Attachment 2 - ENERGY QAP E34.pdf
PDF 2 MB Posted
- Attached to
- CONUS Laboratory Testing Federal contract opportunity
- Solicitation number
- SPE60321R0508
- Issued by
- Defense Logistics Agency Energy
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PDF (DLA)DLA FORM 1889, OCT 2011
SUPPLEMENTAL QUALITY ASSURANCE PROVISION (SQAP)
SHEET 1 OF 1PREVIOUS EDITION IS USABLE Add Continuation Page
Print Form Email Form Clear Export Data Import Data About Check for Newer Version Contact Us
REV DESCRIPTION DATE APPROVED
ENERGY QAP E34 May 1987
REVISIONS
E34 TEST FOR SULFIDES IN WATER
(a) SCOPE. This method describes a procedure for determining the presence of hydrogen sulfide, which is sometimes formed as a result of bacterial action on the sulfates contained in water bottoms in fuel storage tanks.
(b) APPARATUS. 250 ml conical flask.
(c) MATERIALS.
(1) Dilute (10%) chemically pure sulfuric or hydrochloric acid.
(2) Lead acetate paper.
(d) SAMPLES. Representative water samples from storage tank bottoms must be taken in a glass bottle. In some cases it will be necessary to take the water sample in a Bacon bomb sampler. Samples so taken will always be transferred to a glass bottle. To preclude oxidation by air, the filled bottle must be capped immediately. The sample should be tested as soon as possible after sampling to minimize possible changes in the composition of materials in the water.
(e) PROCEDURE.
(1) The sample must be shaken thoroughly just prior to performing the test to make certain that any sediment present is included in the portion of the sample to be tested.
(2) Transfer 100 ml of the shaken sample into a conical flask. Add 20 ml of dilute (10%) chemically pure sulfuric or hydrochloric acid to the flask. Immediately place a piece of lead acetate paper folded in a "V" shape in the neck of the flask. Bring the water to a boil and continue to gently boil for three or four minutes.
(f) REPORT. The presence of sulfides in the sample will be reported if the lead acetate paper shows a black or brown discoloration.
SUPPLEMENTAL QUALITY ASSURANCE PROVISION (SQAP)
DISTRIBUTION
STATEMENT - A
APPROVED FOR
PUBLIC RELEASE
DISTRIBUTION IS
"UNLIMITED"
DATE
2013-1120
APPROVED BY
DATE
11/20/2013
REVIEWED BY
DATE
11/12/2013
PREPARED BY
DRAWING NUMBERSCALE
CODE ID NO.
52838
SIZE
NSN
MULTIPLE
ITEM
ENERGY QAP E34
DLA Land & Maritime DLA Troop Support DLA Aviation clear
DEFENSE ENERGY SUPPORT CENTER
8725 JOHN J. KINGMAN RD
FORT BELVOIR, VIRGINIA 22060-6222
DLA Energy
PDF (DLA)
DLA FORM 1889, OCT 2011
SUPPLEMENTAL QUALITY ASSURANCE PROVISION (SQAP)
SHEET OF
PREVIOUS EDITION IS USABLE
REV
DESCRIPTION
DATE
APPROVED
REVISIONS
SUPPLEMENTAL QUALITY ASSURANCE PROVISION (SQAP)
DISTRIBUTION STATEMENT - A
APPROVED FOR PUBLIC RELEASE
DISTRIBUTION IS "UNLIMITED"
REV
DESCRIPTION
DATE
APPROVED
REVISIONS
DISTRIBUTION STATEMENT - A
APPROVED FOR PUBLIC RELEASE
DISTRIBUTION IS "UNLIMITED"
SUPPLEMENTAL QUALITY ASSURANCE PROVISION (SQAP)
Supplemental Quality Assurance Provision (SQAP) DSCC Form 2291, Feb 2004 online none standard Quality Assurance
DLA
1 + No Tech Qual Deskbook n/a No Supplemental Quality Assurance Provision (SQAP) interactive October 2011 (added Energy; updated supply center names)
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| description: ENERGY QAP E34 |
| revdate: May 1987 |
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