340 - 20010413C2-4:2 FTS
06/09/26 04:3340 - 2008713C2-6:2 FTS
06/09/26 04:3340 - 3009113C2-8:2 FTS
06/09/26 04:3340 - 1308213C3-HFPO-DA
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
K2605119-003Lab Code:
Sample Name: MW301-12052026
Per- and Polyfluoroalkyl Substances (PFAS) by LC/MS/MS
05/12/26 12:35
NA
ng/L
Basis:
Units:
1633Analysis Method:
MethodPrep Method:
05/20/26 10:45
K2605119
Date Received:
Date Collected:
Service Request:
Ground Water
ALS Environmental - Middletown
Sample Matrix:
Project:
Client:
Analyte Name LOD QDate Analyzed Date
ExtractedDil.MDLLOQResult
Perfluoroalkyl Sulfonic Acids (PFSAs) 0.85Perfluorobutane sulfonic acid (PFBS) 0.840.89 1 06/09/26 04:49 6/8/261.7 J NDPerfluoropentane sulfonic acid (PFPeS) 0.500.94 1 06/09/26 04:49 6/8/261.7 U 1.5Perfluorohexane sulfonic acid (PFHxS) 0.530.91 1 06/09/26 04:49 6/8/261.7 J NDPerfluoroheptane sulfonic acid (PFHpS) 0.500.95 1 06/09/26 04:49 6/8/261.7 U 1.6Perfluorooctane sulfonic acid (PFOS) 0.500.93 1 06/09/26 04:49 6/8/261.7 J NDPerfluorononane sulfonic acid (PFNS) 0.500.96 1 06/09/26 04:49 6/8/261.7 U NDPerfluorodecane sulfonic acid (PFDS) 0.500.97 1 06/09/26 04:49 6/8/261.7 U NDPerfluorododecane sulfonic acid (PFDoS) 0.500.97 1 06/09/26 04:49 6/8/261.7 U
Perfluoroalkyl Carboxylic Acids (PFCAs) 1.7Perfluorobutanoic acid (PFBA) 1.32.0 1 06/09/26 04:49 6/8/262.0 J 1.1Perfluoropentanoic acid (PFPeA) 0.501.0 1 06/09/26 04:49 6/8/261.7 J 1.4Perfluorohexanoic acid (PFHxA) 0.501.0 1 06/09/26 04:49 6/8/261.7 J 1.2Perfluoroheptanoic acid (PFHpA) 0.501.0 1 06/09/26 04:49 6/8/261.7 J 4.2Perfluorooctanoic acid (PFOA) 0.501.0 1 06/09/26 04:49 6/8/261.7
0.68Perfluorononanoic acid (PFNA) 0.501.0 1 06/09/26 04:49 6/8/261.7 J NDPerfluorodecanoic acid (PFDA) 0.751.0 1 06/09/26 04:49 6/8/261.7 U NDPerfluoroundecanoic acid (PFUnDA) 0.501.0 1 06/09/26 04:49 6/8/261.7 U NDPerfluorododecanoic acid (PFDOA) 0.501.0 1 06/09/26 04:49 6/8/261.7 U NDPerfluorotridecanoic acid (PFTrDA) 0.701.0 1 06/09/26 04:49 6/8/261.7 U NDPerfluorotetradecanoic acid (PFTDA) 0.501.0 1 06/09/26 04:49 6/8/261.7 U
Perfluoroalkyl Sulfonamido Substances NDPerfluorooctane sulfonamide (PFOSAm) 0.501.0 1 06/09/26 04:49 6/8/261.7 U NDN-Methylperfluorooctane sulfonamide
(MeFOSA)
0.501.0 1 06/09/26 04:49 6/8/261.7 U
NDN-Ethylperfluorooctane sulfonamide (EtFOSAm)
0.501.0 1 06/09/26 04:49 6/8/261.7 U
NDN-Methylperfluorooctane sulfonamido ethanol (MeFOSE)
0.531.0 1 06/09/26 04:49 6/8/261.7 U
NDN-Ethylperfluorooctane sulfonamido ethanol (EtFOSE)
0.541.0 1 06/09/26 04:49 6/8/261.7 U
NDN-Methylperfluorooctane sulfonamido acetic acid (NMeFOSAA)
