Attachment 1-SOW (12 July 2021).pdf

Statement of Work for

Contracted Laboratory Services

CONUS

12 July 2021

Contents C-1.0 General Description:

C-1.0.1 Service Locations: When ordered, C-1.1 Facilities:

C-1.2 Specifications, Standards and Handbooks:

C-1.3 Scheduling of Services:

C-2.0 Contract Deliverables:

C-2.1 Contract Compliance Plan:

C-2.2 Laboratory Test Reports:

C-2.3 Contract Contingency Plan:

C-2.4 Contract Training Plan:

C-2.5 Safety Plan:

C-2.6 Transportation Plan:

C-2.7 Laboratory Equipment Plan:

C-2.8 Monthly Reporting:

C-3.0 Laboratory Requirements:

C-3.1 Operating Hours:

C-3.2 Staffing:

C-3.3 Knowledge and Skills:

C-3.4 Access:

C-3.5 Equipment Calibration:

C-3.6 Epoxy Lined Sample Cans:

C-3.7 Ellipsometric Tube Deposit Rater (ETR):

C-3.8 Turn-around Times:

C-3.8.1 Baltimore, MD Area:

C-3.8.2 Selby, CA Area:

C-3.8.3 Houston, TX Area:

C-3.9 Retain samples:

C-4.0 Transportation Performance Requirements:

C-5.0 Secured Fuels Performance Requirements:

C-6.0 Surveyor Duties:

C-6.1.1 Third party witness:

C-6.1.2 Sampling of petroleum products:

C-6.1.3 Gauging of petroleum products:

C-6.1.4 Cargo Inspection of petroleum products:

C-7.0 Sample Shipment:

Attachment 1: Products Attachment 2: Series Testing Requirements Attachment 3: Approved Testing Methods

Page | 1

C-1.0 General Description: This Statement of Work (SOW) provides the requirements for laboratory testing services in multiple locations throughout the Continental U.S. (CONUS) region. The Contractor will be responsible for the laboratory testing of government-owned petroleum products in accordance with the specifcations as described herein, and transportation of samples from contracted locations to the contractor’s laboratory. Government-owned products mentioned in this SOW may be shipped to the Contractor’s laboratory for testing.

C-1.0.1 Service Locations: When ordered, the contractor shall be able to provide services required in this SOW to DLA Energy in each of the locations listed below. Contractor facilities must be located within the CONUS region and meet the required turn-around times listed in paragraph C-3.8.

Americas East Locations Helena, AL Columbus,GA NY Harbor Area Montgomery, AL Chicago, IL Coraopolis, PA Moundville, AL Baton Rouge, LA Charleston, SC Jacksonville, AR Boston, MA Rapid City, SD Port Mahon, DE Portland, ME Dallas, TX Port Everglades, FL Anacostia, MD Houston, TX Key West, FL Andrews AFB, MD Craney Island, VA Jacksonville, FL Baltimore, MD Norfolk, VA Tampa, FL Lockhart, MS Yorktown, VA Macon, GA Selma, NC Bremen, GA Jacksonville, NJ

Americas West Locations

Carson, CA Moffett Field, CA Alamogordo, NM Colton, CA McClellan, Park, CA Las Vegas, NV NAS Lemoore, CA Selby, CA Salt Lake City, UT NAS Point Loma, CA Denver, CO Puget Sound, WA

C-1.1 Facilities: The contractor shall have facilities that meet the required turn-around times in section C-3.8. The contractor shall provide the location(s) of the facility where the product shall be tested, facility testing capabilities and contact information.

C-1.2 Specifications, Standards and Handbooks: At each laboratory, the contractor shall retain a copy of all required specifications, standards, test methods, handbooks, etc., per this SOW and perform services in accordance with testing requirements. Military Specifications referenced in Attachment 1 for petroleum product types can be obtained at http://quicksearch.dla.mil or https://assist.dla.mil but can also be requested in writing to the Contracting Officer (CO) or Contracting Officer’s Representative (COR).

C-1.3 Scheduling of Services: After the CO authorizes a task order, the COR or QAR will contact the laboratory to schedule the testing. The contractor shall not perform services under this SOW without a task order or direct authorization from the CO. If a task order was not received, the contractor shall contact the CO or COR prior to any testing. Only the CO can formally, either in writing or verbally, authorize testing and create an obligation.

C-2.0 Contract Deliverables: All plans shall be submitted to the CO for review and acceptance as a part of the technical proposal as documented in the solicitation. Plans shall be kept current for the life of the contract. The government reserves the right to request changes or modifications to any detailed plans at any time throughout the contract performance period. Plans shall be made available for Government review upon request at any time during the contract performance period.

C-2.1 Contract Compliance Plan: The contractor is responsible for compliance with all contract performance requirements. The contractor is responsible for all actions taken by any sub-contractor utilized under this contract. The contractor shall be ISO 9001 and/or ISO/IEC 17025 certified.

Page | 2

C-2.2 Laboratory Test Reports: The contractor shall maintain records evidencing all analysis performed under this contract. All samples tested shall be documented with a detailed report. Reports shall be complete and legible containing information pertaining but not limited to: Lab Name, Test Method, Test Name, Test Results, Test Units, Test Limits.

Reports not containing the appropriate information will need to be corrected and resubmitted by the contractor for approval.

C-2.3 Contract Contingency Plan: The Contract Contingency Plan shall outline contractor actions to ensure there is no significant interruption of services resulting from labor disputes, catastrophic failure of equipment, or the effects of natural disasters/emergencies. The plan shall provide specific details regarding labor issues that may result from potential strike actions, world events, world actions, military contingency and war time manning requirements.

