Attachment 1 QAPs_ E and C.pdf

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TABLE I, Sample Retention1

LOCATION MINIMUM QUANTITY RETENTION PERIOD 1

Bulk Tank Cars/Tank Truck/Intermodal Container

Additives 0.5-gallon (2 liters)2 Until receipt and quality verification of each lot/batch

Fuels 1 gallon (3 liters) 2 15 days for fuels/45 days for lubricating oils

Lubricating Oils 0.25 gallons (1 liter) 2

AVGAS Drums 0,25 gallons (1 liter) (multi-drum composite) 3 45 days

Shipping Tank(s)

2 gallons (8 liters) for Aviation Turbine Fuels 1 gallon (3 liters) for all other Fuels, Lubricating Oils, and Additives

45 days

Tanker/Barge/Pipeline (Composite Line at Custody Transfer Point)

2 gallon (8 liters) for Aviation Turbine

1 gallon (3 liters) for all other Fuels

Tanker/Barge (Composite)

F.O.B. Origin 2 gallons (8 liters) for Aviation Turbine

1 gallon (3 liters) for all other fuels

F.O.B. Destination 2 gallons (8 liters) Until shore tests on-specification Tanker/Barge (Each Compartment)

F.O.B. Origin 1 gallon (3 liters) 45 days F.O.B. Destination 1 gallon (3 liters) Until shore test on-specification

NOTES:

1. Unless otherwise noted in this document or applicable contract, the retention period shall be for the stated number of days after the sample has been taken from the location indicated.

2. If the conveyance is compartmentalized, a proportional sample shall be taken from each compartment such that a total of one liter is collected from the conveyance.

3. A one-liter composite sample of each product lot shall be taken from a predetermined number of randomly selected drums IAW Table III of API MPSM, Chapter 8.1 (ASTM D 4057).

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TABLE III, Tests required aviation gasoline3

PROPERTIES B-1 TEST B-2 TEST B-3 TEST C TEST

Appearance 1,2 X X X X

Color (Visual) X X X X Density or API gravity X X X X Distillation X X X

Copper strip corrosion X X X

Existent gum X X

Vapor pressure X X

Free water determination2 X X X

Lead content X X Potential gum X Color (Saybolt)

Freeze Point

Knock Value Total Sulfur Oxidation Stability

1. Obtain sample in a clear round 1 quart glass bottle, swirl the bottle vigorously so a vortex is formed. Visually check for sediment at the point of the vortex. If sediment is visible, an investigation is necessary in order to determine the source of the contaminant (a spot larger than 3 mm diameter indicates corrective action may be required to prevent the delivery of contaminated fuel).

2. AVGAS samples shall be checked for particulate and water. Particulate shall be determined visually upstream of filter separators and/or by the particle assessment method downstream of the filter separator. Free water shall be determined downstream of filter separator using a water detector (AEL Aqua-Glo test method or Hydro-Light).

3. For determining correct testing results (rounding protocol) see 4.2.2.2.1 Testing Rounding Protocol

TABLE IV, Tests required for aviation turbine 7

Appearance 1 X X X X Color (visual) X X X X Density or API gravity X X X X Particulate matter X X X

Freezing point X X X

Existent gum X X X Vapor pressure (JP-4 only) X X X Flash point (except JP-4) 11 X X X X Water reaction2

Lead content (If contaminated with leaded fuels suspected)

X X X

Fuel system icing inhibitor 3 X X X Filtration time X X X MSEP (JP-4, JP-8, F-24, F-27, Jet A & Jet A-1) 4,5

Conductivity (JP-4 and JP-8, F-24, F-27 & Jet A-1) 6

Thermal stability (B-1 requirement applies only to JPTS and marine/multi-product mode receipt tank sample)10

X X

Color (Saybolt) X

Acid number X

Peroxide Number 8 X

Fatty Acid Methyl Ester (FAME) 9 X X X

1. Obtain sample in a clear round 1 quart glass bottle, swirl the bottle vigorously so a vortex is formed. Visually check for sediment at the point of the vortex. If sediment is visible, an investigation is necessary to determine the source of the contaminant (a spot larger than 3 mm diameter indicates corrective action may be required to prevent the delivery of contaminated fuel).

2. Optional or at the request of Service Control Point.

3. If product contains FSII, product shall be checked on delivery into a bulk storage tank and every month thereafter.

4. If the capability does not exist to perform this test at the terminal, send sample to the nearest Service laboratory that has capability. In the event operational necessity dictates issue of product before results are obtained from the Service laboratory, shipments may be made, however, when laboratory results indicate failure, notify DLA Energy Quality Operations Division.

5. In all cases where MSEP is measured, conductivity will also be measured using ASTM D2624. For unadditized Jet A that is injected outbound of a facility an MSEP shall be performed using either D7224 or D8073 where possible. If either method is not available testing may be conducted with D3948. Passing results for D3948 will be considered acceptable. Failing fuels shall be retested using D7224 or D8073. If the fuel passes D7224 with a minimum limit of 85 or D8073 with a limit of 88 the fuel is considered to be acceptable with no further action. If the fuel fails D7224 or D8073, an investigation shall be performed.

6. If fuel contains conductivity additive, wait approximately 2 minutes after obtaining sample for charges in the fuel to dissipate before performing CU testing.

