Part 6 Reference Reports Wayne Oakland DCSpec_Rev_02-19.pdf

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Attached to
761/20035. SAR Former Wayne Oakland Oil
Solicitation number
RFQ 171 200000000255 5
Issued by
Benzie County, Riverview City, Michigan

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Written by GovTribe AI ·

This is a corrected laboratory analysis report from the Michigan Department of Environmental Quality Environmental Laboratory documenting groundwater sample testing from what appears to be a site investigation in Wayne and Oakland counties. The report contains analytical results for multiple soil boring samples (SB-7 through SB-11) collected at depths between 5 and 11.5 feet, along with equipment blanks and trip blanks analyzed during April 2009. The samples were analyzed for volatile organic compounds using EPA Method 8260, base neutral acid compounds using EPA Method 8270, polychlorinated biphenyls (PCBs) using EPA Method 8082, and dissolved metals using EPA Method 6020.

The analytical results indicate that most volatile organic compounds and base neutral acid compounds were not detected across all samples, with several exceptions showing low-level detections of petroleum-related compounds and aromatic hydrocarbons. Specifically, samples SB-8, SB-9, and SB-10 detected naphthalene at concentrations of 35, 7.8, and not detected respectively, along with various other aromatic compounds at trace levels. Dissolved metals analysis detected chromium in samples SB-8 (4.7 µg/L) and SB-9 and SB-10 (1.5 µg/L each), while cadmium and lead were not detected in any samples. All PCB Aroclors tested showed non-detectable results across all samples. Equipment and trip blanks demonstrated proper quality control with no detections, confirming the validity of the field sampling procedures and laboratory analysis.

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Part 1 Specifications 20035.pdf PDF
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Part 8 Reference Reports Wayne Oakland DCSpec_Rev_02-19.pdf PDF
Part 10 Reference Reports Wayne Oakland DCSpec_Rev-02-19.pdf PDF
Part 9 Reference Reports Wayne Oakland DCSpec_Rev02-19.pdf PDF
Part 12 Reference Reports Wayne Oakland DCSpec_Rev-02-19.pdf PDF
Part 13 Waste Characterization and Figures Wayne Oakland DCSpec.pdf PDF
Addendum No. 3.pdf PDF
Part 5 Reference Reports Wayne Oakland DCSpec_Rev_02-19.pdf PDF
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Part 2 Reference Reports Wayne Oakland DCSpec_Rev_02-19.pdf PDF
Part 3 Reference Reports Wayne Oakland DCSpec_Rev_02-19.pdf PDF
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20035 Addendum No. 1 04_27_20.pdf PDF
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MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

CORRECTED REPORT

Sample Number: AB32571 SB-7 (6.5-11.5')

Base Neutral Acid Compounds

Compound

Date Tested:

RL

Analytical Method:

CAS #

8270 Analyst:

Qualifier

04/15/2009 SMH

Extraction Method: Extraction Date: 04/13/2009 971Volume:3510 Qualifier:

Dilution FactorResult ug/L

78-59-1 Isophorone 1 1.0Not Detected

121-69-7 N,N-dimethylaniline 5.1 1.0Not Detected

91-20-3 Naphthalene 1 1.0Not Detected

98-95-3 Nitrobenzene 2.1 1.0Not Detected

100-61-8 N-methylaniline 1 1.0Not Detected

67-75-9 N-Nitrosodimethylamine 5.1 1.0Not Detected

621-64-7 N-Nitrosodi-n-propylamine 2.1 1.0Not Detected

86-30-6 N-Nitrosodiphenylamine 2.1 1.0Not Detected

87-86-5 Pentachlorophenol 21 1.0Not Detected

85-01-8 Phenanthrene 1 1.01.6

108-95-2 Phenol 5.1 1.0Not Detected

129-00-0 Pyrene 1 1.0Not Detected

110-86-1 Pyridine 21 1.0Not Detected

632-22-4 Tetramethylurea 1 1.0Not Detected

Probable petroleum product(s) present.

PCBs as Aroclors

Compound

Date Tested:

RL

Analytical Method:

CAS #

8082 Analyst:

Qualifier

04/24/2009 MF

Extraction Method: Extraction Date: 04/14/2009 980Volume:3510 Qualifier:

Dilution FactorResult ug/L

SURROGATE #Decachlorobiphenyl# 44.8

SURROGATE #Tetrachloro-m-xylene# 41.8

12674-11-2 Aroclor 1016 0.1 1.0Not Detected

11104-28-2 Aroclor 1221 0.1 1.0Not Detected

11141-16-5 Aroclor 1232 0.1 1.0Not Detected

53469-21-9 Aroclor 1242 0.1 1.0Not Detected

12672-29-6 Aroclor 1248 0.1 1.0Not Detected

11097-69-1 Aroclor 1254 0.1 1.0Not Detected

11096-82-5 Aroclor 1260 0.1 1.0Not Detected

37324-23-5 Aroclor 1262 0.1 1.0Not Detected

11100-14-4 Aroclor 1268 0.1 1.0Not Detected

CAS# : Chemical Abstract Service Registry Number

RL : Reporting Limit

ND : Not Detected ug / L : microgram / liter (ppb) mg / L : milligram / liter (ppm) ug / Kg : microgram / kilogram (ppb) mg / Kg : milligram / kilogram (ppm)

Laboratory Contacts

Inorganic Unit Mgr: Sandy Gregg

Organic Unit Mgr: Carol Smith

Systems Mgmt Unit: George Krisztian

Page 53 of 10090400113Lab Work Order #:

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

CORRECTED REPORT

Sample Number: AB32571 SB-7 (6.5-11.5')

Date TestedAnalyte Name MethodCAS# QualifierResult AnalystRLUnit

Dig. Diss. Metals Water KS3010/20004/17/2009Completed

7440-43-9 Cadmium - Dissolved KS6020/200.804/27/20090.2µg/LND

7440-47-3 Chromium - Dissolved KS6020/200.804/27/20091µg/L1.0

7439-92-1 Lead - Dissolved KS6020/200.804/27/20091µg/LND

Florisil Cleanup DT362004/21/2009Completed

Gel Permeation Cleanup DT364004/20/2009Completed

CAS# : Chemical Abstract Service Registry Number

RL : Reporting Limit

ND : Not Detected ug / L : microgram / liter (ppb) mg / L : milligram / liter (ppm) ug / Kg : microgram / kilogram (ppb) mg / Kg : milligram / kilogram (ppm)

Laboratory Contacts

Inorganic Unit Mgr: Sandy Gregg

Organic Unit Mgr: Carol Smith

Page 54 of 10090400113Lab Work Order #:

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

CORRECTED REPORT

Sample Number: AB32572 SB-8 (5-10')

Library Search-Volatiles

Compound

Date Tested:

RL

Analytical Method:

CAS #

8260 Analyst:

Qualifier

04/14/2009 RD

Dilution FactorResult ug/L

1-Methyl naphthalene LB73

Cyclopropyl benzene LB34

Dimethyl dihydro Indene LB40

Dimethyl dihydro Indene isomer LB32

Ethyl dimethyl benzene LB35

Methyl Indan LB41

Phenyl butene LB120

Tetrahydro naphthalene LB32

Tetramethyl benzene LB38

Volatile Compounds

Compound

Date Tested:

RL

Analytical Method:

CAS #

8260 Analyst:

Qualifier

04/14/2009 RD

Dilution FactorResult ug/L

SURROGATE #Bromofluorobenzene# 100

SURROGATE #Dibromofluoromethane# 99.6

SURROGATE #Toluene-d8# 98.3

630-20-6 1,1,1,2-Tetrachloroethane 1 1.0Not Detected

71-55-6 1,1,1-Trichloroethane 1 1.0Not Detected

79-34-5 1,1,2,2-Tetrachloroethane 1 1.0Not Detected

79-00-5 1,1,2-Trichloroethane 1 1.0Not Detected

75-34-3 1,1-Dichloroethane 1 1.0Not Detected

75-35-4 1,1-Dichloroethylene 1 1.0Not Detected

87-61-6 1,2,3-Trichlorobenzene 5 1.0Not Detected

96-18-4 1,2,3-Trichloropropane 1 1.0Not Detected

526-73-8 1,2,3-Trimethylbenzene 1 1.026

120-82-1 1,2,4-Trichlorobenzene 5 1.0Not Detected

95-63-6 1,2,4-Trimethylbenzene 1 1.082

96-12-8 1,2-Dibromo-3-chloropropane 5 1.0Not Detected

106-93-4 1,2-Dibromoethane 1 1.0Not Detected

95-50-1 1,2-Dichlorobenzene 1 1.0Not Detected

107-06-2 1,2-Dichloroethane 1 1.0Not Detected

78-87-5 1,2-Dichloropropane 1 1.0Not Detected

108-67-8 1,3,5-Trimethylbenzene 1 1.021

541-73-1 1,3-Dichlorobenzene 1 1.0Not Detected

106-46-7 1,4-Dichlorobenzene 1 1.0Not Detected

78-93-3 2-Butanone (MEK) 5 1.0Not Detected

591-78-6 2-Hexanone 5 1.0Not Detected

CAS# : Chemical Abstract Service Registry Number

RL : Reporting Limit

ND : Not Detected ug / L : microgram / liter (ppb) mg / L : milligram / liter (ppm) ug / Kg : microgram / kilogram (ppb) mg / Kg : milligram / kilogram (ppm)

Laboratory Contacts

Inorganic Unit Mgr: Sandy Gregg

Organic Unit Mgr: Carol Smith

Page 55 of 10090400113Lab Work Order #:

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

CORRECTED REPORT

Sample Number: AB32572 SB-8 (5-10')

