D-4_Dredge_Material_Testing_Report.pdf
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- Attached to
- Eau Gallie Muck Removal Project Area A1
- Solicitation number
- B-6-25-24
- Issued by
- Brevard County, Florida
About this file
This document is a laboratory analytical report from Pace Analytical Services, LLC for the IRL Muck Dredging project, commissioned by Taylor Engineering. The report details comprehensive environmental testing of multiple solid sediment samples collected on November 8, 2017, from various locations, with analyses conducted between November 9-30, 2017. The testing covered multiple parameters including mercury, total nitrogen, phosphorus, pesticides, metals, and polycyclic aromatic hydrocarbons (PAHs) using EPA-approved methodologies.
The laboratory report provides detailed quality control data, certification information, and analytical results for 37 distinct sample sites, with each sample undergoing multiple analytical tests. The samples were collected from what appears to be a dredging project, likely related to the Eau Gallie Muck Removal Project Area A1, with samples labeled systematically (e.g., A1-029, A2-20). The testing protocols adhered to TNI/NELAC standards and the laboratory's Quality Assurance Manual, with results reported on a dry weight basis and adjusted for moisture content, sample size, and potential dilutions. The comprehensive analysis suggests the samples were part of an environmental assessment to characterize sediment composition and potential contaminants prior to a large-scale dredging operation.
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Text version
#=CL#
November 30, 2017
LIMS USE: FR - DAVID STITES
LIMS OBJECT ID: 35347296
35347296 Project:
Pace Project No.:
RE:
David L. Stites Taylor Engineering 10151 Deerwood Park Blvd.
Bldg. 300, Suite 300 Jacksonville, FL 32256
IRL MUCK DREDGING
Dear David Stites:
Enclosed are the analytical results for sample(s) received by the laboratory between November 09, 2017 and November 10, 2017. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely, Martha Montero martha.montero@pacelabs.com
Project Manager (386)672-5668
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC 8 East Tower Circle
Ormond Beach, FL 32174 (386)672-5668
For Bidding Purposes Only
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
35347296
IRL MUCK DREDGING
Ormond Beach Certification IDs 8 East Tower Circle, Ormond Beach, FL 32174 Alabama Certification #: 41320 Connecticut Certification #: PH-0216 Delaware Certification: FL NELAC Reciprocity Florida Certification #: E83079 Georgia Certification #: 955 Guam Certification: FL NELAC Reciprocity Hawaii Certification: FL NELAC Reciprocity Illinois Certification #: 200068 Indiana Certification: FL NELAC Reciprocity Kansas Certification #: E-10383 Louisiana Certification #: FL NELAC Reciprocity Louisiana Environmental Certificate #: 05007 Maryland Certification: #346 Michigan Certification #: 9911 Mississippi Certification: FL NELAC Reciprocity Missouri Certification #: 236 Montana Certification #: Cert 0074
Nebraska Certification: NE-OS-28-14 Nevada Certification: FL NELAC Reciprocity New Jersey Certification #: FL022 New York Certification #: 11608 North Carolina Environmental Certificate #: 667 North Carolina Certification #: 12710 Oklahoma Certification #: D9947 Pennsylvania Certification #: 68-00547 Puerto Rico Certification #: FL01264 South Carolina Certification: #96042001 Tennessee Certification #: TN02974 Texas Certification: FL NELAC Reciprocity US Virgin Islands Certification: FL NELAC Reciprocity Virginia Environmental Certification #: 460165 Wyoming Certification: FL NELAC Reciprocity West Virginia Certification #: 9962C Wisconsin Certification #: 399079670 Wyoming (EPA Region 8): FL NELAC Reciprocity
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC 8 East Tower Circle
Ormond Beach, FL 32174 (386)672-5668
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
35347296
IRL MUCK DREDGING
Lab ID Sample ID Matrix Date Collected Date Received
35347296001 A1-029 Solid 11/08/17 13:10 11/09/17 10:10
35347296002 A1-029 Solid 11/08/17 13:10 11/09/17 10:10
35347296003 A1-056 Solid 11/08/17 12:45 11/09/17 10:10
35347296004 A1-056 Solid 11/08/17 12:45 11/09/17 10:10
35347296005 A1-066 Solid 11/08/17 12:20 11/09/17 10:10
35347296006 A1-066 Solid 11/08/17 12:20 11/09/17 10:10
35347296007 A1-069 Solid 11/08/17 11:50 11/09/17 10:10
35347296008 A1-069 Solid 11/08/17 11:50 11/09/17 10:10
35347296009 A1A-02 Solid 11/08/17 15:15 11/09/17 10:10
35347296010 A1A-02 Solid 11/08/17 15:15 11/09/17 10:10
35347296011 A1A-08 Solid 11/08/17 15:00 11/09/17 10:10
35347296012 A1A-08 Solid 11/08/17 15:00 11/09/17 10:10
35347296013 A1A-17 Solid 11/08/17 15:25 11/09/17 10:10
35347296014 A1A-17 Solid 11/08/17 15:25 11/09/17 10:10
35347296015 A1A-28 Solid 11/08/17 15:45 11/09/17 10:10
35347296016 A1A-28 Solid 11/08/17 15:45 11/09/17 10:10
35347296017 A1A-33 Solid 11/08/17 16:55 11/09/17 10:10
35347296018 A1A-33 Solid 11/08/17 16:55 11/09/17 10:10
35347296019 A1A-36 Solid 11/08/17 16:10 11/09/17 10:10
35347296020 A1A-36 Solid 11/08/17 16:10 11/09/17 10:10
35347296021 A1A-53 Solid 11/08/17 16:35 11/09/17 10:10
35347296022 A1A-53 Solid 11/08/17 16:35 11/09/17 10:10
35347296024 A2-20 Solid 11/08/17 11:05 11/09/17 10:10
35347296025 A2-20 Solid 11/08/17 11:05 11/09/17 10:10
35347296026 A2-21 Solid 11/08/17 10:40 11/09/17 10:10
35347296027 A2-21 Solid 11/08/17 10:40 11/09/17 10:10
35347296028 A2-38 Solid 11/08/17 10:15 11/09/17 10:10
35347296029 A2-38 Solid 11/08/17 10:15 11/09/17 10:10
35347296030 A2-44 Solid 11/08/17 09:55 11/09/17 10:10
35347296031 A2-44 Solid 11/08/17 09:55 11/09/17 10:10
35347296032 A4-X1 Solid 11/08/17 09:30 11/09/17 10:10
35347296033 A4-X1 Solid 11/08/17 09:30 11/09/17 10:10
35347296034 A4-X2 Solid 11/08/17 09:10 11/09/17 10:10
