Attachment 1 - SOW CONUS LAB.pdf

Statement of Work for

Contracted Laboratory Services

CONUS

17 May 2021

Contents C-1.0 General Description:

C-1.0.1 Service Locations: When ordered, C-1.1 Facilities:

C-1.2 Specifications, Standards and Handbooks:

C-1.3 Scheduling of Services:

C-2.0 Contract Deliverables:

C-2.1 Contract Compliance Plan:

C-2.2 Laboratory Test Reports:

C-2.3 Contract Contingency Plan:

C-2.4 Contract Training Plan:

C-2.5 Safety Plan:

C-2.6 Transportation Plan:

C-2.7 Laboratory Equipment Plan:

C-2.8 Monthly Reporting:

C-3.0 Laboratory Requirements:

C-3.1 Operating Hours:

C-3.2 Staffing:

C-3.3 Knowledge and Skills:

C-3.4 Access:

C-3.5 Equipment Calibration:

C-3.6 Epoxy Lined Sample Cans:

C-3.7 Ellipsometric Tube Deposit Rater (ETR):

C-3.8 Turn-around Times:

C-3.8.1 Baltimore, MD Area:

C-3.8.2 Selby, CA Area:

C-3.8.3 Houston, TX Area:

C-3.9 Retain samples:

C-4.0 Transportation Performance Requirements:

C-5.0 Secured Fuels Performance Requirements:

C-6.0 Surveyor Duties:

C-6.1.1 Third party witness:

C-6.1.2 Sampling of petroleum products:

C-6.1.3 Gauging of petroleum products:

C-6.1.4 Cargo Inspection of petroleum products:

C-7.0 Sample Shipment:

Attachment 1: Products Attachment 2: Series Testing Requirements Attachment 3: Approved Testing Methods

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C-1.0 General Description: This Statement of Work (SOW) provides the requirements for laboratory testing services in multiple locations throughout the Continental U.S. (CONUS) region. The Contractor will be responsible for the laboratory testing of government-owned petroleum products in accordance with the specifications as described herein, and transportation of samples from contracted locations to the contractor’s laboratory. Government-owned products mentioned in this SOW may be shipped to the Contractor’s laboratory for testing.

C-1.0.1 Service Locations: When ordered, the contractor shall be able to provide services required in this SOW to DLA Energy in each of the locations listed below. Contractor facilities must be located within the CONUS region and meet the required turn-around times listed in paragraph C-3.8.

Americas East Locations Helena, AL Columbus,GA NY Harbor Area Montgomery, AL Chicago, IL Coraopolis, PA Moundville, AL Baton Rouge, LA Charleston, SC Jacksonville, AR Boston, MA Rapid City, SD Port Mahon, DE Portland, ME Dallas, TX Port Everglades, FL Anacostia, MD Houston, TX Key West, FL Andrews AFB, MD Craney Island, VA Jacksonville, FL Baltimore, MD Norfolk, VA Tampa, FL Lockhart, MS Yorktown, VA Macon, GA Selma, NC Bremen, GA Jacksonville, NJ

Americas West Locations Carson, CA Moffett Field, CA Alamogordo, NM Colton, CA McClellan, Park, CA Las Vegas, NV NAS Lemoore, CA Selby, CA Salt Lake City, UT NAS Point Loma, CA Denver, CO Puget Sound, WA

C-1.1 Facilities: The contractor shall have facilities that meet the required turn-around times in section C-3.8. The contractor shall provide the location(s) of the facility where the product shall be tested, facility testing capabilities and contact information.

C-1.2 Specifications, Standards and Handbooks: At each laboratory, the contractor shall retain a copy of all required specifications, standards, test methods, handbooks, etc., per this SOW and perform services in accordance with testing requirements. Military Specifications referenced in Attachment 1 for petroleum product types can be obtained at http://quicksearch.dla.mil or https://assist.dla.mil but can also be requested in writing to the Contracting Officer (CO) or Contracting Officer’s Representative (COR).

C-1.3 Scheduling of Services: After the CO authorizes a task order, the COR or QAR will contact the laboratory to schedule the testing. The contractor shall not perform services under this SOW without a task order or direct authorization from the CO. If a task order was not received, the contractor shall contact the CO or COR prior to any testing. Only the CO can formally, either in writing or verbally, authorize testing and create an obligation.

C-2.0 Contract Deliverables: All plans shall be submitted to the CO for review and acceptance as a part of the technical proposal as documented in the solicitation. Plans shall be kept current for the life of the contract. The government reserves the right to request changes or modifications to any detailed plans at any time throughout the contract performance period. Plans shall be made available for Government review upon request at any time during the contract performance period.

C-2.1 Contract Compliance Plan: The contractor is responsible for compliance with all contract performance requirements. The contractor is responsible for all actions taken by any sub-contractor utilized under this contract. The contractor shall be ISO 9001 and/or ISO/IEC 17025 certified.

C-2.2 Laboratory Test Reports: The contractor shall maintain records evidencing all analysis performed under this contract. All samples tested shall be documented with a detailed report. Reports shall be complete and legible containing

Page | 2 information pertaining but not limited to: Lab Name, Test Method, Test Name, Test Results, Test Units, Test Limits.