Volatile Compounds

Compound

Date Tested:

RL

Analytical Method:

CAS #

8260 Analyst:

Qualifier

04/14/2009 RD

Dilution FactorResult ug/L

91-57-6 2-Methylnaphthalene X 55 1.0120

67-64-1 2-Propanone (acetone) 20 1.0Not Detected

108-10-1 4-Methyl-2-pentanone (MIBK) 5 1.0Not Detected

107-13-1 Acrylonitrile Z5 1.0Not Detected

71-43-2 Benzene 1 1.05.2

108-86-1 Bromobenzene 1 1.0Not Detected

74-97-5 Bromochloromethane 1 1.0Not Detected

75-27-4 Bromodichloromethane 1 1.0Not Detected

75-25-2 Bromoform 1 1.0Not Detected

74-83-9 Bromomethane 5 1.0Not Detected

75-15-0 Carbon disulfide 1 1.0Not Detected

56-23-5 Carbon tetrachloride 1 1.0Not Detected

108-90-7 Chlorobenzene 1 1.0Not Detected

75-00-3 Chloroethane 5 1.0Not Detected

67-66-3 Chloroform 1 1.0Not Detected

74-87-3 Chloromethane 5 1.0Not Detected

156-59-2 cis-1,2-Dichloroethylene 1 1.0Not Detected

10061-01-5 cis-1,3-Dichloropropylene 1 1.0Not Detected

110-82-7 Cyclohexane 5 1.0Not Detected

124-48-1 Dibromochloromethane 1 1.0Not Detected

74-95-3 Dibromomethane 1 1.0Not Detected

75-71-8 Dichlorodifluoromethane 55 1.0Not Detected

60-29-7 Diethyl ether 5 1.0Not Detected

108-20-3 Diisopropyl Ether 5 1.0Not Detected

100-41-4 Ethylbenzene 1 1.019

637-92-3 Ethyltertiarybutylether 5 1.0Not Detected

67-72-1 Hexachloroethane 5 1.0Not Detected

98-82-8 Isopropylbenzene 1 1.03.3

108383,106423 m & p - Xylene 2 1.022

74-88-4 Methyl iodide 71 1.0Not Detected

75-09-2 Methylene chloride 5 1.0Not Detected

1634-04-4 Methyltertiarybutylether 1 1.0Not Detected

91-20-3 Naphthalene X5 1.097

104-51-8 n-Butylbenzene 1 1.04.2

103-65-1 n-Propylbenzene 1 1.05.9

95-47-6 o-Xylene 1 1.03.3

99-87-6 p-Isopropyl toluene 1 1.04.2

135-98-8 sec-Butylbenzene 1 1.02.3

100-42-5 Styrene 1 1.0Not Detected

98-06-6 tert-Butylbenzene 1 1.0Not Detected

CAS# : Chemical Abstract Service Registry Number

RL : Reporting Limit

ND : Not Detected ug / L : microgram / liter (ppb) mg / L : milligram / liter (ppm) ug / Kg : microgram / kilogram (ppb) mg / Kg : milligram / kilogram (ppm)

Laboratory Contacts

Inorganic Unit Mgr: Sandy Gregg

Organic Unit Mgr: Carol Smith

Page 56 of 10090400113Lab Work Order #:

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

CORRECTED REPORT

Sample Number: AB32572 SB-8 (5-10')

Volatile Compounds

Compound

Date Tested:

RL

Analytical Method:

CAS #

8260 Analyst:

Qualifier

04/14/2009 RD

Dilution FactorResult ug/L

75-65-0 tertiary Butyl Alcohol 50 1.0Not Detected

994-05-8 tertiaryAmylmethylether 5 1.0Not Detected

127-18-4 Tetrachloroethylene 1 1.0Not Detected

109-99-9 Tetrahydrofuran 5 1.0Not Detected

108-88-3 Toluene 1 1.0Not Detected

156-60-5 trans-1,2-Dichloroethylene 1 1.0Not Detected

10061-02-6 trans-1,3-Dichloropropylene 1 1.0Not Detected

110-57-6 trans-1,4-Dichloro-2-butene Z5 1.0Not Detected

79-01-6 Trichloroethylene 1 1.0Not Detected

75-69-4 Trichlorofluoromethane 1 1.0Not Detected

75-01-4 Vinyl chloride 1 1.0Not Detected

Unidentified peaks present in sample.

Base Neutral Acid Compounds

Compound

Date Tested:

RL

Analytical Method:

CAS #

8270 Analyst:

Qualifier

04/21/2009 SMH

Extraction Method: Extraction Date: 04/16/2009 980Volume:3510 Qualifier:

Dilution FactorResult ug/L

SURROGATE #2 - Fluorobiphenyl# 58.4

SURROGATE #2,4,6-Tribromophenol# 72.6

SURROGATE #2-Fluorophenol# 19.6

SURROGATE #Nitrobenzene - D5# 56.9

SURROGATE #Phenol - D6# 10.8

SURROGATE #p-Terphenyl-D14# 62.2

120-82-1 1,2,4-Trichlorobenzene 2 1.0Not Detected

95-95-4 2,4,5-Trichlorophenol 5.1 1.0Not Detected

88-06-2 2,4,6-Trichlorophenol 4.1 1.0Not Detected

120-83-2 2,4-Dichlorophenol 10 1.0Not Detected

105-67-9 2,4-Dimethylphenol 5.1 1.0Not Detected

51-28-5 2,4-Dinitrophenol 26 1.0Not Detected

121-14-2 2,4-Dinitrotoluene 5.1 1.0Not Detected

606-20-2 2,6-Dinitrotoluene 5.1 1.0Not Detected

95-51-2 2-Chloroaniline 5.1 1.0Not Detected

91-58-7 2-Chloronaphthalene 2 1.0Not Detected

95-57-8 2-Chlorophenol 10 1.0Not Detected

534-52-1 2-Methyl-4,6-dinitrophenol 20 1.0Not Detected

91-57-6 2-Methylnaphthalene 5.1 1.041

95-48-7 2-Methylphenol (o-Cresol) 10 1.0Not Detected

88-74-4 2-Nitroaniline 20 1.0Not Detected

88-75-5 2-Nitrophenol 5.1 1.0Not Detected

CAS# : Chemical Abstract Service Registry Number

RL : Reporting Limit

ND : Not Detected ug / L : microgram / liter (ppb) mg / L : milligram / liter (ppm) ug / Kg : microgram / kilogram (ppb) mg / Kg : milligram / kilogram (ppm)

Laboratory Contacts

Inorganic Unit Mgr: Sandy Gregg

Organic Unit Mgr: Carol Smith

Page 57 of 10090400113Lab Work Order #:

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

CORRECTED REPORT

Sample Number: AB32572 SB-8 (5-10')

Base Neutral Acid Compounds

Compound

Date Tested:

RL

Analytical Method:

CAS #

8270 Analyst:

Qualifier

04/21/2009 SMH

Extraction Method: Extraction Date: 04/16/2009 980Volume:3510 Qualifier:

Dilution FactorResult ug/L

108394,106445 3 & 4-Methylphenol 20 1.0Not Detected

99-09-2 3-Nitroaniline 20 1.0Not Detected

101-55-3 4-Bromophenyl phenyl ether 2 1.0Not Detected

59-50-7 4-Chloro-3-methyl-phenol 5.1 1.0Not Detected

106-47-8 4-Chloroaniline 10 1.0Not Detected

7005-72-3 4-Chlorodiphenylether 1 1.0Not Detected

100-01-6 4-Nitroaniline 20 1.0Not Detected

100-02-7 4-Nitrophenol 26 1.0Not Detected

83-32-9 Acenaphthene 1 1.01.6

208-96-8 Acenaphthylene 1 1.0Not Detected

62-53-3 Aniline 4.1 1.0Not Detected

120-12-7 Anthracene 1 1.0Not Detected

103-33-3 Azobenzene 2 1.0Not Detected

56-55-3 Benzo[a]anthracene 1 1.0Not Detected

50-32-8 Benzo[a]pyrene 1 1.0Not Detected

205-99-2 Benzo[b]fluoranthene 1 1.0Not Detected

191-24-2 Benzo[g,h,i]perylene 1 1.0Not Detected

207-08-9 Benzo[k]fluoranthene 1 1.0Not Detected

100-51-6 Benzyl Alcohol 551 1.0Not Detected

111-91-1 Bis(2-chloroethoxy)methane 2 1.0Not Detected

111-44-4 Bis(2-chloroethyl)ether 1 1.0Not Detected

108-60-1 Bis(2-chloroisopropyl)ether 1 1.0Not Detected

117-81-7 Bis(2-ethylhexyl)phthalate 5.1 1.0Not Detected

85-68-7 Butyl benzyl phthalate 5.1 1.0Not Detected

86-74-8 Carbazole 5.1 1.0Not Detected

218-01-9 Chrysene 1 1.0Not Detected

53-70-3 Dibenz[a,h]anthracene 2 1.0Not Detected

132-64-9 Dibenzofuran 4.1 1.0Not Detected

84-66-2 Diethylphthalate 5.1 1.0Not Detected

131-11-3 Dimethyl phthalate 5.1 1.0Not Detected

84-74-2 Di-n-butyl phthalate 5.1 1.0Not Detected

117-84-0 Di-n-octyl phthalate 5.1 1.0Not Detected

206-44-0 Fluoranthene 1 1.0Not Detected

86-73-7 Fluorene 1 1.01.7

118-74-1 Hexachlorobenzene 1 1.0Not Detected

87-68-3 Hexachlorobutadiene 1 1.0Not Detected

77-47-4 Hexachlorocyclopentadiene 5Z10 1.0Not Detected

67-72-1 Hexachloroethane 1 1.0Not Detected

193-39-5 Indeno(1,2,3-c,d)pyrene 2 1.0Not Detected

78-59-1 Isophorone 1 1.0Not Detected

CAS# : Chemical Abstract Service Registry Number

RL : Reporting Limit

ND : Not Detected ug / L : microgram / liter (ppb) mg / L : milligram / liter (ppm) ug / Kg : microgram / kilogram (ppb) mg / Kg : milligram / kilogram (ppm)