35347296035 A4-X2 Solid 11/08/17 09:10 11/09/17 10:10
35347296036 A2-12 Solid 11/08/17 11:25 11/09/17 10:10
35347296037 A2-12 Solid 11/08/17 11:25 11/09/17 10:10
35347296038 Blank Solid 11/09/17 20:00 11/10/17 10:10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC 8 East Tower Circle
Ormond Beach, FL 32174 (386)672-5668
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
35347296
IRL MUCK DREDGING
Lab ID Sample ID Method Analytes ReportedAnalysts
35347296001 A1-029 EPA 7471 1MLO
ASTM D2974-87 1RAK
EPA 350.1 1CLL
EPA 351.2 1JDW
EPA 365.4 1JDW
EPA 9056 2CMD
35347296002 A1-029 EPA 8081 22BP1
EPA 6010 7BTS
EPA 8270 21JDT
ASTM D2974-87 1RAK
35347296003 A1-056 EPA 7471 1MLO
ASTM D2974-87 1RAK
EPA 350.1 1CLL
EPA 351.2 1JDW
EPA 365.4 1JDW
EPA 9056 2CMD
35347296004 A1-056 EPA 8081 22BP1
EPA 6010 7BTS
EPA 8270 21JDT
ASTM D2974-87 1RAK
35347296005 A1-066 EPA 7471 1MLO
ASTM D2974-87 1RAK
EPA 350.1 1CLL
EPA 351.2 1JDW
EPA 365.4 1JDW
EPA 9056 2CMD
35347296006 A1-066 EPA 8081 22BP1
EPA 6010 7BTS, MMT
EPA 8270 21JDT
ASTM D2974-87 1RAK
35347296007 A1-069 EPA 7471 1MLO
ASTM D2974-87 1RAK
EPA 350.1 1CLL
EPA 351.2 1JDW
EPA 365.4 1JDW
EPA 9056 2CMD
35347296008 A1-069 EPA 8081 22BP1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC 8 East Tower Circle
Ormond Beach, FL 32174 (386)672-5668
Pace Project No.:
Project:
35347296
IRL MUCK DREDGING
Lab ID Sample ID Method Analytes ReportedAnalysts
EPA 6010 7BTS, MMT
EPA 8270 21JDT
ASTM D2974-87 1RAK
35347296009 A1A-02 EPA 7471 1MLO
ASTM D2974-87 1RAK
EPA 350.1 1CLL
EPA 351.2 1JDW
EPA 365.4 1JDW
EPA 9056 2CMD
35347296010 A1A-02 EPA 8081 22BP1
EPA 6010 7BTS, MMT
EPA 8270 21JDT
ASTM D2974-87 1RAK
35347296011 A1A-08 EPA 7471 1MLO
ASTM D2974-87 1RAK
EPA 350.1 1CLL
EPA 351.2 1JDW
EPA 365.4 1JDW
EPA 9056 2CMD
35347296012 A1A-08 EPA 8081 22BP1
EPA 6010 7BTS, MMT
EPA 8270 21JDT
ASTM D2974-87 1RAK
35347296013 A1A-17 EPA 7471 1MLO
ASTM D2974-87 1RAK
EPA 350.1 1CLL
EPA 351.2 1JDW
EPA 365.4 1JDW
EPA 9056 2CMD
35347296014 A1A-17 EPA 8081 22BP1
EPA 6010 7BTS, MMT
EPA 8270 21JDT
ASTM D2974-87 1RAK
35347296015 A1A-28 EPA 7471 1MLO
ASTM D2974-87 1RAK
EPA 350.1 1CLL
EPA 351.2 1JDW
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC 8 East Tower Circle
Ormond Beach, FL 32174 (386)672-5668
Pace Project No.:
Project:
35347296
IRL MUCK DREDGING
Lab ID Sample ID Method Analytes ReportedAnalysts
EPA 365.4 1JDW
EPA 9056 2CMD
35347296016 A1A-28 EPA 8081 22BP1
EPA 6010 7BTS, MMT
EPA 8270 21JDT
ASTM D2974-87 1RAK
35347296017 A1A-33 EPA 7471 1MLO
ASTM D2974-87 1RAK
EPA 350.1 1CLL
EPA 351.2 1JDW
EPA 365.4 1JDW
EPA 9056 2CMD
35347296018 A1A-33 EPA 8081 22BP1
EPA 6010 7BTS, MMT
EPA 8270 21JDT
ASTM D2974-87 1RAK
35347296019 A1A-36 EPA 7471 1MLO
ASTM D2974-87 1RAK
EPA 350.1 1CLL
EPA 351.2 1JDW
EPA 365.4 1JDW
EPA 9056 2CMD
35347296020 A1A-36 EPA 8081 22BP1
EPA 6010 7BTS, MMT
EPA 8270 21JDT
ASTM D2974-87 1RAK
35347296021 A1A-53 EPA 7471 1MLO
ASTM D2974-87 1RAK
EPA 350.1 1CLL
EPA 351.2 1JDW
EPA 365.4 1JDW
EPA 9056 2CMD
35347296022 A1A-53 EPA 8081 22BP1
EPA 6010 7BTS, MMT
EPA 8270 21JDT
ASTM D2974-87 1RAK
35347296024 A2-20 EPA 7471 1MLO
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC 8 East Tower Circle
Ormond Beach, FL 32174 (386)672-5668
Pace Project No.:
Project:
35347296
IRL MUCK DREDGING
Lab ID Sample ID Method Analytes ReportedAnalysts
ASTM D2974-87 1RAK
EPA 350.1 1CLL
EPA 351.2 1JDW
EPA 365.4 1JDW
EPA 9056 2CMD
35347296025 A2-20 EPA 8081 22BP1
EPA 6010 7BTS, MMT
EPA 8270 21JDT
ASTM D2974-87 1RAK
35347296026 A2-21 EPA 7471 1MLO
ASTM D2974-87 1RAK
EPA 350.1 1CLL
EPA 351.2 1JDW
EPA 365.4 1JDW
EPA 9056 2CMD
35347296027 A2-21 EPA 8081 22BP1
EPA 6010 7BTS, MMT
EPA 8270 21JDT
ASTM D2974-87 1RAK
35347296028 A2-38 EPA 7471 1MLO
ASTM D2974-87 1RAK
EPA 350.1 1CLL
EPA 351.2 1JDW
EPA 365.4 1JDW
EPA 9056 2CMD
35347296029 A2-38 EPA 8081 22BP1
EPA 6010 7BTS, MMT
EPA 8270 21JDT
ASTM D2974-87 1RAK
35347296030 A2-44 EPA 7471 1MLO
ASTM D2974-87 1RAK
EPA 350.1 1CLL
EPA 351.2 1JDW
EPA 365.4 1JDW
EPA 9056 2CMD
35347296031 A2-44 EPA 8081 22BP1
EPA 6010 7BTS, MMT
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC 8 East Tower Circle
Ormond Beach, FL 32174 (386)672-5668
Pace Project No.:
Project:
35347296
IRL MUCK DREDGING
Lab ID Sample ID Method Analytes ReportedAnalysts
EPA 8270 21JDT
ASTM D2974-87 1RAK
35347296032 A4-X1 EPA 7471 1MLO
ASTM D2974-87 1RAK
EPA 350.1 1CLL
EPA 351.2 1JDW
EPA 365.4 1JDW
EPA 9056 2CMD
35347296033 A4-X1 EPA 8081 22BP1
EPA 6010 7BTS, MMT
EPA 8270 21JDT
ASTM D2974-87 1RAK
35347296034 A4-X2 EPA 7471 1MLO
ASTM D2974-87 1RAK
EPA 350.1 1CLL
EPA 351.2 1JDW
EPA 365.4 1JDW
EPA 9056 2CMD
35347296035 A4-X2 EPA 8081 22BP1
EPA 6010 7BTS, MMT
EPA 8270 21JDT
ASTM D2974-87 1RAK
35347296036 A2-12 EPA 7471 1MLO
ASTM D2974-87 1RAK
EPA 350.1 1CLL
EPA 351.2 1JDW
EPA 365.4 1JDW
EPA 9056 2CMD
35347296037 A2-12 EPA 8081 22BP1
EPA 6010 7BTS, MMT
EPA 8270 21JDT
ASTM D2974-87 1RAK
35347296038 Blank EPA 8081 22BP1
EPA 8270 21JDT
ASTM D2974-87 1CS2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC 8 East Tower Circle
Ormond Beach, FL 32174 (386)672-5668
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
35347296
IRL MUCK DREDGING
Sample: A1-029 Lab ID: 35347296001 Collected: 11/08/17 13:10 Received: 11/09/17 10:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualPQL
Analytical Method: EPA 7471 Preparation Method: EPA 74717471 Mercury
Mercury 0.038 mg/kg 11/20/17 14:42 7439-97-611/17/17 15:350.033 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 54.9 % 11/20/17 09:570.10 1
Analytical Method: EPA 350.1 Preparation Method: EPA 350.1350.1 Ammonia
Nitrogen, Ammonia 4.5 mg/kg 11/15/17 15:15 7664-41-711/14/17 09:181.1 1
Analytical Method: EPA 351.2 Preparation Method: EPA 351.2351.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total 1180 mg/kg 11/15/17 15:49 7727-37-911/10/17 08:12249 5