C-2.4 Contract Training Plan: The contractor shall provide a detailed plan that identifies employee training requirements and procedures necessary to maintain proficiency. The plan shall identify length of training, training sources and a brief description of courses such as safety, environmental protection and job qualification training. The contractor is responsible for ensuring all individual training requirements are accomplished. The contractor must demonstrate current participation in a proficiency program or suitable means to verify laboratory performance.

C-2.5 Safety Plan: The contractor shall provide a detailed plan outlining the policy, procedures and actions necessary to maintain a safe working environment for employees and visitors. The plan shall cover the products stored, handled, Safety Data Sheets (SDS) and guidelines regarding the safe handling of such products and shall be maintained and updated over the course of the contract.

C-2.6 Transportation Plan: The contractor is required to submit a plan for review to transport the petroleum samples to an approved laboratory for testing or shipping (contractor supplied transport, third party delivery service, etc.) and how they plan on tracking the chain of custody to the contractor’s facility. Product quality must be preserved and not altered by shipment. DLA Energy or it’s subcontractor(s) do not have the ability or certification to ship or package fuel samples.

C-2.7 Laboratory Equipment Plan: The contractor will furnish, and update annually, to the CO and COR the status by name, model and serviceability of all equipment used in laboratory testing. Equipment that malfunctions or is non-serviceable shall be reported to the CO and COR within 48 hours with a mitigation plan to provide testing capability.

C-2.8 Monthly Reporting: The contractor shall provide a monthly written report to the CO and COR with the number of laboratory tests performed, what testing was included and the location.

C-3.0 Laboratory Requirements: The below are general requirements for all contractor laboratories. Laboratories are required to have the listed referee test methods which is referenced in the product specifications and international test methods (ASTM, EI, etc.).

C-3.1 Operating Hours: The contractor shall be responsible for adjusting hours of operation to meet workload demands and turn-around times in section C-3.8.

C-3.2 Staffing: The contractor shall provide sufficient staffing to accomplish all functions and tasks to include simultaneous operations of performing multiple tests at a time, and provide the contact information for laboratory manager or assistant laboratory manager if the laboratory is not manned 24 hours, seven days a week.

C-3.3 Knowledge and Skills: The contractor shall ensure that personnel assigned to all tasks have the requisite knowledge and skills to meet the performance standards and comply with all applicable federal laws, state laws, regulations, and codes. All supervisors and key employees shall be able to read and understand English so they can understand and follow oral or written instructions directions, directives, regulations, and operating procedures. All supervisors and contractor key employees shall be capable of writing in English to compose the required detailed reports.

C-3.4 Access: The contractor shall allow DLA Energy representatives to witness testing or sampling. It shall provide the applicable information for access, provide follow-up to obtain access (for personnel and vehicles) to all facilities that product is tested or sampled. For areas that require special admission the contractor will assist gaining access.

Page | 3

C-3.5 Equipment Calibration: The laboratories shall have a system of calibration equivalent to ISO/IEC 17025.

All testing shall be performed in accordance with the appropriate international or local test methods approved for use by DLA Energy and listed in this SOW.

C-3.6 Epoxy Lined Sample Cans: The contractor shall maintain a supply of 10 unused epoxy lined fuel sample shipping containers to be provided to DLA Energy personnel per request. Sample containers shall be stored to ensure they are clean and free from all substances that might contaminate the product being sampled. Containers must meet the following specifics: Complies with ASTM D-4306, height not to exceed 9 inches, diameter not to exceed 7 inches, capacity 1 USG, Bung Plug ¾” with lock-wire hole, carrying handle able to be shipped as hazardous material.

C-3.7 Ellipsometric Tube Deposit Rater (ETR): The contractor shall perform ASTM D3241 Annex 3 ETR within the testing turn-around times in section C-3.8 Sample Testing Turnaround Times. ETR is the preferred method and shall be treated as the referee method.

C-3.8 Turn-around Times: The contractor shall perform testing in accordance with the turn-around times listed in the table below. Turn-around time starts when the contractor is notified that the sample is prepared for transportation from sample location to the servicing laboratory. Turn-around time ends when testing results are completed and delivered to DLA Energy. DLA-Energy will give the contractor at least 12 hours of advance notice ofthe sample being prepared for shipment (turn-around time start) (prime contractor is responsible for any sub-contractor actions). The 12 hours of advance notice is not included in the turn-around time. If testing cannot be completed within the turn-around time the contractor will immediately notify the CO and COR. The contractor shall specify the problem and the estimated completion date and time. If there is a need for an expedited test, it will be a maximum turn-around time of 18 hours unless otherwise stated in C-3.8.1, C-3.8.2, or C-3.8.3.

C-3.8.1 Baltimore, MD Area: Mission requirements dictate a turn-around time for Jet A petroleum sample(s) to be tested at this location. Jet A sample results must be received within 16 hours. The 16-hour turn-around starts when the sample is prepared for transportation at the location and the contractor is notified for sample pickup. DLA Energy will provide the contractor an initial forecast then a 24-hour notification prior to sample collection as times can be adjusted by weather, berthing space or ullage.

C-3.8.2 Selby, CA Area: Mission requirements dictate a turn-around time for Jet A and F-76 petroleum sample(s) to be tested at this location. Sample results for Jet A shall be received within 8 hours and for F-76 must be received within 24 hours unless otherwise coordinated with the QAR. DLA Energy will provide the contractor an initial forecast and notification of 24-hours prior to sample collection as times can be adjusted by weather, berthing space or ullage. The turn-around starts when the sample is prepared for transportation at the storage location and the contractor is notified for sample pickup.