Reports not containing the appropriate information will need to be corrected and resubmitted by the contractor for approval.

C-2.3 Contract Contingency Plan: The Contract Contingency Plan shall outline contractor actions to ensure there is no significant interruption of services resulting from labor disputes, catastrophic failure of equipment, or the effects of natural disasters/emergencies. The plan shall provide specific details regarding labor issues that may result from potential strike actions, world events, world actions, military contingency and war time manning requirements.

C-2.4 Contract Training Plan: The contractor shall provide a detailed plan that identifies employee training requirements and procedures necessary to maintain proficiency. The plan shall identify length of training, training sources and a brief description of courses such as safety, environmental protection and job qualification training. The contractor is responsible for ensuring all individual training requirements are accomplished. The contractor must demonstrate current participation in a proficiency program or suitable means to verify laboratory performance.

C-2.5 Safety Plan: The contractor shall provide a detailed plan outlining the policy, procedures and actions necessary to maintain a safe working environment for employees and visitors. The plan shall cover the products stored, handled, Safety Data Sheets (SDS) and guidelines regarding the safe handling of such products and shall be maintained and updated over the course of the contract.

C-2.6 Transportation Plan: The contractor is required to submit a plan for review to transport the petroleum samples to an approved laboratory for testing or shipping (contractor supplied transport, third party delivery service, etc.) and how they plan on tracking the chain of custody to the contractor’s facility. Product quality must be preserved and not altered by shipment. DLA Energy or it’s subcontractor(s) do not have the ability or certification to ship or package fuel samples.

C-2.7 Laboratory Equipment Plan: The contractor will furnish, and update annually, to the CO and COR the status by name, model and serviceability of all equipment used in laboratory testing. Equipment that malfunctions or is non-serviceable shall be reported to the CO and COR within 48 hours with a mitigation plan to provide testing capability.

C-2.8 Monthly Reporting: The contractor shall provide a monthly written report to the CO and COR with the number of laboratory tests performed, what testing was included and the location.

C-3.0 Laboratory Requirements: The below are general requirements for all contractor laboratories. Laboratories are required to have the listed referee test methods which is referenced in the product specifications and international test methods (ASTM, EI, etc.).

C-3.1 Operating Hours: The contractor shall be responsible for adjusting hours of operation to meet workload demands and turn-around times in section C-3.8.

C-3.2 Staffing: The contractor shall provide sufficient staffing to accomplish all functions and tasks to include simultaneous operations of performing multiple tests at a time, and provide the contact information for laboratory manager or assistant laboratory manager if the laboratory is not manned 24 hours, seven days a week.

C-3.3 Knowledge and Skills: The contractor shall ensure that personnel assigned to all tasks have the requisite knowledge and skills to meet the performance standards and comply with all applicable federal laws, state laws, regulations, and codes. All supervisors and key employees shall be able to read and understand English so they can understand and follow oral or written instructions directions, directives, regulations, and operating procedures. All supervisors and contractor key employees shall be capable of writing in English to compose the required detailed reports.

C-3.4 Access: The contractor shall allow DLA Energy representatives to witness testing or sampling. It shall provide the applicable information for access, provide follow-up to obtain access (for personnel and vehicles) to all facilities that product is tested or sampled. For areas that require special admission the contractor will assist gaining access.

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C-3.5 Equipment Calibration: The laboratories shall have a system of calibration equivalent to ISO/IEC 17025.

All testing shall be performed in accordance with the appropriate international or local test methods approved for use by DLA Energy and listed in this SOW.

C-3.6 Epoxy Lined Sample Cans: The contractor shall maintain a supply of 10 unused epoxy lined fuel sample shipping containers to be provided to DLA Energy personnel per request. Sample containers shall be stored to ensure they are clean and free from all substances that might contaminate the product being sampled. Containers must meet the following specifics: Complies with ASTM D-4306, height not to exceed 9 inches, diameter not to exceed 7 inches, capacity 1 USG, Bung Plug ¾” with lock-wire hole, carrying handle able to be shipped as hazardous material.

C-3.7 Ellipsometric Tube Deposit Rater (ETR): The contractor shall perform ASTM D3241 Annex 3 ETR within the testing turn-around times in section C-3.8 Sample Testing Turnaround Times. ETR is the preferred method and shall be treated as the referee method.

C-3.8 Turn-around Times: The contractor shall perform testing in accordance with the turn-around times listed in the table below. Turn-around time starts when the contractor is notified that the sample is prepared for transportation from sample location to the servicing laboratory. Turn-around time ends when testing results are completed and delivered to DLA Energy. DLA-Energy will give the contractor at least 12 hours of advance notice ofthe sample being prepared for shipment (turn-around time start) (prime contractor is responsible for any sub-contractor actions). The 12 hours of advance notice is not included in the turn-around time. If testing cannot be completed within the turn-around time the contractor will immediately notify the CO and COR. The contractor shall specify the problem and the estimated completion date and time. If there is a need for an expedited test, it will be a maximum turn-around time of 18 hours unless otherwise stated in C-3.8.1, C-3.8.2, or C-3.8.3.