Analytical Method: EPA 365.4 Preparation Method: EPA 365.4365.4 Phosphorus, Total
Phosphorus, Total (as P) 210 mg/kg 11/15/17 15:49 7723-14-011/10/17 08:1249.8 5
Analytical Method: EPA 9056 Preparation Method: EPA 90569056 IC Anions 48hr
Nitrogen, NO2 plus NO3 5.1U mg/kg 11/10/17 03:1111/09/17 17:0010.2 1 Orthophosphate as P 10.2U mg/kg 11/10/17 03:1111/09/17 17:0020.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/30/2017 11:25 AM
Pace Analytical Services, LLC 8 East Tower Circle
Ormond Beach, FL 32174 (386)672-5668
Pace Project No.:
Project:
35347296
IRL MUCK DREDGING
Sample: A1-029 Lab ID: 35347296002 Collected: 11/08/17 13:10 Received: 11/09/17 10:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualPQL
Analytical Method: EPA 8081 Preparation Method: EPA 35468081 GCS Pesticides
Aldrin 0.00031U mg/kg 11/23/17 02:27 309-00-211/22/17 08:300.0090 5 alpha-BHC 0.00037U mg/kg 11/23/17 02:27 319-84-6 D311/22/17 08:300.0090 5 beta-BHC 0.00041U mg/kg 11/23/17 02:27 319-85-711/22/17 08:300.0090 5 delta-BHC 0.00046U mg/kg 11/23/17 02:27 319-86-8 M111/22/17 08:300.0090 5 gamma-BHC (Lindane) 0.00079U mg/kg 11/23/17 02:27 58-89-911/22/17 08:300.0090 5 Chlordane (Technical) 0.084U mg/kg 11/23/17 02:27 57-74-911/22/17 08:300.090 5 4,4'-DDD 0.00069U mg/kg 11/23/17 02:27 72-54-811/22/17 08:300.0090 5 4,4'-DDE 0.00032U mg/kg 11/23/17 02:27 72-55-911/22/17 08:300.0090 5 4,4'-DDT 0.00051U mg/kg 11/23/17 02:27 50-29-311/22/17 08:300.0090 5 Dieldrin 0.00021U mg/kg 11/23/17 02:27 60-57-111/22/17 08:300.0090 5 Endosulfan I 0.00013U mg/kg 11/23/17 02:27 959-98-811/22/17 08:300.0090 5 Endosulfan II 0.00030U mg/kg 11/23/17 02:27 33213-65-911/22/17 08:300.0090 5 Endosulfan sulfate 0.00023U mg/kg 11/23/17 02:27 1031-07-8 CH11/22/17 08:300.0090 5 Endrin 0.00028U mg/kg 11/23/17 02:27 72-20-811/22/17 08:300.0090 5 Endrin aldehyde 0.00035U mg/kg 11/23/17 02:27 7421-93-411/22/17 08:300.018 5 Endrin ketone 0.00042U mg/kg 11/23/17 02:27 53494-70-5 CH11/22/17 08:300.0090 5 Heptachlor 0.00021U mg/kg 11/23/17 02:27 76-44-811/22/17 08:300.0090 5 Heptachlor epoxide 0.00059U mg/kg 11/23/17 02:27 1024-57-311/22/17 08:300.0090 5 Methoxychlor 0.0056U mg/kg 11/23/17 02:27 72-43-511/22/17 08:300.0090 5 Toxaphene 0.039U mg/kg 11/23/17 02:27 8001-35-211/22/17 08:300.090 5 Surrogates Tetrachloro-m-xylene (S) 88 % 11/23/17 02:27 877-09-811/22/17 08:3053-140 5 Decachlorobiphenyl (S) 90 % 11/23/17 02:27 2051-24-311/22/17 08:3043-157 5
Analytical Method: EPA 6010 Preparation Method: EPA 30506010 MET ICP
Arsenic 2.3 mg/kg 11/27/17 05:13 7440-38-211/20/17 15:230.55 1 Barium 15.6 mg/kg 11/27/17 05:13 7440-39-311/20/17 15:230.55 1 Cadmium 0.099 mg/kg 11/27/17 05:13 7440-43-911/20/17 15:230.055 1 Chromium 12.8 mg/kg 11/27/17 05:13 7440-47-311/20/17 15:230.27 1 Lead 13.4 mg/kg 11/27/17 05:13 7439-92-1 M111/20/17 15:230.55 1 Selenium 0.67J mg/kg 11/27/17 05:13 7782-49-211/20/17 15:230.82 1 Silver 1.4U mg/kg 11/27/17 12:43 7440-22-4 D3,M111/20/17 15:232.7 10
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Short List Microwave
Acenaphthene 0.038U mg/kg 11/22/17 01:37 83-32-9 P111/21/17 21:170.10 1 Acenaphthylene 0.032U mg/kg 11/22/17 01:37 208-96-8 M1,P111/21/17 21:170.10 1 Anthracene 0.031U mg/kg 11/22/17 01:37 120-12-7 P111/21/17 21:170.10 1 Benzo(a)anthracene 0.030U mg/kg 11/22/17 01:37 56-55-3 P111/21/17 21:170.10 1 Benzo(a)pyrene 0.012U mg/kg 11/22/17 01:37 50-32-8 P111/21/17 21:170.10 1 Benzo(b)fluoranthene 0.078U mg/kg 11/22/17 01:37 205-99-2 P111/21/17 21:170.10 1 Benzo(g,h,i)perylene 0.037U mg/kg 11/22/17 01:37 191-24-2 P111/21/17 21:170.10 1 Benzo(k)fluoranthene 0.022U mg/kg 11/22/17 01:37 207-08-9 P111/21/17 21:170.10 1 Chrysene 0.037U mg/kg 11/22/17 01:37 218-01-9 P111/21/17 21:170.10 1 Dibenz(a,h)anthracene 0.052U mg/kg 11/22/17 01:37 53-70-3 P111/21/17 21:170.10 1 Fluoranthene 0.099J mg/kg 11/22/17 01:37 206-44-0 P111/21/17 21:170.10 1 Fluorene 0.046U mg/kg 11/22/17 01:37 86-73-7 M1,P111/21/17 21:170.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/30/2017 11:25 AM
Pace Analytical Services, LLC 8 East Tower Circle
Ormond Beach, FL 32174 (386)672-5668
Pace Project No.:
Project:
35347296
IRL MUCK DREDGING
Sample: A1-029 Lab ID: 35347296002 Collected: 11/08/17 13:10 Received: 11/09/17 10:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualPQL
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Short List Microwave
Indeno(1,2,3-cd)pyrene 0.052U mg/kg 11/22/17 01:37 193-39-5 P111/21/17 21:170.10 1 1-Methylnaphthalene 0.036U mg/kg 11/22/17 01:37 90-12-0 P111/21/17 21:170.10 1 2-Methylnaphthalene 0.042U mg/kg 11/22/17 01:37 91-57-6 P111/21/17 21:170.10 1 Naphthalene 0.033U mg/kg 11/22/17 01:37 91-20-3 M1,P111/21/17 21:170.10 1 Phenanthrene 0.039U mg/kg 11/22/17 01:37 85-01-8 P111/21/17 21:170.10 1 Pyrene 0.094J mg/kg 11/22/17 01:37 129-00-0 P111/21/17 21:170.10 1 Surrogates Nitrobenzene-d5 (S) 44 % 11/22/17 01:37 4165-60-011/21/17 21:1716-123 1 2-Fluorobiphenyl (S) 44 % 11/22/17 01:37 321-60-811/21/17 21:1732-129 1 p-Terphenyl-d14 (S) 59 % 11/22/17 01:37 1718-51-011/21/17 21:1738-138 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 7.0 % 11/27/17 09:080.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/30/2017 11:25 AM
Pace Analytical Services, LLC 8 East Tower Circle
Ormond Beach, FL 32174 (386)672-5668
Pace Project No.:
Project:
35347296
IRL MUCK DREDGING
Sample: A1-056 Lab ID: 35347296003 Collected: 11/08/17 12:45 Received: 11/09/17 10:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualPQL
Analytical Method: EPA 7471 Preparation Method: EPA 74717471 Mercury
Mercury 0.024 mg/kg 11/21/17 10:09 7439-97-6 M1,R111/20/17 16:300.014 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 45.9 % 11/20/17 09:570.10 1
Analytical Method: EPA 350.1 Preparation Method: EPA 350.1350.1 Ammonia
Nitrogen, Ammonia 6.3 mg/kg 11/15/17 15:17 7664-41-711/14/17 09:180.92 1