7. For determining correct reporting of test results (rounding protocol) see 4.2.2.2.1 Testing Rounding Protocol

8. Only applicable to Jet A use by the Navy.

9. Only for product transported through multi-product systems, including marine transport.

10. For JPTS: Ellipsometer (ETR) or Interferometer (ITR) IAW QAP C16.08-13. ETR is the referee. For all other fuels, follow specification requirements (excluding MSC chartered/contracted tankers and barges in dedicated/long term service).

11. Flash Point at the receiving point is not required for product used by the U.S. Army. This fuel is tested in accordance with Petroleum Laboratory Operations (TM 4-43.31).

TABLE V, Support for secure fuel 4 JP-5 Jet A Jet A-1 7 JP-8 F-24

Min. Max. Min. Max. Min. Max. Min. Max. Min. Max.

Appearance 2 C&B C&B C&B C&B C&B C&B C&B C&B C&B C&B

Gravity, API @ 60 °F D1298/D4052

36.0 48.0 37.0 51.0 37.0 51.0 37.0 51.0 37.0 51.0

Density at 15°C (kg/m3) 788 845 775 840 775 840 775 840 775 840

Weight: lb/USG Calculated 6.6 7.0 6.5 7.0 6.5 7.0 6.5 7.0 6.5 7.0

Distillation (°C) D86 3

10% Recovered 205 205 205 205 205

20% Recovered Report Report

50% Recovered Report Report Report Report Report 90% Recovered Report Report Report Report Report Final Boiling Point 300 300 300 300 300

Freezing point, °C D5972/D2386

-46 -40 -47 -47 -40

Flash point, °C D93/D56 60 38 38 38 38

Particulate Matter (mg/L) D2276, D5452, MIL- DTL- 83133

0.5 0.5 0.5 0.5

0.5

Conductivity (pS/m) D2624 Report Report 50 700 50 700

Copper strip corrosion D130 No.1 No.1 No.1 No.1 No.1

Existent gum (mg/100 mL) D381 7 7 7 7 7 FSII, (vol %) D5006 1 0.07 0.20 0.04 0.15 0.04 0.15

Thermal Stability D3241

Change in pressure drop, mm Hg 25 25 25 25 25 One of the tube deposit rating methods shall be run:

(1) Ellipsometer (ETR) 6 (nm) or Interferometer (ITR) (nm)

85 85 85 85

(2) Heater tube deposit, Visual Tube Rating

(VTR)

< 3 < 3 < 3 < 3 < 3

Fatty Acid Methyl Ester (FAME) 5

50 50 50 50 50

1. Only use FSII meeting specification MIL-DTL-85470, Inhibitor, Icing, Fuel System, High Flash, NATO Code S-1745.

2. Fuel shall be clear, bright, and free of water and sediment on visual examination. Sample will be taken downstream of final filtration on refueler or hydrant servicing equipment.

3. Distillation property criteria are specified in ASTM D86 scale units. ASTM D2887 results shall be converted to estimated D86 results by application of the correlation in Appendix X4, “Correlation for Jet and Diesel Fuel (Procedures A and B)” of D2887 for comparison with the specified property criteria. Distillation residue and loss limits provide control of the distillation process during the D86 test method and do not apply to D2887.

4. Alternate test methods may be performed provided they are authorized by the specification of the product being tested. Referee test methods are preferred.

5. Only for product transported through multi-product systems. FAME (fatty acid methyl esters) is defined as material meeting the limits of EN14214 or ASTM D6751. FAME that fails to meet the biodiesel quality standards are not permitted in aviation turbine fuel.

6. Tube deposit rating shall be measured by ASTM D3241 ETR Ellipsometer (ETR), when available: otherwise, use Interferometer (ITR) or visual (VTR). ETR shall be the referee procedure, otherwise ITR.

7. DEF STAN 91-091, ASTM D1655 and GOST R 52050 are acceptable.

TABLE VI, Tests required for automotive gasoline

Appearance X X X X Color (Visual) X X X X Water and Particulate (Visual Check) X X X X Density or API gravity X X X X

Vapor pressure X X

Copper strip corrosion X X Unwashed gum/Solvent-washed gum X X 1

Knock rating (RON and MON) X 2 X 2

Oxidation stability X

1. Unwashed gum, without solvent wash, shall not increase by more than 2 mg as compared to the original product. In the event of gum increase exceeding 2 mg, run type A test as defined in the legend.

2. Perform only if Lead Content is performed and fails and/or contamination with another product is suspected. In the case of pipeline, this test shall be performed when considered necessary.

TABLE VII, Tests required for E85 (ASTM D5798) 1, 2

Water X X X Ethanol Volume X X X Vapor Pressure X X X Sulfur X X Acidity X Solvent Washed Gum X X pH X Unwashed Gum X Copper X X

1. For cleaning see 5.9.4.2

2. In accordance with DOE Handbook for Handling, Storing and Dispensing E85 and Other Ethanol- Gasoline Blends, it is recommended at a minimum to test the following every one to two months: electrical conductivity, particulate content, hydrocarbon content (D5501 with D5798), water content and RVP. The DOE Guidebook link is https://www.afdc.energy.gov/uploads/publication/ethanol_handbook.pdf (May need to save file vs open document)

TABLE VIII, Tests required for diesel fuels and kerosene

Appearance 1 X X X X Color (Visual) X X X X Density X X X X Distillation X X

Flash point X X X X Carbon residue (F-76 only) X X Cloud point X

Pour point (F-76 only) X

Copper strip corrosion X

Cetane index 2 X

Viscosity (F-76 only) X

Water & sediment by centrifuge X Particulate (F-76 only) X X Storage stability (F-76 only) X

Sulfur 3, 4 X X

Fatty Acid Methyl Ester (FAME) (F-76 only) X X

Lubricity (F-76 only) X X

1. For NATO F-76, if the sample has no visible particulates, but is otherwise not clear and bright per ASTM D4176, procedure 1, then the product shall meet the requirements of ASTM D2709, 0.05 percent volume of water and sediment, maximum. The fuel is acceptable for appearance if the water and sediment content is

0.05 percent volume or less. If the sample fails ASTM D4176, procedure 1, because it contains visible sediment or particulate matter, but meets the requirement of 10 mg /L, maximum, in accordance with ASTM D5452 or ASTM D6217, then the fuel shall be considered acceptable provided all other requirements are met.