0.501.0 1 06/09/26 04:49 6/8/261.7 U
NDN-Ethylperfluorooctane sulfonamido acetic acid (NEtFOSAA)
0.611.0 1 06/09/26 04:49 6/8/261.7 U
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
Per- and Polyfluoroalkyl Substances (PFAS) by LC/MS/MS
05/12/26 12:35
NA
ng/L
Basis:
Units:
1633Analysis Method:
MethodPrep Method:
05/20/26 10:45
K2605119
Date Received:
Date Collected:
Service Request:
Ground Water
ALS Environmental - Middletown
Sample Matrix:
Project:
Client:
Analyte Name LOD QDate Analyzed Date
ExtractedDil.MDLLOQResult
Fluorotelomer Sulfonic Acids (FTSAs) ND1H, 1H, 2H, 2H-Perfluorohexanesulfonic acid (4:2 FTS)
0.500.94 1 06/09/26 04:49 6/8/261.7 U
ND1H, 1H, 2H, 2H-Perfluorooctanesulfonic acid (6:2 FTS)
0.501.4 1 06/09/26 04:49 6/8/261.7 U
ND1H, 1H, 2H, 2H-Perfluorodecanesulfonic acid (8:2 FTS)
0.500.96 1 06/09/26 04:49 6/8/261.7 U
Fluorotelomer Carboxylic Acids (FTCAs) ND4,4,5,5,6,6,6-Heptafluorohexanoic acid
(3:3 FTCA)
4.210 1 06/09/26 04:49 6/8/2617 U
ND2H,2H,3H,3H-Perfluorooctanoic acid (5:3
FTCA)
8.210 1 06/09/26 04:49 6/8/2617 U
ND2H,2H,3H,3H-Perfluorodecanoic acid (7:3
FTCA)
7.010 1 06/09/26 04:49 6/8/2617 U
Perfluoroalkyl Ether Sulfonic Acids (PFESAs) NDPerfluoro(2-ethoxyethane) sulfonic acid
(PFEESA)
0.500.89 1 06/09/26 04:49 6/8/261.7 U
ND9-Chlorohexadecafluoro-3-oxanonane-1-sulfonic acid (9-Cl-PF3ONS)
0.500.93 1 06/09/26 04:49 6/8/261.7 U
ND11-Chloroeicosafluoro-3-oxaundecane-1-sulfonic acid (11-Cl-PF3OUdS)
0.500.94 1 06/09/26 04:49 6/8/261.7 U
Perfluoroalkyl Ether Carboxylic Acids (PFECAs) NDPerfluoro-3-methoxypropanoic acid
(PFMPA)
0.501.0 1 06/09/26 04:49 6/8/261.7 U
NDPerfluoro-4-methoxybutanoic acid
(PFMBA)
0.501.0 1 06/09/26 04:49 6/8/261.7 U
NDHexafluoropropyleneoxide dimer acid (HFPO-DA) (GenX)
0.501.0 1 06/09/26 04:49 6/8/261.7 U
NDNonafluoro-3,6-dioxaheptanoic acid
(NFDHA)
0.501.0 1 06/09/26 04:49 6/8/261.7 U
ND4,8-Dioxa-3H-perfluorononanoic acid
(DONA)
0.500.95 1 06/09/26 04:49 6/8/261.7 U
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
Per- and Polyfluoroalkyl Substances (PFAS) by LC/MS/MS
05/12/26 12:35
NA
ng/L
Basis:
Units:
1633Analysis Method:
MethodPrep Method:
05/20/26 10:45
K2605119
Date Received:
Date Collected:
Service Request:
Ground Water
ALS Environmental - Middletown
Sample Matrix:
Project:
Client:
Surrogate Name Q% Rec Control Limits Date Analyzed
06/09/26 04:4940 - 1358713C3-PFBS
06/09/26 04:4940 - 1307813C3-PFHxS
06/09/26 04:4940 - 1307513C8-PFOS
06/09/26 04:495 - 1308513C4-PFBA
06/09/26 04:4940 - 1308313C5-PFPeA 06/09/26 04:4940 - 1308213C5-PFHxA 06/09/26 04:4940 - 1307713C4-PFHpA
06/09/26 04:4940 - 1307913C8-PFOA
