Part 5 Reference Reports Wayne Oakland DCSpec_Rev_02-19.pdf
PDF 5 MB Posted
- Attached to
- 761/20035. SAR Former Wayne Oakland Oil
- Solicitation number
- RFQ 171 200000000255 5
- Issued by
- Benzie County, Riverview City, Michigan
About this file
Summary
This document comprises laboratory analysis reports from the Michigan Department of Environmental Quality Environmental Laboratory related to environmental testing conducted at the Wayne Oakland Oil site (Project No. 3940096) located in Royal Oak, Michigan. The testing involved groundwater and soil samples collected between March and December 2009 to assess contamination from petroleum products. The laboratory performed comprehensive chemical analysis including volatile organic compounds (VOCs), semi-volatile organic compounds (SVOCs), pesticides, PCBs, and heavy metals testing using EPA-approved analytical methods including Methods 8260, 8270, 8082, and various inorganic digestion methods. Multiple sample types were analyzed, including monitoring well water samples, soil boring samples, and quality control samples (trip blanks, field blanks, equipment blanks, and matrix spike/matrix spike duplicate samples).
The laboratory reports document analysis of approximately 78 water samples and 16 soil samples with total charges of $8,209.00 for water testing (Work Order #90400113) and $8,261.00 for additional water testing, along with separate sediment analysis charges of $804.50 and $2,589.50. Results indicated presence of petroleum-related compounds including naphthalene, methylnaphthalene, benzene, and other aromatic hydrocarbons in groundwater at depths between 5 and 11.5 feet below grade. Lead concentrations in certain soil samples exceeded background levels (ranging up to 1,700 micrograms per kilogram), while most volatile and semi-volatile organic analytes and pesticides were non-detected. The completion dates ranged from June 3 through January 14, 2010, with samples collected by Mike Brennan of the MDEQ-RRD Warren Southeast Michigan District Office.
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1.00 1.50
2.50
9.00
11.00
647.51 647.01
646.01
639.51
637.51
Concrete
Natural Collapse
Bentonite Chips
Filter Pack Sand
PVC Screen
Natural Collapse
D E
P T
H (f t.)
CONSTRUCTION
REMARKS
E
LE
V A
T
IO
N (f t.)
WELL
DETAILS
S Y
M B
O L
D E
P T
H (f t.)WELL CONSTRUCTION DETAILS V A
S
STRATA
0.0
WATER LEVEL:
DATE:
TIME:
Wayne Oakland Oil 3940096 Royal Oak, MI
SEAL
DRILLING CONTRACTOR:
DRILLING METHOD:
DATE COMPLETED:
0.000.49'
Type:
Interval:
None None
GS
SANDPACK
Diameter:
Type:
Interval:
Diameter:
Type:
Interval:
648.5
USGS
M. Brennan
8" Steel 0 ft above grade to 1 ft below grade
SCREEN
PROJECT:
PROJECT NO:
PROJECT LOCATION:
GROUND SURFACE ELEVATION:
DATUM:
LOGGED BY:
Sand Filter Pack 2.5-9 ft below grade
Sheet 1 of 1COMPLETION REPORT OF WELL No. MW-1 / SB-14
TRC
2"
PVC
0.49 - 4 ft below grade
Type:
Interval:
PROTECTIVE CASING
648.51
Type:
Interval:
WELL DEVELOPMENT DATA
DATE:
METHOD:
7/29/2009
Overpumping with occasional surging.
Diameter:
Type:
Interval:
2"
PVC
4-9 ft below grade
Bentonite Chips
1.5 - 2.5 ft below grade
Terra Probe
Direct Push
7/29/2009
GROUT
RISER CASING
5.00 7/29/09
CONCRETE
CEMENT/BENTONITE GROUT
FILTER PACK
BENTONITE
BENTONITE/NATURAL COLLAPSE
FILL
SAND
SILT
CLAY
GRAVELLY CLAY
ASPHALT
TOPSOIL
INTERBEDDED SAND, SILT, CLAY
COMPLETION REPORT OF
WELL No. MW-1 / SB-14
Sheet 1 of 1
TPC
TRC
GS
TOP OF PROTECTIVE CASING
TOP OF RISER CASING
GROUND SURFACE
LEGEND
101 South Washington Square, Suite 400 Lansing, MI 48933 Telephone: (517) 337-0111 Fax: (517) 337-0417
3.00
9.00
648.03
646.03
640.03
Concrete
Natural Collapse
Bentonite Chips
Filter Pack Sand
PVC Screen
D E
P T
H (f t.)
CONSTRUCTION
REMARKS
E
LE
V A
T
IO
N (f t.)
WELL
DETAILS
S Y
M B
O L
D E
P T
H (f t.)WELL CONSTRUCTION DETAILS V A
S
STRATA
0.0
WATER LEVEL:
DATE:
TIME:
Wayne Oakland Oil 3940096 Royal Oak, MI
SEAL
DRILLING CONTRACTOR:
DRILLING METHOD:
DATE COMPLETED:
0.000.61'
Type:
Interval:
None None
GS
SANDPACK
Diameter:
Type:
Interval:
Diameter:
Type:
Interval:
649.0
USGS
M. Brennan
8" Steel 0 ft above grade to 1 ft below grade
SCREEN
PROJECT:
PROJECT NO:
PROJECT LOCATION:
GROUND SURFACE ELEVATION:
DATUM:
LOGGED BY:
Sand Filter Pack 3-9 ft below grade
Sheet 1 of 1COMPLETION REPORT OF WELL No. MW-2
TRC
2"
PVC
0.61 - 4 ft below grade
Type:
Interval:
PROTECTIVE CASING
649.03
Type:
Interval:
WELL DEVELOPMENT DATA
DATE:
METHOD:
7/29/2009
Overpumping with occasional surging.
Diameter:
Type:
Interval:
2"
PVC
4-9 ft below grade
Bentonite Chips 1 - 3 ft below grade
Terra Probe
4.25" HSA
7/29/2009
GROUT
RISER CASING
5.00
CONCRETE
CEMENT/BENTONITE GROUT
FILTER PACK
BENTONITE
BENTONITE/NATURAL COLLAPSE
FILL
SAND
SILT
CLAY
GRAVELLY CLAY
ASPHALT
TOPSOIL
INTERBEDDED SAND, SILT, CLAY
COMPLETION REPORT OF
WELL No. MW-2
Sheet 1 of 1
TPC
TRC
GS
TOP OF PROTECTIVE CASING
TOP OF RISER CASING
GROUND SURFACE
LEGEND
101 South Washington Square, Suite 400 Lansing, MI 48933
3.00
9.00
647.66
645.66
639.66
Concrete
Natural Collapse
Bentonite Chips
Filter Pack Sand
PVC Screen
D E
P T
H (f t.)
CONSTRUCTION
REMARKS
E
LE
V A
T
IO
N (f t.)
WELL
DETAILS
S Y
M B
O L
D E
P T
H (f t.)WELL CONSTRUCTION DETAILS V A
S
STRATA
0.0
WATER LEVEL:
DATE:
TIME:
Wayne Oakland Oil 3940096 Royal Oak, MI
SEAL
DRILLING CONTRACTOR:
DRILLING METHOD:
DATE COMPLETED:
0.000.52'
Type:
Interval:
None None
GS
SANDPACK
Diameter:
Type:
Interval:
Diameter:
Type:
Interval:
648.7
USGS
M. Brennan
8" Steel 0 ft above grade to 1 ft below grade
SCREEN
PROJECT:
PROJECT NO:
PROJECT LOCATION:
GROUND SURFACE ELEVATION:
DATUM:
LOGGED BY:
Sand Filter Pack 3-9 ft below grade
Sheet 1 of 1COMPLETION REPORT OF WELL No. MW-3
TRC
2"
PVC
0.52 - 4 ft below grade
Type:
Interval:
PROTECTIVE CASING
648.66
Type:
Interval:
WELL DEVELOPMENT DATA
DATE:
METHOD:
7/29/2009
Overpumping with occasional surging.