2. Cetane Index can only be run if no ignition improvers are present. Otherwise, Cetane number shall be given.

3. Kerosene. Grade No.-1K only, if intended for non-flue connected burner.

4. Sulfur testing is required for ULSD or LSD believed to be contaminated with a higher sulfur content fuel.

TABLE IX, Test required for BDI

Appearance 1 X X X X Distillation X X Flash Point X X X X Cloud Point or LTFT/CFPP X Viscosity X Copper Strip Corrosion X Water and Sediment X Sulfur X Ramsbottom Carbon Residue X X Particulate Content X X Acid Number X Ash Content X

Biodiesel Content X X X Oxidation Stability X

NOTE:

1. Obtain a sample in a clear round 1 quart bottle, swirl the bottle vigorously so a vortex is formed. Visually check for sediment at the point of the vortex. If sediment is visible, an investigation is necessary in order to determine the source of contamination.

TABLE X, Tests required for burner fuel oils

BS&W 1 (centrifuge) X X X X Density/API Gravity X X X X Viscosity X X Ash X Carbon Residue X

Sediment by extraction X

Pour point X

NOTE:

1. Perform only if water is observed.

TABLE XI, Tests required for residual marine fuel (RME 180 grade)

Kinematic Viscosity X X X X Density at 15o C X X X X Flash Point X X X X

CCAI X

Hydrogen Sulfide X

Total sediment aged X X

Carbon Residue X X

Sulfur X

Pour Point X

Water X X

Sodium X

TABLE XII, Tests required for residual marine fuel (RMG 380 grade)

Kinematic Viscosity X X X X Density at 15o C X X X X

CCAI X

Hydrogen Sulfide X

Total sediment aged X X

Water` X X

Sodium X

TABLE XIII, Test required for marine gas oil (DMA grade)

Kinematic Viscosity X

Density at 15 o C X X X

Cetane Index X

Oxidation Stability X X

Carbon Residue X X

Fatty Acid Methyl Ester (FAME) X X

TABLE XIV, Tests required for bulk lubrication oils 1, 2

PROPERTIES B-1 TEST C TEST

Appearance (to include visual sediment & water) X X Emulsion test 3 X

Density or API Gravity X X Viscosity 4 X Flash point X

Foam test X

Water 3 X

Solid contaminants 3 X

1. For application of these tests see Table IX.

2. B-2 tests are listed in Table XXII.

3. Only if the specification has this requirement.

. For MIL-PRF-17331 and MIL-PRF-9000 viscosity is not required unless the tank has been in long term storage for 3 months.

TABLE XV, Type B-2 tests for bulk lubricating oils 2

CHARACTERISTICS

SPECIFICATION

MIL-PRF-6081

(LA6)

MIL-PRF-9000

(LO6)

MIL-PRF-17331

(LTL)

MIL-PRF-32644

(CLB)

Appearance / workmanship X X X X Color X Viscosity @ 100°C X X X Viscosity @ 54°C Viscosity @ 40°C X 1 X X X Viscosity @ -40°C X Viscosity @ -54°C X

Relative density X

Pour point X X X Acid number X X X Total Base number X

Corrosion & oxidation stability X

Evaporation loss

Precipitation number

Ash/Sulfated Ash X X Emulsion X

Foam test X X1 X Water content X

Particulate content / trace sediment X X X Trace metals

Hydrolytic stability

Minimum retest frequency (months) 36 24 24 36 Visual check frequency (months) 12

Military symbol(s) None 9250 2190-TEP None

NATO Code Numbers O-133 O-278 O-250 None

1. Option A may be used for Government owned 2190 TEP if the conditions are met as required by ASTM D892.

2. For packaged product information refer to MIL-STD-3004-2. Only an approved laboratory under the DoD Shelf-Life Program can authorize a shelf-life extension of any item. For laboratories that cannot perform the full B-2 series tests, recommend the following statement be included in the remarks section of the lab report: "All required tests for shelf-life extension were not performed. This lab report does not give authorization to extend the shelf-life extension of this item."

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Table XVIII, Test Series Definition

TYPE DESCRIPTION

A Complete specification test as per specification detailed in the contract

B-1 A limited subset of principle characteristics of the type A full test specification requirement most likely to be affected by transportation of a product.

B-2 A more rigorous subset of the type A full test specification requirement than the type B-1 test schedule and aimed at those parameters susceptible to deterioration through aging, weathering, and long-term storage conditions.

B-3 Partial analysis for contamination; in particular, for controlling the re-injection of pipeline interface products.

Appearance To confirm that no free water and/or visual solid particulate are present in the fuel and that the fuel has a “clear & bright” appearance at ambient temperature.

C A limited number of tests performed to identify and compare product properties to ensure that no major changes have taken place during the fuel transfer process by any means of transport.

