Attachment 7 - C and E QAPS.pdf

DEFENSE LOGISTICS AGENCY ENERGY Page 1 of 1

8725 JOHN J. KINGMAN ROAD

FORT BELVOIR, VIRGINIA 22060-6222

DISTRIBUTION STATEMENT A: APPROVED FOR PUBLIC RELEASE. DISTRIBUTION IS UNLIMITED

Signature

Prepared by:

Quality/Technical Support Office Approval:

Contracting Approval:

C1.02 ASSIST DATABASE OF SPECIFICATIONS (DEC 2016)

Unless otherwise specified, current versions of defense or federal specifications and standards, military handbooks, commercial item descriptions, qualified product lists, and other related technical documents cited in this solicitation/contract can be accessed from the Department of Defense (DoD) Acquisition Streamlining and Standardization Information System (ASSIST) database at https://assist.dla.mil under ASSIST-Quick Search or http://quicksearch.dla.mil. ASSIST is the official source for all Defense Standardization Program documents and contains the most current information on documents prepared by DoD, as well as information on how to acquire referenced non-Government standards that have been adopted for DoD use. Note that commercial or foreign specifications are not located on ASSIST and must be obtained from the relevant sponsoring organization (e.g. ASTM, SAE, API, ISO, etc.). Registered ASSIST account holders may establish profiles to receive automatic E-mail alerts when changes are planned or made to documents of interest by selecting criteria on the [Alert Portal Profile Maintenance] screens accessed from the [User Profile] menu. Users may also view or download a bi-monthly summary of changes to the ASSIST database under the [ASSIST Update] menu.

Basic instructions on how to use ASSIST:

1. Go to http://quicksearch.dla.mil/.

2. Type in the numeric portion of the specification or Qualified Product List (QPL) and click on the Search button.

3. Look through the search results to find the desired document and click on the Document ID.

a. For specifications: click on the .pdf link under Media.

b. For QPL information: click on the View Qualified Product Database (QPD) data link to open the QPD

i. Click on the link in the Govt Designation Column to view qualified products

1. To view qualified source plants, click on the Source Plants link under the Related Links column

DEFENSE LOGISTICS AGENCY ENERGY

FORT BELVOIR, VIRGINIA 22060-6222

DISTRIBUTION STATEMENT – A: APPROVED FOR PUBLIC RELEASE. DISTRIBUTION IS UNLIMITED

C16.01 TURBINE FUEL, AVIATION (JP5) (DLA ENERGY MAY 2024)

NATIONAL STOCK NUMBER PRODUCT NOMENCLATURE DLA ENERGY PRODUCT

9130-00-273-2379 Turbine Fuel, Aviation, JP-5 JP5 9130-01-499-9521 Turbine Fuel, Aviation, JP-5 (Bunker fuel overseas locations only) JP5

Product shall meet MIL-DTL-5624X, Turbine Fuel, Aviation, Grade JP-5, dated February 12, 2024.

(a) SPECIFICATION MODIFICATION: The requirements of Table I in the specification are modified as follows:

a. FILTRATION TIME TESTING. Round upwards when reporting the filtration time, in minutes. For example, a filtration time of 4 minutes, 22 seconds, would be reported as 5 minutes.

b. FLASH POINT TESTING. The referee procedure for performing flash point testing of JP-5 shall be the manual method of the latest revision of ASTM D93, as opposed to the automated version of ASTM D93.

c. FLASH POINT.

i. All batches of JP-5 that are presented for Government acceptance at origin and for subsequent shipment through a multiproduct pipeline, shall meet a minimum flash point requirement of 62.5°C. This requirement is meant to address multiproduct commercial pipelines and does not apply to multiproduct systems within a facility.

ii. In the U.S. all JP-5 deliveries in California, Oregon, Washington, and Alaska shall have a minimum Flash Point of 62.5 oC at the custody transfer point.

iii. In Australia all JP-5 deliveries shall have a minimum Flash Point of 61.5°C at the custody transfer point.

d. ACID NUMBER. For JP-5 delivered to Kodiak Island, Alaska, the maximum total acid number shall be 0.020 mg KOH/g.

e. MICRO-SEPAROMETER (MSEP) REQUIREMENTS.

i. Prior to initial production under this contract, the Contractor shall elect, on a one-time basis, which MSEP limit to meet for the balance of the contract. If the Contractor introduces Fuel System Icing Inhibitor (FSII) and/or Corrosion Inhibitor/Lubricity Improver (CI/LI) after verification of product conformance with the MSEP requirement, the product is not required to meet a fixed limit on subsequent MSEP tests.

ii. If the Contractor elects to verify conformance with the MSEP requirement on a sample of product that does not contain FSII and CI/LI, an additional MSEP test shall be performed on a hand blend containing jet fuel, FSII, CI/LI, and Antioxidant (only if required). The FSII shall be added to this hand blend at a concentration range between 0.08 volume percent minimum and 0.11 volume percent maximum. The amount of the CI/LI added to this hand blend shall be within the concentration range specified in QPL-25017.

f. ADDITIONAL REQUIREMENT APPLICABLE TO DEEP FREEZE PROGRAM ONLY. The Deep Freeze Program is for Antarctic operations of the Department of Defense and other federal agencies; whereby JP-5 sulfur content shall not exceed 0.0015 mass-percent (15 ppm).

(b) ADDITIVES.

a. Additives are required for deliveries of JP-5, per MIL-DTL-5624X, dated February 12, 2024, unless addition is excluded by specific solicitation line item, applicable contract clause, or another contractual requirement. FSII included in jet fuel shall conform to MIL-DTL- 85470C, Inhibitor, Icing, Fuel System, High Flash, dated March 5, 2024.

b. The CI/LI additive(s) used shall conform to MIL-PRF-25017H Inhibitor, Corrosion/Lubricity Improver, Fuel Soluble, w/Amendment 1, dated August 4, 2011, and revalidated May 25, 2021,

c. Line injection of additives (FSII and CI/LI) from shipping tank to delivery conveyance or other free on board (FOB) point is permitted under the following conditions:

i. Additives must be proportionately injected throughout the entire loading process to ensure the additive is homogeneously blended into the jet fuel. The Contractor shall maintain records evidencing the homogeneous blending of all line injected additives. Such methods may include meter or tank gauge readings or test results taken at intervals to provide confidence in the injection process.

ii. When FSII is required, additive concentration must be verified based on a representative sample from each shipping conveyance.