06/09/26 04:4940 - 1307613C9-PFNA
06/09/26 04:4940 - 1307413C6-PFDA
06/09/26 04:4930 - 1306713C7-PFUnDA 06/09/26 04:4910 - 1305913C2-PFDoDA 06/09/26 04:4910 - 1305413C2-PFTeDA
06/09/26 04:4940 - 1305813C8-FOSA
06/09/26 04:4910 - 13056D3-MeFOSA 06/09/26 04:4910 - 13057D5-EtFOSA 06/09/26 04:4910 - 13053D7-MeFOSE 06/09/26 04:4910 - 13052D9-EtFOSE 06/09/26 04:4940 - 17062D3-MeFOSAA 06/09/26 04:4925 - 13560D5-EtFOSAA
06/09/26 04:4940 - 2008113C2-4:2 FTS
06/09/26 04:4940 - 2008013C2-6:2 FTS
06/09/26 04:4940 - 3008113C2-8:2 FTS
06/09/26 04:4940 - 1307213C3-HFPO-DA
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
K2605119-004Lab Code:
Sample Name: MW601-12052026
Per- and Polyfluoroalkyl Substances (PFAS) by LC/MS/MS
05/12/26 13:06
NA
ng/L
Basis:
Units:
1633Analysis Method:
MethodPrep Method:
05/20/26 10:45
K2605119
Date Received:
Date Collected:
Service Request:
Ground Water
ALS Environmental - Middletown
Sample Matrix:
Project:
Client:
Analyte Name LOD QDate Analyzed Date
ExtractedDil.MDLLOQResult
Perfluoroalkyl Sulfonic Acids (PFSAs) 1.2Perfluorobutane sulfonic acid (PFBS) 0.840.89 1 06/09/26 05:05 6/8/261.7 J NDPerfluoropentane sulfonic acid (PFPeS) 0.500.94 1 06/09/26 05:05 6/8/261.7 U 2.0Perfluorohexane sulfonic acid (PFHxS) 0.530.91 1 06/09/26 05:05 6/8/261.7 NDPerfluoroheptane sulfonic acid (PFHpS) 0.500.95 1 06/09/26 05:05 6/8/261.7 U 2.1Perfluorooctane sulfonic acid (PFOS) 0.500.93 1 06/09/26 05:05 6/8/261.7 NDPerfluorononane sulfonic acid (PFNS) 0.500.96 1 06/09/26 05:05 6/8/261.7 U NDPerfluorodecane sulfonic acid (PFDS) 0.500.97 1 06/09/26 05:05 6/8/261.7 U NDPerfluorododecane sulfonic acid (PFDoS) 0.500.97 1 06/09/26 05:05 6/8/261.7 U
Perfluoroalkyl Carboxylic Acids (PFCAs) 2.0Perfluorobutanoic acid (PFBA) 1.32.0 1 06/09/26 05:05 6/8/262.0 1.7Perfluoropentanoic acid (PFPeA) 0.501.0 1 06/09/26 05:05 6/8/261.7 1.9Perfluorohexanoic acid (PFHxA) 0.501.0 1 06/09/26 05:05 6/8/261.7 2.0Perfluoroheptanoic acid (PFHpA) 0.501.0 1 06/09/26 05:05 6/8/261.7 7.5Perfluorooctanoic acid (PFOA) 0.501.0 1 06/09/26 05:05 6/8/261.7 1.1Perfluorononanoic acid (PFNA) 0.501.0 1 06/09/26 05:05 6/8/261.7 J NDPerfluorodecanoic acid (PFDA) 0.751.0 1 06/09/26 05:05 6/8/261.7 U NDPerfluoroundecanoic acid (PFUnDA) 0.501.0 1 06/09/26 05:05 6/8/261.7 U NDPerfluorododecanoic acid (PFDOA) 0.501.0 1 06/09/26 05:05 6/8/261.7 U NDPerfluorotridecanoic acid (PFTrDA) 0.701.0 1 06/09/26 05:05 6/8/261.7 U NDPerfluorotetradecanoic acid (PFTDA) 0.501.0 1 06/09/26 05:05 6/8/261.7 U
Perfluoroalkyl Sulfonamido Substances NDPerfluorooctane sulfonamide (PFOSAm) 0.501.0 1 06/09/26 05:05 6/8/261.7 U NDN-Methylperfluorooctane sulfonamide
