KGS1057896_Appendix 2_General Waste Profiles.pdf

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Hazardous & Non-Hazardous Waste Collection, Management & Removal Services
Solicitation number
63-63-KGS1057806
Issued by
North Carolina

About this file

This document is a Waste Profile Form from North Carolina State University detailing two specific waste streams: used oil (Profile #6) and broken mercury-containing bulbs (Profile #185). The form provides comprehensive technical and regulatory information for waste disposal, including physical characteristics, chemical composition, generator details, and EPA waste codes. Both waste streams are generated on-site by the university and classified as hazardous waste, with the used oil being a liquid petroleum-based product and the broken bulbs containing trace amounts of mercury.

The waste profiles include detailed specifications for shipping, handling, and disposal, with specific focus on regulated constituents, TCLP (Toxicity Characteristic Leaching Procedure) limits, and environmental compliance. The used oil waste is composed of 30-70% petroleum oil, 10% synthetic oil, and 10% vegetable oil, while the broken bulbs contain 99.99% broken glass with mercury levels ranging from 0.001% to 0.1%. Both waste streams are classified as Large Quantity Generator (LQG) status and require specialized handling under federal and state environmental regulations, with multiple EPA waste codes applicable to each profile.

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C: PHYSICAL CHARACTERISTICS OF WASTE (@70°F)

D: CHEMICAL COMPOSITION OF WASTE

Constituent Key Min Max UOM

WATER = 10 % SYNTHETIC OIL = 30 %

PETROLEUM OIL Range 30 70 % VEGETABLE OIL = 10 %

MINERAL SPIRITS = 30 %

E: ADDITIONAL INFORMATION:

A: GENERATOR INFORMATION North Carolina State University GEN #: NCD000830737

Yes No

EPA ID#:Name:

Site Address: 2620 Wolf Village Way City: Raleigh State : NC Zip : 27695

City: Raleigh State : NC Zip : 27695Campus Box 8007Mailing Address:

Email: mdlong3@ncsu.edu Phone: (919) 515-6863 Fax: (919) 515-6307Contact: Mike Long

Manifest ER Phone #: (877) 577-2669 Generator Subpart P: State ID#:

Generator Status: LQG SQG VSQG/CESQG

Disposal Restrictions:

NAICS code(s)(primary reporting first):

TSDF Approval List: Yes No

Yes NoVarious Generator:

CUSTOMER/BILLING/BROKER INFORMATION Same as Generating Facility address:

Customer #:

Phone:

State: NCCity: RALEIGH

Customer Name: North Carolina State University

Address: CAMPUS BOX 8007

Contact:

Zip: 27695-0001

Fax:Email: mdlong3@ncsu.edu

B: WASTE DESCRIPTION Waste Common Name: 101 USED OIL

Process generating Waste (be specific): SPENT LUBRICANTS FROM MAINTENANCE

Form: W206 - Waste oil

Source: G11 - Discarding off-specification or out-of-date chemicals or products (unused chemicals or products - corresponds to P and U hazardous waste codes)

Origin: 1 - Generated on-site from a product process or service activity

Unused Commercial Product:

Yes No Spill Residue:

Yes

No Loosepack:

No Lab Pack:

No

Generator has provided the following: Analysis Formulary SDS Sample

Layers: Physical State

Multi-layered

Bi-Layered

Solid %:

Sludge %:

Free Liquid %:

100Single Layered

Odor:

None

Mild

Strong Description:

pH: N/A ≤2.0 >2.01-4.00

4.01 - 10.00 10.01-12.49 ≥12.5 Actual:

Liquid Flash Point:

<73˚ F 73<100˚ F 100<140˚ F 140-200˚ F >200˚F

None Actual: ˚C

˚F

BTU/lbs range: <2000 2000-5000

>5001-10,000 >10,000 Boiling Point:

≤95˚ F

>95˚ F Halogens %: <3%

Constituent Key Min Max UOM

PCB Yes No VOC (ppm) No selection TOC <1%

PCB TSCA Regulated Yes No Subject to Subpart CC: Yes No

WASTE PROFILE FORM

NCS-101Profile #: 6Revision #:

Water %: 0 Pumpable:

No Color: amber

Debris Monolith Powder

Compressed Gas

Specific Gravity

(water=1, oil<1, sol >1)

Est. Actual

N/A 0.8-1.0

Viscosity

(Low-water,Med-oil, High-

Honey)

Low (Water)

CHECK ALL THAT MAY APPLY:

Asbestos, Non-friable

Dioxins

Infectious

Oxidizer

Ammonia

APHIS Waste

Dust Hazard

Medical (sharps,needles)

Pesticide/Herbicide

Asbestos, Friable

CERCLA

Flammable Solid

Organic Peroxide

PFAS/PFOA

phenolics Profile Subpart P

PUSO

Radioactive

RCRA Debris

REACTIVITY:

Cyanide Reactive Explosive

Polymerizes

Pyrophoric

Reactive (Other)/Temp Sensitive

Reactive Metals Shock Sensitive

Sulfide Reactive

Water Reactive

Others

DocuSign Envelope ID: 9F51231B-1850-494F-AB33-62E67B6160AC mailto:mdlong3@ncsu.edu

METALS: TCLP Limit Range UOM TCLP Limit Range UOM

(mg/l) (mg/l)

A b o v e

B e lo w

N o t P re s e n t

D004 Arsenic (As) 5.0

D005 Barium (Ba) 100.0

D006 Cadmium (Cd) 1.0

D007 Chromium (Cr) 5.0

D008 Lead (Pb) 5.0

D009 Mercury (Hg) 0.2

D010 Selenium (Se) 1.0

D011 Silver (Ag) 5.0

N/A None

N/A

N/A

N/A

N/A

N/A

N/A

None

None

None

None

None

None

N/A None

D023 o-Cresol 200.0

D024 m-Cresol 200.0

D025 p-Cresol 200.0

D026 Cresol (Total) 200.0

D027 1,4-Dichlorobenzene 7.5

D030 2,4-Dinitrotoluene 0.1

D032 Hexachlorobenzene 0.1

H: SHIPPING INFORMATION:

A b o v e

B e lo w

N o t

P re s e n t

Antimony (Sb)

Beryllium (Be)

Hexavalent Chrome (Cr+6)

Cobalt (Co)

Copper (Cu)

Nickel (Ni)

Thallium (TI)

Vanadium (V)

Zinc (Zn)

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

None

None

None

None

None

None

None

None

N/A None

TCLP Limit (mg/l)

A b o v e

B e lo w

N o t

P re s e n t

Range UOM

D029 1,1-Dichloroethylene 0.7

D035 Methyl ethyl ketone 200.0

D039 Tetrachloroethylene 0.7

D040 Trichloroethylene 0.5

D043 Vinyl Chloride 0.2

N/A

N/A

N/A

N/A

None

None

None

None

N/A None

VOLATILES: TCLP Limit (mg/l)

A b o v e

B e lo w

N o t

P re s e n t

Range UOM

D018 Benzene 0.5

D019 Carbon Tetrachloride 0.5

D021 Chlorobenzene 100.0

D022 Chloroform 6.0

D028 1,2-Dichloroethane 0.5

N/A

N/A

None

None

None

None

N/A None

TCLP Limit (mg/l)

A b o v e

B e lo w

N o t P re s e n

N/A

N/A

N/A None

N/A None

PESTICIDE/HERBICIDES: TCLP Limit (mg/l)

A b o v e

B e lo w

N o t

P re s e n t

D012 Endrin 0.0

N/A None D016 2,4-D 10.0

N/A None D017 2,4,5-TP (Silvex) 1.0

N/A None D020 Chlordane 0.0

N/A None D031 Hepachlor (& it's epoxides)

0.0

Range UOM TCLP Limit (mg/l)

D013 Lindane 0.4

D014 Methoxychlor 10.0

D015 Toxaphene 0.5

A b o v e

B e lo w

N o t

P re s e n t

Range UOM

D033 Hexachlorobutadiene 0.5

D034 Hexachloroethane 3.0

D036 Nitrobenzene 2.0

D037 Pentachlorophenol 100.0

D038 Pyridine 5.0

D041 2,4,5-Trichlorophenol 400.0

D042 2,4,6-Trichlorophenol 2.0

N/A

N/A

N/A

N/A

None

None

None

None

None

N/A None

SEMI-VOLATILES: TCLP Limit (mg/l)

A b o v e

B e lo w

N o t

P re s e n t

N/A None

N/A

N/A

N/A

N/A

N/A

None

None

None

None

None

N/A None

G: REGULATED CONSTITUENTS: Check any regulated constituent above regulatory limit and note value. Check source(s) used :

Source(s):

Analytical

Generator Knowledge

SDS

F: USEPA / STATE / GENERATOR STATE WASTE

IDENTIFICATION:

Federal Universal Waste: Yes No EPA Exemption ref

EPA Waste Code(s): NONE

State Code(s): PA509

State Regulated Waste: Yes No Generator State Universal Waste: WA Designation: Yes No yesLANDFILL INFORMATION

This waste is a Waste water (TOC<1%, TSS<1%) Non-waste water

IDENTIFY ALL UHC's IN THIS WASTESTREAM :

Waste Subject to Land Disposal Restrictions (LDR)? No

DocuSign Envelope ID: 9F51231B-1850-494F-AB33-62E67B6160AC

Process Code(s):

Disposal Instructions/Comments:

GENERATOR CERTIFICATION

To the best of my knowledge and belief, I hereby warrant and represent that the information contained and submitted in the waste profile and all attached documents is true, accurate, and complete and that no material fact has been omitted as to make this misleading. I understand that others may rely on this inform ation in the handling and processing of the waste material described herein. By signing this waste profile, I am certifying that I am authorized to sign such documentation on behalf of the generator.