Analytical Method: EPA 351.2 Preparation Method: EPA 351.2351.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total 1050 mg/kg 11/15/17 15:50 7727-37-911/10/17 08:12193 5
Analytical Method: EPA 365.4 Preparation Method: EPA 365.4365.4 Phosphorus, Total
Phosphorus, Total (as P) 219 mg/kg 11/15/17 15:50 7723-14-011/10/17 08:1238.7 5
Analytical Method: EPA 9056 Preparation Method: EPA 90569056 IC Anions 48hr
Nitrogen, NO2 plus NO3 4.5U mg/kg 11/10/17 02:4811/09/17 17:009.0 1 Orthophosphate as P 9.0U mg/kg 11/10/17 02:4811/09/17 17:0018.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/30/2017 11:25 AM
Pace Analytical Services, LLC 8 East Tower Circle
Ormond Beach, FL 32174 (386)672-5668
Pace Project No.:
Project:
35347296
IRL MUCK DREDGING
Sample: A1-056 Lab ID: 35347296004 Collected: 11/08/17 12:45 Received: 11/09/17 10:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualPQL
Analytical Method: EPA 8081 Preparation Method: EPA 35468081 GCS Pesticides
Aldrin 0.00033U mg/kg 11/23/17 03:25 309-00-211/22/17 08:300.0096 5 alpha-BHC 0.00039U mg/kg 11/23/17 03:25 319-84-6 D311/22/17 08:300.0096 5 beta-BHC 0.00043U mg/kg 11/23/17 03:25 319-85-711/22/17 08:300.0096 5 delta-BHC 0.00049U mg/kg 11/23/17 03:25 319-86-811/22/17 08:300.0096 5 gamma-BHC (Lindane) 0.00083U mg/kg 11/23/17 03:25 58-89-911/22/17 08:300.0096 5 Chlordane (Technical) 0.089U mg/kg 11/23/17 03:25 57-74-911/22/17 08:300.096 5 4,4'-DDD 0.00074U mg/kg 11/23/17 03:25 72-54-811/22/17 08:300.0096 5 4,4'-DDE 0.00034U mg/kg 11/23/17 03:25 72-55-911/22/17 08:300.0096 5 4,4'-DDT 0.00054U mg/kg 11/23/17 03:25 50-29-311/22/17 08:300.0096 5 Dieldrin 0.00023U mg/kg 11/23/17 03:25 60-57-111/22/17 08:300.0096 5 Endosulfan I 0.00014U mg/kg 11/23/17 03:25 959-98-811/22/17 08:300.0096 5 Endosulfan II 0.00032U mg/kg 11/23/17 03:25 33213-65-911/22/17 08:300.0096 5 Endosulfan sulfate 0.00024U mg/kg 11/23/17 03:25 1031-07-811/22/17 08:300.0096 5 Endrin 0.00029U mg/kg 11/23/17 03:25 72-20-811/22/17 08:300.0096 5 Endrin aldehyde 0.00037U mg/kg 11/23/17 03:25 7421-93-411/22/17 08:300.019 5 Endrin ketone 0.00045U mg/kg 11/23/17 03:25 53494-70-511/22/17 08:300.0096 5 Heptachlor 0.00022U mg/kg 11/23/17 03:25 76-44-811/22/17 08:300.0096 5 Heptachlor epoxide 0.00062U mg/kg 11/23/17 03:25 1024-57-311/22/17 08:300.0096 5 Methoxychlor 0.0059U mg/kg 11/23/17 03:25 72-43-511/22/17 08:300.0096 5 Toxaphene 0.041U mg/kg 11/23/17 03:25 8001-35-211/22/17 08:300.096 5 Surrogates Tetrachloro-m-xylene (S) 81 % 11/23/17 03:25 877-09-811/22/17 08:3053-140 5 Decachlorobiphenyl (S) 87 % 11/23/17 03:25 2051-24-311/22/17 08:3043-157 5
Analytical Method: EPA 6010 Preparation Method: EPA 30506010 MET ICP
Arsenic 3.1 mg/kg 11/27/17 05:33 7440-38-211/20/17 15:230.64 1 Barium 11.4 mg/kg 11/27/17 05:33 7440-39-311/20/17 15:230.64 1 Cadmium 0.057J mg/kg 11/27/17 05:33 7440-43-911/20/17 15:230.064 1 Chromium 13.6 mg/kg 11/27/17 05:33 7440-47-311/20/17 15:230.32 1 Lead 12.9 mg/kg 11/27/17 05:33 7439-92-111/20/17 15:230.64 1 Selenium 0.83J mg/kg 11/27/17 05:33 7782-49-211/20/17 15:230.95 1 Silver 1.6U mg/kg 11/27/17 12:47 7440-22-4 D311/20/17 15:233.2 10
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Short List Microwave
Acenaphthene 0.040U mg/kg 11/22/17 03:10 83-32-9 P111/21/17 21:170.11 1 Acenaphthylene 0.034U mg/kg 11/22/17 03:10 208-96-8 P111/21/17 21:170.11 1 Anthracene 0.034U mg/kg 11/22/17 03:10 120-12-7 P111/21/17 21:170.11 1 Benzo(a)anthracene 0.032U mg/kg 11/22/17 03:10 56-55-3 P111/21/17 21:170.11 1 Benzo(a)pyrene 0.013U mg/kg 11/22/17 03:10 50-32-8 P111/21/17 21:170.11 1 Benzo(b)fluoranthene 0.083U mg/kg 11/22/17 03:10 205-99-2 P111/21/17 21:170.11 1 Benzo(g,h,i)perylene 0.040U mg/kg 11/22/17 03:10 191-24-2 P111/21/17 21:170.11 1 Benzo(k)fluoranthene 0.024U mg/kg 11/22/17 03:10 207-08-9 P111/21/17 21:170.11 1 Chrysene 0.039U mg/kg 11/22/17 03:10 218-01-9 P111/21/17 21:170.11 1 Dibenz(a,h)anthracene 0.056U mg/kg 11/22/17 03:10 53-70-3 P111/21/17 21:170.11 1 Fluoranthene 0.10J mg/kg 11/22/17 03:10 206-44-0 P111/21/17 21:170.11 1 Fluorene 0.050U mg/kg 11/22/17 03:10 86-73-7 P111/21/17 21:170.11 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/30/2017 11:25 AM
Pace Analytical Services, LLC 8 East Tower Circle
Ormond Beach, FL 32174 (386)672-5668
Pace Project No.:
Project:
35347296
IRL MUCK DREDGING
Sample: A1-056 Lab ID: 35347296004 Collected: 11/08/17 12:45 Received: 11/09/17 10:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualPQL
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Short List Microwave
Indeno(1,2,3-cd)pyrene 0.056U mg/kg 11/22/17 03:10 193-39-5 P111/21/17 21:170.11 1 1-Methylnaphthalene 0.039U mg/kg 11/22/17 03:10 90-12-0 P111/21/17 21:170.11 1 2-Methylnaphthalene 0.045U mg/kg 11/22/17 03:10 91-57-6 P111/21/17 21:170.11 1 Naphthalene 0.036U mg/kg 11/22/17 03:10 91-20-3 P111/21/17 21:170.11 1 Phenanthrene 0.042U mg/kg 11/22/17 03:10 85-01-8 P111/21/17 21:170.11 1 Pyrene 0.056U mg/kg 11/22/17 03:10 129-00-0 P111/21/17 21:170.11 1 Surrogates Nitrobenzene-d5 (S) 43 % 11/22/17 03:10 4165-60-011/21/17 21:1716-123 1 2-Fluorobiphenyl (S) 43 % 11/22/17 03:10 321-60-811/21/17 21:1732-129 1 p-Terphenyl-d14 (S) 70 % 11/22/17 03:10 1718-51-011/21/17 21:1738-138 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 11.3 % 11/27/17 09:080.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/30/2017 11:25 AM
Pace Analytical Services, LLC 8 East Tower Circle
Ormond Beach, FL 32174 (386)672-5668
Pace Project No.:
Project:
35347296
IRL MUCK DREDGING
Sample: A1-066 Lab ID: 35347296005 Collected: 11/08/17 12:20 Received: 11/09/17 10:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualPQL
Analytical Method: EPA 7471 Preparation Method: EPA 74717471 Mercury
Mercury 0.026 mg/kg 11/21/17 10:15 7439-97-611/20/17 16:300.016 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 41.3 % 11/20/17 09:570.10 1
