B.08.03 19R4000 Amendment 2 Water Analysis 1-6-2020.pdf

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ANALYTICAL REPORT

CLIENT

FJNC

4170 Percival Rd.

Columbia, SC 29229

ATTENTION

Robert Bryson

PROJECT ID

Well Water Test - FJNC

LABORATORY REPORT NUMBER

219030723

DATE

03/19/2019

Primary Data Review By Secondary Data Review By

Ashley B. Amick

Authorized Signature Project Manager, Access Analytical, Inc.

aamick@accessanalyticalinc.com

PLEASE NOTE:

- Unless otherwise noted, all analysis on this report performed at Gulf Coast Analytical Labs (GCAL), 7979 Innovation Park Dr., Baton Rouge, LA 70820.

- GCAL is SCDHEC certified laboratory # 73006, NCDENR certified lab # 618, GA certified lab # LA-01955, NELAP certified laboratory # 01955

- Local support services for this project are provided by Access Analytical, Inc.. Access Analytical is a representative of GCAL serving clients in the SC/NC/GA areas. All questions regarding this report should be directed to your local Access Analytical representative at 803.781.4243 or toll free at 888.315.4243.

Page 1 of 11Lab Report#: 219030723

Lab Cover

ANALYTICAL RESULTS

PERFORMED BY

GCAL, LLC

7979 Innovation Park Dr.

Baton Rouge, LA 70820

(225) 769-4900

Report Date 03/19/2019

GCAL Report 219030723

9999999999

Project Well Water Test - FJNC

Deliver To Additional Recipients Robert Bryson Lab Reports, Access Analytical

FJNC

4170 Percival Rd.

Columbia, SC 29229

LELAP CERTIFICATE NUMBER: 01955

DOD-ELAP ACCREDITATION NUMBER: 74960

Page 2 of 11Lab Report#: 219030723

Report#: 219030723

Project ID: Well Water Test - FJNC Report Date: 03/19/2019

Laboratory Endorsement

Sample analysis was performed in accordance with approved methodologies provided by the Environmental Protection Agency or other recognized agencies. The samples and their corresponding extracts will be maintained for a period of 30 days unless otherwise arranged. Following this retention period the samples will be disposed in accordance with GCAL's Standard Operating Procedures.

Common Abbreviations that may be Utilized in this Report

ND Indicates the result was Not Detected at the specified reporting limit NO Indicates the sample did not ignite when preliminary test performed for EPA Method 1030 DO Indicates the result was Diluted Out MI Indicates the result was subject to Matrix Interference TNTC Indicates the result was Too Numerous To Count SUBC Indicates the analysis was Sub-Contracted FLD Indicates the analysis was performed in the Field DL Detection Limit LOD Limit of Detection LOQ Limit of Quantitation RE Re-analysis CF HPLC or GC Confirmation 00:01 Reported as a time equivalent to 12:00 AM

Reporting Flags that may be Utilized in this Report

J or I Indicates the result is between the MDL and LOQ J DOD flag on analyte in the parent sample for MS/MSD outside acceptance criteria U Indicates the compound was analyzed for but not detected B or V Indicates the analyte was detected in the associated Method Blank Q Indicates a non-compliant QC Result (See Q Flag Application Report)

* Indicates a non-compliant or not applicable QC recovery or RPD – see narrative E Organics - The result is estimated because it exceeded the instrument calibration range E Metals - % diference for the serial dilution is > 10% L Reporting Limits adjusted to meet risk-based limit.

P RPD between primary and confirmation result is greater than 40 DL Diluted analysis – when appended to Client Sample ID

Sample receipt at GCAL is documented through the attached chain of custody. In accordance with NELAC, this report shall be reproduced only in full and with the written permission of GCAL. The results contained within this report relate only to the samples reported. The documented results are presented within this report.

This report pertains only to the samples listed in the Report Sample Summary and should be retained as a permanent record thereof. The results contained within this report are intended for the use of the client. Any unauthorized use of the information contained in this report is prohibited.

I certify that this data package is in compliance with The NELAC Institute (TNI) Standard 2009 and terms and conditions of the contract and Statement of Work both technically and for completeness, for other than the conditions in the case narrative. Release of the data contained in this hardcopy data package and in the computer readable data submitted has been authorized by the Quality Assurance Manager or his/her designee, as verified by the following signature.

Estimated uncertainty of measurement is available upon request. This report is in compliance with the DOD QSM as specified in the contract if applicable.