Authorized Signature

James R Atkinson Haz-Waste Specialist

Authorized Printed Name Title Date

US DOT DESCRIPTION: USE THE FULL BASIC DESCRIPTION ON THE HAZARDOUS WASTE MANIFEST including Technical constituents:

Non-RCRA, Non-DOT Regulated Material, (PETROLEUM OIL), Shipping Frequency Average Shipment Quantity

Monthly

Method of Shipment: Bulk Liquid Bulk Solid Container (type/size): 55

2/19/2024

Constituent Key Min Max UOM

Petroleum Distillates/Minieral Spirits

Range 0 100 % water Range 0 10 %

Acetone Range 0 10 %

Metals Range 0 10 %

Trichloroethylene Range 0 1 %

Acetonitrile Range 0 10 %

Alphatic Hydrocarbons Range 10 20 %

Aromatic Hydrocarbons Range 10 20 %

Benzene Range 0 0.1 %

Ethanol Range 0 10 %

E: ADDITIONAL INFORMATION:

A: GENERATOR INFORMATION North Carolina State University GEN #: NCD000830737

Yes No

EPA ID#:Name:

Site Address: 2620 Wolf Village Way City: Raleigh State : NC Zip : 27695

City: Raleigh State : NC Zip : 27695Campus Box 8007Mailing Address:

Email: mdlong3@ncsu.edu Phone: (919) 515-6863 Fax: (919) 515-6307Contact: Mike Long

Manifest ER Phone #: (877) 577-2669 Generator Subpart P: State ID#:

Generator Status: LQG SQG VSQG/CESQG

Disposal Restrictions:

NAICS code(s)(primary reporting first):

TSDF Approval List: Yes No

Yes NoVarious Generator:

CUSTOMER/BILLING/BROKER INFORMATION Same as Generating Facility address:

Customer #:

Phone:

State: NCCity: RALEIGH

Customer Name: North Carolina State University

Address: CAMPUS BOX 8007

Contact:

Zip: 27695-0001

Fax:Email: mdlong3@ncsu.edu

B: WASTE DESCRIPTION Waste Common Name: 102 - NON HALOGENATED SOLVENTS

Process generating Waste (be specific): CONSOLIDATED SPENT SOLVENTS

Form: W203 - Concentrated non-halogenated (e.g., non-chlorinated) solvent

Source: G22 - Laboratory analytical wastes (used chemicals from laboratory operations)

Origin: 1 - Generated on-site from a product process or service activity

Solid %:

Sludge %:

Free Liquid %:

Strong Description: aromatic pH: N/A ≤2.0 >2.01-4.00 4.01 - 10.00 10.01-12.49

<73˚ F 73<100˚ F 100<140˚ F 140-200˚ F >200˚F

≥12.5 Actual:

BTU/lbs range: <2000 2000-5000 >5001-10,000

>10,000 Boiling Point: ≤95˚ F >95˚ F Halogens %: <3%

Methyl Ethyl Ketone Range 0 10 %

Methylene Chloride Range 0 1 %

Oils Range 0 10 %

Organic Solvents Range 0 5 %

Tetrachloroethylene Range 0 1 %

Toluene Range 0 10 %

Chloroform Range 0 1 %

Ethyl Acetate Range 0 0.1 %

Xylene Range 0 10 %

PCB Yes No VOC (ppm) VOCs >= 500 ppm TOC >10%

PCB TSCA Regulated Yes

No Subject to Subpart CC:

Yes No

WASTE PROFILE FORM

NCS-102Profile #: 6Revision #:

Yes No Color: amber

Specific Gravity

(water=1, oil<1, sol >1)

Est. Actual

N/A 0.8-1.0

Viscosity

(Low-water,Med-oil, High-

Honey)

Low (Water)

DocuSign Envelope ID: 9F51231B-1850-494F-AB33-62E67B6160AC

A b o v e

B e lo w

N o t P re s e n t

D004 Arsenic (As) 5.0

D005 Barium (Ba) 100.0

D006 Cadmium (Cd) 1.0

D007 Chromium (Cr) 5.0

D008 Lead (Pb) 5.0

D009 Mercury (Hg) 0.2

N/A

N/A

N/A

N/A

N/A

None

None

None

None

None

None

N/A None

A b o v e

B e lo w

N o t

P re s e n

Cobalt (Co)

Copper (Cu)

Nickel (Ni)

Thallium (TI)

Vanadium (V)

Zinc (Zn)

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

None

None

None

None

None

None

None

None

N/A None

TCLP Limit (mg/l)

A b o v e

B e lo w

N o t

P re s e n t

D040 Trichloroethylene 0.5

D043 Vinyl Chloride 0.2

N/A None

0-10

0-1

0-1

TCLP(MG/L)

TCLP(MG/L)

TCLP(MG/L)

N/A None

VOLATILES: TCLP Limit (mg/l)

A b o v e

B e lo w

N o t

P re s e n t

Range UOM

D018 Benzene 0.5

D019 Carbon Tetrachloride 0.5

D021 Chlorobenzene 100.0

0-1

N/A

N/A

TCLP(MG/L)

None

None

None

N/A None

TCLP Limit (mg/l)

A b o v e

B e lo w

N o t P re s e n

N/A

N/A

N/A None

N/A None

PESTICIDE/HERBICIDES: TCLP Limit (mg/l)

A b o v e

B e lo w

N o t

P re s e n t

N/A None D020 Chlordane 0.0

N/A None D031 Hepachlor (& it's epoxides)

0.0

Range UOM TCLP Limit (mg/l)

D013 Lindane 0.4

D014 Methoxychlor 10.0

D015 Toxaphene 0.5

A b o v e

B e lo w

N o t

P re s e n t

Range UOMSEMI-VOLATILES: TCLP Limit (mg/l)

A b o v e

B e lo w

N o t

P re s e n t

D023 o-Cresol 200.0 N/A None D033 Hexachlorobutadiene 0.5

D024 m-Cresol 200.0 N/A None D034 Hexachloroethane 3.0

G: REGULATED CONSTITUENTS: Check any regulated constituent above regulatory limit and note value. Check source(s) used :

Source(s):

Analytical

Generator Knowledge

SDS

F: USEPA / STATE / GENERATOR STATE WASTE

IDENTIFICATION:

Federal Universal Waste: Yes No EPA Exemption ref

EPA Waste Code(s): D001,D004,D005,D006,D007,D008,D010,D011,D018,D022,D035,D036,D038,D040,F001,F002,F003,F005,U002,U003,U009,U012,U019,U031,U037,U044,U056,U0 57,U108,U112,U113,U117,U140,U154,U159,U162,U169,U213,U214,U220,U239

State Code(s):

State Regulated Waste: Yes No

LANDFILL INFORMATION

Generator State Universal Waste: Yes No WA Designation:

This waste is a Waste water (TOC<1%, TSS<1%) Non-waste water

IDENTIFY ALL UHC's IN THIS WASTESTREAM :

Waste Subject to Land Disposal Restrictions (LDR)?

yes

CHECK ALL THAT MAY APPLY:

Ammonia

Asbestos, Friable

Asbestos, Non-friable APHIS Waste CERCLA

Dioxins Dust Hazard Flammable Solid

Infectious Medical (sharps,needles) Organic Peroxide

Oxidizer phenolics

Radioactive

Pesticide/Herbicide PFAS/PFOA

PUSOProfile Subpart P

Cyanide Reactive

Explosive

Reactive (Other)/Temp Sensitive

Reactive Metals

Shock Sensitive

H: SHIPPING INFORMATION:

US DOT DESCRIPTION: USE THE FULL BASIC DESCRIPTION ON THE HAZARDOUS WASTE MANIFEST including Technical constituents:

Disposal Instructions/Comments:

GENERATOR CERTIFICATION

To the best of my knowledge and belief, I hereby warrant and represent that the information contained and submitted in the waste profile and all attached documents is true, accurate, and complete and that no material fact has been omitted as to make this misleading. I understand that others may rely on this inform ation in the handling and processing of the waste material described herein. By signing this waste profile, I am certifying that I am authorized to sign such documentation on behalf of the generator.