(c) Conformance to specification requirements at the custody transfer point is required, however, prior to shipment, a laboratory hand blend of JP-5 fuel with all additives required by this contract shall be tested to verify compliance with the required specification (except for MSEP). MSEP analysis shall be performed per the Contractor’s election in MIL-DTL-5624X, dated February 12, 2024.

(d) ADDITIONAL SAMPLING: The government may request a sample of JP5 during each quarter of contract performance not to exceed 5 gallons. Samples shall be shipped in a 5-gallon epoxy lined can (preferred) or five 1-gallon epoxy lined cans. (NOTE: These samples are in addition to those required in accordance with Quality Assurance Provision (QAP) E1). The sample shall be shipped to

Naval Air Station HAZMART 5-Gallon TEST SAMPLE 22680 Hammond Road Bldg. 2385 Patuxent River, MD 20670 Attn: Terrence Dickerson, AB44100 Fuels & Lubricants Phone: (301) 757-0447; Email: terrence.w.dickerson.civ@us.navy.mil mailto:terrence.w.dickerson.civ@us.navy.mil

FORT BELVOIR, VIRGINIA 22060-6222

The paperwork provided with these samples shall include the following information:

Contract Number Contractor’s Name Product Refinery Location Quantity of Tank/Batch Full-Specification Test Report

(e) BATCH SAMPLING: The Contractor shall provide one 20 mL sample per each individual tank in a procurement batch.

For each 20 mL sample provided by the Contractor, the Contractor shall also submit a Refinery Certificate of Quality (RCQ), or Certificate of Analysis (CoA), as applicable, with the JP-5 sample when submitting to the US Naval Research Laboratory. The RCQ or CoA for each individual tank shall be representative of Level A testing for the JP-5 product.

NOTE: This sample is in addition to those required in accordance with Quality Assurance Provision (QAP) E1

QUANTITY OF SAMPLE WHEN SAMPLED SUBMISSION PERIOD

20 mL Upon completion of each individual procurement batch Shipped within 30 days of procurement batch delivery

“Batch” Definition in accordance with MIL-STD-3004-1A, 3.1.9: A specific quantity of product that is processed or utilized as a single unit and tested to meet test criteria and specifications.

The sample from each tank/batch shall be either an all-level sample or a composite of upper, middle, and lower samples. A copy of the batch’s full-specification test report shall accompany each sample. The sample container shall be any 20 mL amber borosilicate vial with a polytetrafluoroethylene (PTFE) lined screw cap. A tracking number for the samples shall be provided to: Terrence Dickerson at terrence.w.dickerson.civ@us.navy.mil or (301) 757-0447. Samples shall be shipped to:

Naval Air Station HAZMART 20mL TEST SAMPLE 22680 Hammond Road Bldg. 2385 Patuxent River, MD 20670 Attn: Terrence Dickerson, AB44100 Fuels & Lubricants

• Contract Number

• Contractor’s Name

• Product

• Refinery Location

• Quantity of Tank/Batch

• Full-Specification Test Report

For samples containing synthetic components, include the following additional information:

• Manufacturer of synthetic component

• Batch Number

• Date of Test Report

• Quantity of Tank/Batch

• Percent Composition

• Production Process of Synthetic Component

• Feedstock

• Full-Specification Test Report

Prepared by

Quality Technical Support Office Approval

Contracting Approval

FORT BELVOIR, VIRGINIA 22060-6222

C16.23 FUEL, NAVAL DISTILLATE (F-76) (DLA ENERGY FEBRUARY 2024)

NATIONAL STOCK NUMBER PRODUCT NOMENCLATURE DLA ENERGY PRODUCT CODE

9140-00-273-2377 Fuel, Naval Distillate F76

For supplies delivered under this contract, the Contractor shall conform to all International, Federal, State, and local environmental requirements applicable to the geographic location of the receiving activity on the date of delivery. The Contractor shall also comply with all applicable International Agreements, Treaties, Conventions, and the like to which the United States is a signatory or with whose terms the receiving activity has otherwise agreed to comply, including but not limited to, the requirements of MARPOL 73/78 Annex VI Regulations 14 and 18. The Contractor shall be responsible for determining the existence of all such requirements prior to the time deliveries are made. This includes delivery of fuel and documentation in a manner consistent with any existing or after-imposed Title V (Clean Air Act) Permits. The list of such requirements contained in this contract is not intended to be a complete list, and the Contractor shall be responsible for determining the existence of all such requirements. In the event that an International, Federal, State, and/or local environmental requirement, as identified above, is more stringent than a requirement contained in this contract, the Contractor shall deliver product(s) that complies with the more stringent requirement. Product(s) that fails to meet the more stringent requirement will be considered nonconforming supply. Product(s) to be supplied shall fully meet the requirements of the applicable specification(s). In the event that compliance with the more stringent requirement causes the contractor to incur additional costs, the contractor may request an equitable adjustment.

Unless otherwise indicated by the Contractor in writing, prior to award, the product offered shall be required to fully meet all applicable specifications. The supplier shall provide to the receiving vessel a “Statutory Sample” of at least 400 mL in volume, taken from the receiving vessel’s inlet bunker manifold, together with a Bunker Delivery Note (BDN). This sample will be sealed and carry a sample tag that provides the documentation required per MARPOL 73/78, Annex VI Regulation 18.

a) Naval Distillate Fuel (F-76) shall conform to the requirements of Military specification MIL-DTL-16884P dated 26 Sept 2017.

Nomenclature for Naval Distillate Fuel (F-76) is shown above.

b) SPECIFICATION MODIFICATIONS:

1) Flash Point: All batches of F-76 that are presented for Government acceptance at origin shall meet a minimum flash point requirement of 62.5 degrees Celsius (°C).