C-3.8.3 Houston, TX Area: Mission requirements dictate a turn-around time for Jet-A petroleum sample(s) to be tested at this location. When an expedited Jet-A request is made, sample results shall be received within 8 hours unless otherwise coordinated with the QAR. DLA Energy will provide the contractor an initial forecast and notification 12 hours prior to sample collection as times can be adjusted by weather, berthing space or ullage. The turn-around time starts when the sample is prepared for transportation at the storage location and the contractor is notified for sample pickup.

Maximum Turn-around Hours Chart A Series 48 hours B Series 36 hours C Series 24 hours

Individual tests 24 hours Expedite 18 hours

Secured Fuel Performance 8 hours

Page | 4

C-3.9 Retain samples: After analysis, the contractor shall retain samples for a minimum of 45 days. In the event of a suspected quality issue or dispute, a longer sample retention period may be requested by DLA Energy. The contractor shall be responsible for disposal of excess fuel samples and sample containers.

C-4.0 Transportation Performance Requirements: The contractor shall be responsible for packing and transporting all petroleum samples from a job site to the laboratory in accordance with federal and laws and regulations. When requested by DLA Energy personnel, the contractor shall be able to provide an epoxy line sample can, detailed in C-3.6 for replacement. When sample transportation is not required of the contractor, they shall be notified in advance.

C-5.0 Secured Fuels Performance Requirements: Due to mission demands DLA Energy shall request petroleum testing under Attachment 2 from MIL-STD-3004-1 table XII. DLA-Energy will provide the contractor with as much advance notice as possible as the turn-around time shall not exceed 8 hours after receipt of sample at the laboratory.

Specifics/logistics shall be scheduled by the QAR after a task order for the secured fuels testing services is issued.

C-6.0 Surveyor Duties: When ordered, the contractor shall represent DLA Energy to ensure all specifications, regulations, ASTM, API MPMS are followed when a DLA Energy representative is not available at locations mentioned in C-1.0.1. Personnel shall be International Federation of Inspection Agencies or TIC council or equivalent certified to perform the duties defined in the following subparagraphs.

C-6.1.1 Third party witness: When ordered, the contractor shall act as a third party witness to observe operations and report findings to the DLA Energy point of contact with a detailed report within 24 hours. DLA Energy will provide written instructions specific to the operations and objectives in the task order. The following are examples of operations commonly preformed: Tank to tank transfers, off-loading vessels, barges, tank trucks, containers, loading vessels, barges, tank trucks, containers.

C-6.1.2 Sampling of petroleum products: When ordered, the contractor shall be capablity of performing sampling of pipelines, vessels, barges, tank trucks, storage tanks, or any containers that may hold fuel in accordance with API MPMS and/or ASTM D4057, when requested. The contractor shall supply all equipment and material needed to perform tasks.

C-6.1.3 Gauging of petroleum products: When ordered, the contractor shall be capable of performing gauging of vessels (to include bunkers), barges, tank trucks, storage tanks, or any containers that may hold fuel. The Contractor shall supply all equipment and material need to perform task.

C-6.1.4 Cargo Inspection of petroleum products: When ordered, the contractor shall oversee operations to include:

Gauging, Sampling, Atmospheric Measuring, Tank cleanliness, Lightering transfers, and complete certified detailed reports within 24 hours. The Contractor shall supply all equipment and material needed to perform tasks.

Note: The contractor will have the authority to stop any operations that are thought to be unsafe but must immediately contact the POC named on the Task Order to explain why.

C-7.0 Sample Shipment: The contractor shall, upon request, be responsible for shipping fuel samples from locations in C-1.0.1 to the laboratories in the chart below. Fuel samples shall be shipped within 48 hours of request and arrive to the below laboratory within five calendar days.

Naval Air Systems Command HAZMART Bldg. 2385 22680 Hammond Road Patuxent River, MD 20670

US ARMY TARDEC

Petroleum Laboratory Bldg. 5085 U Avenue, Bldg 85 New Cumberland, PA 17070-

Aerospace Fuels Laboratory AFPA/PTPLA 2430 C Street, Bldg 70, Area B Wright Patterson AFB OH 45433-

Naval Research Laboratory 4555 Overlook Avenue, SW Washington, DC 20375

Southwest Research Institute 6220 Culebra Rd San Antonio, TX 78238-5166

Air Force Research Laboratory AFRL 2977 Hobson Way

WPAFB, OH 45433

Page | 5

Attachment 1: Products Specifications shall dictate the testing required and the contractor shall develop a plan based on product specifications (A level testing) and MIL-STD-3004-1 (B-1, B-2, B-3, C test). MIL-STD_3004-1 describes products to be tested, types of testing required and additional information as required. All referenced material can be obtained at http://quicksearch.dla.mil/, https://assist.dla.mil/, or by contacting the CO, COR, or QAR.

Jet Fuels Aviation Turbine Fuel, Grade JET A (Specification: ASTM D1655 latest version) and JET A-1, NATO F-35 (DEF Stan 91-091 latest version) Aviation Turbine Fuel, Kerosene Types, Grade JP-8 NATO F-34 (Specification: MIL-DTL-83133, latest version) Aviation Turbine Fuel, Grade JP-5 NATO F-44 (Specification: MIL-DTL-5624, latest version) Aviation Turbine Fuel, Thermally Stable, Grade JPTS (Specification: MIL-DTL-25524 latest version)

Aviation, Gasoline, NATO F-18 ASTM D910. (latest version)

Diesel Fuels Diesel Fuel, Navy Distillate NATO F-76 (Specification: MIL-DTL-16884, latest versions) Diesel Fuel Oil, Grades: Ultra-low sulfur No.1 & No. 2, Low Sulfur No.1 & No. 2 (Specification: ASTM D975, latest version) Diesel Fuel Oil, Biodiesel blends B6-B20 (Specification: ASTM D7467 latest version)