C-3.8.1 Baltimore, MD Area: Mission requirements dictate a turn-around time for Jet A petroleum sample(s) to be tested at this location. Jet A sample results must be received within 16 hours. The 16-hour turn-around starts when the sample is prepared for transportation at the location and the contractor is notified for sample pickup. DLA Energy will provide the contractor an initial forecast then a 24-hour notification prior to sample collection as times can be adjusted by weather, berthing space or ullage.

C-3.8.2 Selby, CA Area: Mission requirements dictate a turn-around time for Jet A and F-76 petroleum sample(s) to be tested at this location. Sample results for Jet A shall be received within 8 hours and for F-76 must be received within 24 hours unless otherwise coordinated with the QAR. DLA Energy will provide the contractor an initial forecast and notification of 24-hours prior to sample collection as times can be adjusted by weather, berthing space or ullage. The turn-around starts when the sample is prepared for transportation at the storage location and the contractor is notified for sample pickup.

C-3.8.3 Houston, TX Area: Mission requirements dictate a turn-around time for Jet-A petroleum sample(s) to be tested at this location. When an expedited Jet-A request is made, sample results shall be received within 8 hours unless otherwise coordinated with the QAR. DLA Energy will provide the contractor an initial forecast and notification 12 hours prior to sample collection as times can be adjusted by weather, berthing space or ullage. The turn-around time starts when the sample is prepared for transportation at the storage location and the contractor is notified for sample pickup.

C-3.9 Retain samples: After analysis, the contractor shall retain samples for a minimum of 45 days. In the event of a suspected quality issue or dispute, a longer sample retention period may be requested by DLA Energy. The contractor

Maximum Turn-around Hours Chart A Series 48 hours B Series 36 hours C Series 24 hours

Individual tests 24 hours Expedite 18 hours

Secured Fuel Performance 8 hours

Page | 4 shall be responsible for disposal of excess fuel samples and sample containers.

C-4.0 Transportation Performance Requirements: The contractor shall be responsible for packing and transporting all petroleum samples from a job site to the laboratory in accordance with federal and laws and regulations. When requested by DLA Energy personnel, the contractor shall be able to provide an epoxy line sample can, detailed in C-3.6 for replacement. When sample transportation is not required of the contractor, they shall be notified in advance.

C-5.0 Secured Fuels Performance Requirements: Due to mission demands DLA Energy shall request petroleum testing under Attachment 2 from MIL-STD-3004-1 table XII. DLA-Energy will provide the contractor with as much advance notice as possible as the turn-around time shall not exceed 8 hours after receipt of sample at the laboratory.

Specifics/logistics shall be scheduled by the QAR after a task order for the secured fuels testing services is issued.

C-6.0 Surveyor Duties: When ordered, the contractor shall represent DLA Energy to ensure all specifications, regulations, ASTM, API MPMS are followed when a DLA Energy representative is not available at locations mentioned in C-1.0.1. Personnel shall be International Federation of Inspection Agencies or TIC council or equivalent certified to perform the duties defined in the following subparagraphs.

C-6.1.1 Third party witness: When ordered, the contractor shall act as a third party witness to observe operations and report findings to the DLA Energy point of contact with a detailed report within 24 hours. DLA Energy will provide written instructions specific to the operations and objectives in the task order. The following are examples of operations commonly preformed: Tank to tank transfers, off-loading vessels, barges, tank trucks, containers, loading vessels, barges, tank trucks, containers.

C-6.1.2 Sampling of petroleum products: When ordered, the contractor shall be capablity of performing sampling of pipelines, vessels, barges, tank trucks, storage tanks, or any containers that may hold fuel in accordance with API MPMS and/or ASTM D4057, when requested. The contractor shall supply all equipment and material needed to perform tasks.

C-6.1.3 Gauging of petroleum products: When ordered, the contractor shall be capable of performing gauging of vessels (to include bunkers), barges, tank trucks, storage tanks, or any containers that may hold fuel. The Contractor shall supply all equipment and material need to perform task.

C-6.1.4 Cargo Inspection of petroleum products: When ordered, the contractor shall oversee operations to include:

Gauging, Sampling, Atmospheric Measuring, Tank cleanliness, Lightering transfers, and complete certified detailed reports within 24 hours. The Contractor shall supply all equipment and material needed to perform tasks.

Note: The contractor will have the authority to stop any operations that are thought to be unsafe but must immediately contact the POC named on the Task Order to explain why.

C-7.0 Sample Shipment: The contractor shall, upon request, be responsible for shipping fuel samples from locations in C-1.0.1 to the laboratories in the chart below. Fuel samples shall be shipped within 48 hours of request and arrive to the below laboratory within five calendar days.

Naval Air Systems Command HAZMART Bldg. 2385 22680 Hammond Road Patuxent River, MD 20670

US ARMY TARDEC

Petroleum Laboratory Bldg. 5085 U Avenue, Bldg 85 New Cumberland, PA 17070-

Aerospace Fuels Laboratory AFPA/PTPLA 2430 C Street, Bldg 70, Area B Wright Patterson AFB OH 45433-

Naval Research Laboratory 4555 Overlook Avenue, SW Washington, DC 20375

Southwest Research Institute 6220 Culebra Rd San Antonio, TX 78238-5166

Air Force Research Laboratory AFRL 2977 Hobson Way

WPAFB, OH 45433

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Attachment 1: Products Specifications shall dictate the testing required and the contractor shall develop a plan based on product specifications (A level testing) and MIL-STD-3004-1 (B-1, B-2, B-3, C test). MIL-STD_3004-1 describes products to be tested, types of testing required and additional information as required. All referenced material can be obtained at http://quicksearch.dla.mil/, https://assist.dla.mil/, or by contacting the CO, COR, or QAR.