2) F-76 offered from a location other than where refined (excludes synthesized material as defined in section 3.2.2 and 3.2.3 of MIL- DTL-16884P) requires testing for FAME content by test method ASTM D7963, BS EN 14078, or IP 579. ASTM D7963 is considered to be the referee test method.

3) In Australia, all deliveries of F-76 shall have a minimum Flash Point of 62.5°C at the custody transfer point.

4) Ash, mass%: All batches of F-76 shall not exceed 0.010% Ash by ASTM D482.

c) MATERIALS: The F-76 supplied under this contract shall not contain un-hydrotreated light cycle oils or contain any stabilizer additives, or any other additive or material not explicitly allowed per section 3.2 of MIL-DTL-16884P.

For F-76 containing a synthetic component, the synthetic component shall be certified to Tables A-I and A-II of MIL-DTL-16884P; for synthesized iso-paraffins, the synthetic component shall be certified to Tables B-I and B-II of MIL-DTL-16884P. It is not necessary to analyze each batch of the synthetic component for compliance with Table A-II (or Table B-II, as applicable) once it is demonstrated that the process scheme is adequately controlled and if no significant changes to existing production operations have been made, such as a turnaround event on a refinery unit used to produce the synthetic component or a change in feedstock material. The signed F-76 synthetic component certification page shall be supplied for each shipment which includes synthetic paraffinic materials, attesting that no changes to the production process have been made, and certifying that the last certificate of analysis, dated and including Table A-II (or Table B-II, as applicable) results, is still valid.

d) ADDITIVES:

1) Lubricity Improver Additive (LIA) – Lubricity additives are allowed in F-76. The LIA additive(s) used shall conform to MIL-PRF- 32490A, Performance Specification, Additive, Lubricity Improver, Distillate Fuel, dated 24 May 2019 and found in ASSIST and shall

FORT BELVOIR, VIRGINIA 22060-6222

be listed in the electronic Qualified Products List (QPL)-32490, located in the Qualified Products Database (QPD) found at https://assist.dla.mil/ (or http://quicksearch.dla.mil) . Instructions on how to use ASSIST are located in QAP C1.02. Either Grade A.

Grade B, or Grade C material is suitable for treatment of de-sulfurized F-76. Additive concentration shall not exceed the maximum allowable concentration applicable to the specific additive selected for inclusion in finished F-76.

2) Information pertaining to qualification of additives not currently listed on QPL-32490 may be obtained from Commander, Naval Sea Systems Command, ATTN: SEA 05S, 1333 Isaac Hull Avenue, SE, Stop 5160, Washington Navy Yard, DC 20376-5160, USA, or by e-mailing CommandStandards@navy.mil.

3) Dyes and Markers - Red dye required in off-highway diesel fuel in accordance with 40 CFR Part 80 as modified by the Environmental Protection Agency's interim final rule published in the Federal Register dated July 14, 1994 shall not be added to F-

76. The finished product shall show no visual evidence of red dye. This F-76 product is for military, off-highway use only and must be segregated at all times from any diesel fuel used on-highway. NOTE: Red dye does not apply to Atlantic/Europe/Mediterranean or Western Pacific Overseas Bulk purchase programs unless offering refinery is located in the United States or one of its possessions.

e) ADDITIONAL SAMPLING: The government may request a sample of F-76 during each quarter of contract performance not to exceed 5 gallons. Samples shall be shipped in a 5-gallon epoxy lined can (preferred) or five 1-gallon epoxy lined cans. (NOTE: These samples are in addition to those required in accordance with Quality Assurance Provision (QAP) E1). The sample shall be shipped to:

Naval Air Station HAZMART 5-gallon TEST SAMPLE 22680 Hammond Road Bldg. 2385 Patuxent River, MD 20670 Attn: Terrence Dickerson, AB44100 Fuels & Lubricants Phone: (301) 757-0447; Email: terrence.w.dickerson.civ@us.navy.mil

The paperwork provided with these samples shall include the following information:

Contract Number Contractor’s Name Product Refinery Location Quantity of Tank/Batch Full-Specification Test Report

f) BATCH SAMPLING: The Contractor shall provide one 20 mL sample per each individual tank in a procurement batch.

For each 20 mL sample provided by the Contractor, the Contractor shall also submit a Refinery Certificate of Quality (RCQ), or Certificate of Analysis (CoA), as applicable, with the F-76 sample when submitting to the US Naval Research Laboratory.

The RCQ or CoA for each individual tank shall be representative of Level A testing for the F-76 product.

NOTE: This sample is in addition to those required in accordance with Quality Assurance Provision (QAP) E1

QUANTITY OF SAMPLE WHEN SAMPLED SUBMISSION PERIOD

20 mL Upon completion of each individual procurement batch

Shipped within 30 days of delivery of procurement batch

“Batch” Definition in accordance with MIL-STD-3004-1A, 3.1.9: A specific quantity of product that is processed or utilized as a single unit and tested to meet test criteria and specifications.

The sample from each tank/batch shall be either an all-level sample or a composite of upper, middle, and lower samples. A copy of the full-specification test report shall accompany each sample. The sample container will be any 20 mL amber borosilicate vial with a polytetrafluoroethylene (PTFE) lined screw cap. A tracking number for the samples shall be provided to: Terrence Dickerson at terrence.w.dickerson.civ@us.navy.mil or (301) 757-0447. Samples shall be shipped to:

mailto:CommandStandards@navy.mil

FORT BELVOIR, VIRGINIA 22060-6222

Naval Air Station HAZMART 20mL TEST SAMPLE 22680 Hammond Road Bldg. 2385 Patuxent River, MD 20670 Attn: Terrence Dickerson, AB44100 Fuels & Lubricants

Contract Number Contractor’s Name Product Refinery Location Quantity of Tank/Batch Full-Specification Test Report

For samples containing synthetic components, include the following additional information:

Manufacturer of synthetic component Batch Number Date of Test Report Quantity of Tank/Batch Percent Composition Production Process of Synthetic Component Feedstock Full-Specification Test Report

g) TRACEABILITY:

1) F-76 fuel supplied under this contract shall maintain traceability with respect to additives and materials, which is defined as the ability to trace the individual batch of fuel back to the original point of manufacture through documentation.