C+ (C-Plus) C-test plus additional tests. These tests are to be performed to ensure that critical properties are fulfilled and/or additives are present at the correct concentration.

DEFENSE LOGISTICS AGENCY ENERGY Page 1 of 1

8725 JOHN J. KINGMAN ROAD

FORT BELVOIR, VIRGINIA 22060-6222

DISTRIBUTION STATEMENT – A: APPROVED FOR PUBLIC RELEASE. DISTRIBUTION IS UNLIMITED

Signature

Prepared by:

Quality/Technical Support

Office Approval:

Contracting Approval:

C1.02 ASSIST DATABASE OF SPECIFICATIONS (DEC 2016)

Unless otherwise specified, current versions of defense or federal specifications and standards, military handbooks, commercial item descriptions, qualified product lists, and other related technical documents cited in this solicitation/contract can be accessed from the Department of Defense (DoD) Acquisition Streamlining and Standardization Information System

(ASSIST) database at https://assist.dla.mil under ASSIST-Quick Search or http://quicksearch.dla.mil. ASSIST is the official source for all Defense Standardization Program documents and contains the most current information on documents prepared by DoD, as well as information on how to acquire referenced non-Government standards that have been adopted for

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Basic instructions on how to use ASSIST:

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2017-08-07T09:00:32-0400

TAYLOR.LORI.L.1391585080

2017-08-07T09:22:23-0400

SHEPHERD.SANDRA.S.1012568459

2017-11-20T09:19:52-0500

BANISZEWSKI.DANIEL.J.1287388698

DEFENSE LOGISTICS AGENCY ENERGY Page 1 of 2

C16.01 TURBINE FUEL, AVIATION (JP5) (DLA ENERGY APRIL 2018)

NATIONAL STOCK NUMBER PRODUCT NOMENCLATURE DLA ENERGY PRODUCT

9130-00-273-2379 Turbine Fuel, Aviation, JP-5 JP5

9130-01-499-9521 Turbine Fuel, Aviation, JP-5 (Bunker fuel overseas locations only) JP5

Product shall meet MIL-DTL-5624W, Turbine Fuel, Aviation, Grade JP-5, dated March 28, 2016.

(a) SPECIFICATION MODIFICATION: The requirements of Table I in the specification are modified as follows:

a. FILTRATION TIME TESTING. Round upwards when reporting the filtration time, in minutes. For example, a filtration time of 4 minutes, 22 seconds, would be reported as 5 minutes.

b. FLASH POINT TESTING. The referee procedure for performing flash point testing of JP-5 shall be the manual method of ASTM D93 as opposed to the automated version of ASTM D93.

c. FLASH POINT.

i. All batches of JP-5 that are presented for Government acceptance at origin and for subsequent shipment through a multiproduct pipeline, shall meet a minimum flash point requirement of 62.5°C.

ii. In the U.S. all JP-5 deliveries in California, Oregon, and Washington shall have a minimum Flash Point of 62.5 oC at the custody transfer point.

iii. In Australia all JP-5 deliveries shall have a minimum Flash Point of 61.5°C at the custody transfer point.

d. ACID NUMBER. For JP-5 delivered to Kodiak Island, Alaska, the maximum total acid number shall be 0.020 mg KOH/g.

e. MICRO-SEPAROMETER (MSEP) REQUIREMENTS.

i. Prior to initial production under this contract, the Contractor shall elect, on a one-time basis, which MSEP limit to meet for the balance of the contract. If the Contractor introduces Fuel System Icing Inhibitor (FSII) and/or Corrosion Inhibitor/Lubricity Improver (CI/LI) after verification of product conformance with the MSEP requirement, the product is not required to meet a fixed limit on subsequent MSEP tests.

ii. If the Contractor elects to verify conformance with the MSEP requirement on a sample of product that does not contain FSII and CI/LI, an additional MSEP test shall be performed on a hand blend containing jet fuel, FSII, CI/LI, and Antioxidant (only if required). The FSII shall be added to this hand blend at a concentration range between 0.08 volume percent minimum and 0.11 volume percent maximum. The amount of the CI/LI added to this hand blend shall be within the concentration range specified in QPL-25017.

f. ADDITIONAL REQUIREMENT APPLICABLE TO DEEP FREEZE PROGRAM ONLY. The Deep Freeze Program is for Antarctic operations of the Department of Defense and other federal agencies; whereby JP-5 sulfur content shall not exceed 0.0015 mass-percent (15 ppm).

(b) ADDITIVES.

a. Additives are required for deliveries of JP-5, per MIL-DTL-5624W, unless addition is excluded by specific solicitation line item, applicable contract clause, or other contractual requirement. FSII included in jet fuel shall conform to MIL-DTL- 85470B, Inhibitor, Icing, Fuel System, High Flash, Notice 1 dated June 15, 1999 and revalidated March 24, 2004.

b. The CI/LI additive(s) used shall conform to MIL-PRF-25017H Inhibitor, Corrosion/Lubricity Improver, Fuel Soluble, w/Amendment 1, dated August 4, 2011

c. Line injection of additives (FSII and CI/LI) from shipping tank to delivery conveyance or other free on board (FOB) point is permitted under the following conditions:

i.Additives must be proportionately injected throughout the entire loading process to ensure the additive is homogeneously blended into the jet fuel. The Contractor shall maintain records evidencing the homogeneous blending of all line injected additives. Such methods may include meter or tank gauge readings or test results taken at intervals to provide confidence in the injection process.

ii. When FSII is required, additive concentration must be verified based on a representative sample from each shipping conveyance.