Diameter:
Type:
Interval:
2"
PVC
4-9 ft below grade
Bentonite Chips 1 - 3 ft below grade
Terra Probe
4.25" HSA
7/29/2009
GROUT
RISER CASING
5.00
CONCRETE
CEMENT/BENTONITE GROUT
FILTER PACK
BENTONITE
BENTONITE/NATURAL COLLAPSE
FILL
SAND
SILT
CLAY
GRAVELLY CLAY
ASPHALT
TOPSOIL
INTERBEDDED SAND, SILT, CLAY
COMPLETION REPORT OF
WELL No. MW-3
Sheet 1 of 1
TPC
TRC
GS
TOP OF PROTECTIVE CASING
TOP OF RISER CASING
GROUND SURFACE
LEGEND
101 South Washington Square, Suite 400 Lansing, MI 48933
3.50
9.50
12.00
647.59
645.09
639.09
636.59
Concrete
Natural Collapse
Bentonite Chips
Filter Pack Sand
PVC Screen
D E
P T
H (f t.)
CONSTRUCTION
REMARKS
E
LE
V A
T
IO
N (f t.)
WELL
DETAILS
S Y
M B
O L
D E
P T
H (f t.)WELL CONSTRUCTION DETAILS V A
S
STRATA
0.0
WATER LEVEL:
DATE:
TIME:
Wayne Oakland Oil 3940096 Royal Oak, MI
SEAL
DRILLING CONTRACTOR:
DRILLING METHOD:
DATE COMPLETED:
0.000.29'
Type:
Interval:
None None
GS
SANDPACK
Diameter:
Type:
Interval:
Diameter:
Type:
Interval:
648.6
USGS
M. Brennan
8" Steel 0 ft above grade to 1 ft below grade
SCREEN
PROJECT:
PROJECT NO:
PROJECT LOCATION:
GROUND SURFACE ELEVATION:
DATUM:
LOGGED BY:
Sand Filter Pack 3.5-12 ft below grade
Sheet 1 of 1COMPLETION REPORT OF WELL No. MW-4 / SB-MW-4
TRC
2"
PVC
0.29 - 4 ft below grade
Type:
Interval:
PROTECTIVE CASING
648.59
Type:
Interval:
WELL DEVELOPMENT DATA
DATE:
METHOD:
11/11/2009
Overpumping with occasional surging.
Diameter:
Type:
Interval:
2"
PVC
4.5-9.5 ft below grade
Bentonite Chips 1 - 3.5 ft below grade
Terra Probe
Direct Push / HSA
11/10/2009
GROUT
RISER CASING
6.00 11/10/09
CONCRETE
CEMENT/BENTONITE GROUT
FILTER PACK
BENTONITE
BENTONITE/NATURAL COLLAPSE
FILL
SAND
SILT
CLAY
GRAVELLY CLAY
ASPHALT
TOPSOIL
INTERBEDDED SAND, SILT, CLAY
COMPLETION REPORT OF
WELL No. MW-4 / SB-MW-4
Sheet 1 of 1
TPC
TRC
GS
TOP OF PROTECTIVE CASING
TOP OF RISER CASING
GROUND SURFACE
LEGEND
101 South Washington Square, Suite 400 Lansing, MI 48933
4.00
10.30
12.00
646.58
643.58
637.28
635.58
Concrete
Natural Collapse
Bentonite Chips
Filter Pack Sand
PVC Screen
Natural Collapse
D E
P T
H (f t.)
CONSTRUCTION
REMARKS
E
LE
V A
T
IO
N (f t.)
WELL
DETAILS
S Y
M B
O L
D E
P T
H (f t.)WELL CONSTRUCTION DETAILS V A
S
STRATA
0.0
WATER LEVEL:
DATE:
TIME:
Wayne Oakland Oil 3940096 Royal Oak, MI
SEAL
DRILLING CONTRACTOR:
DRILLING METHOD:
DATE COMPLETED:
0.000.39'
Type:
Interval:
None None
GS
SANDPACK
Diameter:
Type:
Interval:
Diameter:
Type:
Interval:
647.6
USGS
M. Brennan
8" Steel 0 ft above grade to 1 ft below grade
SCREEN
PROJECT:
PROJECT NO:
PROJECT LOCATION:
GROUND SURFACE ELEVATION:
DATUM:
LOGGED BY:
Sand Filter Pack 4-10.3 ft below grade
Sheet 1 of 1COMPLETION REPORT OF WELL No. MW-5 / SB-MW-5
TRC
2"
PVC
0.39 - 5.3 ft below grade
Type:
Interval:
PROTECTIVE CASING
647.58
Type:
Interval:
WELL DEVELOPMENT DATA
DATE:
METHOD:
11/10/2009
Overpumping with occasional surging.
Diameter:
Type:
Interval:
2"
PVC
5.3-10.3 ft below grade
Bentonite Chips 1 - 4 ft below grade
Terra Probe
Direct Push / HSA
11/10/2009
GROUT
RISER CASING
6.50 11/10/09
CONCRETE
CEMENT/BENTONITE GROUT
FILTER PACK
BENTONITE
BENTONITE/NATURAL COLLAPSE
FILL
SAND
SILT
CLAY
GRAVELLY CLAY
ASPHALT
TOPSOIL
INTERBEDDED SAND, SILT, CLAY
COMPLETION REPORT OF
WELL No. MW-5 / SB-MW-5
Sheet 1 of 1
TPC
TRC
GS
TOP OF PROTECTIVE CASING
TOP OF RISER CASING
GROUND SURFACE
LEGEND
101 South Washington Square, Suite 400 Lansing, MI 48933
9.20
12.00
647.48
644.98
639.28
636.48
Concrete
Natural Collapse
Bentonite Chips
Filter Pack Sand
PVC Screen
D E
P T
H (f t.)
CONSTRUCTION
REMARKS
E
LE
V A
T
IO
N (f t.)
WELL
DETAILS
S Y
M B
O L
D E
P T
H (f t.)WELL CONSTRUCTION DETAILS V A
S
STRATA
0.0
WATER LEVEL:
DATE:
TIME:
Wayne Oakland Oil 3940096 Royal Oak, MI
SEAL
DRILLING CONTRACTOR:
DRILLING METHOD:
DATE COMPLETED:
0.000.44'
Type:
Interval:
None None
GS
SANDPACK
Diameter:
Type:
Interval:
Diameter:
Type:
Interval:
648.5
USGS
M. Brennan
8" Steel 0 ft above grade to 1 ft below grade
SCREEN
PROJECT:
PROJECT NO:
PROJECT LOCATION:
GROUND SURFACE ELEVATION:
DATUM:
LOGGED BY:
Sand Filter Pack 3.5-12 ft below grade
Sheet 1 of 1COMPLETION REPORT OF WELL No. MW-6 / SB-MW-6
TRC
2"
PVC
0.44 - 4.2 ft below grade
Type:
Interval:
PROTECTIVE CASING
648.48
Type:
Interval:
WELL DEVELOPMENT DATA
DATE:
METHOD:
NA
NA
Diameter:
Type:
Interval:
2"
PVC
4.2-9.2 ft below grade
Bentonite Chips 1 - 3.5 ft below grade
Terra Probe
Direct Push / HSA
11/10/2009
GROUT
RISER CASING
6.50 11/10/09
CONCRETE
CEMENT/BENTONITE GROUT
FILTER PACK
BENTONITE
BENTONITE/NATURAL COLLAPSE
FILL
SAND
SILT
CLAY
GRAVELLY CLAY
ASPHALT
TOPSOIL
INTERBEDDED SAND, SILT, CLAY
COMPLETION REPORT OF
WELL No. MW-6 / SB-MW-6
Sheet 1 of 1
TPC
TRC
GS
TOP OF PROTECTIVE CASING
TOP OF RISER CASING
GROUND SURFACE
LEGEND
101 South Washington Square, Suite 400 Lansing, MI 48933
5.50
11.00
12.00
647.42
642.92
637.42
636.42
Concrete
Natural Collapse
Bentonite Chips
Filter Pack Sand PVC Screen
D E
P T
H (f t.)
