DRAFT Exhibit D.pdf
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- Analytical Services
- Solicitation number
- BSA478026
- Issued by
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Department of Energy Office of Science
About this file
This document is Exhibit D, a template specification for the format and contents required in radiochemical data validation packages submitted to Brookhaven National Laboratory.
The template establishes standardized documentation requirements across three analytical methodologies: Gamma Spectroscopy Results, Proportional Counter or Liquid Scintillator Results, and Alpha Spectroscopy Results. For each methodology, contractors must submit identical core documentation components including: case narratives, chain of custody forms, holding time documentation, analysis results data sheets with uncertainties and minimum detectable concentrations (MDCs), data completeness inventories, calibration documentation (initial and most recent), field and laboratory duplicates, laboratory control spikes, method blank analysis, raw data and calculations, background control charts, NIST traceable standards certificates with preparation documents, and Brookhaven National Laboratory requests for information or telecon records. Specific to Proportional Counter/Liquid Scintillator analysis, contractors must additionally provide matrix spike recovery results and quench curve control charts. The template is based on Lockheed Analytical Laboratory's LAL-91-SOP-0088 procedure for radiochemical data validation dated June 23, 1992, and serves as the baseline quality assurance and data integrity standard for all radiochemical analytical work performed under contract.
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Other files
| File | Type | Posted |
|---|---|---|
| DRAFT Exhibit E 2026.pdf | ||
| DRAFT Exhibit B 2026.pdf | ||
| DRAFT Exhibit F and Tech.pdf | ||
| DRAFT Exhibit C and Qualifiers 2026.pdf | ||
| DRAFT Exhibit A 2026.pdf | ||
| DRAFT Exhibit H 2026.pdf | ||
| DRAFT Exhibit G 2026.pdf | ||
| DRAFT Fee Schedule.xlsx | XLSX spreadsheet | |
| DRAFT SOW 26 Jan 2026.pdf |
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Text version
Exhibit D
Format for Data Validation Package:
Radiochemical Results
DRAFT
Brookhaven National Laboratory’s Format for Radiochemical Data Validation Packages*
Gamma Spectroscopy
Results
Proportional Counter or Liquid
Scintillator Results
Alpha Spectroscopy Results
Case Narrative
Chain of Custody Forms
Holding Times
Gamma Spec Analysis
Results Data Sheet with uncertainties and MDCs
Proportional or Scintillation
Counter Analysis Results Data
Sheet w uncertainties and MDCs
Alpha Spec Analysis Results
Data Sheet with uncertainties and MDCs
Data Completeness
Inventory
Data Completeness Inventory
Data Completeness Inventory
GeLi Calibration
Documentation (Initial and most recent)
HV Plateaus and Efficiency
Calibration Documentation (Initial and most recent, including self absorption curves/tables)
Alpha Spec Calibration
Documentation (Initial and most recent, including self absorption correction curve/table)
Field/Laboratory Duplicates
Laboratory Control Spikes
(LCS)
Laboratory Control Spikes (LCS)
Laboratory Control Spikes
(LCS)
Method Blank Analysis
NA
Matrix Spike Recovery and Its
Duplicate Results
Matrix Spike Recovery and Its
Duplicate Results
Raw Data and Calculations
Background and LCS
Control Charts
Background, Quench Curve and
LCS Control Charts
Background and LCS Control
Charts
NIST Traceable Standards
Certificates and Std.
Preparation Documents
NIST Traceable Standards
Certificates and Std. Preparation
Documents
NIST Traceable Standards
Certificates and Std. Preparation
Documents
BNL Requests for
Information/Telecon
Records
BNL Requests for
Information/Telecon Records
BNL Requests for
Information/Telecon Records
*Based on Lockheed Analytical Laboratory ‘s LAL-91-SOP-0088 procedure entitled “Radiochemical
Data Validation procedure dated June 23, 1992.
File details come from the government source that posted it. Updated .