Jet Fuels Aviation Turbine Fuel, Grade JET A (Specification: ASTM D1655 latest version) and JET A-1, NATO F-35 (DEF Stan 91-091 latest version) Aviation Turbine Fuel, Kerosene Types, Grade JP-8 NATO F-34 (Specification: MIL-DTL-83133, latest version) Aviation Turbine Fuel, Grade JP-5 NATO F-44 (Specification: MIL-DTL-5624, latest version) Aviation Turbine Fuel, Thermally Stable, Grade JPTS (Specification: MIL-DTL-25524 latest version)

Aviation Turbine Fuel, Grade JP-4 NATO F-40 (Specification: MIL-DTL-5624, latest version) Aviation, Gasoline, NATO F-18 ASTM D910. Unleaded Specification: ASTM D7547, latest version)

Diesel Fuels Diesel Fuel, Navy Distillate NATO F-76 (Specification: MIL-DTL-16884, latest versions) Diesel Fuel Oil, Grades: Ultra-low sulfur No.1 & No. 2, Low Sulfur No.1 & No. 2 (Specification: ASTM D975, latest version) Diesel Fuel Oil, Biodiesel blends B6-B20 (Specification: ASTM D7467 latest version)

Marine Residual Fuel Oil Grade (RME-180, RMG-380, MGO) (Specification: ISO 8217 latest version) Diesel Fuel Oil (Specification: ASTM D975, latest version)

Unleaded Fuels Fuel, Automotive Spark Ignition Engine Grades (Specification: ASTM D4814, latest version) Unleaded Gasohol, (Midgrade, Premium, Regular) Specification: ASTM D4814, (latest version) Fuel Ethanol (E85) for Automotive Spark-Ignition Engines (Specification ASTM D5798 latest version) Additives Fuel System Icing Inhibitor, High Flash (FSII) (Specification: MIL-DTL-85470 latest version) Corrosion Inhibitor (CI) (Specification: MIL-PRF-25017 latest version) Lube Oils Lubrication Oil, Steam Turbine and Gear (LTL) MIL Symbol 2190 (Specification: MIL-PRF-17331 latest version) Lubrication Oil, LO6, MIL Symbol 9250, Shipboard Internal Combustion, High Output Diesel (Specification:

MIL-PRF-6081 latest version) Lubrication Oil, LA7, (Specification: SAE J 1966 latest version) Fuel Oil Fuel Oil Reclaimed (FOR) (specification: MIL-PRF-24951 latest version) http://quicksearch.dla.mil/ https://assist.dla.mil/

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Attachment 2: Series Testing Requirements The list below provides tests by name and methods that shall be required to be performed on petroleum products at the contractor’s laboratory in accordance with product specifications MIL-STD-3004-1, specifications, and authorized test methods. The contractor must refer to paragraph C-2.4 for instructions on how to incorporate and indicate if they cannot perform authorized method or submit a formal exception request to the DLA Energy CO for acceptance. Tests shall be requested by series or individually by a DLA Energy representative as situation warrants.

1. A Series (Specification testing in accordance with Attachment 1 and MIL-STD-3004-1)

2. B-1 Series (MIL-STD-3004-1 list tests required in group)

3. B-2 Series (MIL-STD-3004-1 list tests required in group)

4. B-3Series (MIL-STD-3004-1 list tests required in group)

5. C Series (MIL-STD-3004-1 list tests required in group)

Individual Tests: Individual tests may be requested from any test included in the A, B or C series or from the tables below.

Note: Tests are grouped by physical or chemical property and do not imply equivalency. Verify that the test is appropriate to the product specification prior to analysis.

1. Secured fuel Series Testing Requirements for Aviation fuel.

Page | 7

2. Jet A & Jet A-1 (NATO F35) Series Testing Requirements for Specifications ASTM D1655 and Def Stan 91-

A Series Characteristics ASTM D1655 Def Stan

91-091 B-1

Series B-2

Series B-3 Series C-Series

Appearance/Workmanship X X X X X X Color (Visual) X X X X X X Particulate Contamination/Particulate Matter

X X X X X

Particle Count (Particulate)

X

Total Acidity X X X Aromatics X X Total Sulfur X X Mercaptan Sulfur X X Doctor Test X X Distillation X X X X X Flash Point X X X X X X API Gravity or Density at 15°C

X X X X X X

Freezing Point X X X X X Viscosity at minus 20°C X X Smoke Point X X Naphthalenes X X Specific Energy (Net Heat of Combustion)

X X

Copper Strip X X X X X Thermal Stability X X X X Existent Gum X X X X X Microseparometer X X X X X Electrical Conductivity X X X X X Lubricity X Color, Saybolt X X Particulate Contamination/Particulate Matter with Filtration Time