Analytical Method: EPA 350.1 Preparation Method: EPA 350.1350.1 Ammonia
Nitrogen, Ammonia 6.9 mg/kg 11/15/17 15:22 7664-41-711/14/17 09:180.85 1
Analytical Method: EPA 351.2 Preparation Method: EPA 351.2351.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total 378 mg/kg 11/15/17 15:51 7727-37-911/10/17 08:12179 5
Analytical Method: EPA 365.4 Preparation Method: EPA 365.4365.4 Phosphorus, Total
Phosphorus, Total (as P) 63.0 mg/kg 11/15/17 15:51 7723-14-011/10/17 08:1235.8 5
Analytical Method: EPA 9056 Preparation Method: EPA 90569056 IC Anions 48hr
Nitrogen, NO2 plus NO3 4.0U mg/kg 11/10/17 02:2411/09/17 17:007.9 1 Orthophosphate as P 7.9U mg/kg 11/10/17 02:2411/09/17 17:0015.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/30/2017 11:25 AM
Pace Analytical Services, LLC 8 East Tower Circle
Ormond Beach, FL 32174 (386)672-5668
Pace Project No.:
Project:
35347296
IRL MUCK DREDGING
Sample: A1-066 Lab ID: 35347296006 Collected: 11/08/17 12:20 Received: 11/09/17 10:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualPQL
Analytical Method: EPA 8081 Preparation Method: EPA 35468081 GCS Pesticides
Aldrin 0.00030U mg/kg 11/23/17 03:44 309-00-211/22/17 08:300.0087 5 alpha-BHC 0.00035U mg/kg 11/23/17 03:44 319-84-6 D311/22/17 08:300.0087 5 beta-BHC 0.00039U mg/kg 11/23/17 03:44 319-85-711/22/17 08:300.0087 5 delta-BHC 0.00045U mg/kg 11/23/17 03:44 319-86-811/22/17 08:300.0087 5 gamma-BHC (Lindane) 0.00076U mg/kg 11/23/17 03:44 58-89-911/22/17 08:300.0087 5 Chlordane (Technical) 0.081U mg/kg 11/23/17 03:44 57-74-911/22/17 08:300.087 5 4,4'-DDD 0.00067U mg/kg 11/23/17 03:44 72-54-811/22/17 08:300.0087 5 4,4'-DDE 0.00031U mg/kg 11/23/17 03:44 72-55-911/22/17 08:300.0087 5 4,4'-DDT 0.00049U mg/kg 11/23/17 03:44 50-29-311/22/17 08:300.0087 5 Dieldrin 0.00020U mg/kg 11/23/17 03:44 60-57-111/22/17 08:300.0087 5 Endosulfan I 0.00013U mg/kg 11/23/17 03:44 959-98-811/22/17 08:300.0087 5 Endosulfan II 0.00029U mg/kg 11/23/17 03:44 33213-65-911/22/17 08:300.0087 5 Endosulfan sulfate 0.00022U mg/kg 11/23/17 03:44 1031-07-8 CH11/22/17 08:300.0087 5 Endrin 0.00027U mg/kg 11/23/17 03:44 72-20-811/22/17 08:300.0087 5 Endrin aldehyde 0.00034U mg/kg 11/23/17 03:44 7421-93-411/22/17 08:300.017 5 Endrin ketone 0.00041U mg/kg 11/23/17 03:44 53494-70-5 CH11/22/17 08:300.0087 5 Heptachlor 0.00020U mg/kg 11/23/17 03:44 76-44-811/22/17 08:300.0087 5 Heptachlor epoxide 0.00057U mg/kg 11/23/17 03:44 1024-57-311/22/17 08:300.0087 5 Methoxychlor 0.0054U mg/kg 11/23/17 03:44 72-43-511/22/17 08:300.0087 5 Toxaphene 0.038U mg/kg 11/23/17 03:44 8001-35-211/22/17 08:300.087 5 Surrogates Tetrachloro-m-xylene (S) 90 % 11/23/17 03:44 877-09-811/22/17 08:3053-140 5 Decachlorobiphenyl (S) 91 % 11/23/17 03:44 2051-24-311/22/17 08:3043-157 5
Analytical Method: EPA 6010 Preparation Method: EPA 30506010 MET ICP
Arsenic 2.3 mg/kg 11/27/17 05:39 7440-38-211/20/17 15:230.50 1 Barium 9.1 mg/kg 11/27/17 05:39 7440-39-311/20/17 15:230.50 1 Cadmium 0.080 mg/kg 11/27/17 05:39 7440-43-911/20/17 15:230.050 1 Chromium 10.6 mg/kg 11/27/17 05:39 7440-47-311/20/17 15:230.25 1 Lead 11.9 mg/kg 11/27/17 05:39 7439-92-111/20/17 15:230.50 1 Selenium 0.68J mg/kg 11/27/17 05:39 7782-49-211/20/17 15:230.75 1 Silver 1.3U mg/kg 11/27/17 13:00 7440-22-4 D311/20/17 15:232.5 10
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Short List Microwave
Acenaphthene 0.037U mg/kg 11/22/17 03:33 83-32-9 P111/21/17 21:170.10 1 Acenaphthylene 0.031U mg/kg 11/22/17 03:33 208-96-8 P111/21/17 21:170.10 1 Anthracene 0.031U mg/kg 11/22/17 03:33 120-12-7 P111/21/17 21:170.10 1 Benzo(a)anthracene 0.029U mg/kg 11/22/17 03:33 56-55-3 P111/21/17 21:170.10 1 Benzo(a)pyrene 0.012U mg/kg 11/22/17 03:33 50-32-8 P111/21/17 21:170.10 1 Benzo(b)fluoranthene 0.075U mg/kg 11/22/17 03:33 205-99-2 P111/21/17 21:170.10 1 Benzo(g,h,i)perylene 0.036U mg/kg 11/22/17 03:33 191-24-2 P111/21/17 21:170.10 1 Benzo(k)fluoranthene 0.022U mg/kg 11/22/17 03:33 207-08-9 P111/21/17 21:170.10 1 Chrysene 0.036U mg/kg 11/22/17 03:33 218-01-9 P111/21/17 21:170.10 1 Dibenz(a,h)anthracene 0.050U mg/kg 11/22/17 03:33 53-70-3 P111/21/17 21:170.10 1 Fluoranthene 0.033U mg/kg 11/22/17 03:33 206-44-0 P111/21/17 21:170.10 1 Fluorene 0.045U mg/kg 11/22/17 03:33 86-73-7 P111/21/17 21:170.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/30/2017 11:25 AM
Pace Analytical Services, LLC 8 East Tower Circle
Ormond Beach, FL 32174 (386)672-5668
Pace Project No.:
Project:
35347296
IRL MUCK DREDGING
Sample: A1-066 Lab ID: 35347296006 Collected: 11/08/17 12:20 Received: 11/09/17 10:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualPQL
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Short List Microwave
Indeno(1,2,3-cd)pyrene 0.050U mg/kg 11/22/17 03:33 193-39-5 P111/21/17 21:170.10 1 1-Methylnaphthalene 0.035U mg/kg 11/22/17 03:33 90-12-0 P111/21/17 21:170.10 1 2-Methylnaphthalene 0.040U mg/kg 11/22/17 03:33 91-57-6 P111/21/17 21:170.10 1 Naphthalene 0.032U mg/kg 11/22/17 03:33 91-20-3 P111/21/17 21:170.10 1 Phenanthrene 0.038U mg/kg 11/22/17 03:33 85-01-8 P111/21/17 21:170.10 1 Pyrene 0.050U mg/kg 11/22/17 03:33 129-00-0 P111/21/17 21:170.10 1 Surrogates Nitrobenzene-d5 (S) 46 % 11/22/17 03:33 4165-60-011/21/17 21:1716-123 1 2-Fluorobiphenyl (S) 44 % 11/22/17 03:33 321-60-811/21/17 21:1732-129 1 p-Terphenyl-d14 (S) 61 % 11/22/17 03:33 1718-51-011/21/17 21:1738-138 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 2.5 % 11/27/17 09:08 D60.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/30/2017 11:25 AM
Pace Analytical Services, LLC 8 East Tower Circle
Ormond Beach, FL 32174 (386)672-5668
Pace Project No.:
Project:
35347296
IRL MUCK DREDGING
Sample: A1-069 Lab ID: 35347296007 Collected: 11/08/17 11:50 Received: 11/09/17 10:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualPQL
Analytical Method: EPA 7471 Preparation Method: EPA 74717471 Mercury