2) All traceability documentation shall be sufficient to guarantee that at no point have any unauthorized materials or additives been blended into the final product or any of its associated blend components per section 3.2 Material of MIL-DTL-16884P.

3) For all F-76 supplied, the traceability documentation shall consist of statement(s) attesting to the materials composition, which includes materials derived from non-petroleum sources, additives and their concentration levels. Additives and concentrations to be reported include LIAs outlined in section d.1 above and any trace additives resulting from existing tank heels, product trail-back in a multiproduct system, all product blending operations, etc.

4) If F-76 is produced by means of blending, the traceability requirement and documentation for additives and materials shall apply to each blending component used from the point of manufacture through the blend operation. Materials composition, additives and their concentration levels shall be included. The requirement and intent of traceability for blend components is not to obtain full certificates of analysis of each individual blend component, but for certification that no unapproved additives or materials are present in blend components used.

5) The form titled: “F-76 Traceability Signature Page” (attached below) shall be used to document conformance with the provisions of this traceability paragraph. The offeror/supplier shall comply with this requirement utilizing one of the three options below and notification shall be provided to both the contracting office and QT@dla.mil during the pre-award phase which option was chosen for compliance. Documents provided in conjunction with individual shipments shall be uploaded into Wide Area Work Flow as attachments under the quality tab.

i) OPTION 1 – As part of the offeror submission package the offeror shall provide the traceability signature page from each entity in the supply chain providing and/or handling F-76 product and/or blending components all the way back to the point of manufacture. For each individual shipment, the supplier will submit a traceability page signed only by the awardee.

ii) OPTION 2 – As part of the offer submission package the offeror shall provide the traceability signature page, signed only by the offeror. Upon award and prior to the first shipment the awardee shall provide the signed traceability signature page from each entity in the supply chain providing and/or handling F-76 product and/or blending components all the way back to the point of manufacture. For each individual shipment, the supplier will submit a traceability page signed only by the awardee.

iii) OPTION 3 – As part of the offeror submission package, the offeror shall provide the traceability signature page, signed only by the offeror. For each individual shipment, the awardee shall provide the signed traceability signature page from each entity mailto:QT@dla.mil

FORT BELVOIR, VIRGINIA 22060-6222

in the supply chain providing and/or handling F-76 product and/or blending components all the way back to the point of manufacture.

Regardless of the option chosen, the traceability sheet signed by offeror shall be submitted to both the contracting office and to QT@dla.mil during pre-award phase.

For OPTION 1 or OPTION 2, the purpose of the awardee submitting a signed traceability page with each shipment is to confirm that the initial traceability certification is still valid at the time of F-76 product shipment.

6) If at any point during the contract period the traceability information provided under OPTION 1 or OPTION 2 becomes invalid (i.e.

the supply chain is altered or the source of F-76 product or a blending component changes), the supplier shall notify both the contracting office and QT@dla.mil and updated documentation shall be provided.

Quality Technical Directorate Approval:

FORT BELVOIR, VIRGINIA 22060-6222

F-76 Traceability Signature Page

Contract or Solicitation Number:

CLIN:

Order Number:

Shipment Number:

Traceability OPTION selected per paragraph g.5 (circle or otherwise indicate which one of the three options is chosen):

OPTION 1 OPTION 2 OPTION 3

F-76 fuel supplied under the above contract, CLIN, order number and shipment number maintains traceability with respect the materials composition, additives and their concentration levels. This signed statement certifies that at no point have any unauthorized un- hydrotreated light cycle oils, other unauthorized materials, or additives been blended into the final product or any of its associated blend components per the most recent revision of MIL-DTL-16884 at date of contract award. All materials and additives are listed below. The percentage of each material as defined in sections 3.2, 3.2.2, and 3.2.3 (i.e. refined hydrocarbon distillate fuel, Fischer-Tropsch, Hydroprocessed Renewable Diesel, etc.) and the concentration level for each additive are also shown. For the purposes of the offeror submission this signed statement attests that no unapproved additives or materials will be added to batches or components of batches of F-76 for delivery under government contracts.

Signature:

Printed Name:

Title:

Company Name:

Date:

Material Percent

Additive Concentration Responsible Party for Injection

FORT BELVOIR, VIRGINIA 22060-6222

F-76 Synthetic Component Certification

Contract or Solicitation Number:

CLIN:

Order Number:

Shipment Number:

Synthetic paraffinic materials supplied as indicated with the above contract, CLIN, order number, and shipment number is derived from either Fischer-Tropsch (FT) or Hydroprocessed Renewable Diesel (HRD) methods. This signed statement certifies that since the last certificate of analysis (COA), including table A-II or B-II results of MIL-DTL-16884P, Appendix A or B, no changes, including feedstock material, production location, or production processes have been made. In addition, no turnaround events have been executed on any units utilized to produce the synthetic paraffinic materials since the last COA, including table A-II or B-II, properties were tested. Please supply the date of the most recent COA and an identifying number for that report in the space provided below.

DATE OF COA: _

LAB REPORT ID NUMBER

Signature:

Printed Name:

Title:

Company Name:

Date:

FORT BELVOIR, VIRGINIA 22060-6222

C16.64-1 TURBINE FUEL, AVIATION (JP8) (INLAND EAST GULF/OFFSHORE) (ROCKY

MOUNTAIN/WEST) (WESTPAC) (ATL/EUR/MED) (PC&S) (DLA OCT ENERGY 2022)

NATIONAL STOCK NUMBER PRODUCT NOMENCLATURE DLA ENERGY PRODUCT CODE

9130-01-031-5816 Turbine Fuel, Aviation JP8

Aviation Turbine Fuel (JP8) shall conform to MIL-DTL-83133K, dated July 18, 2018 Supplies delivered under this contract shall conform to all Federal, State, and local environmental requirements applicable to the geographic location of the receiving activity on the date of delivery. This includes delivery of fuel and documentation in a manner consistent with any existing or after-imposed Title V (Clean Air Act) Permits. The list of such requirements contained in this contract is not intended to be a complete list, and the Contractor shall be responsible for determining the existence of all such requirements. Selected regional environmental requirements are highlighted in the SPECIFICATIONS (CONT’D) clause. In the event that a Federal, State, or local environmental requirement is more stringent than a fuel specification contained in this contract, the Contractor shall deliver product that complies with the more stringent fuel specification. Product that fails to meet the more stringent fuel specification will be considered to be a nonconforming supply.