Marine Residual Fuel Oil Grade (RME-180, RMG-380, MGO) (Specification: ISO 8217 latest version) Unleaded Fuels Fuel, Automotive Spark Ignition Engine Grades (Specification: ASTM D4814, latest version) Unleaded Gasohol, (Midgrade, Premium, Regular) Specification: ASTM D4814, (latest version) Fuel Ethanol (E85) for Automotive Spark-Ignition Engines (Specification ASTM D5798 latest version) Additives Fuel System Icing Inhibitor, High Flash (FSII) (Specification: MIL-DTL-85470 latest version) Corrosion Inhibitor (CI) (Specification: MIL-PRF-25017 latest version) Lube Oils Lubrication Oil, Steam Turbine and Gear (LTL) MIL Symbol 2190 (Specification: MIL-PRF-17331 latest version) Lubrication Oil, LO6, MIL Symbol 9250, Shipboard Internal Combustion, High Output Diesel (Specification:

MIL-PRF-6081 latest version) Fuel Oil Fuel Oil Reclaimed (FOR) (specification: MIL-PRF-24951 latest version) http://quicksearch.dla.mil/ https://assist.dla.mil/

Page | 6

Attachment 2: Series Testing Requirements The list below provides tests by name and methods that shall be required to be performed on petroleum products at the contractor’s laboratory in accordance with product specifications MIL-STD-3004-1, specifications, and authorized test methods. The contractor must refer to paragraph C-2.4 for instructions on how to incorporate and indicate if they cannot perform authorized method or submit a formal exception request to the DLA Energy CO for acceptance. Tests shall be requested by series or individually by a DLA Energy representative as situation warrants.

1. A Series (Specification testing in accordance with Attachment 1 and MIL-STD-3004-1)

2. B-1 Series (MIL-STD-3004-1 list tests required in group)

3. B-2 Series (MIL-STD-3004-1 list tests required in group)

4. B-3Series (MIL-STD-3004-1 list tests required in group)

5. C Series (MIL-STD-3004-1 list tests required in group)

Individual Tests: Individual tests may be requested from any test included in the A, B or C series or from the tables below.

Note: Tests are grouped by physical or chemical property and do not imply equivalency. Verify that the test is appropriate to the product specification prior to analysis.

1. Secured Fuel Series Testing Requirements and Specification Limits JP-5 Jet A Jet A-17 JP-8 F-24

Min. Max. Min. Max. Min. Max. Min. Max. Min. Max.

Appearance 2

Gravity, API @ 60 °F D1298/D4052 36.0 48.0 37.0 51.0 37.0 51.0 37.0 51.0 37.0 51.0

Density at 15°C (kg/m3) 788 845 775 840 775 840 775 840 775 840 Weight: lb/USG Calculated 6.6 7.0 6.5 7.0 6.5 7.0 6.5 7.0 6.5 7.0 Distillation (°C) D863

10% Recovered 205 205 205 205 205 20% Recovered Report Report 50% Recovered Report Report Report Report Report 90% Recovered Report Report Report Report Report Final Boiling Point 300 300 300 300 300 Freezing point, °C D5972/D2386

-46

-40

-47

-47

-40

Flash point, °C D93/D56 60 38 38 38 38

Particulate Matter (mg/L) D2276, D5452, Appendix C of MIL- DTL- 83133

0.5

Conductivity (pS/m) D2624 Report Report 50 700 50 700 Copper strip corrosion D130 No.1 No.1 No.1 No.1 No.1 Water reaction D1094 1b Existent gum (mg/100 mL) D381 7 7 7 7 7 FSII, (vol %) D5006 1 0.07 0.20 0.04 0.15 0.04 0.15 Thermal Stability D3241

Change in pressure drop, mm Hg 25 25 25 25 25 One of the tube deposit rating methods shall be run:

(1) Ellipsometer (ETR)6 (nm) or Interferometer (ITR) (nm)

(2) Heater tube deposit, Visual Tube Rating (VTR)

< 3

< 3 < 3 < 3 < 3

Fatty Acid Methyl Ester (FAME)5

Page | 7

2. Jet A & Jet A-1 (NATO F35) Series Testing Requirements for Specifications ASTM D1655 and Def Stan 91-

A Series Characteristics Def Stan

91-091

ASTM

D1655

B-1 Series

B-2 Series

B-3 Series

C-Series

Appearance X X X X X X Color (Visual) X X X X X X Density or API Gravity X X X X X X Particulate Matter X X X X X Particle Count X X Total Acidity X X X Aromatics X X Total Sulfur X X Mercaptan Sulfur X X Doctor Test X X Distillation X X X X X Viscosity X X Smoke Point X X Naphthalenes X X Specific Energy X X Hydrogen Content X Calculated Cetane Index X Copper Strip Corrosion X X X X X Freezing Point X X X X X Existent Gum X X X X X Flash Point X X X X X X Water Reaction Lead Content (if present) X X X X

FSII X X X X X

Filtration Time

MSEP X X X X X

Electrical Conductivity X X X X X Thermal Stability X X X X Color (Saybolt) X X X Peroxide Number X

FAME X X X X X

Lubricity X

X

Page | 8

3. JP8 (NATO F34) Series Testing Requirements for Specifications MIL-DTL-83133

Characteristics MIL DTL

83133 B-1

Series B-2

B-3 Series C-Series

Appearance/Workmanship X X X X X Color (Visual) X X X X X Particulate Contamination/Particulate Matter

X X X X

Particle Count X Total Acidity X X Aromatics X Total Sulfur X Mercaptan Sulfur X Doctor Test X Distillation X X X X Flash Point X X X X X API Gravity or Density at 15°C X X X X X Freezing Point X X X X Viscosity at minus 20°C X Specific Energy (Net Heat of Combustion)