Mercury 0.081 mg/kg 11/21/17 10:20 7439-97-611/20/17 16:300.037 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 73.5 % 11/20/17 09:570.10 1
Analytical Method: EPA 350.1 Preparation Method: EPA 350.1350.1 Ammonia
Nitrogen, Ammonia 66.3 mg/kg 11/15/17 15:24 7664-41-711/14/17 09:181.9 1
Analytical Method: EPA 351.2 Preparation Method: EPA 351.2351.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total 3080 mg/kg 11/15/17 15:52 7727-37-911/10/17 08:12415 5
Analytical Method: EPA 365.4 Preparation Method: EPA 365.4365.4 Phosphorus, Total
Phosphorus, Total (as P) 476 mg/kg 11/15/17 15:52 7723-14-011/10/17 08:1282.9 5
Analytical Method: EPA 9056 Preparation Method: EPA 90569056 IC Anions 48hr
Nitrogen, NO2 plus NO3 9.4U mg/kg 11/10/17 01:1411/09/17 17:0018.7 1 Orthophosphate as P 18.7U mg/kg 11/10/17 01:14 M111/09/17 17:0037.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/30/2017 11:25 AM
Pace Analytical Services, LLC 8 East Tower Circle
Ormond Beach, FL 32174 (386)672-5668
Pace Project No.:
Project:
35347296
IRL MUCK DREDGING
Sample: A1-069 Lab ID: 35347296008 Collected: 11/08/17 11:50 Received: 11/09/17 10:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualPQL
Analytical Method: EPA 8081 Preparation Method: EPA 35468081 GCS Pesticides
Aldrin 0.00036U mg/kg 11/23/17 04:03 309-00-211/22/17 08:300.011 5 alpha-BHC 0.00043U mg/kg 11/23/17 04:03 319-84-6 D311/22/17 08:300.011 5 beta-BHC 0.00048U mg/kg 11/23/17 04:03 319-85-711/22/17 08:300.011 5 delta-BHC 0.00054U mg/kg 11/23/17 04:03 319-86-811/22/17 08:300.011 5 gamma-BHC (Lindane) 0.00093U mg/kg 11/23/17 04:03 58-89-911/22/17 08:300.011 5 Chlordane (Technical) 0.099U mg/kg 11/23/17 04:03 57-74-911/22/17 08:300.11 5 4,4'-DDD 0.00082U mg/kg 11/23/17 04:03 72-54-811/22/17 08:300.011 5 4,4'-DDE 0.00038U mg/kg 11/23/17 04:03 72-55-911/22/17 08:300.011 5 4,4'-DDT 0.00060U mg/kg 11/23/17 04:03 50-29-311/22/17 08:300.011 5 Dieldrin 0.00025U mg/kg 11/23/17 04:03 60-57-111/22/17 08:300.011 5 Endosulfan I 0.00016U mg/kg 11/23/17 04:03 959-98-811/22/17 08:300.011 5 Endosulfan II 0.00036U mg/kg 11/23/17 04:03 33213-65-911/22/17 08:300.011 5 Endosulfan sulfate 0.00027U mg/kg 11/23/17 04:03 1031-07-8 CH11/22/17 08:300.011 5 Endrin 0.00033U mg/kg 11/23/17 04:03 72-20-811/22/17 08:300.011 5 Endrin aldehyde 0.00041U mg/kg 11/23/17 04:03 7421-93-411/22/17 08:300.021 5 Endrin ketone 0.00050U mg/kg 11/23/17 04:03 53494-70-5 CH11/22/17 08:300.011 5 Heptachlor 0.00024U mg/kg 11/23/17 04:03 76-44-811/22/17 08:300.011 5 Heptachlor epoxide 0.00069U mg/kg 11/23/17 04:03 1024-57-311/22/17 08:300.011 5 Methoxychlor 0.0066U mg/kg 11/23/17 04:03 72-43-511/22/17 08:300.011 5 Toxaphene 0.046U mg/kg 11/23/17 04:03 8001-35-211/22/17 08:300.11 5 Surrogates Tetrachloro-m-xylene (S) 48 % 11/23/17 04:03 877-09-8 S011/22/17 08:3053-140 5 Decachlorobiphenyl (S) 43 % 11/23/17 04:03 2051-24-311/22/17 08:3043-157 5
Analytical Method: EPA 6010 Preparation Method: EPA 30506010 MET ICP
Arsenic 6.7 mg/kg 11/27/17 05:54 7440-38-211/20/17 15:230.72 1 Barium 19.0 mg/kg 11/27/17 05:54 7440-39-311/20/17 15:230.72 1 Cadmium 0.23 mg/kg 11/27/17 05:54 7440-43-911/20/17 15:230.072 1 Chromium 43.3 mg/kg 11/27/17 13:04 7440-47-311/20/17 15:233.6 10 Lead 31.2 mg/kg 11/27/17 05:54 7439-92-111/20/17 15:230.72 1 Selenium 1.7 mg/kg 11/27/17 05:54 7782-49-211/20/17 15:231.1 1 Silver 1.8U mg/kg 11/27/17 13:04 7440-22-4 D311/20/17 15:233.6 10
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Short List Microwave
Acenaphthene 0.045U mg/kg 11/22/17 03:56 83-32-9 P111/21/17 21:170.12 1 Acenaphthylene 0.039U mg/kg 11/22/17 03:56 208-96-8 P111/21/17 21:170.12 1 Anthracene 0.038U mg/kg 11/22/17 03:56 120-12-7 P111/21/17 21:170.12 1 Benzo(a)anthracene 0.036U mg/kg 11/22/17 03:56 56-55-3 P111/21/17 21:170.12 1 Benzo(a)pyrene 0.015U mg/kg 11/22/17 03:56 50-32-8 P111/21/17 21:170.12 1 Benzo(b)fluoranthene 0.19 mg/kg 11/22/17 03:56 205-99-2 P111/21/17 21:170.12 1 Benzo(g,h,i)perylene 0.045U mg/kg 11/22/17 03:56 191-24-2 P111/21/17 21:170.12 1 Benzo(k)fluoranthene 0.027U mg/kg 11/22/17 03:56 207-08-9 P111/21/17 21:170.12 1 Chrysene 0.044U mg/kg 11/22/17 03:56 218-01-9 P111/21/17 21:170.12 1 Dibenz(a,h)anthracene 0.063U mg/kg 11/22/17 03:56 53-70-3 P111/21/17 21:170.12 1 Fluoranthene 0.15 mg/kg 11/22/17 03:56 206-44-0 P111/21/17 21:170.12 1 Fluorene 0.056U mg/kg 11/22/17 03:56 86-73-7 P111/21/17 21:170.12 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/30/2017 11:25 AM
Pace Analytical Services, LLC 8 East Tower Circle
Ormond Beach, FL 32174 (386)672-5668
Pace Project No.:
Project:
35347296
IRL MUCK DREDGING
Sample: A1-069 Lab ID: 35347296008 Collected: 11/08/17 11:50 Received: 11/09/17 10:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualPQL
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Short List Microwave
Indeno(1,2,3-cd)pyrene 0.063U mg/kg 11/22/17 03:56 193-39-5 P111/21/17 21:170.12 1 1-Methylnaphthalene 0.044U mg/kg 11/22/17 03:56 90-12-0 P111/21/17 21:170.12 1 2-Methylnaphthalene 0.050U mg/kg 11/22/17 03:56 91-57-6 P111/21/17 21:170.12 1 Naphthalene 0.040U mg/kg 11/22/17 03:56 91-20-3 P111/21/17 21:170.12 1 Phenanthrene 0.047U mg/kg 11/22/17 03:56 85-01-8 P111/21/17 21:170.12 1 Pyrene 0.13 mg/kg 11/22/17 03:56 129-00-0 P111/21/17 21:170.12 1 Surrogates Nitrobenzene-d5 (S) 47 % 11/22/17 03:56 4165-60-011/21/17 21:1716-123 1 2-Fluorobiphenyl (S) 42 % 11/22/17 03:56 321-60-811/21/17 21:1732-129 1 p-Terphenyl-d14 (S) 41 % 11/22/17 03:56 1718-51-011/21/17 21:1738-138 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 20.5 % 11/27/17 09:080.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/30/2017 11:25 AM
Pace Analytical Services, LLC 8 East Tower Circle
Ormond Beach, FL 32174 (386)672-5668
Pace Project No.:
Project:
35347296
IRL MUCK DREDGING