CONSTRUCTION
REMARKS
E
LE
V A
T
IO
N (f t.)
WELL
DETAILS
S Y
M B
O L
D E
P T
H (f t.)WELL CONSTRUCTION DETAILS V A
S
STRATA
0.0
WATER LEVEL:
DATE:
TIME:
Wayne Oakland Oil 3940096 Royal Oak, MI
SEAL
DRILLING CONTRACTOR:
DRILLING METHOD:
DATE COMPLETED:
0.000.37'
Type:
Interval:
None None
GS
SANDPACK
Diameter:
Type:
Interval:
Diameter:
Type:
Interval:
648.4
USGS
M. Brennan
8" Steel 0 ft above grade to 1 ft below grade
SCREEN
PROJECT:
PROJECT NO:
PROJECT LOCATION:
GROUND SURFACE ELEVATION:
DATUM:
LOGGED BY:
Sand Filter Pack 5.5-12 ft below grade
Sheet 1 of 1COMPLETION REPORT OF WELL No. MW-7 / SB-MW-7
TRC
2"
PVC
0.37 - 4.2 ft below grade
Type:
Interval:
PROTECTIVE CASING
648.42
Type:
Interval:
WELL DEVELOPMENT DATA
DATE:
METHOD:
7/29/2010
Overpumping with occasional surging.
Diameter:
Type:
Interval:
2"
PVC
6-11 ft below grade
Bentonite Chips 1 - 5.5 ft below grade
Terra Probe
Direct Push / HSA
7/28/2010
GROUT
RISER CASING
7.00 7/28/10
CONCRETE
CEMENT/BENTONITE GROUT
FILTER PACK
BENTONITE
BENTONITE/NATURAL COLLAPSE
FILL
SAND
SILT
CLAY
GRAVELLY CLAY
ASPHALT
TOPSOIL
INTERBEDDED SAND, SILT, CLAY
COMPLETION REPORT OF
WELL No. MW-7 / SB-MW-7
Sheet 1 of 1
TPC
TRC
GS
TOP OF PROTECTIVE CASING
TOP OF RISER CASING
GROUND SURFACE
LEGEND
101 South Washington Square, Suite 400 Lansing, MI 48933
2.50
3.50
6.00
647.10
645.60
644.60
642.10
Concrete
Bentonite Chips
Filter Pack Sand Stainless Steel Implant
D E
P T
H (f t.)
CONSTRUCTION
REMARKS
E
LE
V A
T
IO
N (f t.)
WELL
DETAILS
S Y
M B
O L
D E
P T
H (f t.)WELL CONSTRUCTION DETAILS V A
S
STRATA
0.0
WATER LEVEL:
DATE:
TIME:
Wayne Oakland Oil 3940096 Royal Oak, MI
SEAL
DRILLING CONTRACTOR:
DRILLING METHOD:
DATE COMPLETED:
0.00NA
Type:
Interval:
None None
GS
SANDPACK
Diameter:
Type:
Interval:
Diameter:
Type:
Interval:
648.1
USGS
M. Brennan
7" Steel 0 ft above grade to 1 ft below grade
SCREEN
PROJECT:
PROJECT NO:
PROJECT LOCATION:
GROUND SURFACE ELEVATION:
DATUM:
LOGGED BY:
Sand Filter Pack 2.5-6 ft below grade
Sheet 1 of 1COMPLETION REPORT OF WELL No. SB-SGW-1
TRC
0.25" OD (0.17" ID)
Nylon Tubing 0 - 3.0 ft below grade
Type:
Interval:
PROTECTIVE CASING
648.10
Type:
Interval:
WELL DEVELOPMENT DATA
DATE:
METHOD:
NA
NA
Diameter:
Type:
Interval:
0.5" ID
Stainless Steel Implant 3-3.5 ft below grade
Bentonite Chips 1 - 2.5 ft below grade
Terra Probe
Direct Push
7/28/2010
GROUT
RISER CASING
4.50 7/28/10
CONCRETE
CEMENT/BENTONITE GROUT
FILTER PACK
BENTONITE
BENTONITE/NATURAL COLLAPSE
FILL
SAND
SILT
CLAY
GRAVELLY CLAY
ASPHALT
TOPSOIL
INTERBEDDED SAND, SILT, CLAY
COMPLETION REPORT OF
WELL No. SB-SGW-1
Sheet 1 of 1
TPC
TRC
GS
TOP OF PROTECTIVE CASING
TOP OF RISER CASING
GROUND SURFACE
LEGEND
101 South Washington Square, Suite 400 Lansing, MI 48933
2.50
3.50
6.00
647.10
645.60
644.60
642.10
Concrete
Bentonite Chips
Filter Pack Sand Stainless Steel Implant
D E
P T
H (f t.)
CONSTRUCTION
REMARKS
E
LE
V A
T
IO
N (f t.)
WELL
DETAILS
S Y
M B
O L
D E
P T
H (f t.)WELL CONSTRUCTION DETAILS V A
S
STRATA
0.0
WATER LEVEL:
DATE:
TIME:
Wayne Oakland Oil 3940096 Royal Oak, MI
SEAL
DRILLING CONTRACTOR:
DRILLING METHOD:
DATE COMPLETED:
0.00NA
Type:
Interval:
None None
GS
SANDPACK
Diameter:
Type:
Interval:
Diameter:
Type:
Interval:
648.1
USGS
M. Brennan
7" Steel 0 ft above grade to 1 ft below grade
SCREEN
PROJECT:
PROJECT NO:
PROJECT LOCATION:
GROUND SURFACE ELEVATION:
DATUM:
LOGGED BY:
Sand Filter Pack 2.5-6 ft below grade
Sheet 1 of 1COMPLETION REPORT OF WELL No. SB-SGW-2
TRC
0.25" OD (0.17" ID)
Nylon Tubing 0 - 3.0 ft below grade
Type:
Interval:
PROTECTIVE CASING
648.10
Type:
Interval:
WELL DEVELOPMENT DATA
DATE:
METHOD:
NA
NA
Diameter:
Type:
Interval:
0.5" ID
Stainless Steel Implant 3-3.5 ft below grade
Bentonite Chips 1 - 2.5 ft below grade
Terra Probe
Direct Push
7/28/2010
GROUT
RISER CASING
4.50 7/28/10
CONCRETE
CEMENT/BENTONITE GROUT
FILTER PACK
BENTONITE
BENTONITE/NATURAL COLLAPSE
FILL
SAND
SILT
CLAY
GRAVELLY CLAY
ASPHALT
TOPSOIL
INTERBEDDED SAND, SILT, CLAY
COMPLETION REPORT OF
WELL No. SB-SGW-2
Sheet 1 of 1
TPC
TRC
GS
TOP OF PROTECTIVE CASING
TOP OF RISER CASING
GROUND SURFACE
LEGEND
101 South Washington Square, Suite 400 Lansing, MI 48933
5.00
7.00
648.40
645.40
644.40
642.40
Concrete
Bentonite Chips
Filter Pack Sand Stainless Steel Implant
D E
P T
H (f t.)