(MeFOSA)
0.501.0 1 06/09/26 05:05 6/8/261.7 U
NDN-Ethylperfluorooctane sulfonamide (EtFOSAm)
0.501.0 1 06/09/26 05:05 6/8/261.7 U
NDN-Methylperfluorooctane sulfonamido ethanol (MeFOSE)
0.531.0 1 06/09/26 05:05 6/8/261.7 U
NDN-Ethylperfluorooctane sulfonamido ethanol (EtFOSE)
0.541.0 1 06/09/26 05:05 6/8/261.7 U
NDN-Methylperfluorooctane sulfonamido acetic acid (NMeFOSAA)
0.501.0 1 06/09/26 05:05 6/8/261.7 U
NDN-Ethylperfluorooctane sulfonamido acetic acid (NEtFOSAA)
0.611.0 1 06/09/26 05:05 6/8/261.7 U
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
Per- and Polyfluoroalkyl Substances (PFAS) by LC/MS/MS
05/12/26 13:06
NA
ng/L
Basis:
Units:
1633Analysis Method:
MethodPrep Method:
05/20/26 10:45
K2605119
Date Received:
Date Collected:
Service Request:
Ground Water
ALS Environmental - Middletown
Sample Matrix:
Project:
Client:
Analyte Name LOD QDate Analyzed Date
ExtractedDil.MDLLOQResult
Fluorotelomer Sulfonic Acids (FTSAs) ND1H, 1H, 2H, 2H-Perfluorohexanesulfonic acid (4:2 FTS)
0.500.94 1 06/09/26 05:05 6/8/261.7 U
ND1H, 1H, 2H, 2H-Perfluorooctanesulfonic acid (6:2 FTS)
0.501.4 1 06/09/26 05:05 6/8/261.7 U
ND1H, 1H, 2H, 2H-Perfluorodecanesulfonic acid (8:2 FTS)
0.500.96 1 06/09/26 05:05 6/8/261.7 U
Fluorotelomer Carboxylic Acids (FTCAs) ND4,4,5,5,6,6,6-Heptafluorohexanoic acid
(3:3 FTCA)
4.210 1 06/09/26 05:05 6/8/2617 U
ND2H,2H,3H,3H-Perfluorooctanoic acid (5:3
FTCA)
8.210 1 06/09/26 05:05 6/8/2617 U
ND2H,2H,3H,3H-Perfluorodecanoic acid (7:3
FTCA)
7.010 1 06/09/26 05:05 6/8/2617 U
Perfluoroalkyl Ether Sulfonic Acids (PFESAs) NDPerfluoro(2-ethoxyethane) sulfonic acid
(PFEESA)
0.500.89 1 06/09/26 05:05 6/8/261.7 U
ND9-Chlorohexadecafluoro-3-oxanonane-1-sulfonic acid (9-Cl-PF3ONS)
0.500.93 1 06/09/26 05:05 6/8/261.7 U
ND11-Chloroeicosafluoro-3-oxaundecane-1-sulfonic acid (11-Cl-PF3OUdS)
0.500.94 1 06/09/26 05:05 6/8/261.7 U
Perfluoroalkyl Ether Carboxylic Acids (PFECAs) NDPerfluoro-3-methoxypropanoic acid
(PFMPA)
0.501.0 1 06/09/26 05:05 6/8/261.7 U
NDPerfluoro-4-methoxybutanoic acid
(PFMBA)
0.501.0 1 06/09/26 05:05 6/8/261.7 U
NDHexafluoropropyleneoxide dimer acid (HFPO-DA) (GenX)
0.501.0 1 06/09/26 05:05 6/8/261.7 U
NDNonafluoro-3,6-dioxaheptanoic acid
(NFDHA)
0.501.0 1 06/09/26 05:05 6/8/261.7 U
ND4,8-Dioxa-3H-perfluorononanoic acid
(DONA)
0.500.95 1 06/09/26 05:05 6/8/261.7 U
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
Per- and Polyfluoroalkyl Substances (PFAS) by LC/MS/MS
05/12/26 13:06
NA
ng/L
Basis:
Units:
1633Analysis Method:
MethodPrep Method:
05/20/26 10:45
K2605119
Date Received:
Date Collected:
Service Request:
Ground Water
ALS Environmental - Middletown
Sample Matrix:
Project:
Client:
Surrogate Name Q% Rec Control Limits Date Analyzed
06/09/26 05:0540 - 1358713C3-PFBS
06/09/26 05:0540 - 1308213C3-PFHxS
06/09/26 05:0540 - 1308013C8-PFOS
06/09/26 05:055 - 1308713C4-PFBA
06/09/26 05:0540 - 1308413C5-PFPeA 06/09/26 05:0540 - 1308513C5-PFHxA 06/09/26 05:0540 - 1308113C4-PFHpA
06/09/26 05:0540 - 1308213C8-PFOA
06/09/26 05:0540 - 1308313C9-PFNA
06/09/26 05:0540 - 1308113C6-PFDA
06/09/26 05:0530 - 1307613C7-PFUnDA 06/09/26 05:0510 - 1307013C2-PFDoDA 06/09/26 05:0510 - 1306913C2-PFTeDA
06/09/26 05:0540 - 1306413C8-FOSA
06/09/26 05:0510 - 13062D3-MeFOSA 06/09/26 05:0510 - 13060D5-EtFOSA 06/09/26 05:0510 - 13064D7-MeFOSE 06/09/26 05:0510 - 13065D9-EtFOSE 06/09/26 05:0540 - 17068D3-MeFOSAA 06/09/26 05:0525 - 13567D5-EtFOSAA
06/09/26 05:0540 - 2008113C2-4:2 FTS
06/09/26 05:0540 - 2008513C2-6:2 FTS
06/09/26 05:0540 - 3009113C2-8:2 FTS
06/09/26 05:0540 - 1307613C3-HFPO-DA
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
Printed 6/12/2026 11:53:13 AM 26-0000772926 rev 00Superset Reference:
K2605119-005Lab Code:
Sample Name: MW602-12052026
Per- and Polyfluoroalkyl Substances (PFAS) by LC/MS/MS
05/12/26 13:28
NA
ng/L
Basis:
Units:
1633Analysis Method:
MethodPrep Method:
05/20/26 10:45
K2605119
Date Received:
Date Collected:
Service Request:
Ground Water
ALS Environmental - Middletown
Sample Matrix:
Project:
Client:
Analyte Name LOD QDate Analyzed Date
ExtractedDil.MDLLOQResult
Perfluoroalkyl Sulfonic Acids (PFSAs) 1.3Perfluorobutane sulfonic acid (PFBS) 0.840.89 1 06/09/26 05:53 6/8/261.7 J
0.53Perfluoropentane sulfonic acid (PFPeS) 0.500.94 1 06/09/26 05:53 6/8/261.7 J 4.8Perfluorohexane sulfonic acid (PFHxS) 0.530.91 1 06/09/26 05:53 6/8/261.7 NDPerfluoroheptane sulfonic acid (PFHpS) 0.500.95 1 06/09/26 05:53 6/8/261.7 U 2.8Perfluorooctane sulfonic acid (PFOS) 0.500.93 1 06/09/26 05:53 6/8/261.7 NDPerfluorononane sulfonic acid (PFNS) 0.500.96 1 06/09/26 05:53 6/8/261.7 U NDPerfluorodecane sulfonic acid (PFDS) 0.500.97 1 06/09/26 05:53 6/8/261.7 U NDPerfluorododecane sulfonic acid (PFDoS) 0.500.97 1 06/09/26 05:53 6/8/261.7 U
Perfluoroalkyl Carboxylic Acids (PFCAs) 3.3Perfluorobutanoic acid (PFBA) 1.32.0 1 06/09/26 05:53 6/8/262.0 3.2Perfluoropentanoic acid (PFPeA) 0.501.0 1 06/09/26 05:53 6/8/261.7 2.6Perfluorohexanoic acid (PFHxA) 0.501.0 1 06/09/26 05:53 6/8/261.7 2.1Perfluoroheptanoic acid (PFHpA) 0.501.0 1 06/09/26 05:53 6/8/261.7 8.7Perfluorooctanoic acid (PFOA) 0.501.0 1 06/09/26 05:53 6/8/261.7