(c) Conformance to specification requirements at the custody transfer point is required, however, prior to shipment, a laboratory hand blend of JP-5 fuel with all additives required by this contract shall be tested to verify compliance with the required specification (except for MSEP). MSEP analysis shall be performed per the Contractor’s election in MIL-DTL-5624W.

(d) BATCH SAMPLING: The Contractor shall provide one 20 mL sample per each individual tank in a procurement batch.

NOTE: This sample is in addition to those required in accordance with Quality Assurance Provision (QAP) E1

QUANTITY OF SAMPLE WHEN SAMPLED SUBMISSION PERIOD

20 mL Upon completion of each individual procurement batch Shipped within 30 days of procurement batch delivery

“Batch” Definition in accordance with MIL-STD-3004, 3.1.9: A specific quantity of product that is processed or utilized as a single unit and tested to meet test criteria and specifications.

DEFENSE LOGISTICS AGENCY ENERGY Page 2 of 2

The sample from each tank/batch shall be either an all-level sample or a composite of upper, middle, and lower samples. A copy of the batch’s full-specification test report shall accompany each sample. The sample container shall be any 20 mL amber borosilicate vial with a polytetrafluoroethylene (PTFE) lined screw cap. A tracking number for the samples shall be provided to: Thomas Loegel at thomas.loegel@nrl.navy.mil or (202) 767-1716. Samples shall be shipped to:

US Naval Research Laboratory ATTN: Thomas Loegel, Code 6181

JP-5 Component Analysis Library Project 4555 Overlook Ave., S.W.

Washington D.C. 20375-5320

The paperwork provided with these samples shall include the following information:

• Contract Number

• Contractor’s Name

• Product

• Refinery Location

• Quantity of Tank/Batch

• For samples containing synthetic components, include the following additional information:

• Manufacturer of synthetic component

• Batch Number

• Date of Test Report

• Quantity of Tank/Batch

• Percent Composition

• Production Process of Synthetic Component

• Feedstock

Prepared by

Quality Technical Support Office Approval

Contracting Approval mailto:Robert.morris@nrl.navy.mil

C16.01 TURBINE FUEL, AVIATION (JP5) (DLA ENERGY APRIL 2018)

c. FLASH POINT.

e. MICRO-SEPAROMETER (MSEP) REQUIREMENTS.

(b) ADDITIVES.

c. Line injection of additives (FSII and CI/LI) from shipping tank to delivery conveyance or other free on board (FOB) point is permitted under the following conditions:

2018-04-25T09:13:12-0400

YEN.CHENG.H.1539446041

2018-04-25T09:18:48-0400

BANISZEWSKI.DANIEL.J.1287388698

2018-04-26T16:45:01-0400

SHEPHERD.SANDRA.S.1012568459

DEFENSE LOGISTICS AGENCY ENERGY

C16.08-1 TURBINE FUEL, AVIATION (JET A) (DLA ENERGY JUL 2022)

NATIONAL STOCK NUMBER PRODUCT NOMENCLATURE PRODUCT CODE

9130-00-359-2026 Turbine Fuel, Aviation, Jet A JAA

Supplies delivered under this contract shall conform to all Federal, State, and local environmental requirements applicable to the geographic location of the receiving activity on the date of delivery. This includes delivery of fuel and documentation in a manner consistent with any existing or after-imposed Title V (Clean Air Act) Permits.

(a) PRODUCT REQUIREMENTS. Jet A shall conform to the requirements of the latest version of ASTM D 1655, Standard Specification for Aviation Turbine Fuels, except as modified below, at the custody transfer point.

(b) SPECIFICATION MODIFICATIONS

(1) Microseparometer (MSEP).

(i) The following MSEP ratings apply in the presence of the additives listed below. Values apply at point of manufacture:

Jet-A Additive MSEP Rating, min.

Fuel System Icing Inhibitor (FSII) 85

Corrosion Inhibitor/Lubricity Improver (CI/LI) 80 Fuel System Icing Inhibitor (FSII) and Corrosion

Inhibitor/Lubricity Improver (CI/LI)

(ii) MSEP shall be performed on unadditized Jet A that has a custody transfer point on the distribution system using, D7224 or D8073. If either method is not available testing may be conducted with D3948. Passing results (min 85) for D3948 will be considered acceptable. Test failures using D3948 shall be retested using D7224 or D8073. If fuel passes D7224 with a minimum limit of 85 or D8073 with a limit of 88, the fuel is acceptable with no further action.

(2) Fatty Acid Methyl Ester (FAME)

(i) For offerors that will be offering Jet A FOB Destination and/or Origin TT, which involves staging jet fuel at a terminal via a multi-product pipeline, a Certificate of Quality of the issue tank must include testing for FAME for Acceptance of the fuel. The Test method to be used is either IP 585, IP 583, IP 590, IP 599, or ASTM D 7797. The Referee Method is IP

585. Current ASTM D1655 Jet A specification allows no more than 50 parts per million of FAME in jet fuel.

(c) ADDITIVES.

(1) Additives shall not be premixed with other additives before injection into the fuel.

(2) FUEL SYSTEM ICING INHIBITOR (FSII). When required by contract line item-

(i) FSII shall be added to the fuel and shall be Diethylene Glycol Monomethyl Ether (DIEGME) conforming to the latest version of ASTM D4171, Standard Specification for FSIIs, Type III or MIL-DTL-85470B, dated June 15, 1999, revalidated August 28, 2019, Inhibitor, Icing, Fuel System, High Flash, NATO Code Number S-1745.