Laboratory Contacts

Inorganic Unit Mgr: Sandy Gregg

Organic Unit Mgr: Carol Smith

Page 58 of 10090400113Lab Work Order #:

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

CORRECTED REPORT

Sample Number: AB32572 SB-8 (5-10')

Base Neutral Acid Compounds

Compound

Date Tested:

RL

Analytical Method:

CAS #

8270 Analyst:

Qualifier

04/21/2009 SMH

Extraction Method: Extraction Date: 04/16/2009 980Volume:3510 Qualifier:

Dilution FactorResult ug/L

121-69-7 N,N-dimethylaniline 5.1 1.0Not Detected

91-20-3 Naphthalene 1 1.035

98-95-3 Nitrobenzene 2 1.0Not Detected

100-61-8 N-methylaniline 1 1.0Not Detected

67-75-9 N-Nitrosodimethylamine 5.1 1.0Not Detected

621-64-7 N-Nitrosodi-n-propylamine 2 1.0Not Detected

86-30-6 N-Nitrosodiphenylamine 2 1.0Not Detected

87-86-5 Pentachlorophenol 20 1.0Not Detected

85-01-8 Phenanthrene 1 1.01.8

108-95-2 Phenol 5.1 1.0Not Detected

129-00-0 Pyrene 1 1.0Not Detected

110-86-1 Pyridine 20 1.0Not Detected

632-22-4 Tetramethylurea 1 1.0Not Detected

Probable petroleum product(s) present.

PCBs as Aroclors

Compound

Date Tested:

RL

Analytical Method:

CAS #

8082 Analyst:

Qualifier

04/24/2009 MF

Extraction Method: Extraction Date: 04/14/2009 950Volume:3510 Qualifier:

Dilution FactorResult ug/L

SURROGATE #Decachlorobiphenyl# 29.7

SURROGATE #Tetrachloro-m-xylene# 32.8

12674-11-2 Aroclor 1016 0.11 1.0Not Detected

11104-28-2 Aroclor 1221 K0.24 1.0Not Detected

11141-16-5 Aroclor 1232 0.11 1.0Not Detected

53469-21-9 Aroclor 1242 0.11 1.0Not Detected

12672-29-6 Aroclor 1248 0.11 1.0Not Detected

11097-69-1 Aroclor 1254 0.11 1.0Not Detected

11096-82-5 Aroclor 1260 0.11 1.0Not Detected

37324-23-5 Aroclor 1262 0.11 1.0Not Detected

11100-14-4 Aroclor 1268 0.11 1.0Not Detected

CAS# : Chemical Abstract Service Registry Number

RL : Reporting Limit

ND : Not Detected ug / L : microgram / liter (ppb) mg / L : milligram / liter (ppm) ug / Kg : microgram / kilogram (ppb) mg / Kg : milligram / kilogram (ppm)

Laboratory Contacts

Inorganic Unit Mgr: Sandy Gregg

Organic Unit Mgr: Carol Smith

Page 59 of 10090400113Lab Work Order #:

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

CORRECTED REPORT

Sample Number: AB32572 SB-8 (5-10')

Date TestedAnalyte Name MethodCAS# QualifierResult AnalystRLUnit

Dig. Diss. Metals Water KS3010/20004/17/2009Completed

7440-43-9 Cadmium - Dissolved KS6020/200.804/27/20090.2µg/LND

7440-47-3 Chromium - Dissolved KS6020/200.804/27/20091µg/L4.7

7439-92-1 Lead - Dissolved KS6020/200.804/27/20091µg/LND

Florisil Cleanup DT362004/21/2009Completed

Gel Permeation Cleanup DT364004/20/2009Completed

CAS# : Chemical Abstract Service Registry Number

RL : Reporting Limit

ND : Not Detected ug / L : microgram / liter (ppb) mg / L : milligram / liter (ppm) ug / Kg : microgram / kilogram (ppb) mg / Kg : milligram / kilogram (ppm)

Laboratory Contacts

Inorganic Unit Mgr: Sandy Gregg

Organic Unit Mgr: Carol Smith

Page 60 of 10090400113Lab Work Order #:

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

CORRECTED REPORT

Sample Number: AB32573 SB-9 (5-10')

Library Search-Volatiles

Compound

Date Tested:

RL

Analytical Method:

CAS #

8260 Analyst:

Qualifier

04/14/2009 RD

Dilution FactorResult ug/L

1-Methyl naphthalene LB11

Cyclopropyl benzene LB8.9

Dimethyl dihydro Indene LB7.6

Dimethyl dihydro Indene isomer LB17

Dimethyl dihydro Indene isomer 3 LB10

Methyl indan LB8.4

Phenyl butene LB23

Tetramethyl benzene LB6.6

Tetramethyl benzene isomer LB6.0

Volatile Compounds

Compound

Date Tested:

RL

Analytical Method:

CAS #

8260 Analyst:

Qualifier

04/13/2009 RD

Dilution FactorResult ug/L

SURROGATE #Bromofluorobenzene# 101

SURROGATE #Dibromofluoromethane# 100

SURROGATE #Toluene-d8# 100

630-20-6 1,1,1,2-Tetrachloroethane 1 1.0Not Detected

71-55-6 1,1,1-Trichloroethane 1 1.0Not Detected

79-34-5 1,1,2,2-Tetrachloroethane 1 1.0Not Detected

79-00-5 1,1,2-Trichloroethane 1 1.0Not Detected

75-34-3 1,1-Dichloroethane 1 1.0Not Detected

75-35-4 1,1-Dichloroethylene 1 1.0Not Detected

87-61-6 1,2,3-Trichlorobenzene 5 1.0Not Detected

96-18-4 1,2,3-Trichloropropane 1 1.0Not Detected

526-73-8 1,2,3-Trimethylbenzene 1 1.07.5

120-82-1 1,2,4-Trichlorobenzene 5 1.0Not Detected

95-63-6 1,2,4-Trimethylbenzene 1 1.014

96-12-8 1,2-Dibromo-3-chloropropane 5 1.0Not Detected

106-93-4 1,2-Dibromoethane 1 1.0Not Detected

95-50-1 1,2-Dichlorobenzene 1 1.0Not Detected

107-06-2 1,2-Dichloroethane 1 1.0Not Detected

78-87-5 1,2-Dichloropropane 1 1.0Not Detected

108-67-8 1,3,5-Trimethylbenzene 1 1.0Not Detected

541-73-1 1,3-Dichlorobenzene 1 1.0Not Detected

106-46-7 1,4-Dichlorobenzene 1 1.0Not Detected

78-93-3 2-Butanone (MEK) 5 1.0Not Detected

591-78-6 2-Hexanone 5 1.0Not Detected

CAS# : Chemical Abstract Service Registry Number

RL : Reporting Limit

ND : Not Detected ug / L : microgram / liter (ppb) mg / L : milligram / liter (ppm) ug / Kg : microgram / kilogram (ppb) mg / Kg : milligram / kilogram (ppm)

Laboratory Contacts

Inorganic Unit Mgr: Sandy Gregg

Organic Unit Mgr: Carol Smith

Page 61 of 10090400113Lab Work Order #:

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

CORRECTED REPORT

Sample Number: AB32573 SB-9 (5-10')

Volatile Compounds

Compound

Date Tested:

RL

Analytical Method:

CAS #

8260 Analyst:

Qualifier

04/13/2009 RD

Dilution FactorResult ug/L

91-57-6 2-Methylnaphthalene X 55 1.011

67-64-1 2-Propanone (acetone) 20 1.0Not Detected

108-10-1 4-Methyl-2-pentanone (MIBK) 5 1.0Not Detected

107-13-1 Acrylonitrile Z5 1.0Not Detected

71-43-2 Benzene 1 1.03.3

108-86-1 Bromobenzene 1 1.0Not Detected

74-97-5 Bromochloromethane 1 1.0Not Detected

75-27-4 Bromodichloromethane 1 1.0Not Detected

75-25-2 Bromoform 1 1.0Not Detected

74-83-9 Bromomethane 5 1.0Not Detected

75-15-0 Carbon disulfide 1 1.0Not Detected

56-23-5 Carbon tetrachloride 1 1.0Not Detected

108-90-7 Chlorobenzene 1 1.0Not Detected

75-00-3 Chloroethane 5 1.0Not Detected

67-66-3 Chloroform 1 1.0Not Detected

74-87-3 Chloromethane 5 1.0Not Detected

156-59-2 cis-1,2-Dichloroethylene 1 1.0Not Detected

10061-01-5 cis-1,3-Dichloropropylene 1 1.0Not Detected

110-82-7 Cyclohexane 5 1.0Not Detected

124-48-1 Dibromochloromethane 1 1.0Not Detected

74-95-3 Dibromomethane 1 1.0Not Detected

75-71-8 Dichlorodifluoromethane 75 1.0Not Detected

60-29-7 Diethyl ether 5 1.0Not Detected

108-20-3 Diisopropyl Ether 5 1.0Not Detected

100-41-4 Ethylbenzene 1 1.010

637-92-3 Ethyltertiarybutylether 5 1.0Not Detected

67-72-1 Hexachloroethane 5 1.0Not Detected

98-82-8 Isopropylbenzene 1 1.01.5

108383,106423 m & p - Xylene 2 1.05.4

74-88-4 Methyl iodide 1 1.0Not Detected

75-09-2 Methylene chloride 5 1.0Not Detected

1634-04-4 Methyltertiarybutylether 1 1.0Not Detected

91-20-3 Naphthalene X5 1.07.8

104-51-8 n-Butylbenzene 1 1.01.1

103-65-1 n-Propylbenzene 1 1.02.5

95-47-6 o-Xylene 1 1.01.0

99-87-6 p-Isopropyl toluene 1 1.0Not Detected

135-98-8 sec-Butylbenzene 1 1.0Not Detected

100-42-5 Styrene 1 1.0Not Detected

98-06-6 tert-Butylbenzene 1 1.01.1

CAS# : Chemical Abstract Service Registry Number

RL : Reporting Limit

ND : Not Detected ug / L : microgram / liter (ppb) mg / L : milligram / liter (ppm) ug / Kg : microgram / kilogram (ppb) mg / Kg : milligram / kilogram (ppm)