0.55Perfluorononanoic acid (PFNA) 0.501.0 1 06/09/26 05:53 6/8/261.7 J NDPerfluorodecanoic acid (PFDA) 0.751.0 1 06/09/26 05:53 6/8/261.7 U NDPerfluoroundecanoic acid (PFUnDA) 0.501.0 1 06/09/26 05:53 6/8/261.7 U NDPerfluorododecanoic acid (PFDOA) 0.501.0 1 06/09/26 05:53 6/8/261.7 U NDPerfluorotridecanoic acid (PFTrDA) 0.701.0 1 06/09/26 05:53 6/8/261.7 U NDPerfluorotetradecanoic acid (PFTDA) 0.501.0 1 06/09/26 05:53 6/8/261.7 U
Perfluoroalkyl Sulfonamido Substances NDPerfluorooctane sulfonamide (PFOSAm) 0.501.0 1 06/09/26 05:53 6/8/261.7 U NDN-Methylperfluorooctane sulfonamide
(MeFOSA)
0.501.0 1 06/09/26 05:53 6/8/261.7 U
NDN-Ethylperfluorooctane sulfonamide (EtFOSAm)
0.501.0 1 06/09/26 05:53 6/8/261.7 U
NDN-Methylperfluorooctane sulfonamido ethanol (MeFOSE)
0.531.0 1 06/09/26 05:53 6/8/261.7 U
NDN-Ethylperfluorooctane sulfonamido ethanol (EtFOSE)
0.541.0 1 06/09/26 05:53 6/8/261.7 U
NDN-Methylperfluorooctane sulfonamido acetic acid (NMeFOSAA)
0.501.0 1 06/09/26 05:53 6/8/261.7 U
NDN-Ethylperfluorooctane sulfonamido acetic acid (NEtFOSAA)
0.611.0 1 06/09/26 05:53 6/8/261.7 U
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
Per- and Polyfluoroalkyl Substances (PFAS) by LC/MS/MS
05/12/26 13:28
NA
ng/L
Basis:
Units:
1633Analysis Method:
MethodPrep Method:
05/20/26 10:45
K2605119
Date Received:
Date Collected:
Service Request:
Ground Water
ALS Environmental - Middletown
Sample Matrix:
Project:
Client:
Analyte Name LOD QDate Analyzed Date
ExtractedDil.MDLLOQResult
Fluorotelomer Sulfonic Acids (FTSAs) ND1H, 1H, 2H, 2H-Perfluorohexanesulfonic acid (4:2 FTS)
0.500.94 1 06/09/26 05:53 6/8/261.7 U
ND1H, 1H, 2H, 2H-Perfluorooctanesulfonic acid (6:2 FTS)
0.501.4 1 06/09/26 05:53 6/8/261.7 U
ND1H, 1H, 2H, 2H-Perfluorodecanesulfonic acid (8:2 FTS)
0.500.96 1 06/09/26 05:53 6/8/261.7 U
Fluorotelomer Carboxylic Acids (FTCAs) ND4,4,5,5,6,6,6-Heptafluorohexanoic acid
(3:3 FTCA)
4.210 1 06/09/26 05:53 6/8/2617 U
ND2H,2H,3H,3H-Perfluorooctanoic acid (5:3
FTCA)
8.210 1 06/09/26 05:53 6/8/2617 U
ND2H,2H,3H,3H-Perfluorodecanoic acid (7:3
FTCA)
7.010 1 06/09/26 05:53 6/8/2617 U
Perfluoroalkyl Ether Sulfonic Acids (PFESAs) NDPerfluoro(2-ethoxyethane) sulfonic acid
(PFEESA)
0.500.89 1 06/09/26 05:53 6/8/261.7 U
ND9-Chlorohexadecafluoro-3-oxanonane-1-sulfonic acid (9-Cl-PF3ONS)
0.500.93 1 06/09/26 05:53 6/8/261.7 U
ND11-Chloroeicosafluoro-3-oxaundecane-1-sulfonic acid (11-Cl-PF3OUdS)
0.500.94 1 06/09/26 05:53 6/8/261.7 U
Perfluoroalkyl Ether Carboxylic Acids (PFECAs) NDPerfluoro-3-methoxypropanoic acid
(PFMPA)
0.501.0 1 06/09/26 05:53 6/8/261.7 U
NDPerfluoro-4-methoxybutanoic acid
(PFMBA)
0.501.0 1 06/09/26 05:53 6/8/261.7 U