Authorized Signature

James R Atkinson Haz-Waste Specialist

Authorized Printed Name Title Date

D036 Nitrobenzene 2.0

D037 Pentachlorophenol 100.0

D038 Pyridine 5.0

N/A

N/A

None

None

None

D025 p-Cresol 200.0

D026 Cresol (Total) 200.0

D027 1,4-Dichlorobenzene 7.5

D030 2,4-Dinitrotoluene 0.1

D032 Hexachlorobenzene 0.1

N/A None

N/A

N/A

N/A

None

None

None

N/A None

UN1992, Waste Flammable liquids, toxic, n.o.s., (METHANOL, TOLUENE), 3 (6.1), II, RQ(D001=100#), ERG(131)

Shipping Frequency Average Shipment Quantity

Monthly

Method of Shipment: Bulk Liquid Bulk Solid Container (type/size): 55

C: PHYSICAL CHARACTERISTICS OF MATERIAL (@70°F)

D: CHEMICAL COMPOSITION OF MATERIAL

Constituent Key Min Max UOM

ALIPHATIC HYDROCARBONS

MIXTURE

Range 10 20 %

AROMATIC HYDROCARBONS Range 10 20 %

CHLOROFORM Range 0 1 %

ETHANOL Range 0 15 %

ETHYL ACETATE Range 0 10 %

GLYCOL Range 0 10 %

METHANOL Range 0 15 %

METHYL ETHYL KETONE Range 0 10 %

METHYLENE CHLORIDE Range 0 1 %

PETROLEUM DISTILLATES Range 0 10 %

TOLUENE Range 0 10 %

WATER Range 0 15 %

E: ADDITIONAL INFORMATION:

A: GENERATOR INFORMATION North Carolina State University GEN #: NCD000830737

Yes No

EPA ID#:Name:

Site Address: 2620 Wolf Village Way City: Raleigh State : NC Zip : 27695

City: Raleigh State : NC Zip : 27695Campus Box 8007Mailing Address:

Email: katrimbe@ncsu.edu Phone: (919) 515-6859 Fax: (919) 515-6307Contact: Karen Trimberger

Manifest ER Phone #: 8775772669 Generator Subpart P: State ID#:

Generator Status: LQG SQG VSQG/CESQ

G NAICS code(s)(primary reporting first): 611310

TSDF Approval List: Yes No Treatment/Disposal Restrictions:

Yes NoVarious Generator:

CUSTOMER/BILLING/BROKER INFORMATION Same as Generating Facility address:

Customer #:

Phone:

State: NCCity: RALEIGH

Customer Name: North Carolina State University

Address: CAMPUS BOX 8007

Contact:

Zip: 27695-0001

Fax:Email: mdlong3@ncsu.edu

B: MATERIAL DESCRIPTION

Generating Process (be specific):

Common Name: 103 - NON HALOGENATED SOLVENTS FLAM/TOXIC

CONSOLIDATED WASTE FROM ANALYTICAL PROCESSES

Form: W203 - Concentrated non-halogenated (e.g., non-chlorinated) solvent

Source: G22 - Laboratory analytical wastes (used chemicals from laboratory operations)

Origin: 1 - Generated on-site from a product process or service activity

Multi-layered Solid %: 0

Bi-Layered Sludge %:

Single Layered Free Liquid %:

<73˚ F 73<100˚ F 100<140˚ F 140-200˚ F >200˚F None Actual: ˚C

BTU/lbs range: <2000

2000-5000

>5001-10,000

>10,000 Boiling Point:

2,4-D Range 0 0.1 %

ACETONITRILE Range 0 10 %

1,4-DICHLOROBENZENE Range 0 10 %

ACETONE Range 0 10 %

BENZENE Range 0 0.1 %

CUMENE Range 0 1 %

CYCLOHEXANE Range 0 5 %

N-BUTYL ALCOHOL Range 0 10 %

OIL Range 0 10 %

TRICHLOROETHYLENE Range 0 1 %

XYLENE Range 0 10 %

PCB Yes

No VOC (ppm) VOCs >= 500 ppm TOC >10%

PROFILE FORM

NCS-103Profile #: 7Revision #:

Specific Gravity

(water=1, oil<1, sol >1)

Est. Actual

≥0.8, <1

Viscosity

(Low-water,Med-oil, High-

Honey)

Low (Water)

Docusign Envelope ID: C4F37E89-FE31-40EB-934D-D04A299BBA86 mailto:katrimbe@ncsu.edu

A b o v e

B e lo w

N o t P re s e n t

D004 Arsenic (As) 5.0

D005 Barium (Ba) 100.0

D006 Cadmium (Cd) 1.0

D007 Chromium (Cr) 5.0

D008 Lead (Pb) 5.0

D009 Mercury (Hg) 0.2

>5

>100

>1

>5

>5

N/A

>1

TCLP(MG/L)

TCLP(MG/L)

TCLP(MG/L)

TCLP(MG/L)

TCLP(MG/L)

None

TCLP(MG/L)

>5 TCLP(MG/L)

A b o v e

B e lo w

N o t

P re s e n

Cobalt (Co)

Copper (Cu)

Nickel (Ni)

Thallium (TI)

Vanadium (V)

Zinc (Zn)

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

None

None

None

None

None

None

None

None

N/A None

TCLP Limit (mg/l)

A b o v e

B e lo w

N o t

P re s e n t

D040 Trichloroethylene 0.5

D043 Vinyl Chloride 0.2

>0.7

>200

>0.7

>0.5

TCLP(MG/L)

TCLP(MG/L)

TCLP(MG/L)

TCLP(MG/L)

N/A None

VOLATILES: TCLP Limit (mg/l)

A b o v e

B e lo w

N o t

P re s e n t

Range UOM

D018 Benzene 0.5

D019 Carbon Tetrachloride 0.5

D021 Chlorobenzene 100.0

>0.5

>100

>6

TCLP(MG/L)

TCLP(MG/L)

TCLP(MG/L)

TCLP(MG/L)

>0.5 TCLP(MG/L)

TCLP Limit (mg/l)

A b o v e

B e lo w

N o t P re s e n

TCLP(MG/L)

>10

N/A

N/A None

N/A None

PESTICIDE/HERBICIDES: TCLP Limit (mg/l)

A b o v e

B e lo w

N o t

P re s e n t

N/A None D020 Chlordane 0.0

N/A None D031 Hepachlor (& it's epoxides)

0.0

Range UOM TCLP Limit (mg/l)

D013 Lindane 0.4

D014 Methoxychlor 10.0

D015 Toxaphene 0.5

A b o v e

B e lo w

N o t

P re s e n t

Range UOM

D033 Hexachlorobutadiene 0.5 N/A None

SEMI-VOLATILES: TCLP Limit (mg/l)

A b o v e

B e lo w

N o t

P re s e n t

D023 o-Cresol 200.0 N/A None

G: REGULATED CONSTITUENTS: Check any regulated constituent above regulatory limit and note value. Check source(s) used :

Source(s):

Analytical

Generator Knowledge

SDS

F: USEPA / STATE / GENERATOR STATE WASTE

IDENTIFICATION:

Federal Universal Waste: Yes No EPA Exemption ref

EPA Waste Code(s): D001,D004,D005,D006,D007,D008,D010,D011,D016,D018,D019,D021,D022,D027,D028,D029,D035,D036,D038,D039,D040,F001,F002,F003,F005,U002,U003,U0 19,U031,U044,U055,U057,U108,U112,U117,U140,U154,U213,U220,U239

State Code(s):

State Regulated Waste: Yes No Generator State Universal Waste: Yes No WA Designation:

LANDFILL INFORMATION

This waste is a Waste water (TOC<1%, TSS<1%) Non-waste water

IDENTIFY ALL UHC's IN THIS WASTESTREAM :

CHECK ALL THAT MAY APPLY:

Asbestos, Non-friable

Ammonia

APHIS Waste

Asbestos, Friable

CERCLA

Dioxins Dust Hazard Flammable Solid

Infectious Medical (sharps,needles) Organic Peroxide

Oxidizer Pesticide/Herbicide PFAS/PFOA

Docusign Envelope ID: C4F37E89-FE31-40EB-934D-D04A299BBA86

D026 Cresol (Total) 200.0

D027 1,4-Dichlorobenzene 7.5

D030 2,4-Dinitrotoluene 0.1

D032 Hexachlorobenzene 0.1

H: SHIPPING INFORMATION:

Process Code(s):

Management Instructions/Comments:

GENERATOR CERTIFICATION

To the best of my knowledge and belief, I hereby warrant and represent that the information contained and submitted in the profile and all attached documents is true, accurate, and complete and that no material fact has been omitted as to make this misleading. I understand that others may rely on this inform ation in the handling and processing of the material described herein. By signing this profile, I am certifying that I am authorized to sign such documentation on behalf of the generator.

Kyle Wilson Haz. Materials Specialist2/3/2025

Authorized Signature Authorized Printed Name Title Date

D034 Hexachloroethane 3.0

D036 Nitrobenzene 2.0

D037 Pentachlorophenol 100.0

D038 Pyridine 5.0

>2

N/A

>5

N/A

TCLP(MG/L)

None

TCLP(MG/L)

None

N/A None

N/A None

N/A

N/A

>7.5

N/A

None

None

TCLP(MG/L)

None

N/A None

US DOT DESCRIPTION: USE THE FULL BASIC DESCRIPTION ON THE BILL OF LADING OR HAZARDOUS WASTE MANIFEST INCLUDING TECHNICAL CONSTITUENTS.