Laboratory Contacts

Inorganic Unit Mgr: Sandy Gregg

Organic Unit Mgr: Carol Smith

Page 62 of 10090400113Lab Work Order #:

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

CORRECTED REPORT

Sample Number: AB32573 SB-9 (5-10')

Volatile Compounds

Compound

Date Tested:

RL

Analytical Method:

CAS #

8260 Analyst:

Qualifier

04/13/2009 RD

Dilution FactorResult ug/L

75-65-0 tertiary Butyl Alcohol 50 1.0Not Detected

994-05-8 tertiaryAmylmethylether 5 1.0Not Detected

127-18-4 Tetrachloroethylene 1 1.0Not Detected

109-99-9 Tetrahydrofuran 5 1.0Not Detected

108-88-3 Toluene 1 1.0Not Detected

156-60-5 trans-1,2-Dichloroethylene 1 1.0Not Detected

10061-02-6 trans-1,3-Dichloropropylene 1 1.0Not Detected

110-57-6 trans-1,4-Dichloro-2-butene Z5 1.0Not Detected

79-01-6 Trichloroethylene 1 1.0Not Detected

75-69-4 Trichlorofluoromethane 1 1.0Not Detected

75-01-4 Vinyl chloride 1 1.0Not Detected

Unidentified peaks present in sample.

Base Neutral Acid Compounds

Compound

Date Tested:

RL

Analytical Method:

CAS #

8270 Analyst:

Qualifier

04/21/2009 SMH

Extraction Method: Extraction Date: 04/16/2009 990Volume:3510 Qualifier:

Dilution FactorResult ug/L

SURROGATE #2 - Fluorobiphenyl# 64.5

SURROGATE #2,4,6-Tribromophenol# 86.3

SURROGATE #2-Fluorophenol# 23.0

SURROGATE #Nitrobenzene - D5# 61.9

SURROGATE #Phenol - D6# 12.9

SURROGATE #p-Terphenyl-D14# 87.2

120-82-1 1,2,4-Trichlorobenzene 2 1.0Not Detected

95-95-4 2,4,5-Trichlorophenol 5.1 1.0Not Detected

88-06-2 2,4,6-Trichlorophenol 4 1.0Not Detected

120-83-2 2,4-Dichlorophenol 10 1.0Not Detected

105-67-9 2,4-Dimethylphenol 5.1 1.0Not Detected

51-28-5 2,4-Dinitrophenol 25 1.0Not Detected

121-14-2 2,4-Dinitrotoluene 5.1 1.0Not Detected

606-20-2 2,6-Dinitrotoluene 5.1 1.0Not Detected

95-51-2 2-Chloroaniline 5.1 1.0Not Detected

91-58-7 2-Chloronaphthalene 2 1.0Not Detected

95-57-8 2-Chlorophenol 10 1.0Not Detected

534-52-1 2-Methyl-4,6-dinitrophenol 20 1.0Not Detected

91-57-6 2-Methylnaphthalene T5.1 1.04.8

95-48-7 2-Methylphenol (o-Cresol) 10 1.0Not Detected

88-74-4 2-Nitroaniline 20 1.0Not Detected

88-75-5 2-Nitrophenol 5.1 1.0Not Detected

CAS# : Chemical Abstract Service Registry Number

RL : Reporting Limit

ND : Not Detected ug / L : microgram / liter (ppb) mg / L : milligram / liter (ppm) ug / Kg : microgram / kilogram (ppb) mg / Kg : milligram / kilogram (ppm)

Laboratory Contacts

Inorganic Unit Mgr: Sandy Gregg

Organic Unit Mgr: Carol Smith

Page 63 of 10090400113Lab Work Order #:

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

CORRECTED REPORT

Sample Number: AB32573 SB-9 (5-10')

Base Neutral Acid Compounds

Compound

Date Tested:

RL

Analytical Method:

CAS #

8270 Analyst:

Qualifier

04/21/2009 SMH

Extraction Method: Extraction Date: 04/16/2009 990Volume:3510 Qualifier:

Dilution FactorResult ug/L

108394,106445 3 & 4-Methylphenol 20 1.0Not Detected

99-09-2 3-Nitroaniline 20 1.0Not Detected

101-55-3 4-Bromophenyl phenyl ether 2 1.0Not Detected

59-50-7 4-Chloro-3-methyl-phenol 5.1 1.0Not Detected

106-47-8 4-Chloroaniline 10 1.0Not Detected

7005-72-3 4-Chlorodiphenylether 1 1.0Not Detected

100-01-6 4-Nitroaniline 20 1.0Not Detected

100-02-7 4-Nitrophenol 25 1.0Not Detected

83-32-9 Acenaphthene 1 1.0Not Detected

208-96-8 Acenaphthylene 1 1.0Not Detected

62-53-3 Aniline 4 1.0Not Detected

120-12-7 Anthracene 1 1.0Not Detected

103-33-3 Azobenzene 2 1.0Not Detected

56-55-3 Benzo[a]anthracene 1 1.0Not Detected

50-32-8 Benzo[a]pyrene 1 1.0Not Detected

205-99-2 Benzo[b]fluoranthene 1 1.0Not Detected

191-24-2 Benzo[g,h,i]perylene 1 1.0Not Detected

207-08-9 Benzo[k]fluoranthene 1 1.0Not Detected

100-51-6 Benzyl Alcohol 551 1.0Not Detected

111-91-1 Bis(2-chloroethoxy)methane 2 1.0Not Detected

111-44-4 Bis(2-chloroethyl)ether 1 1.0Not Detected

108-60-1 Bis(2-chloroisopropyl)ether 1 1.0Not Detected

117-81-7 Bis(2-ethylhexyl)phthalate 5.1 1.0Not Detected

85-68-7 Butyl benzyl phthalate 5.1 1.0Not Detected

86-74-8 Carbazole 5.1 1.0Not Detected

218-01-9 Chrysene 1 1.0Not Detected

53-70-3 Dibenz[a,h]anthracene 2 1.0Not Detected

132-64-9 Dibenzofuran 4 1.0Not Detected

84-66-2 Diethylphthalate 5.1 1.0Not Detected

131-11-3 Dimethyl phthalate 5.1 1.0Not Detected

84-74-2 Di-n-butyl phthalate 5.1 1.0Not Detected

117-84-0 Di-n-octyl phthalate 5.1 1.0Not Detected

206-44-0 Fluoranthene 1 1.0Not Detected

86-73-7 Fluorene 1 1.0Not Detected

118-74-1 Hexachlorobenzene 1 1.0Not Detected

87-68-3 Hexachlorobutadiene 1 1.0Not Detected

77-47-4 Hexachlorocyclopentadiene 5Z10 1.0Not Detected

67-72-1 Hexachloroethane 1 1.0Not Detected

193-39-5 Indeno(1,2,3-c,d)pyrene 2 1.0Not Detected

78-59-1 Isophorone 1 1.0Not Detected

CAS# : Chemical Abstract Service Registry Number

RL : Reporting Limit

ND : Not Detected ug / L : microgram / liter (ppb) mg / L : milligram / liter (ppm) ug / Kg : microgram / kilogram (ppb) mg / Kg : milligram / kilogram (ppm)

Laboratory Contacts

Inorganic Unit Mgr: Sandy Gregg

Organic Unit Mgr: Carol Smith

Page 64 of 10090400113Lab Work Order #:

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

CORRECTED REPORT

Sample Number: AB32573 SB-9 (5-10')

Base Neutral Acid Compounds

Compound

Date Tested:

RL

Analytical Method:

CAS #

8270 Analyst:

Qualifier

04/21/2009 SMH

Extraction Method: Extraction Date: 04/16/2009 990Volume:3510 Qualifier:

Dilution FactorResult ug/L

121-69-7 N,N-dimethylaniline 5.1 1.0Not Detected

91-20-3 Naphthalene 1 1.03.5

98-95-3 Nitrobenzene 2 1.0Not Detected

100-61-8 N-methylaniline 1 1.0Not Detected

67-75-9 N-Nitrosodimethylamine 5.1 1.0Not Detected

621-64-7 N-Nitrosodi-n-propylamine 2 1.0Not Detected

86-30-6 N-Nitrosodiphenylamine 2 1.0Not Detected

87-86-5 Pentachlorophenol 20 1.0Not Detected

85-01-8 Phenanthrene 1 1.0Not Detected

108-95-2 Phenol 5.1 1.0Not Detected

129-00-0 Pyrene 1 1.0Not Detected

110-86-1 Pyridine 20 1.0Not Detected

632-22-4 Tetramethylurea 1 1.0Not Detected

Probable petroleum product(s) present.