CONSTRUCTION
REMARKS
E
LE
V A
T
IO
N (f t.)
WELL
DETAILS
S Y
M B
O L
D E
P T
H (f t.)WELL CONSTRUCTION DETAILS V A
S
STRATA
0.0
WATER LEVEL:
DATE:
TIME:
Wayne Oakland Oil 3940096 Royal Oak, MI
SEAL
DRILLING CONTRACTOR:
DRILLING METHOD:
DATE COMPLETED:
0.00NA
Type:
Interval:
None None
GS
SANDPACK
Diameter:
Type:
Interval:
Diameter:
Type:
Interval:
649.4
USGS
M. Brennan
7" Steel 0 ft above grade to 1 ft below grade
SCREEN
PROJECT:
PROJECT NO:
PROJECT LOCATION:
GROUND SURFACE ELEVATION:
DATUM:
LOGGED BY:
Sand Filter Pack 4-7 ft below grade
Sheet 1 of 1COMPLETION REPORT OF WELL No. SB-SGW-3
TRC
0.25" OD (0.17" ID)
Nylon Tubing 0 - 4.5 ft below grade
Type:
Interval:
PROTECTIVE CASING
649.40
Type:
Interval:
WELL DEVELOPMENT DATA
DATE:
METHOD:
NA
NA
Diameter:
Type:
Interval:
0.5" ID
Stainless Steel Implant 4.5-5 ft below grade
Bentonite Chips 1 - 4 ft below grade
Terra Probe
Direct Push
7/28/2010
GROUT
RISER CASING
6.00 7/28/10
CONCRETE
CEMENT/BENTONITE GROUT
FILTER PACK
BENTONITE
BENTONITE/NATURAL COLLAPSE
FILL
SAND
SILT
CLAY
GRAVELLY CLAY
ASPHALT
TOPSOIL
INTERBEDDED SAND, SILT, CLAY
COMPLETION REPORT OF
WELL No. SB-SGW-3
Sheet 1 of 1
TPC
TRC
GS
TOP OF PROTECTIVE CASING
TOP OF RISER CASING
GROUND SURFACE
LEGEND
101 South Washington Square, Suite 400 Lansing, MI 48933
5.00
6.00
647.40
644.40
643.40
642.40
Concrete
Bentonite Chips
Filter Pack Sand Stainless Steel Implant
D E
P T
H (f t.)
CONSTRUCTION
REMARKS
E
LE
V A
T
IO
N (f t.)
WELL
DETAILS
S Y
M B
O L
D E
P T
H (f t.)WELL CONSTRUCTION DETAILS V A
S
STRATA
0.0
WATER LEVEL:
DATE:
TIME:
Wayne Oakland Oil 3940096 Royal Oak, MI
SEAL
DRILLING CONTRACTOR:
DRILLING METHOD:
DATE COMPLETED:
0.00NA
Type:
Interval:
None None
GS
SANDPACK
Diameter:
Type:
Interval:
Diameter:
Type:
Interval:
648.4
USGS
M. Brennan
7" Steel 0 ft above grade to 1 ft below grade
SCREEN
PROJECT:
PROJECT NO:
PROJECT LOCATION:
GROUND SURFACE ELEVATION:
DATUM:
LOGGED BY:
Sand Filter Pack 4-6 ft below grade
Sheet 1 of 1COMPLETION REPORT OF WELL No. SB-SGW-4
TRC
0.25" OD (0.17" ID)
Nylon Tubing 0 - 4.5 ft below grade
Type:
Interval:
PROTECTIVE CASING
648.40
Type:
Interval:
WELL DEVELOPMENT DATA
DATE:
METHOD:
NA
NA
Diameter:
Type:
Interval:
0.5" ID
Stainless Steel Implant 4.5-5 ft below grade
Bentonite Chips 1 - 4 ft below grade
Terra Probe
Direct Push
7/28/2010
GROUT
RISER CASING
5.50 7/28/10
CONCRETE
CEMENT/BENTONITE GROUT
FILTER PACK
BENTONITE
BENTONITE/NATURAL COLLAPSE
FILL
SAND
SILT
CLAY
GRAVELLY CLAY
ASPHALT
TOPSOIL
INTERBEDDED SAND, SILT, CLAY
COMPLETION REPORT OF
WELL No. SB-SGW-4
Sheet 1 of 1
TPC
TRC
GS
TOP OF PROTECTIVE CASING
TOP OF RISER CASING
GROUND SURFACE
LEGEND
101 South Washington Square, Suite 400 Lansing, MI 48933
4.50
8.00
648.20
645.70
644.70
641.20
Concrete
Bentonite Chips
Filter Pack Sand Stainless Steel Implant
D E
P T
H (f t.)
CONSTRUCTION
REMARKS
E
LE
V A
T
IO
N (f t.)
WELL
DETAILS
S Y
M B
O L
D E
P T
H (f t.)WELL CONSTRUCTION DETAILS V A
S
STRATA
0.0
WATER LEVEL:
DATE:
TIME:
Wayne Oakland Oil 3940096 Royal Oak, MI
SEAL
DRILLING CONTRACTOR:
DRILLING METHOD:
DATE COMPLETED:
0.00NA
Type:
Interval:
None None
GS
SANDPACK
Diameter:
Type:
Interval:
Diameter:
Type:
Interval:
649.2
USGS
M. Brennan
7" Steel 0 ft above grade to 1 ft below grade
SCREEN
PROJECT:
PROJECT NO:
PROJECT LOCATION:
GROUND SURFACE ELEVATION:
DATUM:
LOGGED BY:
Sand Filter Pack 3.5-8 ft below grade
Sheet 1 of 1COMPLETION REPORT OF WELL No. SB-SGW-5
TRC
0.25" OD (0.17" ID)
Nylon Tubing 0 - 4 ft below grade
Type:
Interval:
PROTECTIVE CASING
649.20
Type:
Interval:
WELL DEVELOPMENT DATA
DATE:
METHOD:
NA
NA
Diameter:
Type:
Interval:
0.5" ID
Stainless Steel Implant 4-4.5 ft below grade
Bentonite Chips 1 - 3.5 ft below grade
Terra Probe
Direct Push
7/28/2010
GROUT
RISER CASING
5.50 7/28/10
CONCRETE
CEMENT/BENTONITE GROUT
FILTER PACK
BENTONITE
BENTONITE/NATURAL COLLAPSE
FILL
SAND
SILT
CLAY
GRAVELLY CLAY
ASPHALT
TOPSOIL
INTERBEDDED SAND, SILT, CLAY
COMPLETION REPORT OF
WELL No. SB-SGW-5
Sheet 1 of 1
TPC
TRC
GS
TOP OF PROTECTIVE CASING
TOP OF RISER CASING
GROUND SURFACE
LEGEND
101 South Washington Square, Suite 400 Lansing, MI 48933
4.50
8.00
647.70
645.20
644.20
640.70
Concrete
Bentonite Chips
Filter Pack Sand Stainless Steel Implant
D E
P T
H (f t.)