(ii) FSII shall be added to the fuel so that the resulting concentration in the final blend is between 0.07% and 0.10% by volume.

(iii) When using the 20-ounce aerosol can to introduce FSII during over the wing refueling, determine the fuel quantity and calculate the amount of required additive. This additive shall be added gradually during filling to permit proper blending in the fuel. One can of aerosol additive will inhibit 180 gallons of fuel to 0.087 percent by volume. The use of aerosol FSII is not permitted for U.S. Navy aircraft refueling.

(3) CORROSION INHIBITOR/LUBRICITY IMPROVER (CI/LI). When required by contract line item-

(i) The additive must conform to MIL-PRF-25017H with Amendment 1, dated August 4, 2011, revalidated May 25, 2021, Inhibitor, Corrosion/Lubricity Improver, Fuel Soluble (NATO S-1747), found in ASSIST and shall be listed in the electronic Qualified Products List (QPL)-25017, located in the Qualified Products Database (QPD) found at https://assist.dla.mil (or http://quicksearch.dla.mil) https://assistdocs.com/

DEFENSE LOGISTICS AGENCY ENERGY

(ii) The concentration of CI/LI added to the fuel must be between the minimum effective concentration and the maximum allowable concentration as listed for the CI/LI in QPL-25017.

(4) STATIC DISSIPATER ADDITIVE (SDA). When required by contract line item-

(i) SDA shall be added to the fuel and the conductivity limits of 50 to 600 picosiemens per meter (pS/m) at ambient temperature or 29.4oC (85oF), whichever is lower, unless otherwise directed by the procuring activity.

(5) METAL DEACTIVATOR (MDA). MDA shall not be used unless the supplier has obtained PRIOR written consent from the procuring activity.

(6) Product shall be homogeneously mixed. Until all aviation turbine fuel tanks are coated, it is acceptable to perform stratification tests in lieu of circulating tanks to achieve homogeneity.

(d) REPORTS. Refer to the MATERIAL INSPECTION AND RECEIVING REPORT (QAP E40.01) contract provision for reporting requirements.

Quality / Technical Support Office Approval:

Contracting Approval:

MACLANE.SKYLLAR.B.1252141827 Digitally Signed By:

MACLANE.SKYLLAR.B.1252141827

Date:

2022.08.02 07:51

Digitally Signed By:

C16.08-1 TURBINE FUEL, AVIATION (JET A) (DLA ENERGY APRIL 2020JUNJUL 2022AUG 2021)

(a) PRODUCT REQUIREMENTS. Jet A shall conform to the requirements of the latest version of ASTM D 1655, Standard Specification for Aviation Turbine Fuels, except as modified below, at theat the custody transfer point.

(b) SPECIFICATION MODIFICATIONS

(c) ADDITIVES.

DEFENSE LOGISTICS AGENCY ENERGY Page 1 of 2

C16.09 TURBINE FUEL, AVIATION (JET A1) (DLA ENERGY JUL 2022)

NATIONAL STOCK NUMBER PRODUCT NOMENCLATURE PRODUCT CODE

9130-00-753-5026 Turbine Fuel, Aviation, Jet A-1 JA1

Supplies delivered under this contract shall conform to all Federal, State, and local environmental requirements applicable to the geographic location of the receiving activity on the date of delivery. This includes delivery of fuel and documentation in a manner consistent with any existing or after-imposed Title V (Clean Air Act) Permits. The list of such requirements contained in this contract is not intended to be a complete list, and the Contractor shall be responsible for determining the existence of all such requirements. Selected regional environmental requirements are highlighted in the SPECIFICATIONS (CONT’D) clause. In the event that a Federal, State, or local environmental requirement is more stringent than a fuel specification contained in this contract, the Contractor shall deliver product that complies with the more stringent fuel specification. Product that fails to meet the more stringent fuel specification will be considered to be a nonconforming supply. Product(s) to be supplied shall fully meet the requirements of the applicable specification(s) as cited above. In the event that compliance with the more stringent fuel specification causes the contractor to incur additional costs, the contractor may request an equitable adjustment.

(a) PRODUCT REQUIREMENTS. Product shall conform to the latest version of ASTM D1655: Standard Specification for Aviation Turbine Fuels with the following modifications. For European, Middle Eastern, and Asian Locations Only: product shall conform to the latest revision of Defence Standard 91-091.

(b) SPECIFICATION MODIFICATIONS.

(1) Microseparometer (MSEP).

(i) The following MSEP ratings apply in the presence of the additives listed below. Values apply at point of manufacture:

Jet A-1 Additive MSEP Rating, min.

Fuel System Icing Inhibitor (FSII) 85 Corrosion Inhibitor/Lubricity Improver (CI/LI) 80

Fuel System Icing Inhibitor (FSII) and Corrosion Inhibitor/Lubricity Improver (CI/LI) 70

a. MSEP shall be performed on unadditized Jet A that has a custody transfer point on the distribution system using, D7224 or D8073. If either method is not available testing may be conducted with D3948. Passing results (min 85) for D3948 will be considered acceptable. Test failures using D3948 shall be retested using D7224 or D8073. If fuel passes D7224 with a minimum limit of 85 or D8073 with a limit of 88, the fuel is acceptable with no further action.

(c) ADDITIVES: Additives shall not be premixed with other additives before injection into the fuel.