NDHexafluoropropyleneoxide dimer acid (HFPO-DA) (GenX)
0.501.0 1 06/09/26 05:53 6/8/261.7 U
NDNonafluoro-3,6-dioxaheptanoic acid
(NFDHA)
0.501.0 1 06/09/26 05:53 6/8/261.7 U
ND4,8-Dioxa-3H-perfluorononanoic acid
(DONA)
0.500.95 1 06/09/26 05:53 6/8/261.7 U
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
Per- and Polyfluoroalkyl Substances (PFAS) by LC/MS/MS
05/12/26 13:28
NA
ng/L
Basis:
Units:
1633Analysis Method:
MethodPrep Method:
05/20/26 10:45
K2605119
Date Received:
Date Collected:
Service Request:
Ground Water
ALS Environmental - Middletown
Sample Matrix:
Project:
Client:
Surrogate Name Q% Rec Control Limits Date Analyzed
06/09/26 05:5340 - 1358313C3-PFBS
06/09/26 05:5340 - 1307913C3-PFHxS
06/09/26 05:5340 - 1307613C8-PFOS
06/09/26 05:535 - 1308313C4-PFBA
06/09/26 05:5340 - 1308313C5-PFPeA 06/09/26 05:5340 - 1308013C5-PFHxA 06/09/26 05:5340 - 1307713C4-PFHpA
06/09/26 05:5340 - 1307813C8-PFOA
06/09/26 05:5340 - 1307713C9-PFNA
06/09/26 05:5340 - 1307713C6-PFDA
06/09/26 05:5330 - 1307313C7-PFUnDA 06/09/26 05:5310 - 1306713C2-PFDoDA 06/09/26 05:5310 - 1306613C2-PFTeDA
06/09/26 05:5340 - 1306113C8-FOSA
06/09/26 05:5310 - 13063D3-MeFOSA 06/09/26 05:5310 - 13063D5-EtFOSA 06/09/26 05:5310 - 13061D7-MeFOSE 06/09/26 05:5310 - 13062D9-EtFOSE 06/09/26 05:5340 - 17065D3-MeFOSAA 06/09/26 05:5325 - 13564D5-EtFOSAA
06/09/26 05:5340 - 2007713C2-4:2 FTS
06/09/26 05:5340 - 2007913C2-6:2 FTS
06/09/26 05:5340 - 3008513C2-8:2 FTS
06/09/26 05:5340 - 1307113C3-HFPO-DA
Analytical Report
ALS Group USA, Corp.
dba ALS Environmental
K2605119-006Lab Code:
Sample Name: MW201-12052026
Per- and Polyfluoroalkyl Substances (PFAS) by LC/MS/MS
05/12/26 13:55
NA
ng/L
Basis:
Units:
1633Analysis Method:
MethodPrep Method:
05/20/26 10:45
K2605119
Date Received:
Date Collected:
Service Request:
Ground Water
ALS Environmental - Middletown
Sample Matrix:
Project:
Client:
Analyte Name LOD QDate Analyzed Date
ExtractedDil.MDLLOQResult
Perfluoroalkyl Sulfonic Acids (PFSAs) NDPerfluorobutane sulfonic acid (PFBS) 0.840.89 1 06/09/26 06:10 6/8/261.7 U NDPerfluoropentane sulfonic acid (PFPeS) 0.500.94 1 06/09/26 06:10 6/8/261.7 U
0.81Perfluorohexane sulfonic acid (PFHxS) 0.530.91 1 06/09/26 06:10 6/8/261.7 J NDPerfluoroheptane sulfonic acid (PFHpS) 0.500.95 1 06/09/26 06:10 6/8/261.7 U 12Perfluorooctane sulfonic acid (PFOS) 0.500.93 1 06/09/26 06:10 6/8/261.7
NDPerfluorononane sulfonic acid (PFNS) 0.500.96 1 06/09/26 06:10 6/8/261.7 U NDPerfluorodecane sulfonic acid (PFDS)…
This is the start of the file's text. The full file is on GovTribe.
File details come from the government source that posted it. Updated .