X

Copper Strip X X X X Thermal Stability X X X Existent Gum X X X X Microseparometer X X X X Electrical Conductivity X X X X Lubricity Colour, Saybolt X X Particulate Contamination/Particulate Matter with Filtration Time

X X X X

Fuel System Icing Inhibitor X X X X

FAME X X X X

Hydrogen Content X Cetane Index, Calculated X Water Reaction Sulfides in Bottom Water

Page | 9

4. JP5 (NATO F44) Series Testing Requirements for Specifications MIL-DTL-5624

Characteristics MIL DTL

B-1

B-2 Series B-3 Series C- Series

Color (Visual) X X X X X Particulate Contamination/ Particulate Matter

X X X X

Particle Count X Total Acidity X X Aromatics X Total Sulfur X Mercaptan Sulfur X Doctor Test X Distillation X X X X Flash Point X X X X X API or Density at 15° C X X X X X Vapor Pressure X Freezing Point X X X X Viscosity at minus 20°C X Smoke Point X Naphthalenes X Specific Energy (Net Heat of Combustion)

X

Copper Strip X X X X Thermal Stability X X X Existent Gum X X X X Microseparometer X Electrical Conductivity X Colour, Saybolt X X Particulate Contamination/Particulate Matter with Filtration Time

X X X X

Fuel System Icing Inhibitor X X X X

FAME X X X X

Hydrogen Content X Cetane Index, Calculated X Water Reaction

Page | 10

5. JPTS Series Testing Requirements for Specifications MIL-DTL-25524

Characteristics MIL DTL 25524 B-1

B-2 Series B-3 Series C TEST

Color, Saybolt X X Total Acid Number X X Aromatics X Mercaptan Sulfur X Doctor Test X Total Sulfur X Distillation X X X X Flash point X X X X X Density X X X X X Freezing point X X X X Viscosity @ -40°C X Net heat of combustion X Hydrogen content X Smoke point X Copper Strip Corrosion X X X X Thermal Stability X X X Existent Gum X X X X Particulate Matter X X X X Particle Counting X Micro-Separometer X

FSII X X X X

Appearance X X X X X Visual Color X X X X X Filtration time X X X

FAME X X X

Page | 11

6. Aviation Gasoline Series Testing Requirements for Specifications ASTM 910.

Characteristics ASTM 910 B-1

Series B-2

B-3 Series C Series

Net heat of combustion X Lean Mixture Motor Octane Number

(MON)

X

Aviation Lean Rating X Performance number X Sulfur Content X Tetraethyl Lead X Dye content (Blue Dye) X Vapor Pressure X X X Density at 15°C X X X X X Distillation X X X X Freezing Point X Copper Strip X X X X Oxidation Stability X Water Reaction X Conductivity X Color, Visual X X X X Existent Gum X X Specific Energy Colour, Lovibond Particulate Matter X X X Free Water Determination X X X Lead Content X X Potential Gum X

Page | 12

7. F-76 Series Testing Requirements for Specification MIL-DTL-16884

Characteristics MIL F

16884 B-1

Series B-2

Demulsification X API Gravity or Density at 15°C X X X X X Distillation X X X Cloud Point X X Color X X X X X Flashpoint X X X X X Particulate Contamination X X X Pour Point X X Viscosity at 40°C X X Acid Number X Ash X Aromatics X Carbon Residue X X X Copper Strip Corrosion X X Hydrogen Content X Ignition Quality (Cetane Number, Cetane Index, or Derived Cetane Number)

X X

Storage Stability X X Sulfur Content X X X Trace Metals (Ca, Pb, Na, K and V) X Lubricity X X X Water and Sediment X X X X

FAME X X X X

Page | 13

8. Fuel System Icing Inhibitor (FSII) (NATO S-1745) Series Testing Requirements for Specifications MIL-DTL- 85470

9. Marine Residual Fuel Oil (RME 180/380) Series Testing Requirements for Specification ISO-8217

Characteristics MIL DTL 85470 B-1

Series B-2

Acid Number X X Color, Platinum Cobalt X Distillation X X Ethylene Glycol X X pH of 25 % solution in water X X Relative density X X X Water (mass %) X X Flash point X X Appearance/Workmanship X X X

A Series Characteristics ISO 8217 B-1

Series B-2

Series B-3

Kinematic Viscosity at 50°C X X X X X Density at 15°C X X X X X Calculated Carbon Aromaticity Index

X X

Sulfur X X Flash point X X X X X Hydrogen sulfide X X Acid Number X X Total Sediment aged X X X Carbon Residue X X X Pour Point X X Water X X X Ash X X Vanadium X Sodium X X Aluminum plus silicon X Used lubricating oils X

Page | 14

10. Lubrication Oil (LTL) (NATO O-250) Series Testing Requirements for Specification MIL-PRF-17331

Characteristics MIL PRF

17331 B-1

Series B-2

Series B-3

Sulfur X n/a Acid Number X n/a Corrosion X X n/a Corrosion, Copper Strip X n/a Water content, mass% X X X n/a X Gravity X X n/a X Flash point X X X n/a Pour Point X X n/a Viscosity @ 4.4°C X X n/a Viscosity @100°C X X X n/a Viscosity @ 40°C X X X n/a X Emulsion test X X X n/a Foam Test X X X n/a Cleanliness (Solid Particle Contamination)

X X X n/a

Neutralization number (acid/base) X X n/a Appearance (to include visual sediment & water)

X X n/a X

Solid contaminants X X X n/a

11. Lubrication Oil (LO6) (NATO O-278) Series Testing Requirements for Specification MIL-PRF-9000

Characteristics MIL PRF 9000 B-1

Series B-2

Series B-3

Series C-Series n/a Appearance/Workmanship X X X X Flash point X X X n/a Foam (stability only) X X X n/a Gravity X X n/a X Metals/Elements:Calcium, Magnesium, Zinc, Phosphorus