Product(s) to be supplied shall fully meet the requirements of the applicable specification(s) as cited above. In the event that compliance with the more stringent fuel specification causes the contractor to incur additional costs, the contractor may request an equitable adjustment

(a) INCIDENTAL CONTAMINANTS. Particulate Matter and Fatty Acid Methyl Ester (FAME) content shall not exceed the limits outlined in Table IV of MIL-DTL-83133K dated July 18, 2018.

(b) SPECIFICATION MODIFICATIONS. Aviation Turbine Fuel (JP8) shall conform to MIL-DTL-83133K, dated July 18, 2018, modified as follows:

(1) TESTING

(i) FILTRATION TIME TESTING. For filtration time testing round upwards when reporting the filtration time, in minutes. For example, a filtration time of 10 minutes, 18 seconds, would be reported as 11 minutes.

(ii) MICROSEPAROMETER (MSEP) RATING LIMITS. See MIL-DTL-83133K, dated July 18, 2018, Table 1, Note 15 for MSEP test method selection criteria.

(A) Prior to initial production under this contract, the Contractor shall elect, on a one-time basis, which MSEP limit will be met for the balance of the contract. If the Contractor introduces fuel system icing inhibitor (FSII), corrosion inhibitor/lubricity improver (CI/LI), and/or static dissipater additive (SDA) after verification of product conformance with the MSEP requirement, the product is not required to meet a fixed limit on subsequent MSEP tests.

(B) If the Contractor elects to verify conformance with the MSEP requirement on a sample of product that does not contain FSII and CI/LI, an additional MSEP test shall be performed on a hand blend containing aviation turbine fuel, FSII, CI/LI, and antioxidant (AO) (AO only if required). The FSII shall be included in this hand blend at a concentration of 0.07 to 0.10 volume percent and the amount of the CI/LI included shall be within the concentration range specified in QPL-25017. The additional MSEP result of this hand blend is a REPORT ONLY requirement and shall be recorded corresponding to item 750X on the Standardized Report Form (see Attachment ). This result shall be recorded with an asterisk next to it, and with a footnote below, stating, “*MSEP result is a ‘Report Only’ requirement.

Original result of (fill in actual result) on product containing the following additives:

(fill in combination of additives).”

(iii) WORKMANSHIP. The workmanship criteria in MIL-DTL-83133K, dated July 18, 2018, paragraph 3.5, is revised to read, “At the custody transfer point, the finished fuel shall be clear and bright and visually free from undissolved water and particulate matter in accordance with the latest revisions of the approved test methods. ASTM D4176 or ASTM D6986, latest versions, may be used. In case of dispute as determined by sample results taken from the custody transfer point, the fuel shall be clear and bright at 21 degrees Celsius (°C) (70 degrees Fahrenheit [°F]) and shall contain no more than 1.0 mg/L of particulate matter. The sample in dispute shall be taken into an area where the sample is permitted to slowly equilibrate to 21°C (70°F); this shall apply to either D4176 or D6986.”

(A) ASTM D6986, latest revision, shall be the referee test method, see requirements, as drafted, in MIL-DTL- 83133K, dated July 18, 2018, section 3.5.

(B) For the latest revision of ASTM D 4176, Procedure 2, with a result of Rating 1, maximum. If the sample fails ASTM D4176 only because it contains visible particulate matter but meets the particulate matter requirements of 1.0 mg/L maximum as stated in MIL-DTL-83133K, Table IV, the workmanship

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criteria is met.

(2) SPECIAL LOCATION REQUIREMENTS

(i) Rocky Mountain/West. Aviation fuel movement via the Chevron Pipeline (Utah, Idaho, or Washington state entry points) shall be limited to total sulfur content of 0.15 mass percent, maximum.

(ii) Alaska. For fuels refined in Alaska and delivered to Alaska locations, the total acid number shall be relaxed to

0.020 mg KOH/g maximum.

(c) ADDITIVES. Additives are required for deliveries of JP8 per MIL-DTL-83133K, dated July 18, 2018, unless addition is excluded by specific solicitation line item, applicable contract clause, or another contractual requirement.

(1) The CI/LI additive(s) used shall be of the type and concentration cited in QPL-25017. To locate this information: (1) Go to the Acquisition Streamlining and Standardization Information System (ASSIST) Quick Search website (URL http://quicksearch.dla.mil/), (2) type "QPL-25017" in the Document ID field, press the Search button, (3) click the QPL- 25017 search result under Document ID, (4) click the "Qualification" link under Overview [or the "View QPD data" link under Revision History], and (5) click the “MIL-PRF- 25017 CATEGORY 1” link under Govt Designation. The concentration range for each additive is listed under the “Source Notes” link under the far-right column of the table.

(2) Metal deactivator additive (MDA) shall not be used in JP8 unless the Contractor has obtained written consent from the Contracting Officer.

(3) The requirement for SDA (see MIL-DTL-83133K, dated July 18, 2018, paragraph 3.3.3 and fuel electrical conductivity requirement in Table I) shall not apply unless stated otherwise in the Schedule. Line injection of additives (FSII, CI/LI, and SDA) from shipping tank to delivery conveyance is permitted under the following conditions:

(i) A laboratory hand blend containing the required additives and aviation turbine fuel shall be tested to verify compliance with the specification.

(ii) Additives shall be proportionately injected throughout the entire loading process to ensure the additive is homogeneously blended into the product. The Contractor shall maintain records evidencing the homogeneous blending of all line-injected additives. Such records shall include meter or tank gauge readings or test results taken at intervals to provide confidence in the injection process.

(iii) When FSII is line injected, additive concentration shall be verified based on a representative sample from each shipping conveyance.

(iv) When SDA is line-injected, and insufficient time is available for the fuel to reach equilibrium before departure of the shipping conveyance, the Contractor shall verify conductivity level on a representative sample from each shipping conveyance. The receiving activity will measure the conductivity and advise DLA Energy if it does not meet the specification requirements.

