grp-8-white-painted-exterior-facia-trim-doors-feb2018.pdf

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FY23 OHARNG CJAG Demolition Project
Solicitation number
W91364-23-B-0005
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This analytical report details the results of testing samples from various buildings and structures at Camp Ravenna in Ohio for the presence of metals and polychlorinated biphenyls (PCBs). Sample locations included white painted facia and trim from several buildings, as well as concrete flooring from an igloo structure. Laboratory tests identified levels of lead in leachate from some painted samples, while PCB tests of the concrete flooring sample showed non-detect results for all Aroclor analytes. Quality control samples like method blanks, laboratory control samples, matrix spikes, and matrix spike duplicates were included to validate the analytical results. Surrogate recoveries were within method acceptance limits except for one sample. This report provides analytical data to characterize waste streams at the site in support of the upcoming FY23 OHARNG CJAG Demolition Project solicited by the Department of the Army Ohio Army National Guard.

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ANALYTICAL REPORT

TestAmerica Laboratories, Inc.

TestAmerica Canton 4101 Shuffel Street NW North Canton, OH 44720 Tel: (330)497-9396

TestAmerica Job ID: 240-90866-1 Client Project/Site: Waste Stream Characterization

For:

Ohio Army National Guard Camp Ravenna 1438 State Route 534 SW Newton Falls, Ohio 44444

Attn: Brad Kline

Authorized for release by:

2/7/2018 12:43:47 PM

Opal Johnson, Project Manager II (330)497-9396 opal.johnson@testamericainc.com

This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature.

Results relate only to the items tested and the sample(s) as received by the laboratory.

https://secure.testamericainc.com/TotalAccess/login.aspx http://www.testamericainc.com/AskTheExpert/Expert_index.htm http://www.testamericainc.com mailto:opal.johnson@testamericainc.com

Table of Contents

Client: Ohio Army National Guard Project/Site: Waste Stream Characterization

TestAmerica Job ID: 240-90866-1

TestAmerica Canton

2/7/2018

Cover Page

Table of Contents

Definitions/Glossary

Case Narrative

Method Summary

Sample Summary

Detection Summary

Client Sample Results

Surrogate Summary

QC Sample Results

QC Association Summary

Lab Chronicle

Certification Summary

Chain of Custody

Definitions/Glossary TestAmerica Job ID: 240-90866-1Client: Ohio Army National Guard

Project/Site: Waste Stream Characterization

Qualifiers

GC Semi VOA

Qualifier Description

U Indicates the analyte was analyzed for but not detected.

Qualifier

X Surrogate is outside control limits

J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.

p The %RPD between the primary and confirmation column/detector is >40%. The lower value has been reported.

Metals

Qualifier Description

U Indicates the analyte was analyzed for but not detected.

Qualifier

Glossary

These commonly used abbreviations may or may not be present in this report.

¤ Listed under the "D" column to designate that the result is reported on a dry weight basis

Abbreviation

%R Percent Recovery

CFL Contains Free Liquid

CNF Contains No Free Liquid

DER Duplicate Error Ratio (normalized absolute difference)

Dil Fac Dilution Factor

DL Detection Limit (DoD/DOE)

DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample

DLC Decision Level Concentration (Radiochemistry)

EDL Estimated Detection Limit (Dioxin)

LOD Limit of Detection (DoD/DOE)

LOQ Limit of Quantitation (DoD/DOE)

MDA Minimum Detectable Activity (Radiochemistry)

MDC Minimum Detectable Concentration (Radiochemistry)

MDL Method Detection Limit

ML Minimum Level (Dioxin)

NC Not Calculated

ND Not Detected at the reporting limit (or MDL or EDL if shown)

PQL Practical Quantitation Limit

QC Quality Control

RER Relative Error Ratio (Radiochemistry)

RL Reporting Limit or Requested Limit (Radiochemistry)

RPD Relative Percent Difference, a measure of the relative difference between two points

TEF Toxicity Equivalent Factor (Dioxin)

TEQ Toxicity Equivalent Quotient (Dioxin)

TestAmerica Canton

Page 3 of 23 2/7/2018

Method Summary

Project/Site: Waste Stream Characterization

Method Method Description LaboratoryProtocol

SW8468082A Polychlorinated Biphenyls (PCBs) by Gas Chromatography TAL CAN

SW8466010C Metals (ICP) TAL CAN

Protocol References:

SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.