X n/a

Pour Point X X n/a Sulfur X n/a Total base number X X n/a Viscosity index X n/a Viscosity at 100°C X X X n/a Viscosity at 40°C X n/a Water (by centrifuge) X X n/a X Ash, sulfated X X X Corrosion, Copper Strip X

Page | 15

12. Diesel Fuel Oil Series Testing Requirements for Specifications ASTM D975

Characteristics ASTM D975 B-1

B-2 Series B-3 Series C-Series

Flash point X X X X X Water and Sediment X X Distillation X X X Kinematic Viscosity X Ash X Sulfur X X X Copper strip corrosion X X Cetane number X Cetane index X X Aromaticity X Cloud Point X X

LTFT/CFPP X

Ramsbottom Carbon Residue

X

Lubricity X Conductivity X API Gravity or Density at 15°C X X X X X

Polycyclic aromatic hydrocarbons

Manganese content Water Content Total Contamination

FAME

Oxidation stability Appearance/Workmanship X X X X X Pour Point (not required) Color Visual

Page | 16

13. Diesel Fuel Oil, Biodiesel blends B6-B20 Series Testing Requirements for Specification ASTM D7467 Characteristics A Series B-1

Series B-2

TEST

B-3

TEST

C

TEST

Appearance X X X X X Distillation X X X Flash Point X X X X X Cloud Point or LTFT/CFPP X X Cetane Number X Cetane Index/Aromaticity X Viscosity @ 40°C X X Copper Strip Corrosion X X Water and Sediment X Sulfur X X Ramsbottom Carbon Residue X X X Particulate Content X X Acid Number X X Ash Content X X Biodiesel Content X X X X Conductivity X Lubricity X Oxidation Stability X X

14. Corrosion Inhibitor (CI) (NATO S-1747) Series Testing Requirements for Specification MIL-PRF-25017

Characteristics MIL-PRF-

25017 B-1

Series B-2

Series B-3

Acid Number X X Lubricity (BOCLE) X pH of 25 % solution in water X X Water Separation (MSEP) X Flash point X X X Appearance/Workmanship X X X Ash Content X X Pour Point X X Density @ 15℃ X X X Viscosity @ 40℃ X

Page | 17

15. Gasoline, Unleaded (NATO F67) Series Testing Requirements for Specifications ASTM D4814

16. Fuel Ethanol E85 Series testing requirements for Specification ASTM D5798

Characteristics A Test

B-1 TEST B-2

TEST

B-3

TEST

C TEST

Appearance X X X X X Water X X X X Ethanol Volume X X X X Vapor Pressure X X X X Sulfur X X X Acidity X X Solvent Washed Gum X X X pH X X Unwashed Gum X X Copper X X X Inorganic Chloride X

Characteristics ASTM D4814 B-1

Series B-2

Vapor Pressure X X X Distillation X X X X Driveability Index X Lead Content X Sulfur X Copper Strip Corrosion X X X Silver Strip Corrosion X Gum Content X X X Oxidation Stability X X Vapor Liquid Ratio X Motor Octane Number (MON) X

Antiknock Index (AKI) X Research Octane Number

(RON)

Manganese Content X API Gravity or Density X X X X X Color, Visual X X X X Visual water and solids X X X X

Page | 18

17. Reclaimed Fuel Oil (FOR) Series Testing Requirements for Specifications MIL-PRF-24951

Characteristics MIL PRF 24951 B-1

Series B-2 Series B-3

Flashpoint X n/a n/a n/a Explosiveness X n/a n/a n/a Water and Sediment X n/a n/a n/a Sediment X n/a n/a n/a Density/API Gravity X n/a n/a n/a Viscosity at 40°C (ASTM D445) X n/a n/a n/a Viscosity at 50°C (ASTM D88) X n/a n/a n/a Pour Point X n/a n/a n/a Neutrality X n/a n/a n/a Sulfur Content X n/a n/a n/a Sulfated Ash X n/a n/a n/a Trace Metals: Arsenic, Cadmium, Chromium and Lead

X n/a n/a n/a

Total Halogen X n/a n/a n/a

Page | 19

Attachment 3: Approved Testing Methods Table 1: Aviation Turbine Fuels

Jet A/JA-1

(ASTM D1655)

JPTS

(MIL-DTL- 25524)

JP-8, NATO F-35,

(MIL-DTL- 83133)

JP-5

(MIL-DTL- 5624)

Appearance Visual, D4176 Visual, D6986 Visual, D6986 Visual Color (Visual)

Visual Visual Visual Visual

Density or API Gravity

D1298, IP 160,

D4052, IP 365

D1298, D4052 (referee), D7777

D1298, IP160,

D4052, D7777, IP 365

D1298, D4052 D7777

Particulate Matter

D2276, IP 216

D5452 (referee), IP 423

D2276, D5452 (referee)

D2276, D5452 D2276, D5452 (referee)

Particle Count IP 564, IP 565, IP 577, D7619

D8166, IP 564, IP

565, IP 577, D7619

D8166, IP 564,

IP 565, IP 577,

D7619

IP 564, ID 565, IP

D7619 (referee)