(4) SPECIAL LOCATION REQUIREMENTS (ATL/EUR/MED ONLY)

(i) For deliveries to La Spezia, Italy, the CI/LI shall be 3.5 g/m3 above the minimum effective concentration as identified in QPL-25017. See paragraph (c)(1) above.

(ii) When AO is added to the hydrotreated portion of the finished product, the percentage of the blend that has been hydrotreated shall be reported.

(iii) The requirement for SDA (see MIL-DTL-83133K, dated July 18, 2018, paragraph 3.3.3 and fuel electrical conductivity requirement in Table I) shall not apply unless stated otherwise in the Schedule.

Quality/Technical Support Office Approval

Signed by:

Date: October, 27, 2022 12:10 http://quicksearch.dla.mil/)

FORT BELVOIR, VIRGINIA 22060-6222

KNAPP.RICHARD.BRU

CE.1027134021

Digitally signed by

KNAPP.RICHARD.BRUCE.1027134021

Date: 2024.04.11 12:46:02 -04'00'

MACLEAN.SARAH.A.1

400398441

Digitally signed by

MACLEAN.SARAH.A.1400398441

Date: 2024.04.11 12:22:48 -04'00'

KARRAS.JASON.EARL

E.1129188177

Digitally signed by

KARRAS.JASON.EARLE.1129188177

Date: 2024.04.11 12:28:51 -04'00'

TABLE I, Sample Retention1

LOCATION MINIMUM QUANTITY RETENTION PERIOD 1

Bulk Tank Cars/Tank Truck/Intermodal Container

Fuels 1 gallon (4 liters) 2 15 days for fuels Lubricating Oils 0.25 gallons (1 liter) 2 45 days for lubricating oils

Drums4 2 gallons (8 liter) (multi-drum composite) 3 45 days

Shipping Tank(s)

2 gallons (8 liters) for Aviation Turbine Fuels 1 gallon (4 liters) for all other Fuels, Lubricating Oils, and Additives

45 days

Tanker/Barge/Pipeline (Composite Line at Custody Transfer Point)

5 gallon (20 liters) for all fuel types 45 days

Tanker/Barge (Composite)

F.O.B. Origin 2 gallons (8 liters) for Aviation Turbine Fuels 1 gallon (4 liters) for all other fuels

45 days

F.O.B. Destination 2 gallons (8 liters) Until shore tests on-specification Tanker/Barge (Each Compartment)

F.O.B. Origin 0.25 gallon (1 liter) 45 days F.O.B. Destination 0.25 gallon (1 liter) Until shore test on-specification

NOTES:

1. Unless otherwise noted in this document or applicable contract, the retention period shall be for the stated number of days after the sample has been taken from the location indicated.

2. If the conveyance is compartmentalized, a proportional sample shall be taken from each compartment.

3. An 8-liter composite sample of each product lot shall be taken from a predetermined number of randomly selected drums IAW Table III of API MPSM, Chapter 8.1 (ASTM D 4057).

4. Applies to DLA Energy managed procurements of products shipped in drums. Does not apply to DLA Aviation managed procurements for packaged products.

TABLE II, Minimum Sampling and Testing Requirements for Petroleum Products Series 1, tankers and barges1

ITEM WHEN TO SAMPLE LOCATION OF SAMPLE TYPE OF SAMPLE2 TEST REQUIRED3

1.a

Prior to Loading

Before acceptance of new materiel and after establishment of new batch4 Each shore storage tank Single Tank Composite or All

Levels A5, 15

1.b After line pack but prior to loading As close to the custody transfer point as possible Line Sample C7,14 Dedicated System B-1 Non-Dedicated System

1.c D uring

Loading

Immediately after start of loading/shipment

As close to the custody transfer point as possible Line Sample C7

1.d After first in Vessel cargo compartment(s) Spot C7,14

1.e During loading

As close to the custody transfer point as possible Line Sample Hourly Visual6,8, Retain10

1.f

A fter Loading

After loading

Each vessel cargo compartment All Level (Combine All Levels into one Volumetric Composite Sample13)

C 6, 8, 11,14

Remainder of B-112

(Retain fuel for B-1 referee testing)

NOTES:

1. Additional requirements to include retain samples may be required. See Quality Assurance Provisions (C or E-QAP) for further details.

2. Refer to ASTM International D4057 for sampling procedures.

3. Test results shall be compared against the quality release certificate. Any discrepancies shall be identified, investigated, and resolved.

4. Upon procurement at refineries, blending installations, etc. and at main installations including national depots & ocean importing points on establishment of new batches.

5. Prior to performing A-level testing, the homogeneity of each batch shall be determined. Refer to paragraph (b)(1)(iii)(C) of this document for additional details.

6. Test for FSII and SDA only if line injected.

7. If sample fails appearance, perform particulate matter using approved methods as outlined in the applicable specification.

8. Lubricity also required for F-76 only if line injected, or determine LIA concentration by volumetric measurement/calculation.

9. First in shall be done after one (1) meter or after line displacement whichever is the greater.

10. For all tanker and barge, a flow-proportional sample taken in accordance with MPMS Chapter 8, Section 2, is preferred at the custody transfer point. However, manual samples taken in accordance with MPMS Chapter 8, Section 1 are acceptable if they are taken hourly throughout the shipment and that the quantity of the composite sample meets the requirements in Table I

11. Best practice is for B-1 test completion for FOB Origin Procurements (or Type A level testing when specified in contract for FOB Destination Procurements) prior to vessel release. Based on QAR decision, vessel may sail after C Tests to meet schedule requirements including to avoid predicted weather; remainder of B-1 tests to be completed before arrival at next load or discharge port. Test report will be provided to designated discharge port.

12. Type A level testing required for FOB Destination Procurements (unless otherwise specified by contract).

13. As defined by API MPMS Chapter 8-1, section 3.22.

14. For product verification purposes. Results of C-test must fall within reproducibility of source tank A-level results.

15. New cargo from same batch, within 30 days, will only require B-1 testing to verify previous A-level test results. B-1 level verification test results should fall withing reproducibility of source tank A-level results.