Laboratory References:

TAL CAN = TestAmerica Canton, 4101 Shuffel Street NW, North Canton, OH 44720, TEL (330)497-9396

TestAmerica Canton

Page 6 of 23 2/7/2018

Client Sample Results

Project/Site: Waste Stream Characterization

Lab Sample ID: 240-90866-1Client Sample ID: 18-001 WHITE PAINTED FACIA-GROUP B Matrix: SolidDate Collected: 01/26/18 11:40

Date Received: 01/26/18 16:30

Method: 6010C - Metals (ICP) - TCLP

RL MDL

Lead 8.0 1.0 0.055 mg/L 02/01/18 14:00 02/02/18 16:08 1

Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier

TestAmerica Canton

Page 9 of 23 2/7/2018

Project/Site: Waste Stream Characterization

Lab Sample ID: 240-90866-3Client Sample ID: 18-003 BLDG 833 WHITE PAINTED

DOOR/TRIM

Matrix: SolidDate Collected: 01/26/18 11:45

Date Received: 01/26/18 16:30

Method: 6010C - Metals (ICP) - TCLP

RL MDL

Lead 7.4 1.0 0.055 mg/L 02/01/18 14:00 02/02/18 16:17 1

Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier

TestAmerica Canton

Page 11 of 23 2/7/2018

Project/Site: Waste Stream Characterization

Lab Sample ID: 240-90866-4Client Sample ID: 18-004 BLDG 832 WHITE PAINTED

DOOR/TRIM

Matrix: SolidDate Collected: 01/26/18 12:10

Date Received: 01/26/18 16:30

Method: 6010C - Metals (ICP) - TCLP

RL MDL

Lead 24 1.0 0.055 mg/L 02/01/18 14:00 02/02/18 16:22 1

Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier

TestAmerica Canton

Page 12 of 23 2/7/2018

Project/Site: Waste Stream Characterization

Lab Sample ID: 240-90866-6Client Sample ID: 18-006 GROUP 7 IGLOO CONCRETE

FLOORING

Matrix: SolidDate Collected: 01/26/18 14:45

Date Received: 01/26/18 16:30

Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography

RL MDL

Aroclor-1016 10000 U 10000 4400 ug/Kg 02/02/18 10:27 02/05/18 14:39 100

Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier

10000 4800 ug/Kg 02/02/18 10:27 02/05/18 14:39 100Aroclor-1221 10000 U

10000 4600 ug/Kg 02/02/18 10:27 02/05/18 14:39 100Aroclor-1232 10000 U

10000 3800 ug/Kg 02/02/18 10:27 02/05/18 14:39 100Aroclor-1242 10000 U

10000 4800 ug/Kg 02/02/18 10:27 02/05/18 14:39 100Aroclor-1248 10000 U

10000 4600 ug/Kg 02/02/18 10:27 02/05/18 14:39 100Aroclor-1254 10000 U

10000 4400 ug/Kg 02/02/18 10:27 02/05/18 14:39 100Aroclor-1260 10000 U

10000 6200 ug/Kg 02/02/18 10:27 02/05/18 14:39 100Aroclor-1262 10000 U

10000 4600 ug/Kg 02/02/18 10:27 02/05/18 14:39 100Aroclor-1268 12000

Tetrachloro-m-xylene 128 14 - 128 02/02/18 10:27 02/05/18 14:39 100

Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery

DCB Decachlorobiphenyl 489 X 02/02/18 10:27 02/05/18 14:39 10010 - 132

Method: 6010C - Metals (ICP) - TCLP

RL MDL

Lead 0.050 U 0.050 0.0028 mg/L 02/01/18 14:00 02/02/18 16:26 1

Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier

TestAmerica Canton

Page 13 of 23 2/7/2018

Surrogate Summary

Project/Site: Waste Stream Characterization

Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography Prep Type: Total/NAMatrix: Solid

Lab Sample ID Client Sample ID (14-128) (10-132)

TCX2 DCBP2

128 489 X240-90866-6

Percent Surrogate Recovery (Acceptance Limits)

18-006 GROUP 7 IGLOO CONCRETE FLOORING

103 408 p X240-90866-6 MS 18-006 GROUP 7 IGLOO

CONCRETE FLOORING

89 360 p X240-90866-6 MSD 18-006 GROUP 7 IGLOO

CONCRETE FLOORING

101 103LCS 240-313346/5-A Lab Control Sample

93 97MB 240-313346/4-A Method Blank

Surrogate Legend

TCX = Tetrachloro-m-xylene

DCBP = DCB Decachlorobiphenyl

TestAmerica Canton

Page 14 of 23 2/7/2018

QC Sample Results

Project/Site: Waste Stream Characterization

Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography

Client Sample ID: Method BlankLab Sample ID: MB 240-313346/4-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 313454 Prep Batch: 313346