Total Acidity IP 354, D3242 ASTM D3242 D3242, IP 345 D3242

Aromatics IP 156, D1319, IP 436, D6379

D1319 (referee), D6379

D1319, IP 156 D1319, D6379

Total Sulfur D1266, D2622, D4294, D5453, IP 336

D1266, D2622, D3120, D4294 (referee) , D5453, D7039

D129, D1266, D2622, D3120, D4294 (referee), D5453, IP 336

D129, D1266, D2622, D3120, D4294 (referee), D5453

Mercaptan Sulfur

IP 342, D3227 D3227 D3227, IP 342 D3227

Doctor Test D4952 D4952 D4952 D4952

Distillation D86, D2887, IP 406, D7344

D7345, IP 123

D86 (referee), D2887, D7345

D86 (referee), D2887, IP 406, IP 123, D7345

D86 (referee) , D7345, D2887

Viscosity IP 71 Section 1, D445, D7042, D7945

D445 (referee), D7042, D7945

D445, D7042, D7945, IP 71

Section 1

D445

Smoke Point IP 598, D1322 D1322 IP 598, D1322 D1322

Naphthalenes D1840 D1840 D1840 D1840

Specific Energy

D3338, D4529, D4809 (referee), IP 12

D3338, D4529, D4809 (referee), D3338, D4529, D4809 (referee), IP 12

D3338, D3338M, D4529, D4809 (referee)

Hydrogen Content

D3343, D3701 D3343, D3701, D7171

D3343, D3701, D5291, D7171

D3701, D5291, D7171

Calculated Cetane Index

D4737 Procedure A

D976, D4737 D976, D4737 D976, D4737

Copper Strip Corrosion

D130, IP 154 D130 D130, IP 154 D130

Freezing Point D5972, IP 435, D7153, IP 529, D7154, IP 528, D2386, IP 16

D2386 (referee), D5972, D7153, D7154

D2386 (referee), D5972, D7153, D7154, IP 16, IP 435, IP 528, IP 529

D2386 (referee), D5972, D7153, D7154

Existent Gum D381, IP 540 D381(referee), IP

D381(referee), IP540

D381(referee), IP

Flash Point D56, D93, D3828, IP 170, IP 523

D56, D93(referee), D3828, IP170

D56, D93 (referee), D3828, IP 170

D56, D93 (referee), D3828

Page | 20

Water Reaction

N/A N/A N/A N/A

Lead Content N/A N/A N/A N/A

FSII D5006 D5006 D5006 D5006

Filtration Time

N/A N/A (Appendix A) (Appendix A), D2276, D5452 ( referee)

MSEP D3948 D3948,

D7224 (referee)

D3948, D7224 (referee, if fully additized)

D3948, D7224 (referee)

Electrical Conductivity

D2624, IP 274 D2624 D2624, IP 274 D2624

Thermal Stability

D3241 (Annex A3, referee)

D3241 (Annex A3 is referee)

D3241 (Annex A3, referee), IP

D3241 (Annex A3, referee)

Color (Saybolt)

D156 D156 (referee), D6045

D156 (referee), D6045

D156 (referee), D6045

Peroxide Number

N/A N/A N/A N/A

FAME D7797, IP 583,

IP 585 (referee), IP 590, IP 599

N/A D7797, IP 583,

IP 585 (referee), IP 590, IP 599

D7797, IP 583, IP

(referee), IP 590, IP

Lubricity D5001 N/A N/A N/A

Page | 21

Table 2: Marine Diesel

F-76 (MIL-DTL-16884)

Appearance D4176 Color (Visual) D1500 (referee), D6045 Density or API Gravity D1298 (referee), D4052, D287, D7777 Distillation D86 (referee), D2887 Flash Point D93(referee), D6450, D3828 Carbon Residue D524(referee), D189, D4530 Cloud Point D2500(referee), D5771, D5772, D5773 Pour point D97(referee), D5949, D5950, D5985 Copper Strip Corrosion D130 Viscosity D445, D7042 Water and Sediment D2709 Particulate D6217 Storage Stability D5304 (referee), D2274 Sulfur D5453(referee), D1266, D2622, D3120, D7039 Fatty Acid Methyl Ester (FAME) BS EN 14078, IP579, D7963 Lubricity D6079 (referee), D7688 Demulsification D1401 Particulate Contamination D6217 (referee), D5452 Acid Number D974 (referee), D664 Ash D482 Aromatics D6591 (referee), D2425 Hydrogen Content D7171 (referee), D4808, D5291 Ignition Quality (Cetane Number, Cetane Index or Derived Cetane Number)

D613 (referee), D976, D6890, D7170

Trace Metals (Ca, Pb, Na, K and V) D7111 (referee), D3605

Table 3: Fuel System Icing Inhibitor

MIL-DTL-85470

Appearance Visual Acid Number D1613 Color, Platinum Cobalt D1209 (referee), E450 Distillation D1078 Ethylene Glycol Per specification pH of 25% solution in water E70 Relative Density D891 (referee), D4052 Water (mass%) D1364 (referee), E1064, E203 Flash Point D93 (referee), D56, D3828

Page | 22

Table 4: Marine Residual Fuel Oil (RME180/380)

ISO 8217

Kinematic Viscosity ISO 3104 Density ISO 3675, ISO 12185 Calculated Carbon Aromaticity Index

(CCAI)

Specification

Sulfur ISO 8754, ISO 14596, D4264 Flash Point ISO 2719 Hydrogen Sulfide IP570 Acid Number D664 Total Sediment, aged ISO 10307-2 Carbon Residue ISO 10370 Pour Point ISO 3016 Water ISO 3733 Ash ISO 6245 Vanadium IP 501 (referee), IP 470, ISO 14597 Sodium IP 501 (referee), IP 470 Aluminum plus silicon IP 501 (referee), IP 470, ISO 10478 Used lubricating Oil (ULO) IP 501 (referee), IP 470, IP 500 Cetane Index ISO 4264

Table 5: Lubrication Oil (LTL) (NATO O-250)