X X X X X

Fuel System Icing Inhibitor X X X X X

FAME X X X X X

Water Reaction Sulfides in Bottom Water

Page | 8

3. JP8 (NATO F34) Series Testing Requirements for Specifications MIL DTL 83133

Characteristics MIL DTL

83133 B-1

Series B-2

Appearance/Workmanship X X X X X Color (Visual) X X X X X Particulate Contamination/Particulate Matter

X X X X

Particle Count X Total Acidity X X Aromatics X Total Sulfur X Mercaptan Sulfur X Doctor Test X Distillation X X X X Flash Point X X X X X API Gravity or Density at 15°C X X X X X Freezing Point X X X X Viscosity at minus 20°C X Specific Energy (Net Heat of Combustion)

X

Copper Strip X X X X Thermal Stability X X X Existent Gum X X X X Microseparometer X X X X Electrical Conductivity X X X X Lubricity Colour, Saybolt X X Particulate Contamination/Particulate Matter with Filtration Time

X X X X

Fuel System Icing Inhibitor X X X X

FAME X X X X

Hydrogen Content X Cetane Index, Calculated X

Page | 9

4. JP5 (NATO F44) Series Testing Requirements for Specifications MIL DTL 5624

Characteristics MIL DTL

B-1

B-2 Series B-3 Series C- Series

Color (Visual) X X X X X Particulate Contamination/ Particulate Matter

X X X X

Particle Count X Total Acidity X X Aromatics X Total Sulfur X Mercaptan Sulfur X Doctor Test X Distillation X X X X Flash Point X X X X X API or Density at 15° C X X X X X Vapor Pressure X Freezing Point X X X X Viscosity at minus 20°C X Smoke Point X Naphthalenes X Specific Energy (Net Heat of Combustion)

X

Copper Strip X X X X Thermal Stability X X X Existent Gum X X X X Microseparometer X Electrical Conductivity X Colour, Saybolt X X Particulate Contamination/Particulate Matter with Filtration Time

X X X X

Fuel System Icing Inhibitor X X X X

FAME X X X X

Hydrogen Content X Cetane Index, Calculated X

Page | 10

5. F-76 Series Testing Requirements for Specifications MIL-DTL-16884

6. Fuel System Icing Inhibitor (FSII) (NATO S-1745) Series Testing Requirements for Specifications MIL-

DTL-85470

Characteristics MIL F

16884 B-1

Series B-2

Demulsification X API Gravity or Density at 15°C X X X X X Distillation X X X Cloud Point X X Color X X X X X Flashpoint X X X X X Particulate Contamination X X X Pour Point X X Viscosity at 40°C X X Acid Number X Ash X Aromatics X Carbon Residue X X X Copper Strip Corrosion X X Hydrogen Content X Ignition Quality (Cetane Number, Cetane Index, or Derived Cetane Number)

X X

Storage Stability X X Sulfur Content X X X Trace Metals (Ca, Pb, Na, K and V) X Lubricity X X X Water and Sediment X X X X

FAME X X X X

A Series Characteristics MIL DTL 85470 B-1

Series B-2

Acid Number X X Color, Platinum Cobalt X Distillation X X Ethylene Glycol X X pH of 25 % solution in water X X Relative density X X X Water (mass %) X X Flash point X X Appearance/Workmanship X X X

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7. Marine Residual Fuel Oil (RME 180/380) Series Testing Requirements for Specification ISO 8217

8. Lubrication Oil (LTL) (NATO O-250) Series Testing Requirements for Specification MIL PRF 17331

Characteristics ISO 8217 B-1

Series B-2

Series B-3

C-Series

Kinematic Viscosity at 50°C X X X X X Density at 15°C X X X X X Calculated Carbon Aromaticity Index

X X

Sulfur X X Flash point X X X X X Hydrogen sulfide X X Acid Number X X Total Sediment aged X X X Carbon Residue X X X Pour Point X X Water X X X Ash X X Vanadium X Sodium X X Aluminum plus silicon X Used lubricating oils X

A Series Characteristics MIL PRF

17331 B-1

Series B-2

Series B-3

Sulfur X n/a Acid Number X n/a Corrosion X X n/a Corrosion, Copper Strip X n/a Water content, mass% X X X n/a X Gravity X X n/a X Flash point X X X n/a Pour Point X X n/a Viscosity @ 4.4°C X X n/a Viscosity @100°C X X X n/a Viscosity @ 40°C X X X n/a X Emulsion test X X X n/a Total sludge, iron and copper (not required) n/a

Foam Test X X X n/a Cleanliness (Solid Particle Contamination)

X X X n/a

Neutralization number (acid/base) X X n/a Appearance (to include visual sediment & water)

X X n/a X

Solid contaminants X X X n/a

Page | 12

9. Lubrication Oil (LO6) (NATO O-278) Series Testing Requirements for Specification MIL PRF 9000

Characteristics MIL PRF 9000 B-1

Series B-2

Series B-3

Series C-Series n/a Appearance/Workmanship X X X X Flash point X X X n/a Foam (stability only) X X X n/a Gravity X X n/a X Metals/Elements:Calcium, Magnesium, Zinc, Phosphorus

X n/a

Pour Point X X n/a Sulfur X n/a Total base number X n/a Viscosity index X n/a Viscosity at 100°C X X X n/a Viscosity at 40°C X n/a Neutralization number (acid/base) X X n/a Solid contaminants X X n/a Emulsion test X X n/a Water (by centrifuge) X X n/a X Ash, sulfated X X X