(1) FUEL SYSTEM ICING INHIBITOR (FSII). When FSII is required by contract line item—

(i) The fuel shall contain 0.07 to 0.10 percent by volume FSII.

(ii) FSII shall be added to the fuel and shall be Diethylene Glycol Monomethyl Ether (DIEGME) conforming to the latest version of ASTM D4171, Standard Specification for FSIIs, Type III or MIL-DTL-85470B, dated June 15, 1999 revalidated August 28, 2019, Inhibitor, Icing, Fuel System, High Flash, NATO Code Number S-1745.

(iii) When using the 20-ounce aerosol can to introduce FSII during over the wing refueling, determine the fuel quantity and calculate the amount of required additive. This additive shall be added gradually during filling to permit proper blending in the fuel. One can of aerosol additive will inhibit 180 gallons of fuel to 0.087 percent by volume. The use of aerosol FSII is not permitted for U.S. Navy aircraft refueling.

(2) CORROSION INHIBITOR/LUBRICITY IMPROVER (CI/LI). When CI/LI is required by contract line item the additive shall conform to the latest revision of MIL-PRF-25017H with amendment 1 dated August 4,2011, revalidated May 25, 2021 and be listed in Qualified Products List (QPL)-25017. In order to obtain dosage data for QPL-25017 additives, log into ASSIST Online, access the Qualified Products Database (QPD), do a search for QPL number 25017, and click the MIL-PRF-25017 Category 1 link. The dosage information is located in the "source notes" for each qualified additive as minimum effective and maximum allowable concentrations in grams per cubic meter (g/m3).

(3) STATIC DISSIPATER ADDITIVE (SDA). When required by contract line item-

(i) SDA shall be added to the fuel and the conductivity limits of 50 to 600 picosiemens per meter (pS/m) at ambient temperature or 29.4oC (85oF), whichever is lower, unless otherwise directed by the procuring activity.

(4) METAL DEACTIVATOR ADDITIVE (MDA). MDA shall not be used unless the supplier has obtained written consent from the procuring activity and user.

(i) Product shall be homogeneously mixed. Until all aviation turbine fuel tanks are coated, it is acceptable to perform stratification tests in lieu of circulating tanks to achieve homogeneity.

Quality/Technical Support Office Approval

Contracting Approval: Digitally signed by

MACLANE.SKYLLAR.B.1252141827

Digitally Signed By: MACLANE.SKYLLAR.B.1252141827

2022.08.03 09:13

C16.09 TURBINE FUEL, AVIATION (JET A1) (DLA ENERGY OCT 2017AUG 2021JULN 2022)

PRODUCT CODE

PRODUCT NOMENCLATURE

NATIONAL STOCK NUMBER

JA1

Turbine Fuel, Aviation, Jet A-1

9130-00-753-5026

(b) SPECIFICATION MODIFICATIONS.

2022-08-15T12:12:18-0400

RALPH.ERIN.S.1229663042

2022-09-08T13:05:30-0400

BANISZEWSKI.DANIEL.J.1287388698

DEFENSE LOGISTICS AGENCY ENERGY Page 1 of 6

C16.23 FUEL, NAVAL DISTILLATE (F-76) (DLA ENERGY AUGUST 2022)

NATIONAL STOCK NUMBER PRODUCT NOMENCLATURE DLA ENERGY PRODUCT CODE

9140-00-273-2377 Fuel, Naval Distillate F76

For supplies delivered under this contract, the Contractor shall conform to all International, Federal, State, and local environmental requirements applicable to the geographic location of the receiving activity on the date of delivery. The Contractor shall also comply with all applicable International Agreements, Treaties, Conventions, and the like to which the United States is a signatory or with whose terms the receiving activity has otherwise agreed to comply, including but not limited to, the requirements of MARPOL 73/78 Annex VI Regulations 14 and 18. The Contractor shall be responsible for determining the existence of all such requirements prior to the time deliveries are made. This includes delivery of fuel and documentation in a manner consistent with any existing or after-imposed Title V (Clean Air Act) Permits. The list of such requirements contained in this contract is not intended to be a complete list, and the Contractor shall be responsible for determining the existence of all such requirements. In the event that an International, Federal, State, and/or local environmental requirement, as identified above, is more stringent than a requirement contained in this contract, the Contractor shall deliver product(s) that complies with the more stringent requirement. Product(s) that fails to meet the more stringent requirement will be considered nonconforming supply. Product(s) to be supplied shall fully meet the requirements of the applicable specification(s). In the event that compliance with the more stringent requirement causes the contractor to incur additional costs, the contractor may request an equitable adjustment.

Unless otherwise indicated by the Contractor in writing, prior to award, the product offered shall be required to fully meet all applicable specifications. The supplier shall provide to the receiving vessel a “Statutory Sample” of at least 400 mL in volume, taken from the receiving vessel’s inlet bunker manifold, together with a Bunker Delivery Note (BDN). This sample will be sealed and carry a sample tag that provides the documentation required per MARPOL 73/78, Annex VI Regulation 18.

a) Naval Distillate Fuel (F-76) shall conform to the requirements of Military specification MIL-DTL-16884P dated 26 Sept 2017.

Nomenclature for Naval Distillate Fuel (F-76) is shown above.

b) SPECIFICATION MODIFICATIONS:

1) Flash Point: All batches of F-76 that are presented for Government acceptance at origin shall meet a minimum flash point requirement of 62.5 degrees Celsius (°C).