CONSTRUCTION
REMARKS
E
LE
V A
T
IO
N (f t.)
WELL
DETAILS
S Y
M B
O L
D E
P T
H (f t.)WELL CONSTRUCTION DETAILS V A
S
STRATA
0.0
WATER LEVEL:
DATE:
TIME:
Wayne Oakland Oil 3940096 Royal Oak, MI
SEAL
DRILLING CONTRACTOR:
DRILLING METHOD:
DATE COMPLETED:
0.00NA
Type:
Interval:
None None
GS
SANDPACK
Diameter:
Type:
Interval:
Diameter:
Type:
Interval:
648.7
USGS
M. Brennan
7" Steel 0 ft above grade to 1 ft below grade
SCREEN
PROJECT:
PROJECT NO:
PROJECT LOCATION:
GROUND SURFACE ELEVATION:
DATUM:
LOGGED BY:
Sand Filter Pack 3.5-8 ft below grade
Sheet 1 of 1COMPLETION REPORT OF WELL No. SB-SGW-6
TRC
0.25" OD (0.17" ID)
Nylon Tubing 0 - 4 ft below grade
Type:
Interval:
PROTECTIVE CASING
648.70
Type:
Interval:
WELL DEVELOPMENT DATA
DATE:
METHOD:
NA
NA
Diameter:
Type:
Interval:
0.5" ID
Stainless Steel Implant 4-4.5 ft below grade
Bentonite Chips 1 - 3.5 ft below grade
Terra Probe
Direct Push
7/28/2010
GROUT
RISER CASING
6.00 7/28/10
CONCRETE
CEMENT/BENTONITE GROUT
FILTER PACK
BENTONITE
BENTONITE/NATURAL COLLAPSE
FILL
SAND
SILT
CLAY
GRAVELLY CLAY
ASPHALT
TOPSOIL
INTERBEDDED SAND, SILT, CLAY
COMPLETION REPORT OF
WELL No. SB-SGW-6
Sheet 1 of 1
TPC
TRC
GS
TOP OF PROTECTIVE CASING
TOP OF RISER CASING
GROUND SURFACE
LEGEND
101 South Washington Square, Suite 400 Lansing, MI 48933
4.50
6.00
647.60
645.10
644.10
642.60
Concrete
Bentonite Chips
Filter Pack Sand Stainless Steel Implant
D E
P T
H (f t.)
CONSTRUCTION
REMARKS
E
LE
V A
T
IO
N (f t.)
WELL
DETAILS
S Y
M B
O L
D E
P T
H (f t.)WELL CONSTRUCTION DETAILS V A
S
STRATA
0.0
WATER LEVEL:
DATE:
TIME:
Wayne Oakland Oil 3940096 Royal Oak, MI
SEAL
DRILLING CONTRACTOR:
DRILLING METHOD:
DATE COMPLETED:
0.00NA
Type:
Interval:
None None
GS
SANDPACK
Diameter:
Type:
Interval:
Diameter:
Type:
Interval:
648.6
USGS
M. Brennan
7" Steel 0 ft above grade to 1 ft below grade
SCREEN
PROJECT:
PROJECT NO:
PROJECT LOCATION:
GROUND SURFACE ELEVATION:
DATUM:
LOGGED BY:
Sand Filter Pack 3.5-6 ft below grade
Sheet 1 of 1COMPLETION REPORT OF WELL No. SB-SGW-7
TRC
0.25" OD (0.17" ID)
Nylon Tubing 0 - 4 ft below grade
Type:
Interval:
PROTECTIVE CASING
648.60
Type:
Interval:
WELL DEVELOPMENT DATA
DATE:
METHOD:
NA
NA
Diameter:
Type:
Interval:
0.5" ID
Stainless Steel Implant 4-4.5 ft below grade
Bentonite Chips 1 - 3.5 ft below grade
Terra Probe
Direct Push
7/28/2010
GROUT
RISER CASING
5.50 7/28/10
CONCRETE
CEMENT/BENTONITE GROUT
FILTER PACK
BENTONITE
BENTONITE/NATURAL COLLAPSE
FILL
SAND
SILT
CLAY
GRAVELLY CLAY
ASPHALT
TOPSOIL
INTERBEDDED SAND, SILT, CLAY
COMPLETION REPORT OF
WELL No. SB-SGW-7
Sheet 1 of 1
TPC
TRC
GS
TOP OF PROTECTIVE CASING
TOP OF RISER CASING
GROUND SURFACE
LEGEND
101 South Washington Square, Suite 400 Lansing, MI 48933
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
RRDDivision:
Report to: CHRISTY CLARK 91200045
Work Site ID : 63000838
WAYNE OAKLAND OIL
Received:
Reported:
Collected By: MIKE BRENNAN
12/02/2009
01/13/2010
MDEQ-RRD-WARREN
SOUTHEAST MICHIGAN DISTRICT OFF
27700 DONALD COURT, WARREN, MI 48092-2793
$2,589.50Total:
Lab Work Order # :
Site Name :
Sample Description Collection DateSample ID Matrix:No:
Samples Received :
AB47450 12/01/2009MW-4 WATER01
AB47451 12/01/2009MW-2 WATER02
AB47452 12/01/2009MW-2 MS WATER03
AB47453 12/01/2009MW-2 MSD WATER04
AB47454 12/01/2009FIELD BLANK WATER05
AB47455 12/01/2009DUP-1 WATER06
AB47456 11/24/2009TRIP BLANK WATER07
AB47457 12/02/2009WASTE (LIQUID DRUM) WATER08
I certify that the analysis performed by the MDEQ Environmental Laboratory are accurate and that the laboratory tests were conducted by methods approved by the U.S. Environmental Protection Agency and other appropriate regulatory agencies.