Page | 13

10. Diesel Fuel Oil (NATO F54) Series Testing Requirements for Specifications ASTM D975, EN 590

Characteristics ASTM

D975

EN 590 B-1

Series B-2

Series B-3

Flash point X X X X X X Water and Sediment X X Distillation X X X X Kinematic Viscosity X X Ash X X Sulfur X X X X Copper strip corrosion X X X Cetane number X X Cetane index X X X Aromaticity X Cloud Point X X X

LTFT/CFPP X X

Ramsbottom Carbon Residue

X X

Lubricity X X Conductivity X API Gravity or Density at 15°C

X X X X X X

Polycyclic aromatic hydrocarbons

X

Manganese content X Water Content X Total Contamination X

FAME X

Oxidation stability X Appearance/Workmanship X X X X X X Pour Point (not required) X Color Visual

Page | 14

11. Corrosion Inhibitor/Lubricity Inhibitor (CI/LI) (NATA S-1747) Series Testing Requirements for Specification MIL-PRF-25017

12. Gasoline, Unleaded (NATO F67) Series Testing Requirements for Specifications ASTM D4814, EN 228

Characteristics MIL-PRF-

25017 B-1

Series B-2

Series B-3

Acid Number X X Solubility X Rust X Lubricity (BOCLE) X pH of 25 % solution in water

X X

Water Separation (MSEP) X Flash point X X X Appearance/Workmanship X X X Ash Content X X Pour Point X X Density @ 15℃ X X X Viscosity @ 40℃ X Electrical Conductivity X Storage Stability X Fuel Injection Fouling X Emulsification Tendency X Accelerated Stability X Metals X

A Series Characteristics ASTM

D4814

EN 228 B-1

Series B-2

Series B-3

Appearance/Workmanship X X X X X X Vapor Pressure X X X X Distillation X X X X X Driveability Index X Lead Content X X Sulfur X X Copper Strip Corrosion X X X X Silver Strip Corrosion X Gum Content X X X X Oxidation Stability X X X Vapor Liquid Ratio X Motor Octane Number

(MON)

X X

Antiknock Index (AKI) X Research Octane Number

(RON)

X

Manganese Content X X Hydrocarbon type content:

olefins and aromatics

X

Benzene content X Oxygen content X Oxygenates content X

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Vapor Lock Index X X API Gravity or Density X X X X X X Color, Visual X X X X Visual water and solids X X X X

Page | 16

Attachment 3: Approved Testing Methods Table 1: Aviation Turbine Fuels

Def Stan 91-

Jet A/A-1

(ASTM

D1655)

JP-8 (MIL-DTL-

83133)

JP-5 (MIL-

DTL-

5624)

Appearance Visual Visual Visual

ASTM D6986

Visual

Color (Visual) Visual Visual Visual Visual Density or API

Gravity

IP365,

D4052

D1298, IP 160,

D4052, IP

D1298, IP160, D4052

(referee), IP 365, D7777

D1298, D4052, D7777

Particulate Matter

IP 423,

D5452, IP 216, D2276,

IP 423, D5452

(referee)

D2276, D5452 (referee), IP

D2276, D5452 (referee)

Particle Count

IP 564, IP 565,

IP 577

IP 564, IP 565, IP

577, D7619

D8166, IP 564, IP

565, IP 577

D7619 (referee)

D8166, IP 564,

IP 565, IP 577

D7619 (referee)

Total Acidity IP 354, D3242 IP 354, D3242 IP 354, D3242 D3242

Aromatics IP 156, D1319, IP 436, D6379

IP 156, D1319, IP

436, D6379

IP 156, D1319

(referee), IP 436, D6379

D1319 (referee), D6379

Total Sulfur IP 336 D1266 D2622, D4294, D5453, IP

D129, D1266, D2622, D3120, D4294 (referee) , D5453, or IP

D129, D1266, D2622, D3120, D4264 (referee), D5453

Mercaptan Sulfur

IP 342, D3227 IP 342, D3227 IP 342, D3227

(referee)

D3227

Doctor Test IP 30 D4952 D4952 D4952

Distillation IP 123, D86 D86, D2887, IP 406, D7344, D7345, IP

D86 (referee), D2887, IP 406, IP 123, D7345

D86 (referee) , D7345, D2887

Viscosity IP 71, D445 IP 71 Section 1, D445, D7042, D7945

IP 71 Section 1, D445 (referee), D7042, D7945

D445

Smoke Point IP 598, D1322 IP 598, D1322 IP 598, D1322 D1322

Naphthalenes D1840 D1840 D1840 D1840

Specific Energy

D3338, D4809 (referee), IP

12, IP 355

D3338, D4529, D4809 (referee), IP 12

D3338, D4529, D4809 (referee), IP

D3338, D3338M, D4529, D4809 (referee)

Hydrogen Content

N/A

D3343, D3701, D3343, D3701, D5291, D7171 (referee)

D3701, D5291, D7171 (referee)