Series 2, pipeline, tank trucks, tank cars, iso-containers1,7

ITEM WHEN TO SAMPLE LOCATION OF SAMPLE TYPE OF SAMPLE 2 TEST REQUIRED3

2.a Prior to Shipm ent

Before acceptance of new materiel and after establishment of new batch4

Each Shipment Storage Tank Single Tank Composite or All Levels A9, 11

2.b After line pack but prior to loading/shipment

As close to the custody transfer point as possible Line Sample C5,6 Dedicated System

B-1 Non-Dedicated System

2.c D uring Shipm ent

Immediately after start of loading/shipment As close to the custody transfer point as possible and downstream of the filter separator (if equipped)

Line Sample C5, 13

2.d Pipeline Only:

Hourly after start of loading or shipment10

As close to the custody transfer point as possible and downstream of the filter separator (if equipped) Line Sample

Apperance5, 12

(Retain fuel for B-1 referee testing)

2.e

Daily on first fill and anytime a new tank is placed on issue (after line displacement) TT, TC, ISO, Refuelers or other over the road transportation modes only

As close to the custody transfer point as possible (Loading Rack or Fill Point) and downstream of the filter separator (if equipped)

Line Sample Color (by visual method) and Appearance5.

If visual fails perform C6

2.f

A fter Loading

Daily for each conveyance mode (Not required for pipeline operations)

Each Cargo Compartment or another point that provides a representative sample All Level

Appearance on each compartment

C on composite 5,6,8

2.g Drums Sample of each lot of product shall be taken from a predetermined number of randomly selected drums14

Multi-drum Composite C13

NOTES:

1. Additional contractual requirements to include retain samples may be required. See Contract Quality Assurance Plans (C or E-QAPs) for further details.

2. Refer to ASTM International D4057 for sampling procedures.

3. Test results shall be compared against the quality release certificate. Any discrepancies shall be identified, investigated, and resolved.

4. Upon procurement at refineries, blending installations, etc., and at main installations including national depots & ocean importing points on establishment of new batches.

5. Test for FSII and SDA only if line injected.

6. If sample fails appearance, perform particulate matter using approved methods as outlined in the applicable specification.

7. Type A level testing required for FOB Destination Procurements (unless otherwise specified by contract).

8. If the conveyance is compartmentalized, a proportional sample shall be taken from each compartment such that a total of one liter is collected from the conveyance.

9. Filtration time testing is required for JP-5 & JP-8 and shall meet contract requirement.

10. For pipeline shipments, a flow-proportional sample taken in accordance with MPMS Chapter 8, Section 2, is preferred at the custody transfer point. However, manual samples taken in accordance with MPMS Chapter 8, Section 1 are acceptable if they are taken hourly throughout the shipment and that the quantity of the composite sample meets the requirements in Table I.

11. Prior to performing A-level testing, the homogeneity of each batch shall be determined. Refer to paragraph (b)(1)(iii)(C) of this document for additional details.

12. Lubricity also required for F-76 only if line injected or determine LIA concentration by volumetric measurement/calculation.

13. For product verification purposes. Results of C-test must fall within reproducibility of source tank results.

14. A composite sample of 2 gallons (8 liters) for Aviation Turbine Fuels and 1 gallon (4 liters) for all other fuels for each lot of product shall be taken from a predetermined number of randomly selected drums. The total number of drums sampled per lot shall, at a minimum, be that cited in Table III of API MPMS chapter 8.1 (ASTM d 4057), but may be increased at the government's option.

Series 3, product receipt and discharges for tankers and barges (FOB Destination)

ITEM WHEN TO SAMPLE LOCATION OF SAMPLE TYPE OF SAMPLE TEST REQUIRED

3.a

Prior to D ischarge

Prior to discharge

From each vessel cargo compartment All Level Appearance and Density1

3.b From each vessel cargo compartment

All Level (Combine All Levels into one Volumetric Composite

Sample)

A

3.d

D uring

D ischarge

Within 30 minutes after start and each hour after until completion

Dock/Discharge Manifold Header Line Sample / Retain Perform Appearance test2,3 and then retain fuel for Referee testing

3.e

A fter

D ischarge

If remainder of fuel will be shipped to another DFSP

Each vessel compartment with fuel remaining on board All Level Retain until discharged at destination

NOTES:

1. Test for flash point on high flash cargo tanks if low and high flash cargoes are carried together aboard the same vessel without segregated venting systems.

2. For aviation fuel delivery, FSII and SDA shall be tested only if line injected. This requires an additional quart sample.

3. Test for additives if line injected downstream of the injector. (If line injecting LIA into F-76, test for lubricity.)

Series 4, product receipt from pipeline (FOB Destination)1

ITEM WHEN TO SAMPLE LOCATION OF SAMPLE TYPE OF SAMPLE TEST REQUIRED

4.c D uring

R eceipt

During pipeline receipt Custody transfer point Line Sample/Retain 5 Gallon Minimum2

4.d During pipeline receipt, immediately after start, Midpoint and 1 hour prior to completion3

As close to the custody transfer point as possible Line C

4.g

A fter

R eceipt

After receipt of fuel Each receipt tank All level A

NOTES:

1. Refer to ASTM International D4057 for sampling procedures.

2. Retain for referee testing in the event a failure occurs on receipt tank. Retain sample for 45 days. Sampling is IAW API MPMS Chapter 8

3. Fuel from a new batch will be considered a new receipt for quality control purposes.

TABLE III, Definitions of Test Series

I. TYPE A: Includes all specification quality conformance tests plus any additional contractual requirements.

II. TYPE B-1 & C: As shown in the table below for each product. Properties and test methods will be in accordance with the product specification for each grade identified in the solicitation/contract.