2) F-76 offered from a location other than where refined (excludes synthesized material as defined in section 3.2.2 and 3.2.3 of MIL- DTL-16884P) requires testing for FAME content by test method ASTM D7963, BS EN 14078, or IP 579. ASTM D7963 is considered to be the referee test method.

3) In Australia, all deliveries of F-76 shall have a minimum Flash Point of 62.5°C at the custody transfer point.

4) Ash, mass%: All batches of F-76 shall not exceed 0.010% Ash by ASTM D482.

c) MATERIALS: The F-76 supplied under this contract shall not contain un-hydrotreated light cycle oils or contain any stabilizer additives, or any other additive or material not explicitly allowed per section 3.2 of MIL-DTL-16884P.

For F-76 containing a synthetic component, the synthetic component shall be certified to Tables A-I and A-II of MIL-DTL-16884P; for synthesized iso-paraffins, the synthetic component shall be certified to Tables B-I and B-II of MIL-DTL-16884P. It is not necessary to analyze each batch of the synthetic component for compliance with Table A-II (or Table B-II, as applicable) once it is demonstrated that the process scheme is adequately controlled and if no significant changes to existing production operations have been made, such as a turnaround event on a refinery unit used to produce the synthetic component or a change in feedstock material. The signed F-76 synthetic component certification page shall be supplied for each shipment which includes synthetic paraffinic materials attesting that no changes to the production process have been made and certifying that the last certificate of analysis, dated and including Table A-II (or Table B-II, as applicable) results, is still valid.

d) ADDITIVES:

1) Lubricity Improver Additive (LIA) – Lubricity additives are allowed in F-76. The LIA additive(s) used shall conform to MIL-PRF-

32490A, Performance Specification, Additive, Lubricity Improver, Distillate Fuel, dated 24 May 2019 and found in ASSIST and shall

DEFENSE LOGISTICS AGENCY ENERGY Page 2 of 6 be listed in the electronic Qualified Products List (QPL)-32490, located in the Qualified Products Database (QPD) found at https://assist.dla.mil/ (or http://quicksearch.dla.mil) . Instructions on how to use ASSIST are located in QAP C1.02. Either Grade A.

Grade B, or Grade C material is suitable for treatment of de-sulfurized F-76. Additive concentration shall not exceed the maximum allowable concentration applicable to the specific additive selected for inclusion in finished F-76.

2) Information pertaining to qualification of additives not currently listed on QPL-32490 may be obtained from Commander, Naval Sea Systems Command, ATTN: SEA 05S, 1333 Isaac Hull Avenue, SE, Stop 5160, Washington Navy Yard, DC 20376-5160, USA, or by e-mailing CommandStandards@navy.mil.

3) Dyes and Markers - Red dye required in off-highway diesel fuel in accordance with 40 CFR Part 80 as modified by the Environmental Protection Agency's interim final rule published in the Federal Register dated July 14, 1994 shall not be added to F-

76. The finished product shall show no visual evidence of red dye. This F-76 product is for military, off-highway use only and must be segregated at all times from any diesel fuel used on-highway. NOTE: Red dye does not apply to Atlantic/Europe/Mediterranean or Western Pacific Overseas Bulk purchase programs unless offering refinery is located in the United States or one of its possessions.

e) BATCH SAMPLING: The Contractor shall provide one 20 mL sample per each individual tank in a procurement batch.

For each 20 mL sample provided by the Contractor, the Contractor shall also submit a Refinery Certificate of Quality (RCQ), or Certificate of Analysis (CoA), as applicable, with the F-76 sample when submitting to the US Naval Research Laboratory.

The RCQ or CoA for each individual tank shall be representative of Level A testing for the F-76 product.

NOTE: This sample is in addition to those required in accordance with Quality Assurance Provision (QAP) E1

QUANTITY OF SAMPLE WHEN SAMPLED SUBMISSION PERIOD

20 mL Upon completion of each individual

Shipped within 30 days of delivery of

“Batch” Definition in accordance with MIL-STD-3004-1A, 3.1.9: A specific quantity of product that is processed or utilized as a single unit and tested to meet test criteria and specifications.

The sample from each tank/batch shall be either an all-level sample or a composite of upper, middle, and lower samples. A copy of the full-specification test report shall accompany each sample. The sample container will be any 20 mL amber borosilicate vial with a polytetrafluoroethylene (PTFE) lined screw cap. A tracking number for the samples shall be provided to: Thomas Loegel at Thomas.loegel@nrl.navy.mil or (202) 404-1157. Samples shall be shipped to:

US Naval Research Laboratory ATTN: Thomas Loegel, Code 6181 F76 Component Analysis Forensic Project 4555 Overlook Ave., S.W.

Washington D.C. 20375-5320

The paperwork provided with these samples shall include the following information:

Contract Number Contractor’s Name Product Refinery Location Quantity of Tank/Batch Full-Specification Test Report https://assist.dla.mil/ https://assist.dla.mil/ https://assist.dla.mil/ https://assist.dla.mil/ https://assist.dla.mil/ http://quicksearch.dla.mil/

DEFENSE LOGISTICS AGENCY ENERGY Page 3 of 6

For samples containing synthetic components, include the following additional information:

Manufacturer of synthetic component Batch Number Date of Test Report Quantity of Tank/Batch Percent Composition Production Process of Synthetic Component Feedstock Full-Specification Test Report

f) TRACEABILITY:

1) F-76 fuel supplied under this contract shall maintain t