MIL-PRF-17331

Sulfur D129, D1552, D2622, D4927, D4951, D6443, D6481, D7751

Acid Number D974 (referee), ASTM D664 Corrosion D665, Procedure B Corrosion, Copper Strip D130 Water Content D6304 (referee), ASTM D7546 API Gravity D287, D1298 (referee), D4052 Flash Point D92, D93 (referee) Pour Point D97 (referee), D5950, D5949 Viscosity @ 4.4°C D445 (referee), D7042 Viscosity @100°C D445 (referee), D7042 Viscosity @40°C D445 (referee), D7042 Emulsion Test D1401 Total Sludge, iron and copper D4310 Foam test D892 Cleanliness (Solid Particle Contamination)

D4898

Neutralization number (acid/base) D974 Appearance (to include visual sediment & water)

Visual

Page | 23

Table 6: Lubrication Oil (LO6) (NATO O-278)

MIL-PRF-9000

Appearance/Workmanship Visual Flash point D92 Foam (stability only) D892 Gravity D287, D1298, D4052 Calcium D4628, D4927, D4951, D6443, D6481

Magnesium D4628, D4927, D4951, D6443 Zinc D4638, D4927, D4951, D6443, D6481 Phosphorus D1091, D4047, D4927, D4951, D6443, D6481 Pour Point D97, D5949, D5950 Sulfur D129, D1552, D2622, D4927, D4951, D6443, D6481 Total base number D2896 Viscosity index D2270 Viscosity at 100°C D445 Viscosity at 40°C D445 Ash, sulfated D874 Corrosion, copper strip D130

Table 7: Diesel Fuel Oil

ASTM D975

Flash point D93 Water and Sediment D2709, D1796 Distillation D86 Kinematic Viscosity D445 Ash D482 Sulfur D2622, D5453 Copper strip corrosion D130 Cetane number D613 Cetane index D976 Aromaticity D1319 Cloud Point D2500

LTFT/CFPP D4539, D6371

Carbon Residue D524 Lubricity D6079, D7688 Conductivity D2624 D4308 Appearance/Workmanship Visual

Table 8: Reclaimed Fuel Oil (FOR)

MIL-PRF-24951

Flashpoint D93 Explosiveness FED-STD-791 Test Method 1151.1 Water and Sediment D1796 Sediment D473 API Gravity or Density at 60°C D287 Viscosity at 40°C D445 Viscosity at 50°C D88 Pour Point D97 Neutrality FED-STD-791 Test Method 5101 Sulfur Content D129 Ash D482 Trace Metals: Arsenic, Cadmium, Chromium and Lead

EPA SW-846, Method 3040/3050 and proposed method for evaluating solid waste

Total Halogen D808-87

Page | 24

Table 9: Diesel Fuel Oil, Biodiesel blends B6-B20 Appearance Visual Acid Number D664 Flash Point D93 (referee) D3828, D56 Cloud Point D2500 (referee), D7397, D5771, D5772, D5773 Cold Filter Plugging Point D6371 Low Temperature Flow Test D4539 Water and Sediment D2709 Carbon Residue D524 Ash D482 Distillation D86 Viscosity D445 Sulfur Content D5453 Cetane Number D613 Cetane Index/Aromaticity D1319 Biodiesel Content D7371 Conductivity D2624/D4308 Lubricity D6079 Oxidation Stability D15751

Table 10: Corrosion Inhibitor

MIL-PRF-25017

Appearance/Workmanship Visual Acid Number ASTM D664 Lubricity (BOCLE) ASTM D5001 pH ASTM D664 Water Separation (MSEP) ASTM D3948 Flash point ASTM D56; ASTM D93 Ash Content ASTM D482 Pour Point ASTM D97; ASTM D5949; ASTM D5950; ASTM

D5985 Density @ 15℃ ASTM D1298; ASTM D4052; pycnometer Viscosity @ 40℃ ASTM D445

Table 11: Motor Gasoline

ASTM D4814

Appearance Visual Vapor Pressure D4953, D5191, D5482 or D6378 Density or API Gravity Distillation D86, D7345 Driveability Index specification Lead Content D3237 D5059 Sulfur D1266, D2622, D3120, D5453, D6920, D7039 Silver Strip Corrosion D7667, D7671 Copper Strip Corrosion D130 Gum Content D381 Oxidation Stability D525 Vapor Liquid Ratio D5188 Motor Octane Number (MON) D2700 Antiknock Index specification Research Octane Number (RON) D2699 Manganese Content D3831 Color Visual Visual Water and Solids D4176

Page | 25

Table 12: Aviation Gasoline (AVGAS) Leaded AvGas

ASTM D910

Appearance Visual Color (Visual) Visual Density or API Gravity D1298, IP160, D4052 Distillation D86 Copper Strip Corrosion D130 Existent Gum D381 Vapor Pressure D323, D5191 Lead Content D3341, D5059 Potential Gum D873 Lean Mixture Octane Number (MON) D2700 Rich Mixture Octane Number (RON) D909 Performance Number D909 Sulfur Content D1266, D2622 D5453 Dye Content D2392 Color (Lovibond) IP569 Specific Energy (Net Heat of Combustion)

D4529, D3338 Freezing Point D2386 Conductivity D2624 Oxidation Stability D873 Oxidation Stability (Potential Gum) D873 Oxidation Stability (Lead Precipitate) D873 Water Reaction D1094

Table 13: Fuel Ethanl E85 Series testing requirements for Specification ASTM D5798

ASTM D5798

Appearance Visual Vapor Pressure D4953, D5190, D5191 Ethanol Content D5501 Acidity D1613, D7795 pHe D6123 Gum Content D381 Inorganic Chloride Content D7319, D7328 Water Content E203 Copper Content D1688 Sulfur Content D5453 Oxidation Stability D525 Inorganic Chloride content D7319, D7328