UN1992, Waste Flammable liquids, toxic, n.o.s., (METHYLENE CHLORIDE, CHLOROFORM), 3 (6.1), II, RQ(D001=100#,D018=10#), ERG(131)

Shipping Frequency Average Shipment Quantity

Monthly

Method of Shipment: Bulk Liquid Bulk Solid Container (type/size): 55

Docusign Envelope ID: C4F37E89-FE31-40EB-934D-D04A299BBA86

Constituent Key Min Max UOM

Acetone Range 0 5 % organic solvents Range 0 5 % aromatic hydrocarbons Range 0 5 % chlorobenzene Range 1 20 % chloroform Range 1 20 % carbon tetrachloride Range 0 5 % ethyl acetate Range 0 5 % 1,1,2,2 tetrachloroethane Range 0 5 % methanol Range 0 5 % methyl ethyl ketone Range 0 5 % methylene chloride Range 1 20 % water Range 10 30 % toluene Range 0 5 % tetrachloroethylene Range 0 5 % ethyl ether Range 0 5 % Acetonitrile Range 0 5 % xylene Range 0 5 % tetrachloromethane Range 0 5 % aliphatic hydrocarbons mixture Range 0 5 % trichloroethane Range 1 20 % ethanol Range 0 5 %

E: ADDITIONAL INFORMATION:

A: GENERATOR INFORMATION North Carolina State University GEN #: NCD000830737

Yes No

EPA ID#:Name:

Site Address: 2620 Wolf Village Way City: Raleigh State : NC Zip : 27695

City: Raleigh State : NC Zip : 27695Campus Box 8007Mailing Address:

Email: mdlong3@ncsu.edu Phone: (919) 515-6863 Fax: (919) 515-6307Contact: Mike Long

Manifest ER Phone #: (877) 577-2669 Generator Subpart P: State ID#:

Generator Status: LQG SQG VSQG/CESQG

Disposal Restrictions:

NAICS code(s)(primary reporting first):

TSDF Approval List: Yes No

Yes NoVarious Generator:

CUSTOMER/BILLING/BROKER INFORMATION Same as Generating Facility address:

Customer #:

Phone:

State: NCCity: RALEIGH

Customer Name: North Carolina State University

Address: CAMPUS BOX 8007

Contact:

Zip: 27695-0001

Fax:Email: mdlong3@ncsu.edu

B: WASTE DESCRIPTION Waste Common Name: 104 - HALOGENATED/NON-HALOGENATED SOLVENTS

Process generating Waste (be specific): CONSOLIDATED WASTE FROM ANALYTICAL PROCESSES

Form: W204 - Concentrated halogenated/ non-halogenated solvent mixture

Source: G22 - Laboratory analytical wastes (used chemicals from laboratory operations)

Origin: 1 - Generated on-site from a product process or service activity

Solid %:

Sludge %:

Free Liquid %:

<73˚ F 73<100˚ F 100<140˚ F 140-200˚ F >200˚F

>10,000 Boiling Point: ≤95˚ F >95˚ F Halogens %: >20%

WASTE PROFILE FORM

NCS-104Profile #: 7Revision #:

Specific Gravity

(water=1, oil<1, sol >1)

Est. Actual

≥0.8, <1

Viscosity

(Low-water,Med-oil, High-

Honey)

Low (Water)

DocuSign Envelope ID: 88A77393-B708-4BB8-A1E3-AD5CE1FFBFF5

A b o v e

B e lo w

N o t P re s e n t

D004 Arsenic (As) 5.0

D005 Barium (Ba) 100.0

D006 Cadmium (Cd) 1.0

D007 Chromium (Cr) 5.0

D008 Lead (Pb) 5.0

D009 Mercury (Hg) 0.2

>5

>100

>1

>5

>5

N/A

>1

TCLP(MG/L)

TCLP(MG/L)

TCLP(MG/L)

TCLP(MG/L)

TCLP(MG/L)

None

TCLP(MG/L)

>5 TCLP(MG/L)

A b o v e

B e lo w

N o t

P re s e n

Cobalt (Co)

Copper (Cu)

Nickel (Ni)

Thallium (TI)

Vanadium (V)

Zinc (Zn)

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

None

None

None

None

None

None

None

None

N/A None

TCLP Limit (mg/l)

A b o v e

B e lo w

N o t

P re s e n t

D040 Trichloroethylene 0.5

D043 Vinyl Chloride 0.2

>0.7

N/A

>0.7

>0.5

TCLP(MG/L)

None

TCLP(MG/L)

TCLP(MG/L)

N/A None

VOLATILES: TCLP Limit (mg/l)

A b o v e

B e lo w

N o t

P re s e n t

Range UOM

D018 Benzene 0.5

D019 Carbon Tetrachloride 0.5

D021 Chlorobenzene 100.0

>100

>6

TCLP(MG/L)

TCLP(MG/L)

TCLP(MG/L)

TCLP(MG/L)

>0.5 TCLP(MG/L)

TCLP Limit (mg/l)

A b o v e

B e lo w

N o t P re s e n

N/A

N/A

N/A None

N/A None

PESTICIDE/HERBICIDES: TCLP Limit (mg/l)

A b o v e

B e lo w

N o t

P re s e n t

N/A None D020 Chlordane 0.0

N/A None D031 Hepachlor (& it's epoxides)

0.0

Range UOM TCLP Limit (mg/l)

D013 Lindane 0.4

D014 Methoxychlor 10.0

D015 Toxaphene 0.5

A b o v e

B e lo w

N o t

P re s e n t

Range UOMSEMI-VOLATILES: TCLP Limit (mg/l)

A b o v e

B e lo w

N o t

P re s e n t

G: REGULATED CONSTITUENTS: Check any regulated constituent above regulatory limit and note value. Check source(s) used :

Source(s):

Analytical

Generator Knowledge

SDS

F: USEPA / STATE / GENERATOR STATE WASTE

IDENTIFICATION:

Federal Universal Waste: Yes No EPA Exemption ref

EPA Waste Code(s): D001,D004,D005,D006,D007,D008,D010,D011,D018,D019,D021,D022,D027,D028,D029,D035,D036,D038,D039,D040,F001,F002,F003,F004,F005,U002,U003,U0 1,U037,U044,U045,U055,U056,U070,U076,U077,U080,U112,U117,U140,U144,U154,U210,U211

State Code(s):

State Regulated Waste: Yes No

LANDFILL INFORMATION

Generator State Universal Waste: Yes No WA Designation:

This waste is a Waste water (TOC<1%, TSS<1%) Non-waste water

IDENTIFY ALL UHC's IN THIS WASTESTREAM :

Infectious Medical (sharps,needles) Organic Peroxide

Oxidizer phenolics

Radioactive

Pesticide/Herbicide PFAS/PFOA

PUSOProfile Subpart P

Reactive (Other)/Temp Sensitive

DocuSign Envelope ID: 88A77393-B708-4BB8-A1E3-AD5CE1FFBFF5

US DOT DESCRIPTION: USE THE FULL BASIC DESCRIPTION ON THE HAZARDOUS WASTE MANIFEST including Technical constituents:

Disposal Instructions/Comments:

GENERATOR CERTIFICATION

To the best of my knowledge and belief, I hereby warrant and represent that the information contained and submitted in the waste profile and all attached documents is true, accurate, and complete and that no material fact has been omitted as to make this misleading. I understand that others may rely on this inform ation in the handling and processing of the waste material described herein. By signing this waste profile, I am certifying that I am authorized to sign such documentation on behalf of the generator.

Authorized Signature

James R Atkinson Haz-Waste Specialist

Authorized Printed Name Title Date

D036 Nitrobenzene 2.0

D037 Pentachlorophenol 100.0

D038 Pyridine 5.0

>5

N/A

None

TCLP(MG/L)

None

D030 2,4-Dinitrotoluene 0.1

D032 Hexachlorobenzene 0.1

N/A None

N/A

>7.5

N/A

None

TCLP(MG/L)

None

N/A None

UN1992, Waste Flammable liquids, toxic, n.o.s., (ACETONE, XYLENE), 3 (6.1), II, RQ(D001=100#), ERG(131)

Shipping Frequency Average Shipment Quantity

Monthly

Method of Shipment: Bulk Liquid Bulk Solid Container (type/size): 55

DocuSign Envelope ID: 88A77393-B708-4BB8-A1E3-AD5CE1FFBFF5

2/21/2024

Constituent Key Min Max UOM aromatic hydrocarbons Range 0 25 % aliphatice hydrocarbons Range 1 25 % barium Range 0 0.1 % Paint Range 5 50 % benzene Range 0 0.5 % silver Range 0 0.1 % cadmium Range 0 0.1 % lead Range 0 0.1 % chromium Range 0 0.1 % toluene Range 0 2 % xylene Range 0 2 % water Range 0 10 % arsenic Range 0 0.1 % methyl ethyl ketone Range 0 0.1 % petroleum based thinner Range 5 25 %

E: ADDITIONAL INFORMATION:

A: GENERATOR INFORMATION North Carolina State University GEN #: NCD000830737

Yes No

EPA ID#:Name:

Site Address: 2620 Wolf Village Way City: Raleigh State : NC Zip : 27695

City: Raleigh State : NC Zip : 27695Campus Box 8007Mailing Address:

Email: mdlong3@ncsu.edu Phone: (919) 515-6863 Fax: (919) 515-6307Contact: Mike Long

Manifest ER Phone #: (877) 577-2669 Generator Subpart P: State ID#:

Generator Status: LQG SQG VSQG/CESQG

Disposal Restrictions:

NAICS code(s)(primary reporting first):

TSDF Approval List: Yes No

Yes NoVarious Generator:

CUSTOMER/BILLING/BROKER INFORMATION Same as Generating Facility address:

Customer #:

Phone:

State: NCCity: RALEIGH

Customer Name: North Carolina State University

Address: CAMPUS BOX 8007

Contact:

Zip: 27695-0001

Fax:Email: mdlong3@ncsu.edu

B: WASTE DESCRIPTION Waste Common Name: 105 - PAINT RELATED MATERIAL

Process generating Waste (be specific): CONSOLIDATION OF PAINT MATERIAL

Form: W209 - Paint, ink, lacquer, or varnish (fluid - not dried out or sludge)

Source: G11 - Discarding off-specification or out-of-date chemicals or products (unused chemicals or products - corresponds to P and U hazardous waste codes)

Origin: 1 - Generated on-site from a product process or service activity

Solid %:

Sludge %:

Free Liquid %:

Strong Description: thinner

<73˚ F 73<100˚ F 100<140˚ F 140-200˚ F >200˚F

>10,000 Boiling Point: ≤95˚ F >95˚ F Halogens %:

WASTE PROFILE FORM

NCS-105Profile #: 4Revision #:

Yes No Color: various

Specific Gravity

(water=1, oil<1, sol >1)

Est. Actual

≥1, <1.2

Viscosity

(Low-water,Med-oil, High-

Honey)

Medium (Oil)

DocuSign Envelope ID: 5444C5B2-2C4E-4E23-803A-4E3D7FD6AB7E

A b o v e

B e lo w

N o t P re s e n t

D004 Arsenic (As) 5.0

D005 Barium (Ba) 100.0

D006 Cadmium (Cd) 1.0

D007 Chromium (Cr) 5.0

D008 Lead (Pb) 5.0

D009 Mercury (Hg) 0.2

>5.0

>100.0

>1.0

>5.0

>5.0

N/A

>1.0

TCLP(MG/L)

TCLP(MG/L)

TCLP(MG/L)

TCLP(MG/L)

TCLP(MG/L)

None

TCLP(MG/L)

>5.0 TCLP(MG/L)

A b o v e

B e lo w

N o t

P re s e n

Cobalt (Co)

Copper (Cu)

Nickel (Ni)

Thallium (TI)

Vanadium (V)

Zinc (Zn)

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

None

None

None

None

None

None

None

None

N/A None

TCLP Limit (mg/l)

A b o v e

B e lo w

N o t

P re s e n t

D040 Trichloroethylene 0.5

D043 Vinyl Chloride 0.2

N/A

>200

N/A

N/A

None

TCLP(MG/L)

None

None

N/A None

VOLATILES: TCLP Limit (mg/l)

A b o v e

B e lo w

N o t

P re s e n t

Range UOM

D018 Benzene 0.5

D019 Carbon Tetrachloride 0.5

D021 Chlorobenzene 100.0

N/A

N/A

TCLP(MG/L)

None

None

None

N/A None

TCLP Limit (mg/l)

A b o v e

B e lo w

N o t P re s e n

N/A

N/A

N/A None

N/A None

PESTICIDE/HERBICIDES: TCLP Limit (mg/l)

A b o v e

B e lo w

N o t

P re s e n t

N/A None D020 Chlordane 0.0

N/A None D031 Hepachlor (& it's epoxides)

0.0

Range UOM TCLP Limit (mg/l)

D013 Lindane 0.4

D014 Methoxychlor 10.0

D015 Toxaphene 0.5

A b o v e

B e lo w

N o t

P re s e n t

Range UOMSEMI-VOLATILES: TCLP Limit (mg/l)

A b o v e

B e lo w

N o t

P re s e n t

G: REGULATED CONSTITUENTS: Check any regulated constituent above regulatory limit and note value. Check source(s) used :

Source(s):

Analytical

Generator Knowledge

SDS

F: USEPA / STATE / GENERATOR STATE WASTE

IDENTIFICATION:

Federal Universal Waste: Yes No EPA Exemption ref

EPA Waste Code(s): D001,D004,D005,D006,D007,D008,D010,D011,D018,D035,F003,F005,U085

State Code(s):

State Regulated Waste: Yes No Generator State Universal Waste: Yes No WA Designation:

LANDFILL INFORMATION

This waste is a Waste water (TOC<1%, TSS<1%) Non-waste water

IDENTIFY ALL UHC's IN THIS WASTESTREAM :

Infectious Medical (sharps,needles) Organic Peroxide

Oxidizer phenolics

Radioactive

Pesticide/Herbicide PFAS/PFOA

PUSOProfile Subpart P

Reactive (Other)/Temp Sensitive

DocuSign Envelope ID: 5444C5B2-2C4E-4E23-803A-4E3D7FD6AB7E

US DOT DESCRIPTION: USE THE FULL BASIC DESCRIPTION ON THE HAZARDOUS WASTE MANIFEST including Technical constituents:

Disposal Instructions/Comments:

GENERATOR CERTIFICATION

To the best of my knowledge and belief, I hereby warrant and represent that the information contained and submitted in the waste profile and all attached documents is true, accurate, and complete and that no material fact has been omitted as to make this misleading. I understand that others may rely on this inform ation in the handling and processing of the waste material described herein. By signing this waste profile, I am certifying that I am authorized to sign such documentation on behalf of the generator.

Authorized Signature

James R. Atkinson Haz-Waste Specialist

Authorized Printed Name Title Date

D036 Nitrobenzene 2.0

D037 Pentachlorophenol 100.0

D038 Pyridine 5.0

N/A

N/A

None

None

None

D030 2,4-Dinitrotoluene 0.1

D032 Hexachlorobenzene 0.1

N/A None

N/A

N/A

N/A

None

None

None

N/A None

UN1263, Waste Paint, 3, II, RQ(D001), ERG(128)

Shipping Frequency Average Shipment Quantity

Monthly

Method of Shipment: Bulk Liquid Bulk Solid Container (type/size): 55

3/1/2024

Constituent Key Min Max UOM water Range 0 20 %

E: ADDITIONAL INFORMATION:

A: GENERATOR INFORMATION North Carolina State University GEN #: NCD000830737

Yes No

EPA ID#:Name:

Site Address: 2620 Wolf Village Way City: Raleigh State : NC Zip : 27695

City: Raleigh State : NC Zip : 27695Campus Box 8007Mailing Address:

Email: mdlong3@ncsu.edu Phone: (919) 515-6863 Fax: (919) 515-6307Contact: Mike Long

Manifest ER Phone #: (877) 577-2669 Generator Subpart P: State ID#:

Generator Status: LQG SQG VSQG/CESQG

Disposal Restrictions:

NAICS code(s)(primary reporting first):

TSDF Approval List: Yes No

Yes NoVarious Generator:

CUSTOMER/BILLING/BROKER INFORMATION Same as Generating Facility address:

Customer #:

Phone:

State: NCCity: RALEIGH

Customer Name: North Carolina State University

Address: CAMPUS BOX 8007

Contact:

Zip: 27695-0001

Fax:Email: mdlong3@ncsu.edu

B: WASTE DESCRIPTION Waste Common Name: 107 - LATEX PAINT

Process generating Waste (be specific): CONSOLIDATED MATERIAL

Form: W209 - Paint, ink, lacquer, or varnish (fluid - not dried out or sludge)

Source: G11 - Discarding off-specification or out-of-date chemicals or products (unused chemicals or products - corresponds to P and U hazardous waste codes)

Origin: 1 - Generated on-site from a product process or service activity

Solid %:

Sludge %:

Free Liquid %:

pH: N/A ≤2.0 >2.01-4.00 4.01 - 10.00 10.01-12.49 ≥12.5 Actual:

>95˚ F latex paint Range 80 100 %

PCB Yes No VOC (ppm) No selection TOC <1%

WASTE PROFILE FORM

NCS-107Profile #: 5Revision #:

Halogens %:

No Color: various

Specific Gravity

(water=1, oil<1, sol >1)

Est. Actual

≥1, <1.2

Viscosity

(Low-water,Med-oil, High-

Honey)

Medium (Oil)