Bob Avery, Laboratory Director
Page 1 of 4091200045Lab Work Order #:
P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
Sample Number: AB47457 WASTE (LIQUID DRUM)
Volatile Compounds
Compound
Date Tested:
RL
Analytical Method:
CAS #
8260 Analyst:
Qualifier
12/04/2009 KCL
Dilution FactorResult ug/L
SURROGATE #Bromofluorobenzene# 96.6
SURROGATE #Dibromofluoromethane# 101
SURROGATE #Toluene-d8# 94.4
630-20-6 1,1,1,2-Tetrachloroethane 10 10Not Detected
71-55-6 1,1,1-Trichloroethane 10 10Not Detected
79-34-5 1,1,2,2-Tetrachloroethane 10 10Not Detected
79-00-5 1,1,2-Trichloroethane 10 10Not Detected
75-34-3 1,1-Dichloroethane 10 10Not Detected
75-35-4 1,1-Dichloroethylene 10 10Not Detected
87-61-6 1,2,3-Trichlorobenzene 50 10Not Detected
96-18-4 1,2,3-Trichloropropane 10 10Not Detected
526-73-8 1,2,3-Trimethylbenzene 10 1068
120-82-1 1,2,4-Trichlorobenzene 50 10Not Detected
95-63-6 1,2,4-Trimethylbenzene 10 10160
96-12-8 1,2-Dibromo-3-chloropropane 50 10Not Detected
106-93-4 1,2-Dibromoethane 10 10Not Detected
95-50-1 1,2-Dichlorobenzene 10 10Not Detected
107-06-2 1,2-Dichloroethane 10 10Not Detected
78-87-5 1,2-Dichloropropane 10 10Not Detected
108-67-8 1,3,5-Trimethylbenzene 10 1029
541-73-1 1,3-Dichlorobenzene 10 10Not Detected
106-46-7 1,4-Dichlorobenzene 10 10Not Detected
78-93-3 2-Butanone (MEK) 50 10Not Detected
591-78-6 2-Hexanone 50 10Not Detected
91-57-6 2-Methylnaphthalene X50 10210
67-64-1 2-Propanone (acetone) 200 10Not Detected
108-10-1 4-Methyl-2-pentanone (MIBK) 50 10Not Detected
107-13-1 Acrylonitrile Z50 10Not Detected
71-43-2 Benzene 10 10Not Detected
108-86-1 Bromobenzene 10 10Not Detected
74-97-5 Bromochloromethane 10 10Not Detected
75-27-4 Bromodichloromethane 10 10Not Detected
75-25-2 Bromoform 10 10Not Detected
74-83-9 Bromomethane 50 10Not Detected
75-15-0 Carbon disulfide 10 10Not Detected
56-23-5 Carbon tetrachloride 10 10Not Detected
108-90-7 Chlorobenzene 10 10Not Detected
75-00-3 Chloroethane 50 10Not Detected
67-66-3 Chloroform 10 10Not Detected
74-87-3 Chloromethane 50 10Not Detected
156-59-2 cis-1,2-Dichloroethylene 10 10Not Detected
CAS# : Chemical Abstract Service Registry Number
RL : Reporting Limit
ND : Not Detected ug / L : microgram / liter (ppb) mg / L : milligram / liter (ppm) ug / Kg : microgram / kilogram (ppb) mg / Kg : milligram / kilogram (ppm)
Laboratory Contacts
Inorganic Unit Mgr: Sandy Gregg
Organic Unit Mgr: Carol Smith
Systems Mgmt Unit: George Krisztian
Page 34 of 4091200045Lab Work Order #:
P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
Sample Number: AB47457 WASTE (LIQUID DRUM)
Volatile Compounds
Compound
Date Tested:
RL
Analytical Method:
CAS #
8260 Analyst:
Qualifier
12/04/2009 KCL
Dilution FactorResult ug/L
10061-01-5 cis-1,3-Dichloropropylene 10 10Not Detected
110-82-7 Cyclohexane 50 10Not Detected
124-48-1 Dibromochloromethane 10 10Not Detected
74-95-3 Dibromomethane 10 10Not Detected
75-71-8 Dichlorodifluoromethane 50 10Not Detected
60-29-7 Diethyl ether 50 10Not Detected
108-20-3 Diisopropyl Ether 50 10Not Detected
100-41-4 Ethylbenzene 10 1026
637-92-3 Ethyltertiarybutylether 50 10Not Detected
67-72-1 Hexachloroethane 50 10Not Detected
98-82-8 Isopropylbenzene 10 1016
108383,106423 m & p - Xylene 20 1044
74-88-4 Methyl iodide 10 10Not Detected
75-09-2 Methylene chloride 50 10Not Detected
1634-04-4 Methyltertiarybutylether 10 10Not Detected
91-20-3 Naphthalene X50 10170
104-51-8 n-Butylbenzene 10 10Not Detected
103-65-1 n-Propylbenzene 10 1023
95-47-6 o-Xylene 10 10Not Detected
99-87-6 p-Isopropyl toluene 10 1011
135-98-8 sec-Butylbenzene 10 10Not Detected
100-42-5 Styrene 10 10Not Detected
98-06-6 tert-Butylbenzene 10 10Not Detected
75-65-0 tertiary Butyl Alcohol 500 10Not Detected
994-05-8 tertiaryAmylmethylether 50 10Not Detected
127-18-4 Tetrachloroethylene 10 10Not Detected
109-99-9 Tetrahydrofuran 50 10Not Detected
108-88-3 Toluene 10 10Not Detected
156-60-5 trans-1,2-Dichloroethylene 10 10Not Detected
10061-02-6 trans-1,3-Dichloropropylene 10 10Not Detected
110-57-6 trans-1,4-Dichloro-2-butene Z50 10Not Detected
79-01-6 Trichloroethylene 10 10Not Detected
75-69-4 Trichlorofluoromethane 10 10Not Detected
75-01-4 Vinyl chloride 10 10Not Detected
Unidentified peaks present in sample.
Base Neutral Acid Compounds
Compound
Date Tested:
RL
Analytical Method:
CAS #
8270 Analyst:
Qualifier
12/10/2009 SMH
Extraction Method: Extraction Date: 12/04/2009 1000Volume:3510 KQualifier:
Dilution FactorResult ug/L
CAS# : Chemical Abstract Service Registry Number
RL : Reporting Limit
ND : Not Detected ug / L : microgram / liter (ppb) mg / L : milligram / liter (ppm) ug / Kg : microgram / kilogram (ppb) mg / Kg : milligram / kilogram (ppm)
Laboratory Contacts
Inorganic Unit Mgr: Sandy Gregg
Organic Unit Mgr: Carol Smith
Page 35 of 4091200045Lab Work Order #:
P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
Sample Number: AB47457 WASTE (LIQUID DRUM)
Base Neutral Acid Compounds
Compound
Date Tested:
RL
Analytical Method:
CAS #
8270 Analyst:
Qualifier
12/10/2009 SMH
Extraction Method: Extraction Date: 12/04/2009 1000Volume:3510 KQualifier:
Dilution FactorResult ug/L
SURROGATE #2 - Fluorobiphenyl# VNot Applicable
SURROGATE #2,4,6-Tribromophenol# VNot Applicable
SURROGATE #2-Fluorophenol# VNot Applicable
SURROGATE #Nitrobenzene - D5# VNot Applicable
SURROGATE #Phenol - D6# VNot Applicable
SURROGATE #p-Terphenyl-D14# VNot Applicable
120-82-1 1,2,4-Trichlorobenzene 5000 2500Not Detected
95-95-4 2,4,5-Trichlorophenol 13000 2500Not Detected
88-06-2 2,4,6-Trichlorophenol 10000 2500Not Detected
120-83-2 2,4-Dichlorophenol 25000 2500Not Detected
105-67-9 2,4-Dimethylphenol 13000 2500Not Detected
51-28-5 2,4-Dinitrophenol 63000 2500Not Detected
121-14-2 2,4-Dinitrotoluene 13000 2500Not Detected
606-20-2 2,6-Dinitrotoluene 13000 2500Not Detected
95-51-2 2-Chloroaniline 13000 2500Not Detected
91-58-7 2-Chloronaphthalene 5000 2500Not Detected
95-57-8 2-Chlorophenol 25000 2500Not Detected
534-52-1 2-Methyl-4,6-dinitrophenol 50000 2500Not Detected
91-57-6 2-Methylnaphthalene 13000 250064000
95-48-7 2-Methylphenol (o-Cresol) 25000 2500Not Detected
88-74-4 2-Nitroaniline 50000 2500Not Detected
88-75-5 2-Nitrophenol 13000 2500Not Detected
108394,106445 3 & 4-Methylphenol 50000 2500Not Detected
99-09-2 3-Nitroaniline 50000 2500Not Detected