Calculated Cetane Index

D976, D4737 D976, D4737 D976, D4737

Copper Strip Corrosion

IP 154, D130 D130 D130, IP 154 D130

Page | 17

Freezing Point IP 16, D2386 D5972, IP 435, D7153, IP 529, D7154, IP

528, D2386, IP 16

D2386 (referee), IP

16, D5972, IP

435, D7153, IP

529, D7154, IP

D2386 (referee), D5972, D7153, D7154

Existent Gum IP 540 D381, IP 540 D381(referee), IP540 D381(referee), IP 540

Flash Point IP 170 D56, D93, D3828, IP 170, IP 523

D56, D93(referee), D3828, IP 170

D56, D93 (referee), D3828

Lead Content N/A N/A N/A N/A FSII IP 424, D5006 D5006 D5006 (referee), IP

D5006

Filtration Time N/A N/A D2276, D5452 (referee)

D2276, D5452( referee)

MSEP D3948 D3948 D3948,

D7224 (referee)

D3948, D7224 (referee)

Electrical Conductivity

IP 274,

D2624

D2624 D2624, IP 274 D2624

Thermal Stability

IP 323. D3241 D3241 (Annex A3 is referee) See C- 5.4.1

D3241 (Annex A3 is considered referee) See C- 5.4.1;

IP 323

D3241 (Annex A3 is referee) See C-5.4.1

Color (Saybolt) D156, D6045 D156 D156 (referee) , D6045

D156 (referee), D6045

Peroxide Number

D3703 N/A N/A

FAME IP 585, IP 590 D7797, IP 583,

IP 585 (referee), IP 590, IP 599

D7797, IP 583,

IP 585 (referee), IP

590, IP 599

D7797, IP 583,

IP 585

(referee), IP 590, IP 599

Lubricity D5001 D5001 N/A N/A

Table 2: Marine Diesel

F-76 (MIL-DTL-16884)

Appearance D4176 Color (Visual) D1500 (referee), D6045 Density or API Gravity D1298 (referee), D4052, D287, D7777 Distillation D86 (referee), D2887 Flash Point D93(referee), D6450, D3828 Carbon Residue D524(referee), D189, D4530 Cloud Point D2500(referee), D5771, D5772, D5773 Pour point D97(referee), D5949, D5950, D5985 Copper Strip Corrosion D130 Viscosity D445, D7042 Water and Sediment D2709 Particulate D6217 Storage Stability D5304 (referee), D2274 Sulfur D5354(referee), D1266, D2622, D3120, D7039 Fatty Acid Methyl Ester (FAME) BS EN 14078, IP579, D7963 Lubricity D6079 (referee), D7688 Demulsification D1401 Particulate Contamination D6217 (referee), D5452 Acid Number D974 (referee), D664 Ash D482

Page | 18

Aromatics D6591 (referee), D2425 Hydrogen Content D7171 (referee), D4808, D5291 Ignition Quality (Cetane Number, Cetane Index or Derived Cetane Number)

D613 (referee), D976, D6890, D7170

Trace Metals (Ca, Pb, Na, K and V) D7111 (referee), D3605

Table 3: Fuel System Icing Inhibitor

MIL-DTL-85470

Appearance Visual Acid Number D1613 Color, Platinum Cobalt D1209 (referee), E450 Distillation D1078 Ethylene Glycol Per specification pH of 25% solution in water E70 Relative Density D891 (referee), D4052 Water (mass%) D1364 (referee), E1064, E203 Flash Point D93 (referee), D56, D3828

Table 4: Marine Residual Fuel Oil (RME180/380)

ISO 8217

Kinematic Viscosity ISO 3104 Density ISO 3675, ISO 12185 Calculated Carbon Aromaticity Index (CCAI)

Specification

Sulfur ISO 8754, ISO 14596, D4264 Flash Point ISO 2719 Hydrogen Sulfide IP570 Acid Number D664 Total Sediment, aged ISO 10307-2 Carbon Residue ISO 10370 Pour Point ISO 3016 Water ISO 3733 Ash ISO 6245 Vanadium IP 501 (referee), IP 470, ISO 14597 Sodium IP 501 (referee), IP 470 Aluminum plus silicon IP 501 (referee), IP 470, ISO 10478 Used lubricating Oil (ULO) IP 501 (referee), IP 470, IP 500 Cetane Index ISO 4264

Table 5: Lubrication Oil (LTL) (NATO O-250)

MIL-PRF-17331

Sulfur D129, D1552, D2622, D4927, D4951, D6443, D6481, D7751

Acid Number D974 (referee), ASTM D664 Corrosion D665, Procedure B Corrosion, Copper Strip D130 Water Content D6304 (referee), ASTM D7546 API Gravity D287, D1298 (referee), D4052 Flash Point D92, D93 (referee) Pour Point D97 (referee), D5950, D5949 Viscosity @ 4.4°C D445 (referee), D7042 Viscosity @100°C D445 (referee), D7042 Viscosity @40°C D445 (referee), D7042 Emulsion Test D1401 Total Sludge, iron and copper D4310 Foam test D892

Page | 19

Cleanliness (Solid Particle Contamination)

D4898

Neutralization number (acid/base) D974 Appearance (to include visual sediment & water)

Visual

Table 6: Lubrication Oil (LO6) (NATO O-278)