CHECK ALL THAT MAY APPLY: Ammonia Asbestos, Friable

Asbestos, Non-friable APHIS Waste CERCLA

Dioxins Dust Hazard Flammable Solid

Infectious Medical (sharps,needles) Organic Peroxide

Others

DocuSign Envelope ID: 4464C895-D0F4-493A-BF9B-AD87468E7E5E

A b o v e

B e lo w

N o t P re s e n t

D004 Arsenic (As) 5.0

D005 Barium (Ba) 100.0

D006 Cadmium (Cd) 1.0

D007 Chromium (Cr) 5.0

D008 Lead (Pb) 5.0

D009 Mercury (Hg) 0.2

N/A

N/A

N/A

N/A

N/A

None

None

None

None

None

None

N/A None

D023 o-Cresol 200.0

D024 m-Cresol 200.0

D025 p-Cresol 200.0

D026 Cresol (Total) 200.0

D027 1,4-Dichlorobenzene 7.5

D030 2,4-Dinitrotoluene 0.1

D032 Hexachlorobenzene 0.1

H: SHIPPING INFORMATION:

A b o v e

B e lo w

N o t

P re s e n

Cobalt (Co)

Copper (Cu)

Nickel (Ni)

Thallium (TI)

Vanadium (V)

Zinc (Zn)

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

None

None

None

None

None

None

None

None

N/A None

TCLP Limit (mg/l)

A b o v e

B e lo w

N o t

P re s e n t

D040 Trichloroethylene 0.5

D043 Vinyl Chloride 0.2

N/A

N/A

N/A

N/A

None

None

None

None

N/A None

VOLATILES: TCLP Limit (mg/l)

A b o v e

B e lo w

N o t

P re s e n t

Range UOM

D018 Benzene 0.5

D019 Carbon Tetrachloride 0.5

D021 Chlorobenzene 100.0

N/A

N/A

None

None

None

None

N/A None

TCLP Limit (mg/l)

A b o v e

B e lo w

N o t P re s e n

N/A

N/A

N/A None

N/A None

PESTICIDE/HERBICIDES: TCLP Limit (mg/l)

A b o v e

B e lo w

N o t

P re s e n t

N/A None D020 Chlordane 0.0

N/A None D031 Hepachlor (& it's epoxides)

0.0

Range UOM TCLP Limit (mg/l)

D013 Lindane 0.4

D014 Methoxychlor 10.0

D015 Toxaphene 0.5

A b o v e

B e lo w

N o t

P re s e n t

Range UOM

D033 Hexachlorobutadiene 0.5

D034 Hexachloroethane 3.0

D036 Nitrobenzene 2.0

D037 Pentachlorophenol 100.0

D038 Pyridine 5.0

N/A

N/A

N/A

N/A

None

None

None

None

None

N/A None

SEMI-VOLATILES: TCLP Limit (mg/l)

A b o v e

B e lo w

N o t

P re s e n t

N/A None

N/A

N/A

N/A

N/A

N/A

None

None

None

None

None

N/A None

G: REGULATED CONSTITUENTS: Check any regulated constituent above regulatory limit and note value. Check source(s) used :

Source(s):

Analytical

Generator Knowledge

SDS

F: USEPA / STATE / GENERATOR STATE WASTE

IDENTIFICATION:

Federal Universal Waste: Yes No EPA Exemption ref

EPA Waste Code(s): NONE

State Code(s): PA206

State Regulated Waste: Yes No Generator State Universal Waste: WA Designation: Yes No yesLANDFILL INFORMATION

This waste is a Waste water (TOC<1%, TSS<1%) Non-waste water

IDENTIFY ALL UHC's IN THIS WASTESTREAM :

Waste Subject to Land Disposal Restrictions (LDR)? No

US DOT DESCRIPTION: USE THE FULL BASIC DESCRIPTION ON THE HAZARDOUS WASTE MANIFEST including Technical constituents:

Non-RCRA, Non-DOT Regulated Material, (Latex Paint

DocuSign Envelope ID: 4464C895-D0F4-493A-BF9B-AD87468E7E5E

GENERATOR CERTIFICATION

To the best of my knowledge and belief, I hereby warrant and represent that the information contained and submitted in the waste profile and all attached documents is true, accurate, and complete and that no material fact has been omitted as to make this misleading. I understand that others may rely on this inform ation in the handling and processing of the waste material described herein. By signing this waste profile, I am certifying that I am authorized to sign such documentation on behalf of the generator.

Authorized Signature

James R Atkinson Haz-Waste Specialist

Authorized Printed Name Title Date

Shipping Frequency Average Shipment Quantity

Monthly

Method of Shipment: Bulk Liquid Bulk Solid Container (type/size): 55

DocuSign Envelope ID: 4464C895-D0F4-493A-BF9B-AD87468E7E5E

2/21/2024

Constituent Key Min Max UOM arsenic Range 0 0.1 % lead Range 0 0.1 % nitric acid Range 0 5 % phosphoric acid Range 0 8 % selenium Range 0 0.1 % chromium Range 0 0.5 % silver Range 0 0.1 % sulfuric acid Range 0 8 % silver Range 0 0.1 % barium Range 0 0.1 % water Range 20 80 % hydrochloric acid Range 1 8 % cadmium Range 0 0.1 %

E: ADDITIONAL INFORMATION:

A: GENERATOR INFORMATION North Carolina State University GEN #: NCD000830737

Yes

No

EPA ID#:Name:

Site Address: 2620 Wolf Village Way City: Raleigh State : NC Zip : 27695

City: Raleigh State : NC Zip : 27695Campus Box 8007Mailing Address:

Email: mdlong3@ncsu.edu Phone: (919) 515-6863 Fax: (919) 515-6307Contact: Mike Long

Manifest ER Phone #: (877) 577-2669 Generator Subpart P: State ID#:

Generator Status: LQG SQG VSQG/CESQG

Disposal Restrictions:

NAICS code(s)(primary reporting first):

TSDF Approval List: Yes No

Yes NoVarious Generator:

CUSTOMER/BILLING/BROKER INFORMATION Same as Generating Facility address:

Customer #:

Phone:

State: NCCity: RALEIGH

Customer Name: North Carolina State University

Address: CAMPUS BOX 8007

Contact:

Zip: 27695-0001

Fax:Email: mdlong3@ncsu.edu

B: WASTE DESCRIPTION Waste Common Name: 108 - MIXED INORGANIC ACIDS

Process generating Waste (be specific): CONSOLIDATED ACIDS FROM RESEARCH

Form: W103 - Spent concentrated acid (5% or more)

Source: G22 - Laboratory analytical wastes (used chemicals from laboratory operations)

Origin: 1 - Generated on-site from a product process or service activity

Solid %:

Sludge %:

Free Liquid %:

PCB Yes No VOC (ppm)

Subject to Subpart CC:

No selection TOC <1%

WASTE PROFILE FORM

NCS-108Profile #: 6Revision #:

Water %: 20 Pumpable:

No Color: clear

Specific Gravity

(water=1, oil<1, sol >1)

Est. Actual

N/A 0.8-1.0

Viscosity

(Low-water,Med-oil, High-

Honey)

Low (Water)

DocuSign Envelope ID: 9F51231B-1850-494F-AB33-62E67B6160AC

A b o v e

B e lo w

N o t P re s e n t

D004 Arsenic (As) 5.0

D005 Barium (Ba) 100.0

D006 Cadmium (Cd) 1.0

D007 Chromium (Cr) 5.0

D008 Lead (Pb) 5.0

D009 Mercury (Hg) 0.2

N/A TCLP(MG/L)

N/A

N/A

N/A

N/A

N/A

TCLP(MG/L)

TCLP(MG/L)

TCLP(MG/L)

TCLP(MG/L)

None

TCLP(MG/L)

N/A TCLP(MG/L)

A b o v e

B e lo w

N o t

P re s e n

Cobalt (Co)

Copper (Cu)

Nickel (Ni)

Thallium (TI)

Vanadium (V)

Zinc (Zn)

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

None

None

None

None

None

None

None

None

N/A None

TCLP Limit (mg/l)

A b o v e

B e lo w

N o t

P re s

D040 Trichloroethylene 0.5

D043 Vinyl Chloride 0.2

N/A

N/A

N/A

N/A

None

None

None

None

N/A None

VOLATILES: TCLP Limit (mg/l)

A b o v e

B e lo w

N o t

P re s

D018 Benzene 0.5

D019 Carbon Tetrachloride 0.5

D021 Chlorobenzene 100.0

N/A

N/A

None

None

None

None

N/A None

TCLP Limit (mg/l)

A b o v e

B e lo w

N o t

P re s

N/A

N/A

N/A None

N/A None

PESTICIDE/HERBICIDES: TCLP Limit (mg/l)

A b o v e

B e lo w

N o t

P re s

N/A None D020 Chlordane 0.0

N/A None D031 Hepachlor (& it's epoxides)

0.0

Range UOM TCLP Limit (mg/l)

D013 Lindane 0.4

D014 Methoxychlor 10.0

D015 Toxaphene 0.5

A b o v e

B e lo w

N o t

P re s

Range UOMSEMI-VOLATILES: TCLP Limit (mg/l)

A b o v e

B e lo w

N o t

P re s

N/A None D033 Hexachlorobutadiene 0.5

N/A None

D024 m-Cresol 200.0 N/A None D034 Hexachloroethane 3.0

N/A None

G: REGULATED CONSTITUENTS: Check any regulated constituent above regulatory limit and note value. Check source(s) used :

Source(s):

Analytical

Generator Knowledge

SDS

F: USEPA / STATE / GENERATOR STATE WASTE

IDENTIFICATION:

Federal Universal Waste: Yes No EPA Exemption ref

EPA Waste Code(s): D002,D004,D005,D006,D007,D008,D010,D011

State Code(s):

State Regulated Waste: Yes No Generator State Universal Waste: Yes No WA Designation:

LANDFILL INFORMATION

This waste is a Waste water (TOC<1%, TSS<1%) Non-waste water

IDENTIFY ALL UHC's IN THIS WASTESTREAM :

APHIS Waste

Dust Hazard

Medical (sharps,needles)

CERCLA

Flammable Solid

Organic Peroxide

Asbestos, Non-friable

Dioxins

Infectious

Oxidizer phenolics

Radioactive

Pesticide/Herbicide PFAS/PFOA

PUSOProfile Subpart P

Reactive (Other)/Temp Sensitive

US DOT DESCRIPTION: USE THE FULL BASIC DESCRIPTION ON THE HAZARDOUS WASTE MANIFEST including Technical constituents:

Disposal Instructions/Comments: NCSU HAS AFL (NO STABLEX)

GENERATOR CERTIFICATION

To the best of my knowledge and belief, I hereby warrant and represent that the information contained and submitted in the waste profile and all attached documents is true, accurate, and complete and that no material fact has been omitted as to make this misleading. I understand that others may rely on this inform ation in the handling and processing of the waste material described herein. By signing this waste profile, I am certifying that I am authorized to sign such documentation on behalf of the generator.

Authorized Signature

James R Atkinson Haz-Waste Specialist

Authorized Printed Name Title Date

D036 Nitrobenzene 2.0

D037 Pentachlorophenol 100.0

D038 Pyridine 5.0

N/A

N/A

None

None

None

D030 2,4-Dinitrotoluene 0.1

D032 Hexachlorobenzene 0.1

N/A None

N/A

N/A

N/A

None

None

None

N/A None

UN3264, Waste Corrosive liquid, acidic, inorganic, n.o.s., (HYDROCHLORIC ACID, SULFURIC ACID), 8, II, RQ(D002=100#), ERG(154)

Shipping Frequency Average Shipment Quantity

Monthly

Method of Shipment: Bulk Liquid Bulk Solid Container (type/size): 55

Constituent Key Min Max UOM

SULFURIC ACID Range 50 60 %

PHOSPHORIC ACID Range 20 30 %

E: ADDITIONAL INFORMATION:

A: GENERATOR INFORMATION North Carolina State University GEN #: NCD000830737

Yes No

EPA ID#:Name:

Site Address: 2620 Wolf Village Way City: Raleigh State : NC Zip : 27695

City: Raleigh State : NC Zip : 27695Campus Box 8007Mailing Address:

Email: katrimbe@ncsu.edu Phone: (919) 515-6859 Fax: (919) 515-6307Contact: Karen Trimberger

Manifest ER Phone #: 8775772669 Generator Subpart P:

State

ID#:

Generator Status: LQG SQG VSQG/CESQG NAICS code(s)(primary reporting first): 611310

TSDF Approval List: Yes No Treatment/Disposal Restrictions:

Yes NoVarious Generator:

CUSTOMER/BILLING/BROKER INFORMATION Same as Generating Facility address:

Customer #:

Phone:

State: NCCity: RALEIGH

Customer Name: North Carolina State University

Address: CAMPUS BOX 8007

Contact:

Zip: 27695-0001

Fax:Email: mdlong3@ncsu.edu

B: MATERIAL DESCRIPTION

Generating Process (be specific):

Common Name: Inorganic Acid Vials

Laboratory Analysis Residue

W119 - Other inorganic liquid (specify in comments)

Form:

G11 - Discarding off-specification or out-of-date chemicals or products (unused chemicals or products - corresponds to P and U hazardous waste codes)

Source:

1 - Generated on-site from a product process or service activity

Origin:

Unused Commercial Product:

Generator has provided the following: Analysis

Formulary SDS Sample

Solid %:

Sludge %:

Free Liquid %:

0Single Layered

>95˚ F

HYDROCHLORIC ACID < 1 %

GLASS VIALS Range 30 50 %

PCB Yes No VOC (ppm) No selection TOC N/A

NCS-108BProfile #:

PROFILE FORM

1Revision #:

Halogens %:

Water %: 50 Pumpable:

No Color:

Debris Monolith

Powder

Specific Gravity

(water=1, oil<1, sol >1)

Est. Actual

N/A

Viscosity

(Low-water,Med-oil, High-

Honey)

N/A

METALS:

TCLP Limit

(mg/l)

A b o v e

B e lo w

N o t P re s e n t

D004 Arsenic (As) 5.0

D005 Barium (Ba) 100.0

D006 Cadmium (Cd) 1.0

D007 Chromium (Cr) 5.0

D008 Lead (Pb) 5.0

D009 Mercury (Hg) 0.2

D010 Selenium (Se) 1.0

D011 Silver (Ag) 5.0

N/A None

N/A

N/A

N/A

N/A

N/A

N/A

None

None

None

None

None

None

N/A None

TCLP Limit

(mg/l) A b o v e

B e lo w

N o t

P re s e n t

Cobalt (Co)

Copper (Cu)

Nickel (Ni)

Thallium (TI)

Vanadium (V)

Zinc (Zn)

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

None

None

None

None

None

None

None

None

N/A None

TCLP Limit

(mg/l)

A b o v e

B e lo w

N o t

P re s e n t

D040 Trichloroethylene 0.5

D043 Vinyl Chloride 0.2

N/A

N/A

N/A

N/A

None

None

None

None

N/A None

VOLATILES:

TCLP Limit

(mg/l)

A b o v e

B e lo w

N o t

P re s e n t

D018 Benzene 0.5

N/A

N/A

None

None

None

None

N/A None

D019 Carbon Tetrachloride 0.5

D021 Chlorobenzene 100.0

D022 Chloroform 6.0

D028 1,2-Dichloroethane 0.5

TCLP Limit

(mg/l)

A b o v e

B e lo w

N o t

P re s e n t

D016 2,4-D 10.0

D017 2,4,5-TP (Silvex) 1.0 N/A None

D020 Chlordane 0.0 N/A None

D031 Hepachlor (& it's epoxides)

0.0 N/A None

PESTICIDE/HERBICIDES:

TCLP Limit

(mg/l)

A b o v e

B e lo w

N o t

P re s e n t

D013 Lindane 0.4 None

D014 Methoxychlor 10.0

N/A

N/A

N/A None

D015 Toxaphene 0.5 N/A None

G: REGULATED CONSTITUENTS: Check any regulated constituent above regulatory limit and note value. Check source(s) used :

Source(s):

Analytical

Generator Knowledge SDS

F: USEPA / STATE / GENERATOR STATE WASTE

IDENTIFICATION:

Federal Universal Waste: Yes No EPA Exemption ref

EPA Waste Code(s): D002

State Code(s):

State Regulated Waste: Yes No Generator State Universal Waste: Yes No WA Designation:DW

LANDFILL INFORMATION

This waste is a Waste water (TOC<1%, TSS<1%) Non-waste water

IDENTIFY ALL UHC's IN THIS WASTESTREAM :

Infectious Medical (sharps,needles) Organic Peroxide

Oxidizer phenolics

Radioactive

Pesticide/Herbicide PFAS/PFOA

PUSOProfile Subpart P

Reactive (Other)/Temp Sensitive

US DOT DESCRIPTION: USE THE FULL BASIC DESCRIPTION ON THE BILL OF LADING OR HAZARDOUS WASTE MANIFEST INCLUDING TECHNICAL CONSTITUENTS.

Management Instructions/Comments:

GENERATOR CERTIFICATION

To the best of my knowledge and belief, I hereby warrant and represent that the information contained and submitted in the profile and all attached documents is true, accurate, and complete and that no material fact has been omitted as to make this misleading. I understand that others may rely on this inform ation in the handling and processing of the material described herein. By signing this profile, I am certifying that I am authorized to sign such documentation on behalf of the generator.