Sample: A1A-02 Lab ID: 35347296009 Collected: 11/08/17 15:15 Received: 11/09/17 10:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualPQL
Analytical Method: EPA 7471 Preparation Method: EPA 74717471 Mercury
Mercury 0.048 mg/kg 11/21/17 10:22 7439-97-611/20/17 16:300.021 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 56.5 % 11/20/17 09:570.10 1
Analytical Method: EPA 350.1 Preparation Method: EPA 350.1350.1 Ammonia
Nitrogen, Ammonia 4.9 mg/kg 11/15/17 15:26 7664-41-711/14/17 09:181.1 1
Analytical Method: EPA 351.2 Preparation Method: EPA 351.2351.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total 614 mg/kg 11/15/17 15:52 7727-37-911/10/17 08:12238 5
Analytical Method: EPA 365.4 Preparation Method: EPA 365.4365.4 Phosphorus, Total
Phosphorus, Total (as P) 89.7 mg/kg 11/15/17 15:52 7723-14-011/10/17 08:1247.6 5
Analytical Method: EPA 9056 Preparation Method: EPA 90569056 IC Anions 48hr
Nitrogen, NO2 plus NO3 5.1U mg/kg 11/10/17 00:5111/09/17 17:0010.1 1 Orthophosphate as P 10.1U mg/kg 11/10/17 00:5111/09/17 17:0020.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/30/2017 11:25 AM
Pace Analytical Services, LLC 8 East Tower Circle
Ormond Beach, FL 32174 (386)672-5668
Pace Project No.:
Project:
35347296
IRL MUCK DREDGING
Sample: A1A-02 Lab ID: 35347296010 Collected: 11/08/17 15:15 Received: 11/09/17 10:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualPQL
Analytical Method: EPA 8081 Preparation Method: EPA 35468081 GCS Pesticides
Aldrin 0.00032U mg/kg 11/23/17 04:22 309-00-211/22/17 08:300.0093 5 alpha-BHC 0.00038U mg/kg 11/23/17 04:22 319-84-6 D311/22/17 08:300.0093 5 beta-BHC 0.00042U mg/kg 11/23/17 04:22 319-85-711/22/17 08:300.0093 5 delta-BHC 0.00047U mg/kg 11/23/17 04:22 319-86-811/22/17 08:300.0093 5 gamma-BHC (Lindane) 0.00081U mg/kg 11/23/17 04:22 58-89-911/22/17 08:300.0093 5 Chlordane (Technical) 0.087U mg/kg 11/23/17 04:22 57-74-911/22/17 08:300.093 5 4,4'-DDD 0.00071U mg/kg 11/23/17 04:22 72-54-811/22/17 08:300.0093 5 4,4'-DDE 0.00033U mg/kg 11/23/17 04:22 72-55-911/22/17 08:300.0093 5 4,4'-DDT 0.00052U mg/kg 11/23/17 04:22 50-29-311/22/17 08:300.0093 5 Dieldrin 0.00022U mg/kg 11/23/17 04:22 60-57-111/22/17 08:300.0093 5 Endosulfan I 0.00014U mg/kg 11/23/17 04:22 959-98-811/22/17 08:300.0093 5 Endosulfan II 0.00031U mg/kg 11/23/17 04:22 33213-65-911/22/17 08:300.0093 5 Endosulfan sulfate 0.00023U mg/kg 11/23/17 04:22 1031-07-8 CH11/22/17 08:300.0093 5 Endrin 0.00028U mg/kg 11/23/17 04:22 72-20-811/22/17 08:300.0093 5 Endrin aldehyde 0.00036U mg/kg 11/23/17 04:22 7421-93-411/22/17 08:300.018 5 Endrin ketone 0.00044U mg/kg 11/23/17 04:22 53494-70-5 CH11/22/17 08:300.0093 5 Heptachlor 0.00021U mg/kg 11/23/17 04:22 76-44-811/22/17 08:300.0093 5 Heptachlor epoxide 0.00061U mg/kg 11/23/17 04:22 1024-57-311/22/17 08:300.0093 5 Methoxychlor 0.0057U mg/kg 11/23/17 04:22 72-43-511/22/17 08:300.0093 5 Toxaphene 0.040U mg/kg 11/23/17 04:22 8001-35-211/22/17 08:300.093 5 Surrogates Tetrachloro-m-xylene (S) 75 % 11/23/17 04:22 877-09-811/22/17 08:3053-140 5 Decachlorobiphenyl (S) 74 % 11/23/17 04:22 2051-24-311/22/17 08:3043-157 5
Analytical Method: EPA 6010 Preparation Method: EPA 30506010 MET ICP
Arsenic 1.6 mg/kg 11/27/17 05:59 7440-38-211/20/17 15:230.63 1 Barium 16.2 mg/kg 11/27/17 05:59 7440-39-311/20/17 15:230.63 1 Cadmium 0.060J mg/kg 11/27/17 05:59 7440-43-911/20/17 15:230.063 1 Chromium 9.1 mg/kg 11/27/17 05:59 7440-47-311/20/17 15:230.32 1 Lead 8.4 mg/kg 11/27/17 05:59 7439-92-111/20/17 15:230.63 1 Selenium 1.1 mg/kg 11/27/17 05:59 7782-49-211/20/17 15:230.95 1 Silver 1.6U mg/kg 11/27/17 13:08 7440-22-4 D311/20/17 15:233.2 10
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Short List Microwave
Acenaphthene 0.039U mg/kg 11/22/17 04:19 83-32-9 P111/21/17 21:170.11 1 Acenaphthylene 0.033U mg/kg 11/22/17 04:19 208-96-8 P111/21/17 21:170.11 1 Anthracene 0.033U mg/kg 11/22/17 04:19 120-12-7 P111/21/17 21:170.11 1 Benzo(a)anthracene 0.031U mg/kg 11/22/17 04:19 56-55-3 P111/21/17 21:170.11 1 Benzo(a)pyrene 0.082J mg/kg 11/22/17 04:19 50-32-8 P111/21/17 21:170.11 1 Benzo(b)fluoranthene 0.080U mg/kg 11/22/17 04:19 205-99-2 P111/21/17 21:170.11 1 Benzo(g,h,i)perylene 0.038U mg/kg 11/22/17 04:19 191-24-2 P111/21/17 21:170.11 1 Benzo(k)fluoranthene 0.023U mg/kg 11/22/17 04:19 207-08-9 P111/21/17 21:170.11 1 Chrysene 0.038U mg/kg 11/22/17 04:19 218-01-9 P111/21/17 21:170.11 1 Dibenz(a,h)anthracene 0.054U mg/kg 11/22/17 04:19 53-70-3 P111/21/17 21:170.11 1 Fluoranthene 0.11 mg/kg 11/22/17 04:19 206-44-0 P111/21/17 21:170.11 1 Fluorene 0.048U mg/kg 11/22/17 04:19 86-73-7 P111/21/17 21:170.11 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/30/2017 11:25 AM
Pace Analytical Services, LLC 8 East Tower Circle
Ormond Beach, FL 32174 (386)672-5668
Pace Project No.:
Project:
35347296
IRL MUCK DREDGING
Sample: A1A-02 Lab ID: 35347296010 Collected: 11/08/17 15:15 Received: 11/09/17 10:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualPQL
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Short List Microwave
Indeno(1,2,3-cd)pyrene 0.054U mg/kg 11/22/17 04:19 193-39-5 P111/21/17 21:170.11 1 1-Methylnaphthalene 0.038U mg/kg 11/22/17 04:19 90-12-0 P111/21/17 21:170.11 1 2-Methylnaphthalene 0.043U mg/kg 11/22/17 04:19 91-57-6 P111/21/17 21:170.11 1 Naphthalene 0.034U mg/kg 11/22/17 04:19 91-20-3 P111/21/17 21:170.11 1 Phenanthrene 0.040U mg/kg 11/22/17 04:19 85-01-8 P111/21/17 21:170.11 1 Pyrene 0.11 mg/kg 11/22/17 04:19 129-00-0 P111/21/17 21:170.11 1 Surrogates Nitrobenzene-d5 (S) 38 % 11/22/17 04:19 4165-60-011/21/17 21:1716-123 1 2-Fluorobiphenyl (S) 37 % 11/22/17 04:19 321-60-811/21/17 21:1732-129 1 p-Terphenyl-d14 (S) 61 % 11/22/17 04:19 1718-51-011/21/17 21:1738-138 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 8.4 % 11/27/17 09:080.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/30/2017 11:25 AM
Pace Analytical Services, LLC 8 East Tower Circle