RL MDL

Aroclor-1016 100 U 100 44 ug/Kg 02/02/18 10:27 02/05/18 15:38 1

MB MB

Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier

100 U 48100 ug/Kg 02/02/18 10:27 02/05/18 15:38 1Aroclor-1221

100 U 46100 ug/Kg 02/02/18 10:27 02/05/18 15:38 1Aroclor-1232

100 U 38100 ug/Kg 02/02/18 10:27 02/05/18 15:38 1Aroclor-1242

100 U 48100 ug/Kg 02/02/18 10:27 02/05/18 15:38 1Aroclor-1248

100 U 46100 ug/Kg 02/02/18 10:27 02/05/18 15:38 1Aroclor-1254

100 U 44100 ug/Kg 02/02/18 10:27 02/05/18 15:38 1Aroclor-1260

100 U 62100 ug/Kg 02/02/18 10:27 02/05/18 15:38 1Aroclor-1262

100 U 46100 ug/Kg 02/02/18 10:27 02/05/18 15:38 1Aroclor-1268

Tetrachloro-m-xylene 93 14 - 128 02/05/18 15:38 1

MB MB

Surrogate

02/02/18 10:27

Dil FacPrepared AnalyzedQualifier Limits%Recovery

97 02/02/18 10:27 02/05/18 15:38 1DCB Decachlorobiphenyl 10 - 132

Client Sample ID: Lab Control SampleLab Sample ID: LCS 240-313346/5-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 313454 Prep Batch: 313346

Aroclor-1016 2000 1690 ug/Kg 84 47 - 120

Analyte

LCS LCS

DUnitResult Qualifier %Rec

Spike

Added

%Rec.

Limits

Aroclor-1260 2000 1890 ug/Kg 95 46 - 120

Tetrachloro-m-xylene 14 - 128

Surrogate

LCS LCS

Qualifier Limits%Recovery

103DCB Decachlorobiphenyl 10 - 132

Client Sample ID: 18-006 GROUP 7 IGLOO CONCRETE FLOORINGLab Sample ID: 240-90866-6 MS Matrix: Solid Prep Type: Total/NA Analysis Batch: 313454 Prep Batch: 313346

Aroclor-1016 10000 U 2030 5180 J p ug/Kg NC 31 - 120

Analyte

MS MS

DUnitResult Qualifier %Rec

Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Aroclor-1260 10000 U 2030 11700 ug/Kg NC 21 - 122

Tetrachloro-m-xylene 14 - 128

Surrogate

MS MS

Qualifier Limits%Recovery

408 p XDCB Decachlorobiphenyl 10 - 132

Client Sample ID: 18-006 GROUP 7 IGLOO CONCRETE FLOORINGLab Sample ID: 240-90866-6 MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 313454 Prep Batch: 313346

Aroclor-1016 10000 U 2000 4490 J p ug/Kg NC 31 - 120 14 30

Analyte

MSD MSD

DUnitResult Qualifier %Rec

Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD

Aroclor-1260 10000 U 2000 10200 ug/Kg NC 21 - 122 14 30

TestAmerica Canton

Page 15 of 23 2/7/2018

QC Sample Results

Project/Site: Waste Stream Characterization

Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography (Continued)

Client Sample ID: 18-006 GROUP 7 IGLOO CONCRETE FLOORINGLab Sample ID: 240-90866-6 MSD Matrix: Solid Prep Type: Total/NA Analysis Batch: 313454 Prep Batch: 313346

Tetrachloro-m-xylene 14 - 128

Surrogate

MSD MSD

Qualifier Limits%Recovery

360 p XDCB Decachlorobiphenyl 10 - 132

Method: 6010C - Metals (ICP)

Client Sample ID: Method BlankLab Sample ID: MB 240-313205/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 313375 Prep Batch: 313205

RL MDL

Lead 0.050 U 0.050 0.0028 mg/L 02/01/18 14:00 02/02/18 14:58 1

MB MB

Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier

Client Sample ID: Lab Control SampleLab Sample ID: LCS 240-313205/3-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 313375 Prep Batch: 313205

Lead 0.500 0.403 mg/L 81 50 - 150

Analyte

LCS LCS

DUnitResult Qualifier %Rec

Spike

Added

%Rec.

Limits

Client Sample ID: Method BlankLab Sample ID: LB 240-313097/1-B Matrix: Solid Prep Type: TCLP Analysis Batch: 313375 Prep Batch: 313205

RL MDL

Lead 0.050 U 0.050 0.0028 mg/L 02/01/18 14:00 02/02/18 14:53 1

LB LB

Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier

TestAmerica Canton

Page 16 of 23 2/7/2018

1. Cover Page
2. Table of Contents
3. Definitions/Glossary
4. Case Narrative
5. Method Summary
6. Sample Summary
7. Detection Summary
8. Client Sample Results
9. Surrogate Summary
10. QC Sample Results
11. QC Association Summary
12. Lab Chronicle
13. Certification Summary
14. Chain of Custody

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