Authorized Signature Authorized Printed Name Title Date

A b o v e

B e lo w

N o t P re s e n

N/A None

N/A None

N/A None

N/A None

N/A None

SEMI-VOLATILES:

TCLP Limit

(mg/l)

A b o v e

B e lo w

N o t

P re s e n

D026 Cresol (Total) 200.0

D027 1,4-Dichlorobenzene 7.5

D030 2,4-Dinitrotoluene 0.1

D032 Hexachlorobenzene 0.1

Range UOM

TCLP Limit

(mg/l)

N/A None D033 Hexachlorobutadiene 0.5

N/A None D034 Hexachloroethane 3.0

N/A None D036 Nitrobenzene 2.0

N/A None D037 Pentachlorophenol 100.0

N/A None D038 Pyridine 5.0

N/A None D041 2,4,5-Trichlorophenol 400.0

N/A None D042 2,4,6-Trichlorophenol 2.0

UN3264, Waste Corrosive liquid, acidic, inorganic, n.o.s., (SULFURIC ACID, PHOSPHORIC ACID), 8, II, RQ(D002=100#), ERG(154)

Shipping Frequency Average Shipment Quantity

As Needed 1 x 55 gallon

Constituent Key Min Max UOM acetone Cresol Range 0 1 %

Aresenic, barium, cadmium, chrlomium

Range 0 1 % lead, selenium, silver, benzene Range 0 1 % carbon tetrachloride, chlorobenzene, Range 0 1 % chloroform, dichloroethane Range 0 1 %

E: ADDITIONAL INFORMATION:

A: GENERATOR INFORMATION North Carolina State University GEN #: NCD000830737

Yes

No

EPA ID#:Name:

Site Address: 2620 Wolf Village Way City: Raleigh State : NC Zip : 27695

City: Raleigh State : NC Zip : 27695Campus Box 8007Mailing Address:

Email: mdlong3@ncsu.edu Phone: (919) 515-6863 Fax: (919) 515-6307Contact: Mike Long

Manifest ER Phone #: (877) 577-2669 Generator Subpart P: State ID#:

Generator Status: LQG SQG VSQG/CESQG

Disposal Restrictions:

NAICS code(s)(primary reporting first):

TSDF Approval List: Yes No

Yes NoVarious Generator:

CUSTOMER/BILLING/BROKER INFORMATION Same as Generating Facility address:

Customer #:

Phone:

State: NCCity: RALEIGH

Customer Name: North Carolina State University

Address: CAMPUS BOX 8007

Contact:

Zip: 27695-0001

Fax:Email: mdlong3@ncsu.edu

B: WASTE DESCRIPTION Waste Common Name: 110 - CLEAN UP DEBRIS

Process generating Waste (be specific): LAB AND ANALYTICAL DERIVED WASTE

Form: W002 - Contaminated debris: paper, clothing, rags, wood, empty fiber or plastic containers, glass, piping, other solids (usually from construction, demolition, cleaning, or remediation)

Source: G22 - Laboratory analytical wastes (used chemicals from laboratory operations)

Origin: 1 - Generated on-site from a product process or service activity

Solid %:

Sludge %:

Free Liquid %:

Strong Description: SOLVENT

<73˚ F 73<100˚ F 100<140˚ F 140-200˚ F

>200˚F

BTU/lbs range: <2000 2000-5000 >5001-10,000 >10,000 Boiling Point: ≤95˚ F >95˚ F Halogens %: <3%

Constituent Key Min Max UOM

Acrylamide Range 0 1 % methyl ethyl ketone, tetrachloroethylene

Range 0 1 % trichloroethylene, toluene, methanol, Range 0 1 %

Debris (paper, glass, cardboard, plastic

Range 95 100 %

Vinyl Chloride Range 0 1 %

PCB

Yes No VOC (ppm) No selection TOC <1%

PCB TSCA Regulated Yes No Subject to Subpart CC: Yes No

WASTE PROFILE FORM

NCS-110Profile #: 6Revision #:

Yes No Color: various

Specific Gravity

(water=1, oil<1, sol >1)

Est. Actual

N/A 1.1-1.2

Viscosity

(Low-water,Med-oil, High-

Honey)

High (Tar/Honey)

DocuSign Envelope ID: E94BA3CF-0E43-451E-A9A4-34878E1BEE75

A b o v e

B e lo w

N o t P re s e n t

D004 Arsenic (As) 5.0

D005 Barium (Ba) 100.0

D006 Cadmium (Cd) 1.0

D007 Chromium (Cr) 5.0

D008 Lead (Pb) 5.0

D009 Mercury (Hg) 0.2

<5

<100.0

<1.0

<5.0

<5.0

N/A

<1.0

TCLP(MG/L)

TCLP(MG/L)

TCLP(MG/L)

TCLP(MG/L)

TCLP(MG/L)

None

TCLP(MG/L)

<5.0 TCLP(MG/L)

A b o v e

B e lo w

N o t

P re s

Cobalt (Co)

Copper (Cu)

Nickel (Ni)

Thallium (TI)

Vanadium (V)

Zinc (Zn)

N/A

N/A

N/A

N/A

N/A

N/A

N/A

N/A

None

None

None

None

None

None

None

None

N/A None

TCLP Limit (mg/l)

A b o v e

B e lo w

N o t

P re s

D040 Trichloroethylene 0.5

D043 Vinyl Chloride 0.2

N/A None

<200

<0.7

<0.5

TCLP(MG/L)

TCLP(MG/L)

TCLP(MG/L)

N/A None

VOLATILES: TCLP Limit (mg/l)

A b o v e

B e lo w

N o t

P re s

D018 Benzene 0.5

D019 Carbon Tetrachloride 0.5

D021 Chlorobenzene 100.0

<0.5

<0.5

<100

<6

TCLP(MG/L)

TCLP(MG/L)

TCLP(MG/L)

TCLP(MG/L)

N/A None

TCLP Limit (mg/l)

A b o v e

B e lo w

N o t

P re s

N/A

N/A

N/A None

N/A None

PESTICIDE/HERBICIDES: TCLP Limit (mg/l)

A b o v e

B e lo w

N o t

P re s

N/A None D020 Chlordane 0.0

N/A None D031 Hepachlor (& it's epoxides)

0.0

Range UOM TCLP Limit (mg/l)

D013 Lindane 0.4

D014 Methoxychlor 10.0

D015 Toxaphene 0.5

A b o v e

B e lo w

N o t

P re s

Range UOMSEMI-VOLATILES: TCLP Limit (mg/l)

A b o v e

B e lo w

N o t

P re s

N/A None D033 Hexachlorobutadiene 0.5

N/A None

D024 m-Cresol 200.0 N/A None D034 Hexachloroethane 3.0

N/A None

G: REGULATED CONSTITUENTS: Check any regulated constituent above regulatory limit and note value. Check source(s) used :

Source(s):

Analytical

Generator Knowledge

SDS

F: USEPA / STATE / GENERATOR STATE WASTE

IDENTIFICATION:

Federal Universal Waste: Yes No EPA Exemption ref

EPA Waste Code(s): D001,D004,D005,D006,D007,D008,D010,D011,D018,D021,D022,D024,D026,D027,D028,D035,D038,D039,D040,D043,F001,F002,F003,F004,F005,U007,U188

State Code(s):

State Regulated Waste: Yes No Generator State Universal Waste: Yes No WA Designation:

LANDFILL INFORMATION

This waste is a Waste water (TOC<1%, TSS<1%) Non-waste water

IDENTIFY ALL UHC's IN THIS WASTESTREAM :

APHIS Waste

Dust Hazard

CERCLA

Asbestos, Non-friable

Infectious

Oxidizer phenolics

Radioactive

Pesticide/Herbicide PFAS/PFOA

PUSOProfile Subpart P

Reactive (Other)/Temp Sensitive

DocuSign Envelope ID: E94BA3CF-0E43-451E-A9A4-34878E1BEE75

US DOT DESCRIPTION: USE THE FULL BASIC DESCRIPTION ON THE HAZARDOUS WASTE MANIFEST including Technical constituents:

Process Code(s):

Disposal Instructions/Comments:

GENERATOR CERTIFICATION

To the best of my knowledge and belief, I hereby warrant and represent that the information contained and submitted in the waste profile and all attached documents is true, accurate, and complete and that no material fact has been omitted as to make this misleading. I understand that others may rely on this inform ation in the handling and processing of the waste material described herein. By signing this waste profile, I am certifying that I am authorized to sign such documentation on behalf of the generator.

Authorized Signature

James R Atkinson Haz-Waste Specialist

Authorized Printed Name Title Date

D036 Nitrobenzene 2.0

D037 Pentachlorophenol 100.0

D038 Pyridine 5.0

N/A

N/A

None

None

None

D030 2,4-Dinitrotoluene 0.1

D032 Hexachlorobenzene 0.1

N/A None

N/A

N/A

N/A

None

None

None

N/A None

UN3175, Waste Solids containing flammable liquid, n.o.s., (CRESOL, VINYL CHLORIDE), 4.1, II, RQ(D001=100#), ERG(133)

Shipping Frequency Average Shipment Quantity

Monthly

Method of Shipment: Bulk Liquid Bulk Solid Container (type/size): 55

DocuSign Envelope ID: E94BA3CF-0E43-451E-A9A4-34878E1BEE75

Constituent Key Min Max UOM

DEBRIS: PAPER, PLASTIC, RAGS,

ETC..

= 99 %

MERCURY = 1 %

E: ADDITIONAL INFORMATION:

A: GENERATOR INFORMATION North Carolina State University GEN #: NCD000830737

Yes No

EPA ID#:Name:

Site Address: 2620 Wolf Village Way City: Raleigh State : NC Zip : 27695

City: Raleigh State : NC Zip : 27695Campus Box 8007Mailing Address:

Email: katrimbe@ncsu.edu Phone: (919) 515-6859 Fax: (919) 515-6307Contact: Karen Trimberger

Manifest ER Phone #: 8775772669 Generator Subpart P: State ID#:

Generator Status: LQG SQG VSQG/CESQ

G NAICS code(s)(primary reporting first): 611310

TSDF Approval List: Yes No Treatment/Disposal Restrictions:

Yes NoVarious Generator:

CUSTOMER/BILLIN…

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