MIL-PRF-9000

Appearance/Workmanship Visual

Flash point D92 Foam (stability only) D892

Gravity D287, D1298, D4052 Calcium D4628, D4927, D4951, D6443, D6481

Magnesium D4628, D4927, D4951, D6443 Zinc D4638, D4927, D4951, D6443, D6481

Phosphorus D1091, D4047, D4927, D4951, D6443, D6481 Pour Point D97, D5949, D5950

Sulfur D129, D1552, D2622, D4927, D4951, D6443, D6481

Total base number D2896 Viscosity index D2270

Viscosity at 100°C D445 Viscosity at 40°C D445

Neutralization number (acid/base) D2896 Ash, sulfated D874

Corrosion, copper strip D130

Table 7: Diesel Fuel Oil

ASTM D975 EN 590

Flash point D93 EN ISO2719

Water and Sediment D2709, D1796 N/A Distillation D86 EN ISO3405, EN ISO3924

Kinematic Viscosity D445 EN ISO3104 Ash D482 EN ISO6245

Sulfur D2622, D5453 EN ISO20846, EN ISO20884, EN

ISO13032

Copper strip corrosion D130 EN ISO2160 Cetane number D613 EN ISO5165, EN15195, EN16144

Cetane index D976 EN ISO4264 Aromaticity D1319 N/A Cloud Point D2500 EN23015

LTFT/CFPP D4539, D6371 EN116, EN16329

Carbon Residue D524 EN ISO10370 Lubricity D6079, D7688 EN ISO12156-1

Conductivity D2624 D4308 N/A API Gravity or Density at 15°C N/A EN ISO3675 (referee), EN

ISO12185

Polycyclic aromatic hydrocarbons

N/A EN12916

Manganese content N/A prEN16576 Water Content N/A EN ISO12937

Total Contamination N/A EN12662

FAME N/A EN14078

Oxidation stability N/A EN ISO 12205, EN15751 Appearance/Workmansh ip Visual Visual

Page | 20

Table 8: Reclaimed Fuel Oil (FOR)

MIL-PRF-24951

Flashpoint D93 Explosiveness FED-STD-791 Test Method 1151.1

Water and Sediment D1796 Sediment D473

API Gravity or Density at 60°C D287 Viscosity at 40°C D445 Viscosity at 50°C D88

Pour Point D97 Neutrality FED-STD-791 Test Method 5101

Sulfur Content D129 Ash D482

Trace Metals: Arsenic, Cadmium, Chromium and Lead

EPA SW-846, Method 3040/3050 and proposed method for evaluating solid waste

Total Halogen D808-87

Table 9: Corrosion Inhibitor/Lubricity Inhibitor (CI/LI)

MIL-PRF-25017

Appearance/Workmanship Visual

Acid Number ASTM D664 Solubility Per specification, Section 4.4.1

Rust Per specification, Section 4.4.3.1 Lubricity (BOCLE) Per specification, Section 4.4.4.1; ASTM D5001 pH Per specification, Section 4.4.14; ASTM D664 Water Separation (MSEP) Per specification, Section 4.4.5.1; ASTM D3948

Flash point Per specification, Section 4.4.14; ASTM D56; ASTM D93

Ash Content Per specification, Section 4.4.6; ASTM D482 Pour Point Per specification, Section 4.4.7; ASTM D97; ASTM

D5949; ASTM D5950; ASTM D5985

Density @ 15℃ Per specification, Section 4.4.14; ASTM D1298;

ASTM D4052; pycnometer Viscosity @ 40℃ Per specification, Section 4.4.14; ASTM D445

Electrical Conductivity Per specification, Section 4.4.2.2; ASTM D2624;

ASTM D4308

Storage Stability Per specification, Section 4.4.10 Fuel Injection Fouling Per specification, Section 4.4.11; ASTM D6421

Emulsification Tendency Per specification, Section 4.4.12; FED-STD-791 Method 550

Accelerated Stability Per specification, Section 4.4.13; ASTM D2274 Metals

(no applicable for materials containing < 0.05 mass% ash content)

Per specification, Section 4.4.14, emission spectrography

Page | 21

Table 10: Motor Gasoline

ASTM D4814 EN 228

Appearance Visual Vapor Pressure D4953, D5191, D5482 or D6378 EN13016-1

Density or API Gravity EN ISO3675, EN ISO12185 Distillation D86, D7345 EN ISO3405

Driveability Index specification Lead Content D3237 D5059 EN 237

Sulfur D1266, D2622, D3120, D5453, D6920, D7039

EN ISO13032, EN ISO20846 EN

ISO20884

Silver Strip Corrosion D7667, D7671 Copper Strip Corrosion D130 EN ISO2160

Gum Content D381 EN ISO6246 Oxidation Stability D525 EN ISO7536 Vapor Liquid Ratio D5188

Motor Octane Number (MON) D2700 EN ISO5163 Antiknock Index specification

Research Octane Number

(RON)

D2699 EN ISO5164

Manganese Content D3831 EN ISO16135, EN ISO16136 Hydrocarbon type content

(olefins and aromatics)

EN15553, EN ISO22854

Benzene Content EN238, EN12177, EN ISO22854 Oxygen Content EN1601, EN13132 EN ISO 22854

Oxygenate Content EN1601, EN13132 EN ISO 22854 Vapor Lock Index EN ISO3405

Color Visual Visual Water and Solids D4176