AVGAS

AVIATION

TURBINE

MOGAS

DIESEL/

KEROSENE/

NAVAL DISTILLATE

LUBE OIL

TEST PROPERTIES B-1 C B-1 C B-1 C B-1 C B-1 C

Appearance/ workmanship

Particulate content * *8 *1 *8 Filtration Time * Color (visual) * * * * * * * * * Density/API Gravity/ Specific Gravity

Distillation * * * * Corrosion, Copper Strip * * Existent Gum * * Carbon Residue *1 Vapor Pressure * * Lead Content * *3 Freeze Point * Flash Point * * * * * FSII Content *

MSEP (JP-8, F-24, F-27,

Jet A & Jet A-1)

Conductivity (JP-5 & JP- 8, F-24, F-27 & Jet A-1)

*4

Thermal stability (B-1 requirement applies to JPTS and marine/multi-product mode receipt tank sample)

Sediment & Water Total Sediment aged Viscosity *7 Water Content * *8 *2 Emulsion *2 Foam Test * Knock Rating (RON / MON) *6 Lubricity *1

FAME *5 *1

Solid Contaminants *2

* The procedure to be used for conducting these tests will be as stated in the appropriate product specification and/or contract. For any products not covered under this table, contact Quality Assurance Representative for guidance.

NOTES:

1. F76 only.

2. Only if the specification has this requirement.

3. If contamination with leaded fuels is suspected.

4. If fuel contains conductivity additive, wait approximately 2 minutes after obtaining sample for charges in the fuel to dissipate before performing CU testing.

5. Only for product transported through multi-product systems, including marine transport.

6. Perform only if Lead Content is performed and fails and/or contamination with another product is suspected. In the case of pipeline, this test shall be performed when considered necessary.

7. For MIL-PRF-17331 and MIL-PRF-9000 viscosity is not required unless the tank has been in long term storage for 3 months.

8. Visual check.

TABLE IV, Conversion chart for tank trucks (TT) tank cars (TC), tank wagons (TW), tank & trailer (TRR), and intermodal containers (IMC)1, 2

Last Product Carried

PRODUCT TO BE LOADED5

Gasolines: MUR, MUM, MUP, EFM, E85, 100, 130, JAB

Aviation Turbine Fuels: JAA/A1, JP-8, F-24, JP-5, TS1, KS1/R/N, Aviation Turbine

Fuel3: JPTS

RP1/RP2 JP-10/PF1 Diesel Fuel: F-76 FSII Lubricating Oils

Diesel Fuels:

DF1, DF2,

DS1, DS2,

DSS, DSW,

BDI, MGO

Gasolines4 MUR, MUM, MUP, EFM, E85, 100, 130, JAB

Drain/Empty Steam/Dry Steam/Dry Steam/Dry Steam/Dry Steam/Dry Steam/Dry Steam/Dry Steam/Dry

Aviation Turbine Fuels4, 9

JAA/A1, JP-8, F-24,

JP-5, TS1, KS1/R/N,

Drain/Empty

Drain/Empty

Steam/Dry

Aviation Turbine Fuel3 JPTS Drain/Empty Drain/Empty Drain/Empty Drain/Empty Steam/Dry Steam/Dry Steam/Dry Steam Dry Steam/Dry

RP1/RP2 Steam/Dry Steam/Dry Steam/Dry Drain/Empty Steam/Dry Steam/Dry Steam/Dry Steam/Dry Steam/Dry J10/PF-1 Steam Dry Steam/Dry Steam/Dry Steam Dry Drain/Empty Steam/Dry Steam/Dry Steam/Dry Steam/Dry Petroleum Solvent or Paint Thinner Steam/Dry Steam/Dry Steam/Dry Steam/Dry Steam/Dry Steam/Dry Steam/Dry Steam/Dry Steam/Dry

Diesel Fuel: F-76 Steam/Dry Steam/Dry Steam/Dry Steam/Dry Steam/Dry Drain/Empty Steam/Dry Steam/Dry Drain/Empty Diesel Fuels4 DF1, DF2, DS1, DS2, DSS, DSW, MGO

Steam/Dry Steam/Dry7 Steam/Dry Steam/Dry Steam/Dry Steam/Dry Steam/Dry Steam/Dry Drain/Empty

FSII (SIH) Drain/Empty Drain/Empty Steam/Dry Steam/Dry Steam/Dry Steam/Dry Drain/Empty Steam/Dry Steam/Dry Lubricating Oils NO LOAD NO LOAD NO LOAD NO LOAD NO LOAD NO LOAD NO LOAD Steam/Dry6 Steam/Dry Biodiesel Blends(<B15)4

DF1, DF2, DS1, DS2, DSS,

DSW

Steam/Dry7

NO LOAD

Biodiesel Blends(>B15):

DF1, DF2, DS1, DS2,

BDI

Steam/Dry8

Heavy Fuel Oils, Distillate Fuels4 FS1, FS2, FS4, FS5, FS6

Residual Fuel Oils:

ISO 8217, class F (IFOs)

Naphtha Drain/Empty Steam/Dry Steam/Dry Steam/Dry Steam/Dry Steam/Dry Steam/Dry Steam/Dry Steam/Dry

TABLE IV Continued, Conversion chart for tank trucks (TT) tank cars (TC), tank wagons (TW), tank & trailer (TRR), and intermodal containers (IMC)1, 2

NOTES:

1. For previous cargoes not listed, contact DLA Energy Quality Operations Division at DLAEnergyQualityOperations@dla.mil for acceptability/cleaning procedures.

2. General Instructions for Tank Cars and Trucks

a. Conveyances (all) shall be dry and free from loose rust, scale, and dirt

b. Saran lined equipment should not be steam cleaned; water wash should suffice.

c. Petroleum products shall not be loaded into the conveyances where the previous cargo was caustic, acid, or chlorinated solvents.

d. Tank trucks and cars in liquid fertilizer service shall not load aviation turbine fuels directly but shall carry out at least two loads of commercial gasoline prior to the aviation turbine fuel load.

e. Conversion of Government-owned tank cars from liquid fertilizer service to aviation turbine fuel service shall only be done when no other alternative exists. Tank cars being converted from liquid fertilizer service to a petroleum product shall be adequately cleaned to remove all traces of liquid fertilizer. At a minimum, the equipment must be steam cleaned; dried and must be free from loose rust, scale, and dirt. After cleaning, but before loading aviation turbine fuels, at least two loads of commercial gasoline shall be carried prior to loading aviation turbine fuel.