PCBs as Aroclors

Compound

Date Tested:

RL

Analytical Method:

CAS #

8082 Analyst:

Qualifier

04/24/2009 MF

Extraction Method: Extraction Date: 04/14/2009 960Volume:3510 Qualifier:

Dilution FactorResult ug/L

SURROGATE #Decachlorobiphenyl# 42.7

SURROGATE #Tetrachloro-m-xylene# 41.1

12674-11-2 Aroclor 1016 0.1 1.0Not Detected

11104-28-2 Aroclor 1221 0.1 1.0Not Detected

11141-16-5 Aroclor 1232 0.1 1.0Not Detected

53469-21-9 Aroclor 1242 0.1 1.0Not Detected

12672-29-6 Aroclor 1248 0.1 1.0Not Detected

11097-69-1 Aroclor 1254 0.1 1.0Not Detected

11096-82-5 Aroclor 1260 0.1 1.0Not Detected

37324-23-5 Aroclor 1262 0.1 1.0Not Detected

11100-14-4 Aroclor 1268 0.1 1.0Not Detected

CAS# : Chemical Abstract Service Registry Number

RL : Reporting Limit

ND : Not Detected ug / L : microgram / liter (ppb) mg / L : milligram / liter (ppm) ug / Kg : microgram / kilogram (ppb) mg / Kg : milligram / kilogram (ppm)

Laboratory Contacts

Inorganic Unit Mgr: Sandy Gregg

Organic Unit Mgr: Carol Smith

Page 65 of 10090400113Lab Work Order #:

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

CORRECTED REPORT

Sample Number: AB32573 SB-9 (5-10')

Date TestedAnalyte Name MethodCAS# QualifierResult AnalystRLUnit

Dig. Diss. Metals Water KS3010/20004/17/2009Completed

7440-43-9 Cadmium - Dissolved KS6020/200.804/27/20090.2µg/LND

7440-47-3 Chromium - Dissolved KS6020/200.804/27/20091µg/L1.5

7439-92-1 Lead - Dissolved KS6020/200.804/27/20091µg/LND

Florisil Cleanup DT362004/21/2009Completed

Gel Permeation Cleanup DT364004/20/2009Completed

CAS# : Chemical Abstract Service Registry Number

RL : Reporting Limit

ND : Not Detected ug / L : microgram / liter (ppb) mg / L : milligram / liter (ppm) ug / Kg : microgram / kilogram (ppb) mg / Kg : milligram / kilogram (ppm)

Laboratory Contacts

Inorganic Unit Mgr: Sandy Gregg

Organic Unit Mgr: Carol Smith

Page 66 of 10090400113Lab Work Order #:

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

CORRECTED REPORT

Sample Number: AB32574 EQUIPMENT BLANK-1

Volatile Compounds

Compound

Date Tested:

RL

Analytical Method:

CAS #

8260 Analyst:

Qualifier

04/13/2009 RD

Dilution FactorResult ug/L

SURROGATE #Bromofluorobenzene# 102

SURROGATE #Dibromofluoromethane# 99.9

SURROGATE #Toluene-d8# 99.2

630-20-6 1,1,1,2-Tetrachloroethane 1 1.0Not Detected

71-55-6 1,1,1-Trichloroethane 1 1.0Not Detected

79-34-5 1,1,2,2-Tetrachloroethane 1 1.0Not Detected

79-00-5 1,1,2-Trichloroethane 1 1.0Not Detected

75-34-3 1,1-Dichloroethane 1 1.0Not Detected

75-35-4 1,1-Dichloroethylene 1 1.0Not Detected

87-61-6 1,2,3-Trichlorobenzene 5 1.0Not Detected

96-18-4 1,2,3-Trichloropropane 1 1.0Not Detected

526-73-8 1,2,3-Trimethylbenzene 1 1.0Not Detected

120-82-1 1,2,4-Trichlorobenzene 5 1.0Not Detected

95-63-6 1,2,4-Trimethylbenzene 1 1.0Not Detected

96-12-8 1,2-Dibromo-3-chloropropane 5 1.0Not Detected

106-93-4 1,2-Dibromoethane 1 1.0Not Detected

95-50-1 1,2-Dichlorobenzene 1 1.0Not Detected

107-06-2 1,2-Dichloroethane 1 1.0Not Detected

78-87-5 1,2-Dichloropropane 1 1.0Not Detected

108-67-8 1,3,5-Trimethylbenzene 1 1.0Not Detected

541-73-1 1,3-Dichlorobenzene 1 1.0Not Detected

106-46-7 1,4-Dichlorobenzene 1 1.0Not Detected

78-93-3 2-Butanone (MEK) 5 1.0Not Detected

591-78-6 2-Hexanone 5 1.0Not Detected

91-57-6 2-Methylnaphthalene X 55 1.0Not Detected

67-64-1 2-Propanone (acetone) 20 1.0Not Detected

108-10-1 4-Methyl-2-pentanone (MIBK) 5 1.0Not Detected

107-13-1 Acrylonitrile Z5 1.0Not Detected

71-43-2 Benzene 1 1.0Not Detected

108-86-1 Bromobenzene 1 1.0Not Detected

74-97-5 Bromochloromethane 1 1.0Not Detected

75-27-4 Bromodichloromethane 1 1.0Not Detected

75-25-2 Bromoform 1 1.0Not Detected

74-83-9 Bromomethane 5 1.0Not Detected

75-15-0 Carbon disulfide 1 1.0Not Detected

56-23-5 Carbon tetrachloride 1 1.0Not Detected

108-90-7 Chlorobenzene 1 1.0Not Detected

75-00-3 Chloroethane 5 1.0Not Detected

67-66-3 Chloroform 1 1.0Not Detected

74-87-3 Chloromethane 5 1.0Not Detected

CAS# : Chemical Abstract Service Registry Number

RL : Reporting Limit

ND : Not Detected ug / L : microgram / liter (ppb) mg / L : milligram / liter (ppm) ug / Kg : microgram / kilogram (ppb) mg / Kg : milligram / kilogram (ppm)

Laboratory Contacts

Inorganic Unit Mgr: Sandy Gregg

Organic Unit Mgr: Carol Smith

Page 67 of 10090400113Lab Work Order #:

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

CORRECTED REPORT

Sample Number: AB32574 EQUIPMENT BLANK-1

Volatile Compounds

Compound

Date Tested:

RL

Analytical Method:

CAS #

8260 Analyst:

Qualifier

04/13/2009 RD

Dilution FactorResult ug/L

156-59-2 cis-1,2-Dichloroethylene 1 1.0Not Detected

10061-01-5 cis-1,3-Dichloropropylene 1 1.0Not Detected

110-82-7 Cyclohexane 5 1.0Not Detected

124-48-1 Dibromochloromethane 1 1.0Not Detected

74-95-3 Dibromomethane 1 1.0Not Detected

75-71-8 Dichlorodifluoromethane 75 1.0Not Detected

60-29-7 Diethyl ether 5 1.0Not Detected

108-20-3 Diisopropyl Ether 5 1.0Not Detected

100-41-4 Ethylbenzene 1 1.0Not Detected

637-92-3 Ethyltertiarybutylether 5 1.0Not Detected

67-72-1 Hexachloroethane 5 1.0Not Detected

98-82-8 Isopropylbenzene 1 1.0Not Detected

108383,106423 m & p - Xylene 2 1.0Not Detected

74-88-4 Methyl iodide 1 1.0Not Detected

75-09-2 Methylene chloride 5 1.0Not Detected

1634-04-4 Methyltertiarybutylether 1 1.0Not Detected

91-20-3 Naphthalene X5 1.0Not Detected

104-51-8 n-Butylbenzene 1 1.0Not Detected

103-65-1 n-Propylbenzene 1 1.0Not Detected

95-47-6 o-Xylene 1 1.0Not Detected

99-87-6 p-Isopropyl toluene 1 1.0Not Detected

135-98-8 sec-Butylbenzene 1 1.0Not Detected

100-42-5 Styrene 1 1.0Not Detected

98-06-6 tert-Butylbenzene 1 1.0Not Detected

75-65-0 tertiary Butyl Alcohol 50 1.0Not Detected

994-05-8 tertiaryAmylmethylether 5 1.0Not Detected

127-18-4 Tetrachloroethylene 1 1.0Not Detected

109-99-9 Tetrahydrofuran 5 1.0Not Detected

108-88-3 Toluene 1 1.0Not Detected

156-60-5 trans-1,2-Dichloroethylene 1 1.0Not Detected

10061-02-6 trans-1,3-Dichloropropylene 1 1.0Not Detected

110-57-6 trans-1,4-Dichloro-2-butene Z5 1.0Not Detected

79-01-6 Trichloroethylene 1 1.0Not Detected

75-69-4 Trichlorofluoromethane 1 1.0Not Detected

75-01-4 Vinyl chloride 1 1.0Not Detected

CAS# : Chemical Abstract Service Registry Number

RL : Reporting Limit

ND : Not Detected ug / L : microgram / liter (ppb) mg / L : milligram / liter (ppm) ug / Kg : microgram / kilogram (ppb) mg / Kg : milligram / kilogram (ppm)

Laboratory Contacts

Inorganic Unit Mgr: Sandy Gregg

Organic Unit Mgr: Carol Smith

Page 68 of 10090400113Lab Work Order #:

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

CORRECTED REPORT

Sample Number: AB32574 EQUIPMENT BLANK-1

Base Neutral Acid Compounds

Compound

Date Tested:

RL

Analytical Method:

CAS #

8270 Analyst:

Qualifier

04/21/2009 SMH

Extraction Method: Extraction Date: 04/16/2009 980Volume:3510 Qualifier:

Dilution FactorResult ug/L

SURROGATE #2 - Fluorobiphenyl# 59.8

SURROGATE #2,4,6-Tribromophenol# 78.4

SURROGATE #2-Fluorophenol# 22.5

SURROGATE #Nitrobenzene - D5# 58.5

SURROGATE #Phenol - D6# 12.5

SURROGATE #p-Terphenyl-D14# 86.5

120-82-1 1,2,4-Trichlorobenzene 2 1.0Not Detected

95-95-4 2,4,5-Trichlorophenol 5.1 1.0Not Detected

88-06-2 2,4,6-Trichlorophenol 4.1 1.0Not Detected

120-83-2 2,4-Dichlorophenol 10 1.0Not Detected

105-67-9 2,4-Dimethylphenol 5.1 1.0Not Detected

51-28-5 2,4-Dinitrophenol 26 1.0Not Detected

121-14-2 2,4-Dinitrotoluene 5.1 1.0Not Detected

606-20-2 2,6-Dinitrotoluene 5.1 1.0Not Detected

95-51-2 2-Chloroaniline 5.1 1.0Not Detected

91-58-7 2-Chloronaphthalene 2 1.0Not Detected

95-57-8 2-Chlorophenol 10 1.0Not Detected

534-52-1 2-Methyl-4,6-dinitrophenol 20 1.0Not Detected

91-57-6 2-Methylnaphthalene 5.1 1.0Not Detected

95-48-7 2-Methylphenol (o-Cresol) 10 1.0Not Detected

88-74-4 2-Nitroaniline 20 1.0Not Detected

88-75-5 2-Nitrophenol 5.1 1.0Not Detected

108394,106445 3 & 4-Methylphenol 20 1.0Not Detected

99-09-2 3-Nitroaniline 20 1.0Not Detected

101-55-3 4-Bromophenyl phenyl ether 2 1.0Not Detected

59-50-7 4-Chloro-3-methyl-phenol 5.1 1.0Not Detected

106-47-8 4-Chloroaniline 10 1.0Not Detected

7005-72-3 4-Chlorodiphenylether 1 1.0Not Detected

100-01-6 4-Nitroaniline 20 1.0Not Detected

100-02-7 4-Nitrophenol 26 1.0Not Detected

83-32-9 Acenaphthene 1 1.0Not Detected

208-96-8 Acenaphthylene 1 1.0Not Detected

62-53-3 Aniline 4.1 1.0Not Detected

120-12-7 Anthracene 1 1.0Not Detected

103-33-3 Azobenzene 2 1.0Not Detected

56-55-3 Benzo[a]anthracene 1 1.0Not Detected

50-32-8 Benzo[a]pyrene 1 1.0Not Detected

205-99-2 Benzo[b]fluoranthene 1 1.0Not Detected

191-24-2 Benzo[g,h,i]perylene 1 1.0Not Detected

207-08-9 Benzo[k]fluoranthene 1 1.0Not Detected

CAS# : Chemical Abstract Service Registry Number

RL : Reporting Limit

ND : Not Detected ug / L : microgram / liter (ppb) mg / L : milligram / liter (ppm) ug / Kg : microgram / kilogram (ppb) mg / Kg : milligram / kilogram (ppm)

Laboratory Contacts

Inorganic Unit Mgr: Sandy Gregg

Organic Unit Mgr: Carol Smith

Page 69 of 10090400113Lab Work Order #:

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

CORRECTED REPORT

Sample Number: AB32574 EQUIPMENT BLANK-1

Base Neutral Acid Compounds

Compound

Date Tested:

RL

Analytical Method:

CAS #

8270 Analyst:

Qualifier

04/21/2009 SMH

Extraction Method: Extraction Date: 04/16/2009 980Volume:3510 Qualifier:

Dilution FactorResult ug/L

100-51-6 Benzyl Alcohol 551 1.0Not Detected

111-91-1 Bis(2-chloroethoxy)methane 2 1.0Not Detected

111-44-4 Bis(2-chloroethyl)ether 1 1.0Not Detected

108-60-1 Bis(2-chloroisopropyl)ether 1 1.0Not Detected

117-81-7 Bis(2-ethylhexyl)phthalate 5.1 1.0Not Detected

85-68-7 Butyl benzyl phthalate 5.1 1.0Not Detected

86-74-8 Carbazole 5.1 1.0Not Detected

218-01-9 Chrysene 1 1.0Not Detected

53-70-3 Dibenz[a,h]anthracene 2 1.0Not Detected

132-64-9 Dibenzofuran 4.1 1.0Not Detected

84-66-2 Diethylphthalate 5.1 1.0Not Detected

131-11-3 Dimethyl phthalate 5.1 1.0Not Detected

84-74-2 Di-n-butyl phthalate 5.1 1.0Not Detected

117-84-0 Di-n-octyl phthalate 5.1 1.0Not Detected

206-44-0 Fluoranthene 1 1.0Not Detected

86-73-7 Fluorene 1 1.0Not Detected

118-74-1 Hexachlorobenzene 1 1.0Not Detected

87-68-3 Hexachlorobutadiene 1 1.0Not Detected

77-47-4 Hexachlorocyclopentadiene 5Z10 1.0Not Detected

67-72-1 Hexachloroethane 1 1.0Not Detected

193-39-5 Indeno(1,2,3-c,d)pyrene 2 1.0Not Detected

78-59-1 Isophorone 1 1.0Not Detected

121-69-7 N,N-dimethylaniline 5.1 1.0Not Detected

91-20-3 Naphthalene 1 1.0Not Detected

98-95-3 Nitrobenzene 2 1.0Not Detected

100-61-8 N-methylaniline 1 1.0Not Detected

67-75-9 N-Nitrosodimethylamine 5.1 1.0Not Detected

621-64-7 N-Nitrosodi-n-propylamine 2 1.0Not Detected

86-30-6 N-Nitrosodiphenylamine 2 1.0Not Detected

87-86-5 Pentachlorophenol 20 1.0Not Detected

85-01-8 Phenanthrene 1 1.0Not Detected

108-95-2 Phenol 5.1 1.0Not Detected

129-00-0 Pyrene 1 1.0Not Detected

110-86-1 Pyridine 20 1.0Not Detected

632-22-4 Tetramethylurea 1 1.0Not Detected

CAS# : Chemical Abstract Service Registry Number

RL : Reporting Limit

ND : Not Detected ug / L : microgram / liter (ppb) mg / L : milligram / liter (ppm) ug / Kg : microgram / kilogram (ppb) mg / Kg : milligram / kilogram (ppm)

Laboratory Contacts

Inorganic Unit Mgr: Sandy Gregg

Organic Unit Mgr: Carol Smith

Page 70 of 10090400113Lab Work Order #:

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

CORRECTED REPORT

Sample Number: AB32574 EQUIPMENT BLANK-1

PCBs as Aroclors

Compound

Date Tested:

RL

Analytical Method:

CAS #

8082 Analyst:

Qualifier

04/24/2009 MF

Extraction Method: Extraction Date: 04/14/2009 960Volume:3510 Qualifier:

Dilution FactorResult ug/L

SURROGATE #Decachlorobiphenyl# 52.2

SURROGATE #Tetrachloro-m-xylene# 60.4

12674-11-2 Aroclor 1016 0.1 1.0Not Detected

11104-28-2 Aroclor 1221 0.1 1.0Not Detected

11141-16-5 Aroclor 1232 0.1 1.0Not Detected

53469-21-9 Aroclor 1242 0.1 1.0Not Detected

12672-29-6 Aroclor 1248 0.1 1.0Not Detected

11097-69-1 Aroclor 1254 0.1 1.0Not Detected

11096-82-5 Aroclor 1260 0.1 1.0Not Detected

37324-23-5 Aroclor 1262 0.1 1.0Not Detected

11100-14-4 Aroclor 1268 0.1 1.0Not Detected

Sample Number: AB32574 EQUIPMENT BLANK-1

Date TestedAnalyte Name MethodCAS# QualifierResult AnalystRLUnit

Lab Filtration DS120004/10/2009Completed

Dig. Diss. Metals Water KS3010/20004/17/2009Completed

7440-43-9 Cadmium - Dissolved KS6020/200.804/27/20090.2µg/LND

7440-47-3 Chromium - Dissolved KS6020/200.804/27/20091µg/LND

7439-92-1 Lead - Dissolved KS6020/200.804/27/20091µg/LND

Florisil Cleanup DT362004/21/2009Completed

Gel Permeation Cleanup DT364004/20/2009Completed

CAS# : Chemical Abstract Service Registry Number

RL : Reporting Limit

ND : Not Detected ug / L : microgram / liter (ppb) mg / L : milligram / liter (ppm) ug / Kg : microgram / kilogram (ppb) mg / Kg : milligram / kilogram (ppm)

Laboratory Contacts

Inorganic Unit Mgr: Sandy Gregg

Organic Unit Mgr: Carol Smith

Page 71 of 10090400113Lab Work Order #:

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

CORRECTED REPORT

Sample Number: AB32575 TRIP BLANK

Volatile Compounds

Compound

Date Tested:

RL

Analytical Method:

CAS #

8260 Analyst:

Qualifier

04/13/2009 RD

Dilution FactorResult ug/L

SURROGATE #Bromofluorobenzene# 102

SURROGATE #Dibromofluoromethane# 98.3

SURROGATE #Toluene-d8# 99.3

630-20-6 1,1,1,2-Tetrachloroethane 1 1.0Not Detected

71-55-6 1,1,1-Trichloroethane 1 1.0Not Detected

79-34-5 1,1,2,2-Tetrachloroethane 1 1.0Not Detected

79-00-5 1,1,2-Trichloroethane 1 1.0Not Detected

75-34-3 1,1-Dichloroethane 1 1.0Not Detected

75-35-4 1,1-Dichloroethylene 1 1.0Not Detected

87-61-6 1,2,3-Trichlorobenzene 5 1.0Not Detected

96-18-4 1,2,3-Trichloropropane 1 1.0Not Detected

526-73-8 1,2,3-Trimethylbenzene 1 1.0Not Detected

120-82-1 1,2,4-Trichlorobenzene 5 1.0Not Detected

95-63-6 1,2,4-Trimethylbenzene 1 1.0Not Detected

96-12-8 1,2-Dibromo-3-chloropropane 5 1.0Not Detected

106-93-4 1,2-Dibromoethane 1 1.0Not Detected

95-50-1 1,2-Dichlorobenzene 1 1.0Not Detected

107-06-2 1,2-Dichloroethane 1 1.0Not Detected

78-87-5 1,2-Dichloropropane 1 1.0Not Detected

108-67-8 1,3,5-Trimethylbenzene 1 1.0Not Detected

541-73-1 1,3-Dichlorobenzene 1 1.0Not Detected

106-46-7 1,4-Dichlorobenzene 1 1.0Not Detected

78-93-3 2-Butanone (MEK) 5 1.0Not Detected

591-78-6 2-Hexanone 5 1.0Not Detected

91-57-6 2-Methylnaphthalene X 55 1.0Not Detected

67-64-1 2-Propanone (acetone) 20 1.0Not Detected

108-10-1 4-Methyl-2-pentanone (MIBK) 5 1.0Not Detected

107-13-1 Acrylonitrile Z5 1.0Not Detected

71-43-2 Benzene 1 1.0Not Detected

108-86-1 Bromobenzene 1 1.0Not Detected

74-97-5 Bromochloromethane 1 1.0Not Detected

75-27-4 Bromodichloromethane 1 1.0Not Detected

75-25-2 Bromoform 1 1.0Not Detected

74-83-9 Bromomethane 5 1.0Not Detected

75-15-0 Carbon disulfide 1 1.0Not Detected

56-23-5 Carbon tetrachloride 1 1.0Not Detected

108-90-7 Chlorobenzene 1 1.0Not Detected

75-00-3 Chloroethane 5 1.0Not Detected

67-66-3 Chloroform 1 1.0Not Detected

74-87-3 Chloromethane 5 1.0Not Detected

CAS# : Chemical Abstract Service Registry Number

RL : Reporting Limit

ND : Not Detected ug / L : microgram / liter (ppb) mg / L : milligram / liter (ppm) ug / Kg : microgram / kilogram (ppb) mg / Kg : milligram / kilogram (ppm)

Laboratory Contacts

Inorganic Unit Mgr: Sandy Gregg

Organic Unit Mgr: Carol Smith

Page 72 of 10090400113Lab Work Order #:

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

CORRECTED REPORT

Sample Number: AB32575 TRIP BLANK

Volatile Compounds

Compound

Date Tested:

RL

Analytical Method:

CAS #

8260 Analyst:

Qualifier

04/13/2009 RD

Dilution FactorResult ug/L

156-59-2 cis-1,2-Dichloroethylene 1 1.0Not Detected

10061-01-5 cis-1,3-Dichloropropylene 1 1.0Not Detected

110-82-7 Cyclohexane 5 1.0Not Detected

124-48-1 Dibromochloromethane 1 1.0Not Detected

74-95-3 Dibromomethane 1 1.0Not Detected

75-71-8 Dichlorodifluoromethane 75 1.0Not Detected

60-29-7 Diethyl ether 5 1.0Not Detected

108-20-3 Diisopropyl Ether 5 1.0Not Detected

100-41-4 Ethylbenzene 1 1.0Not Detected

637-92-3 Ethyltertiarybutylether 5 1.0Not Detected

67-72-1 Hexachloroethane 5 1.0Not Detected

98-82-8 Isopropylbenzene 1 1.0Not Detected

108383,106423 m & p - Xylene 2 1.0Not Detected

74-88-4 Methyl iodide 1 1.0Not Detected

75-09-2 Methylene chloride 5 1.0Not Detected

1634-04-4 Methyltertiarybutylether 1 1.0Not Detected

91-20-3 Naphthalene X5 1.0Not Detected

104-51-8 n-Butylbenzene 1 1.0Not Detected

103-65-1 n-Propylbenzene 1 1.0Not Detected

95-47-6 o-Xylene 1 1.0Not Detected

99-87-6 p-Isopropyl toluene 1 1.0Not Detected

135-98-8 sec-Butylbenzene 1 1.0Not Detected

100-42-5 Styrene 1 1.0Not Detected

98-06-6 tert-Butylbenzene 1 1.0Not Detected

75-65-0 tertiary Butyl Alcohol 50 1.0Not Detected

994-05-8 tertiaryAmylmethylether 5 1.0Not Detected

127-18-4 Tetrachloroethylene 1 1.0Not Detected

109-99-9 Tetrahydrofuran 5 1.0Not Detected

108-88-3 Toluene 1 1.0Not Detected

156-60-5 trans-1,2-Dichloroethylene 1 1.0Not Detected

10061-02-6 trans-1,3-Dichloropropylene 1 1.0Not Detected

110-57-6 trans-1,4-Dichloro-2-butene Z5 1.0Not Detected

79-01-6 Trichloroethylene 1 1.0Not Detected

75-69-4 Trichlorofluoromethane 1 1.0Not Detected

75-01-4 Vinyl chloride 1 1.0Not Detected

CAS# : Chemical Abstract Service Registry Number

RL : Reporting Limit

ND : Not Detected ug / L : microgram / liter (ppb) mg / L : milligram / liter (ppm) ug / Kg : microgram / kilogram (ppb) mg / Kg : milligram / kilogram (ppm)

Laboratory Contacts

Inorganic Unit Mgr: Sandy Gregg

Organic Unit Mgr: Carol Smith

Page 73 of 10090400113Lab Work Order #:

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

CORRECTED REPORT

Sample Number: AB32576 SB-10 (5-10')

Library Search-Volatiles

Compound

Date Tested:

RL

Analytical Method:

CAS #

8260 Analyst:

Qualifier

04/14/2009 KCL

Dilution FactorResult ug/L

1-Methyl naphthalene LB7.8

Dihydro methyl Indene LB42

Dimethyl dihydro Indene LB7.8

Dimethyl dihydro Indene isomer LB15

Dimethyl dihydro Indene isomer 3 LB36

Dimethyl dihydro Indene isomer 4 LB7.8

Dimethyl dihydro Indene isomer 5 LB8.2

Dimethyl dihydro Indene isomer 6 LB14

Ethyl methyl benzene LB5.1

Methyl butenyl benzene LB11

Methyl Indan LB14

Methyl Indan isomer LB7.3

Methyl methylethyl benzene LB13

Pentamethyl benzene LB8.3

Propenyl benzene LB15

Tetramethyl benzene LB10

Tetramethyl benzene isomer LB18

Volatile Compounds

Compound

Date Tested:

RL

Analytical Method:

CAS #

8260 Analyst:

Qualifier

04/14/2009 KCL

Dilution FactorResult ug/L

SURROGATE #Bromofluorobenzene# 101

SURROGATE #Dibromofluoromethane# 97.1

SURROGATE #Toluene-d8# 96.2

630-20-6 1,1,1,2-Tetrachloroethane 1 1.0Not Detected

71-55-6 1,1,1-Trichloroethane 1 1.0Not Detected

79-34-5 1,1,2,2-Tetrachloroethane 1 1.0Not Detected

79-00-5 1,1,2-Trichloroethane 1 1.0Not Detected

75-34-3 1,1-Dichloroethane 1 1.0Not Detected

75-35-4 1,1-Dichloroethylene 1 1.0Not Detected

87-61-6 1,2,3-Trichlorobenzene 5 1.0Not Detected

96-18-4 1,2,3-Trichloropropane 1 1.0Not Detected

526-73-8 1,2,3-Trimethylbenzene 1 1.02.3

120-82-1 1,2,4-Trichlorobenzene 5 1.0Not Detected

95-63-6 1,2,4-Trimethylbenzene 1 1.08.1

96-12-8 1,2-Dibromo-3-chloropropane 5 1.0Not Detected

106-93-4 1,2-Dibromoethane 1 1.0Not Detected

CAS# : Chemical Abstract Service Registry Number

RL : Reporting Limit

ND : Not Detected ug / L : microgram / liter (ppb) mg / L : milligram / liter (ppm) ug / Kg : microgram / kilogram (ppb) mg / Kg : milligram / kilogram (ppm)

Laboratory Contacts

Inorganic Unit Mgr: Sandy Gregg

Organic Unit Mgr: Carol Smith

Page 74 of 10090400113Lab Work Order #:

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

CORRECTED REPORT

Sample Number: AB32576 SB-10 (5-10')

Volatile Compounds

Compound

Date Tested:

RL

Analytical Method:

CAS #

8260 Analyst:

Qualifier

04/14/2009 KCL

Dilution FactorResult ug/L

95-50-1 1,2-Dichlorobenzene 1 1.0Not Detected

107-06-2 1,2-Dichloroethane 1 1.0Not Detected

78-87-5 1,2-Dichloropropane 1 1.0Not Detected

108-67-8 1,3,5-Trimethylbenzene 1 1.0Not Detected

541-73-1 1,3-Dichlorobenzene 1 1.0Not Detected

106-46-7 1,4-Dichlorobenzene 1 1.0Not Detected

78-93-3 2-Butanone (MEK) 5 1.0Not Detected

591-78-6 2-Hexanone 5 1.0Not Detected

91-57-6 2-Methylnaphthalene X5 1.0Not Detected

67-64-1 2-Propanone (acetone) 20 1.0Not Detected

108-10-1 4-Methyl-2-pentanone (MIBK) 5 1.0Not Detected

107-13-1 Acrylonitrile Z5 1.0Not Detected

71-43-2 Benzene 1 1.0Not Detected

108-86-1 Bromobenzene 1 1.0Not Detected

74-97-5 Bromochloromethane 1 1.0Not Detected

75-27-4 Bromodichloromethane 1 1.0Not Detected

75-25-2 Bromoform 1 1.0Not Detected

74-83-9 Bromomethane 5 1.0Not Detected

75-15-0 Carbon disulfide 1 1.0Not Detected

56-23-5 Carbon tetrachloride 1 1.0Not Detected

108-90-7 Chlorobenzene 1 1.0Not Detected

75-00-3 Chloroethane 5 1.0Not Detected

67-66-3 Chloroform 1 1.0Not Detected

74-87-3 Chloromethane 5 1.0Not Detected

156-59-2 cis-1,2-Dichloroethylene 1 1.0Not Detected

10061-01-5 cis-1,3-Dichloropropylene 1 1.0Not Detected

110-82-7 Cyclohexane 5 1.0Not Detected

124-48-1 Dibromochloromethane 1 1.0Not Detected

74-95-3 Dibromomethane 1 1.0Not Detected

75-71-8 Dichlorodifluoromethane 5 1.0Not Detected

60-29-7 Diethyl ether 5 1.0Not Detected

108-20-3 Diisopropyl Ether 5 1.0Not Detected

100-41-4 Ethylbenzene 1 1.01.0

637-92-3 Ethyltertiarybutylether 5 1.0Not Detected

67-72-1 Hexachloroethane 5 1.0Not Detected

98-82-8 Isopropylbenzene 1 1.0Not Detected

108383,106423 m & p - Xylene 2 1.0Not Detected

74-88-4 Methyl iodide 1 1.0Not Detected

75-09-2 Methylene chloride 5 1.0Not Detected

1634-04-4 Methyltertiarybutylether 1 1.0Not Detected

CAS# : Chemical Abstract Service Registry Number

RL : Reporting Limit

ND : Not Detected ug / L : microgram / liter (ppb) mg / L : milligram / liter (ppm) ug / Kg : microgram / kilogram (ppb) mg / Kg : milligram / kilogram (ppm)

Laboratory Contacts

Inorganic Unit Mgr: Sandy Gregg

Organic Unit Mgr: Carol Smith

Page 75 of 10090400113Lab Work Order #:

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

CORRECTED REPORT

Sample Number: AB32576 SB-10 (5-10')

Volatile Compounds

Compound

Date Tested:

RL

Analytical Method:

CAS #

8260 Analyst:

Qualifier

04/14/2009 KCL

Dilution FactorResult ug/L

91-20-3 Naphthalene X5 1.0Not Detected

104-51-8 n-Butylbenzene 1 1.0Not Detected

103-65-1 n-Propylbenzene 1 1.0Not Detected

95-47-6 o-Xylene 1 1.0Not Detected

99-87-6 p-Isopropyl toluene 1 1.01.7

135-98-8 sec-Butylbenzene 1 1.01.1

100-42-5 Styrene 1 1.0Not Detected

98-06-6 tert-Butylbenzene 1 1.0Not Detected

75-65-0 tertiary Butyl Alcohol 50 1.0Not Detected

994-05-8 tertiaryAmylmethylether 5 1.0Not Detected

127-18-4 Tetrachloroethylene 1 1.0Not Detected

109-99-9 Tetrahydrofuran 5 1.0Not Detected

108-88-3 Toluene 1 1.0Not Detected

156-60-5 trans-1,2-Dichloroethylene 1 1.0Not Detected

10061-02-6 trans-1,3-Dichloropropylene 1 1.0Not Detected

110-57-6 trans-1,4-Dichloro-2-butene Z5 1.0Not Detected

79-01-6 Trichloroethylene 1 1.0Not Detected

75-69-4 Trichlorofluoromethane 1 1.0Not Detected

75-01-4 Vinyl chloride 1 1.0Not Detected

Unidentified peaks present in sample.

Base Neutral Acid Compounds

Compound

Date Tested:

RL

Analytical Method:

CAS #

8270 Analyst:

Qualifier

04/21/2009 SMH

Extraction Method: Extraction Date: 04/16/2009 970Volume:3510 Qualifier:

Dilution FactorResult ug/L

SURROGATE #2 - Fluorobiphenyl# 64.1

SURROGATE #2,4,6-Tribromophenol# 87.5

SURROGATE #2-Fluorophenol# 20.5

SURROGATE #Nitrobenzene - D5# 57.0

SURROGATE #Phenol - D6# 12.3

SURROGATE #p-Terphenyl-D14# 75.1

120-82-1 1,2,4-Trichlorobenzene 2.1 1.0Not Detected

95-95-4 2,4,5-Trichlorophenol 5.2 1.0Not Detected

88-06-2 2,4,6-Trichlorophenol 4.1 1.0Not Detected

120-83-2 2,4-Dichlorophenol 10 1.0Not Detected

105-67-9 2,4-Dimethylphenol 5.2 1.0Not Detected

51-28-5 2,4-Dinitrophenol 26 1.0Not Detected

121-14-2 2,4-Dinitrotoluene 5.2 1.0Not Detected

606-20-2 2,6-Dinitrotoluene 5.2 1.0Not Detected

CAS# : Chemical Abstract Service Registry Number

RL : Reporting Limit

ND : Not Detected ug / L : microgram / liter (ppb) mg / L : milligram / liter (ppm) ug / Kg : microgram / kilogram (ppb) mg / Kg : milligram / kilogram (ppm)

Laboratory Contacts

Inorganic Unit Mgr: Sandy Gregg

Organic Unit Mgr: Carol Smith

Page 76 of 10090400113Lab Work Order #:

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

CORRECTED REPORT

Sample Number: AB32576 SB-10 (5-10')

Base Neutral Acid Compounds

Compound

Date Tested:

RL

Analytical Method:

CAS #

8270 Analyst:

Qualifier

04/21/2009 SMH

Extraction Method: Extraction Date: 04/16/2009 970Volume:3510 Qualifier:

Dilution FactorResult ug/L

95-51-2 2-Chloroaniline 5.2 1.0Not Detected

91-58-7 2-Chloronaphthalene 2.1 1.0Not Detected

95-57-8 2-Chlorophenol 10 1.0Not Detected

534-52-1 2-Methyl-4,6-dinitrophenol 21 1.0Not Detected

91-57-6 2-Methylnaphthalene 5.2 1.0Not Detected

95-48-7 2-Methylphenol (o-Cresol) 10 1.0Not Detected

88-74-4 2-Nitroaniline 21 1.0Not Detected

88-75-5 2-Nitrophenol 5.2 1.0Not Detected

108394,106445 3 & 4-Methylphenol 21 1.0Not Detected

99-09-2 3-Nitroaniline 21 1.0Not Detected

101-55-3 4-Bromophenyl phenyl ether 2.1 1.0Not Detected

59-50-7 4-Chloro-3-methyl-phenol 5.2 1.0Not Detected

106-47-8 4-Chloroaniline 10 1.0Not Detected

7005-72-3 4-Chlorodiphenylether 1 1.0Not Detected

100-01-6 4-Nitroaniline 21 1.0Not Detected

100-02-7 4-Nitrophenol 26 1.0Not Detected

83-32-9 Acenaphthene 1 1.0Not Detected

208-96-8 Acenaphthylene 1 1.0Not Detected

62-53-3 Aniline 4.1 1.0Not Detected

120-12-7 Anthracene 1 1.0Not Detected

103-33-3 Azobenzene 2.1 1.0Not Detected

56-55-3 Benzo[a]anthracene 1 1.0Not Detected

50-32-8 Benzo[a]pyrene 1 1.0Not Detected

205-99-2 Benzo[b]fluoranthene 1 1.0Not Detected

191-24-2 Benzo[g,h,i]perylene 1 1.0Not Detected

207-08-9 Benzo[k]fluoranthene 1 1.0Not Detected

100-51-6 Benzyl Alcohol 552 1.0Not Detected

111-91-1 Bis(2-chloroethoxy)methane 2.1 1.0Not Detected

111-44-4 Bis(2-chloroethyl)ether 1 1.0Not Detected

108-60-1 Bis(2-chloroisopropyl)ether 1 1.0Not Detected

117-81-7 Bis(2-ethylhexyl)phthalate 5.2 1.0Not Detected

85-68-7 Butyl benzyl phthalate 5.2 1.0Not Detected

86-74-8 Carbazole 5.2 1.0Not Detected

218-01-9 Chrysene 1 1.0Not Detected

53-70-3 Dibenz[a,h]anthracene 2.1 1.0Not Detected

132-64-9 Dibenzofuran 4.1 1.0Not Detected

84-66-2 Diethylphthalate 5.2 1.0Not Detected

131-11-3 Dimethyl phthalate 5.2 1.0Not Detected

84-74-2 Di-n-butyl phthalate 5.2 1.0Not Detected

117-84-0 Di-n-octyl phthalate 5.2 1.0Not Detected

CAS# : Chemical Abstract Service Registry…

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