101-55-3 4-Bromophenyl phenyl ether 5000 2500Not Detected
59-50-7 4-Chloro-3-methyl-phenol 13000 2500Not Detected
106-47-8 4-Chloroaniline 25000 2500Not Detected
7005-72-3 4-Chlorodiphenylether 2500 2500Not Detected
100-01-6 4-Nitroaniline 50000 2500Not Detected
100-02-7 4-Nitrophenol 63000 2500Not Detected
83-32-9 Acenaphthene 2500 25005000
208-96-8 Acenaphthylene 2500 2500Not Detected
62-53-3 Aniline 10000 2500Not Detected
120-12-7 Anthracene 2500 2500Not Detected
103-33-3 Azobenzene 5000 2500Not Detected
56-55-3 Benzo[a]anthracene 2500 2500Not Detected
50-32-8 Benzo[a]pyrene 2500 2500Not Detected
205-99-2 Benzo[b]fluoranthene 2500 2500Not Detected
191-24-2 Benzo[g,h,i]perylene 2500 2500Not Detected
207-08-9 Benzo[k]fluoranthene 2500 2500Not Detected
100-51-6 Benzyl Alcohol 130000 2500Not Detected
CAS# : Chemical Abstract Service Registry Number
RL : Reporting Limit
ND : Not Detected ug / L : microgram / liter (ppb) mg / L : milligram / liter (ppm) ug / Kg : microgram / kilogram (ppb) mg / Kg : milligram / kilogram (ppm)
Laboratory Contacts
Inorganic Unit Mgr: Sandy Gregg
Organic Unit Mgr: Carol Smith
Page 36 of 4091200045Lab Work Order #:
P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
Sample Number: AB47457 WASTE (LIQUID DRUM)
Base Neutral Acid Compounds
Compound
Date Tested:
RL
Analytical Method:
CAS #
8270 Analyst:
Qualifier
12/10/2009 SMH
Extraction Method: Extraction Date: 12/04/2009 1000Volume:3510 KQualifier:
Dilution FactorResult ug/L
111-91-1 Bis(2-chloroethoxy)methane 5000 2500Not Detected
111-44-4 Bis(2-chloroethyl)ether 2500 2500Not Detected
108-60-1 Bis(2-chloroisopropyl)ether 52500 2500Not Detected
117-81-7 Bis(2-ethylhexyl)phthalate 13000 2500Not Detected
85-68-7 Butyl benzyl phthalate 13000 2500Not Detected
86-74-8 Carbazole 13000 2500Not Detected
218-01-9 Chrysene 2500 2500Not Detected
53-70-3 Dibenz[a,h]anthracene 5000 2500Not Detected
132-64-9 Dibenzofuran 10000 2500Not Detected
84-66-2 Diethylphthalate 13000 2500Not Detected
131-11-3 Dimethyl phthalate 13000 2500Not Detected
84-74-2 Di-n-butyl phthalate 13000 2500Not Detected
117-84-0 Di-n-octyl phthalate 13000 2500Not Detected
206-44-0 Fluoranthene 2500 2500Not Detected
86-73-7 Fluorene 2500 25007400
118-74-1 Hexachlorobenzene 2500 2500Not Detected
87-68-3 Hexachlorobutadiene 2500 2500Not Detected
77-47-4 Hexachlorocyclopentadiene Z25000 2500Not Detected
67-72-1 Hexachloroethane 2500 2500Not Detected
193-39-5 Indeno(1,2,3-c,d)pyrene 5000 2500Not Detected
78-59-1 Isophorone 2500 2500Not Detected
121-69-7 N,N-dimethylaniline 13000 2500Not Detected
91-20-3 Naphthalene 2500 250023000
98-95-3 Nitrobenzene 5000 2500Not Detected
100-61-8 N-methylaniline 2500 2500Not Detected
67-75-9 N-Nitrosodimethylamine 513000 2500Not Detected
621-64-7 N-Nitrosodi-n-propylamine 55000 2500Not Detected
86-30-6 N-Nitrosodiphenylamine 5000 2500Not Detected
87-86-5 Pentachlorophenol 50000 2500Not Detected
85-01-8 Phenanthrene 2500 250015000
108-95-2 Phenol 13000 2500Not Detected
129-00-0 Pyrene 2500 2500Not Detected
110-86-1 Pyridine 550000 2500Not Detected
632-22-4 Tetramethylurea 2500 2500Not Detected
RLs raised due to matrix interference.
Probable petroleum product(s) present.
CAS# : Chemical Abstract Service Registry Number
RL : Reporting Limit
ND : Not Detected ug / L : microgram / liter (ppb) mg / L : milligram / liter (ppm) ug / Kg : microgram / kilogram (ppb) mg / Kg : milligram / kilogram (ppm)
Laboratory Contacts
Inorganic Unit Mgr: Sandy Gregg
Organic Unit Mgr: Carol Smith
Page 37 of 4091200045Lab Work Order #:
P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
Sample Number: AB47457 WASTE (LIQUID DRUM)
Pesticide Compounds
Compound
Date Tested:
RL
Analytical Method:
CAS #
8081 Analyst:
Qualifier
12/16/2009 MF
Extraction Method: Extraction Date: 12/08/2009 1000Volume:3510 Qualifier:
Dilution FactorResult ug/L
SURROGATE #Decachlorobiphenyl# VNot Applicable
SURROGATE #Tetrachloro-m-xylene# VNot Applicable
72-54-8 4,4'-DDD 15 500Not Detected
72-55-9 4,4'-DDE 10 500Not Detected
50-29-3 4,4'-DDT 25 500Not Detected
319-84-6 a-BHC 10 500Not Detected
5103-71-9 a-Chlordane 5 500Not Detected
309-00-2 Aldrin 5 500Not Detected
319-85-7 b-BHC 10 500Not Detected
319-86-8 d-BHC 10 500Not Detected
60-57-1 Dieldrin 10 500Not Detected
959-98-8 Endosulfan I 10 500Not Detected
33213-65-9 Endosulfan II 15 500Not Detected
1031-07-8 Endosulfan sulfate 25 500Not Detected
72-20-8 Endrin 10 500Not Detected
7421-93-4 Endrin aldehyde 10 500Not Detected
53494-70-5 Endrin ketone 10 500Not Detected
58-89-9 g-BHC (Lindane) 10 500Not Detected
5103-74-2 g-Chlordane 5 500Not Detected
76-44-8 Heptachlor 5 500Not Detected
1024-57-3 Heptachlor epoxide 5 500Not Detected
87-82-1 Hexabromobenzene 10 500Not Detected
72-43-5 Methoxychlor 25 500Not Detected
2385-85-5 Mirex 10 500Not Detected
59080-40-9 PBB (BP-6) 25 500Not Detected
8001-35-2 Toxaphene 50 500Not Detected
RLs raised due to matrix interference.
CAS# : Chemical Abstract Service Registry Number
RL : Reporting Limit
ND : Not Detected ug / L : microgram / liter (ppb) mg / L : milligram / liter (ppm) ug / Kg : microgram / kilogram (ppb) mg / Kg : milligram / kilogram (ppm)
Laboratory Contacts
Inorganic Unit Mgr: Sandy Gregg
Organic Unit Mgr: Carol Smith
Page 38 of 4091200045Lab Work Order #:
P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
Sample Number: AB47457 WASTE (LIQUID DRUM)
Date TestedAnalyte Name MethodCAS# QualifierResult AnalystRLUnit
Digestion Metals Water KS3010/20012/15/2009Completed
Flash Point TK101012/18/2009degrees C83.5
Digestion Mercury Water TS7470/245.112/17/2009Completed
7439-97-6 Mercury - Total TS7470/245.112/18/2009µg/LND 0.2
7440-38-2 Arsenic - Total KS6020/200.812/21/2009µg/L110 1
7440-39-3 Barium - Total KS6020/200.812/21/2009µg/L140 5
7440-43-9 Cadmium - Total I KS6020/200.812/16/2009µg/LND 2
7440-47-3 Chromium - Total KS6020/200.812/16/2009µg/L41 1
7440-50-8 Copper - Total KS6020/200.812/16/2009µg/L33 1
7439-92-1 Lead - Total D KS6020/200.812/21/2009µg/L2200 1
7782-49-2 Selenium - Total I KS6020/200.812/21/2009µg/LND 10
7440-22-4 Silver -Total I KS6020/200.812/16/2009µg/LND 2
7440-66-6 Zinc - Total KS6020/200.812/16/2009µg/L160 10 pH LU4500H B SM12/09/2009pH8
Due to the oily nature of the sample a pH strip was used to determine the pH of the sample.