Ormond Beach, FL 32174 (386)672-5668
Pace Project No.:
Project:
35347296
IRL MUCK DREDGING
Sample: A1A-08 Lab ID: 35347296011 Collected: 11/08/17 15:00 Received: 11/09/17 10:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualPQL
Analytical Method: EPA 7471 Preparation Method: EPA 74717471 Mercury
Mercury 0.085 mg/kg 11/21/17 10:35 7439-97-611/20/17 16:300.036 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 75.8 % 11/20/17 09:570.10 1
Analytical Method: EPA 350.1 Preparation Method: EPA 350.1350.1 Ammonia
Nitrogen, Ammonia 17.3 mg/kg 11/15/17 15:28 7664-41-711/14/17 09:182.0 1
Analytical Method: EPA 351.2 Preparation Method: EPA 351.2351.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total 3990 mg/kg 11/15/17 15:53 7727-37-911/10/17 08:12496 5
Analytical Method: EPA 365.4 Preparation Method: EPA 365.4365.4 Phosphorus, Total
Phosphorus, Total (as P) 667 mg/kg 11/15/17 15:53 7723-14-011/10/17 08:1299.2 5
Analytical Method: EPA 9056 Preparation Method: EPA 90569056 IC Anions 48hr
Nitrogen, NO2 plus NO3 10.1U mg/kg 11/10/17 00:2711/09/17 17:0020.2 1 Orthophosphate as P 20.2U mg/kg 11/10/17 00:2711/09/17 17:0040.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/30/2017 11:25 AM
Pace Analytical Services, LLC 8 East Tower Circle
Ormond Beach, FL 32174 (386)672-5668
Pace Project No.:
Project:
35347296
IRL MUCK DREDGING
Sample: A1A-08 Lab ID: 35347296012 Collected: 11/08/17 15:00 Received: 11/09/17 10:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualPQL
Analytical Method: EPA 8081 Preparation Method: EPA 35468081 GCS Pesticides
Aldrin 0.00033U mg/kg 11/23/17 04:41 309-00-211/22/17 08:300.0096 5 alpha-BHC 0.00039U mg/kg 11/23/17 04:41 319-84-6 D311/22/17 08:300.0096 5 beta-BHC 0.00044U mg/kg 11/23/17 04:41 319-85-711/22/17 08:300.0096 5 delta-BHC 0.00049U mg/kg 11/23/17 04:41 319-86-811/22/17 08:300.0096 5 gamma-BHC (Lindane) 0.00084U mg/kg 11/23/17 04:41 58-89-911/22/17 08:300.0096 5 Chlordane (Technical) 0.090U mg/kg 11/23/17 04:41 57-74-911/22/17 08:300.096 5 4,4'-DDD 0.00074U mg/kg 11/23/17 04:41 72-54-811/22/17 08:300.0096 5 4,4'-DDE 0.00034U mg/kg 11/23/17 04:41 72-55-911/22/17 08:300.0096 5 4,4'-DDT 0.00054U mg/kg 11/23/17 04:41 50-29-311/22/17 08:300.0096 5 Dieldrin 0.00023U mg/kg 11/23/17 04:41 60-57-111/22/17 08:300.0096 5 Endosulfan I 0.00014U mg/kg 11/23/17 04:41 959-98-811/22/17 08:300.0096 5 Endosulfan II 0.00032U mg/kg 11/23/17 04:41 33213-65-911/22/17 08:300.0096 5 Endosulfan sulfate 0.00024U mg/kg 11/23/17 04:41 1031-07-8 CH11/22/17 08:300.0096 5 Endrin 0.00029U mg/kg 11/23/17 04:41 72-20-811/22/17 08:300.0096 5 Endrin aldehyde 0.00037U mg/kg 11/23/17 04:41 7421-93-411/22/17 08:300.019 5 Endrin ketone 0.00045U mg/kg 11/23/17 04:41 53494-70-5 CH11/22/17 08:300.0096 5 Heptachlor 0.00022U mg/kg 11/23/17 04:41 76-44-811/22/17 08:300.0096 5 Heptachlor epoxide 0.00063U mg/kg 11/23/17 04:41 1024-57-311/22/17 08:300.0096 5 Methoxychlor 0.0059U mg/kg 11/23/17 04:41 72-43-511/22/17 08:300.0096 5 Toxaphene 0.042U mg/kg 11/23/17 04:41 8001-35-211/22/17 08:300.096 5 Surrogates Tetrachloro-m-xylene (S) 58 % 11/23/17 04:41 877-09-811/22/17 08:3053-140 5 Decachlorobiphenyl (S) 58 % 11/23/17 04:41 2051-24-311/22/17 08:3043-157 5
Analytical Method: EPA 6010 Preparation Method: EPA 30506010 MET ICP
Arsenic 4.9 mg/kg 11/27/17 06:04 7440-38-211/20/17 15:230.67 1 Barium 18.3 mg/kg 11/27/17 06:04 7440-39-311/20/17 15:230.67 1 Cadmium 0.25 mg/kg 11/27/17 06:04 7440-43-911/20/17 15:230.067 1 Chromium 42.5 mg/kg 11/27/17 13:12 7440-47-311/20/17 15:233.3 10 Lead 26.9 mg/kg 11/27/17 06:04 7439-92-111/20/17 15:230.67 1 Selenium 1.2 mg/kg 11/27/17 06:04 7782-49-211/20/17 15:231.0 1 Silver 1.7U mg/kg 11/27/17 13:12 7440-22-4 D311/20/17 15:233.3 10
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Short List Microwave
Acenaphthene 0.041U mg/kg 11/22/17 04:42 83-32-9 P111/21/17 21:170.11 1 Acenaphthylene 0.035U mg/kg 11/22/17 04:42 208-96-8 P111/21/17 21:170.11 1 Anthracene 0.034U mg/kg 11/22/17 04:42 120-12-7 P111/21/17 21:170.11 1 Benzo(a)anthracene 0.032U mg/kg 11/22/17 04:42 56-55-3 P111/21/17 21:170.11 1 Benzo(a)pyrene 0.013U mg/kg 11/22/17 04:42 50-32-8 P111/21/17 21:170.11 1 Benzo(b)fluoranthene 0.084U mg/kg 11/22/17 04:42 205-99-2 P111/21/17 21:170.11 1 Benzo(g,h,i)perylene 0.040U mg/kg 11/22/17 04:42 191-24-2 P111/21/17 21:170.11 1 Benzo(k)fluoranthene 0.024U mg/kg 11/22/17 04:42 207-08-9 P111/21/17 21:170.11 1 Chrysene 0.040U mg/kg 11/22/17 04:42 218-01-9 P111/21/17 21:170.11 1 Dibenz(a,h)anthracene 0.056U mg/kg 11/22/17 04:42 53-70-3 P111/21/17 21:170.11 1 Fluoranthene 0.12 mg/kg 11/22/17 04:42 206-44-0 P111/21/17 21:170.11 1 Fluorene 0.050U mg/kg 11/22/17 04:42 86-73-7 P111/21/17 21:170.11 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/30/2017 11:25 AM
Pace Analytical Services, LLC 8 East Tower Circle
Ormond Beach, FL 32174 (386)672-5668
Pace Project No.:
Project:
35347296
IRL MUCK DREDGING
Sample: A1A-08 Lab ID: 35347296012 Collected: 11/08/17 15:00 Received: 11/09/17 10:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualPQL
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Short List Microwave
Indeno(1,2,3-cd)pyrene 0.056U mg/kg 11/22/17 04:42 193-39-5 P111/21/17 21:170.11 1 1-Methylnaphthalene 0.039U mg/kg 11/22/17 04:42 90-12-0 P111/21/17 21:170.11 1 2-Methylnaphthalene 0.045U mg/kg 11/22/17 04:42 91-57-6 P111/21/17 21:170.11 1 Naphthalene 0.036U mg/kg 11/22/17 04:42 91-20-3 P111/21/17 21:170.11 1 Phenanthrene 0.042U mg/kg 11/22/17 04:42 85-01-8 P111/21/17 21:170.11 1 Pyrene 0.11J mg/kg 11/22/17 04:42 129-00-0 P111/21/17 21:170.11 1 Surrogates Nitrobenzene-d5 (S) 41 % 11/22/17 04:42 4165-60-011/21/17 21:1716-123 1 2-Fluorobiphenyl (S) 34 % 11/22/17 04:42 321-60-811/21/17 21:1732-129 1 p-Terphenyl-d14 (S) 45 % 11/22/17 04:42…
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