Authorized Signature GCAL Report 219030723

Page 3 of 11Lab Report#: 219030723

Certifications

Certification Certification Number

DOD ELAP 74960

Alabama 01955

Arkansas 88-0655

Colorado 01955

Delaware 01955

Florida E87854

Georgia 01955

Hawaii 01955

Idaho 01955

Illinois 200048

Indiana 01955

Kansas E-10354

Kentucky 95

Louisiana 01955

Maryland 01955

Massachusetts 01955

Michigan 01955

Mississippi 01955

Missouri 01955

Montana N/A

Nebraska 01955

New Mexico 01955

North Carolina 618

North Dakota R-195

Oklahoma 9403

South Carolina 73006001

South Dakota 01955

Tennessee 01955

Texas T104704178

Vermont 01955

Virginia 460215

Washington C929

USDA Soil Permit P330-16-00234

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Case Narrative

Client: Access Analytical Report: 219030723

Gulf Coast Analytical Laboratories received and analyzed the sample(s) listed on the Report Sample Summary page of this report. Receipt of the sample(s) is documented by the attached chain of custody. This applies only to the sample(s) listed in this report.

No sample integrity or quality control exceptions were identified unless noted below.

No anomalies were found for the analyzed sample(s).

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Sample Summary

GCAL ID Client ID Matrix Collect Date/Time Receive Date/Time

21903072301 OLD SIDE Water 02/28/2019 15:20 03/07/2019 09:35

21903072302 NEW SIDE Water 02/28/2019 14:00 03/07/2019 09:35

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Detect Summary

Summary of Compounds Detected

NEW SIDE

NEW SIDE

Collect Date 02/28/2019 14:00 GCAL ID 21903072302

Receive Date 03/07/2019 09:35 Matrix Water

EPA 6020B

EPA 6020B

CAS# Parameter Result DL LOQ Units

7439-89-6 Iron 35.3J 25.0 100 ug/L

Page 7 of 11Lab Report#: 219030723

Sample Results

Sample Results

OLD SIDE

OLD SIDE

Collect Date 02/28/2019 15:20 GCAL ID 21903072301

Receive Date 03/07/2019 09:35 Matrix Water

EPA 6020B

EPA 6020B

Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch

03/07/2019 15:30 655398 EPA 3010A 1 03/13/2019 16:29 LWZ 655802

7439-89-6 Iron 25.0U 25.0 100 ug/L

NEW SIDE

NEW SIDE

Collect Date 02/28/2019 14:00 GCAL ID 21903072302

Receive Date 03/07/2019 09:35 Matrix Water

EPA 6020B

EPA 6020B

Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch

03/07/2019 15:30 655398 EPA 3010A 1 03/14/2019 01:25 LWZ 655869

7439-89-6 Iron 35.3J 25.0 100 ug/L

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QC Summary

Inorganics QC Summary Inorganics

Analytical Batch 655802 Prep Batch 655398 Prep Method

EPA 3010A

Client ID

GCAL ID

Sample Type Prep Date

Analysis Date Matrix

MB655398

1903097

MB

03/07/2019 15:30 03/13/2019 15:50 Water

LCS655398

1903098

LCS

03/07/2019 15:30 03/13/2019 15:55

EPA 6020B

Units

Result ug/L

DL

Spike

Added Result %R

Control Limits%R

Iron 7439-89-6 25.0U 25.0 5000 4870 97 80 - 120

Analytical Batch 655802 Prep Batch 655398 Prep Method

EPA 3010A

Client ID

GCAL ID

Sample Type Prep Date

Analysis Date Matrix

OLD SIDE

21903072301

SAMPLE

03/07/2019 15:30 03/13/2019 16:29

1903317MS

1903391

MS

03/07/2019 15:30 03/13/2019 16:34

1903317MSD

1903392

MSD

03/07/2019 15:30 03/13/2019 16:39

EPA 6020B

Units

Result ug/L

DL

Spike

Added Result %R

Control Limits%R

Spike Added

Result %R RPD

RPD

Limit

Iron 7439-89-6 0.0 25.0 5000 5270 105 80 - 120 5000 5230 105 1 20

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SAMPLE RECEIVING CHECKLIST *219030723*

SAMPLE DELIVERY GROUP 219030723

Client PM AEC Transport Method 4565 - Access Analytical FEDEX

Profile Number Received By 279160 Savage, Tiffany R

Line Item(s) Receive Date(s) 1 - W-Iron 03/07/19

CHECKLIST YES NO

Samples received with proper thermal preservation?

Radioactivity is <1600 cpm? If no, record cpm value in notes section.

COC relinquished and complete (including sampleIDs, collect times, and sampler)?

All containers received in good condition and within hold time?

All sample labels and containers received match the chain of custody?

Preservative added to any containers?

If received, was headspace for VOC water containers < 6mm?

Samples collected in containers provided by GCAL?

COOLERS

Airbill Thermometer ID: E29 Temp oC

5035-7507-4018 0.5

DISCREPANCIES

None

LAB PRESERVATIONS

None

NOTES

Revision 1.6 Page 1 of 1

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COC & Sample Checklist