Florisil Cleanup DT362012/15/2009Completed
Gel Permeation Cleanup DT364012/14/2009Completed
CAS# : Chemical Abstract Service Registry Number
RL : Reporting Limit
ND : Not Detected ug / L : microgram / liter (ppb) mg / L : milligram / liter (ppm) ug / Kg : microgram / kilogram (ppb) mg / Kg : milligram / kilogram (ppm)
Laboratory Contacts
Inorganic Unit Mgr: Sandy Gregg
Organic Unit Mgr: Carol Smith
Page 39 of 4091200045Lab Work Order #:
P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
Qualifier DescriptionQualifier Code
1 Result(s) and RL(s) are estimated due to low surrogate recovery.
2 Result is estimated due to high surrogate recovery.
3 Result(s) and RL(s) are estimated due to low matrix spike recovery.
4 Result is estimated due to high matrix spike recovery.
5 Result and RL are estimated due to low continuing calibration standard criteria failure.
6 Result is estimated due to high continuing calibration standard criteria failure.
7 Result(s) and RL(s) are estimated due to poor precision.
8 Result(s) and RL(s) are estimated due to low recovery of batch QC.
9 Result outside QC acceptance criteria.
A Value reported is the mean of two or more determinations.
C Value calculated from other independent parameters.
D Analyte value quantified from a dilution(s); reporting limit (RL) raised.
E Result is estimated due to high recovery of batch QC.
F Amenable cyanide was not analyzed due to low level of total cyanide.
G Result and RL are estimated due to initial calibration standard criteria failure.
H Recommended laboratory holding time was exceeded.
I Dilution required due to matrix interference; reporting limit (RL) raised.
J Analyte was positively identified. Value is an estimate.
JA Result is estimated due to multiple Aroclors present.
JC Result is estimated since confirmation analysis did not meet acceptance criteria
JD Due to severe degradation, specific Aroclor identification is difficult and quantitation is estimated.
K RL(s) raised due to matrix interferences.
KR RL(s) raised due to low sample volume submitted.
KS RL(s) raised due to low total solids.
KW RL(s) raised due to light sample weight.
LB Reported library search compounds are tentative identifications with estimated concentrations.
M The level of the method preparation blank (MPB) is reported in the qualifier column.
N Non-homogeneous sample made analysis of sample questionable.
O Result and RL estimated due to analysis from an open vial.
P Recommended sample collection/preservation technique not used; reported result(s) is an estimate.
Q Quantity of sample insufficient to perform analyses requested.
R Result confirmed by re-extraction and analysis.
S Supernatant analyzed.
T Reported value is less than the reporting limit (RL). Result is estimated.
V Value not available due to dilution.
W Reported value is less than the method detection limit (MDL).
X Methods 8260 & 624 are used to analyze volatile organics that have boiling points below 200°C.
2-Methylnaphthalene & naphthalene have boiling points above 200°C and are better suited to analysis by methods 8270 or 625 as semivolatile organics.
PI Possible interference may have affected the accuracy of the laboratory result
Z Result reported below the RL to meet the TDL in RRD Op Memo 2 (10/22/04) multiplied by applicable dilution factor.
CAS# : Chemical Abstract Service Registry Number
RL : Reporting Limit
ND : Not Detected ug / L : microgram / liter (ppb) mg / L : milligram / liter (ppm) ug / Kg : microgram / kilogram (ppb) mg / Kg : milligram / kilogram (ppm)
Laboratory Contacts
Inorganic Unit Mgr: Sandy Gregg
Organic Unit Mgr: Carol Smith
Page 40 of 4091200045Lab Work Order #:
P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
RRDDivision:
Report to: CHRISTY CLARK 91200046
Work Site ID : 63000838
WAYNE OAKLAND OIL
Received:
Reported:
Collected By: MIKE BRENNAN
12/02/2009
01/14/2010
MDEQ-RRD-WARREN
SOUTHEAST MICHIGAN DISTRICT OFF
27700 DONALD COURT, WARREN, MI 48092-2793
$804.50Total:
Lab Work Order # :
Site Name :
Sample Description Collection DateSample ID Matrix:No:
Samples Received :
AB47458 12/02/2009WASTE (SOIL DRUM) SEDIMENT01
I certify that the analysis performed by the MDEQ Environmental Laboratory are accurate and that the laboratory tests were conducted by methods approved by the U.S. Environmental Protection Agency and other appropriate regulatory agencies.
Page 1 of 891200046Lab Work Order #:
P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
Sample Number: AB47458 WASTE (SOIL DRUM)
TCLP Volatile Leachate
Compound
Date Tested:
RL
Analytical Method:
CAS #
8260 Analyst:
Qualifier
12/15/2009 KCL
Extraction Method: Extraction Date: 12/03/20091311 Qualifier:
Dilution FactorResult ug/L
SURROGATE #Bromofluorobenzene# 98.2
SURROGATE #Dibromofluoromethane# 98.3
SURROGATE #Toluene-d8# 94.8
630-20-6 1,1,1,2-Tetrachloroethane 1 1.0Not Detected
71-55-6 1,1,1-Trichloroethane 1 1.0Not Detected
79-34-5 1,1,2,2-Tetrachloroethane 1 1.0Not Detected
79-00-5 1,1,2-Trichloroethane 1 1.0Not Detected
75-34-3 1,1-Dichloroethane 1 1.0Not Detected
75-35-4 1,1-Dichloroethylene 1 1.0Not Detected
87-61-6 1,2,3-Trichlorobenzene 5 1.0Not Detected
96-18-4 1,2,3-Trichloropropane 1 1.0Not Detected
526-73-8 1,2,3-Trimethylbenzene 1 1.06.5
120-82-1 1,2,4-Trichlorobenzene 5 1.0Not Detected
95-63-6 1,2,4-Trimethylbenzene 1 1.01.6
96-12-8 1,2-Dibromo-3-chloropropane 5 1.0Not Detected
106-93-4 1,2-Dibromoethane 1 1.0Not Detected
95-50-1 1,2-Dichlorobenzene 1 1.0Not Detected
107-06-2 1,2-Dichloroethane 1 1.0Not Detected
78-87-5 1,2-Dichloropropane 1 1.0Not Detected
108-67-8 1,3,5-Trimethylbenzene 1 1.02.9
541-73-1 1,3-Dichlorobenzene 1 1.0Not Detected
106-46-7 1,4-Dichlorobenzene 1 1.0Not Detected
78-93-3 2-Butanone (MEK) 5 1.0Not Detected
591-78-6 2-Hexanone 5 1.0Not Detected
91-57-6 2-Methylnaphthalene X5 1.06.5
67-64-1 2-Propanone (acetone) 20 1.0Not Detected
108-10-1 4-Methyl-2-pentanone (MIBK) 5 1.0Not Detected
107-13-1 Acrylonitrile Z5 1.0Not Detected
71-43-2 Benzene 1 1.0Not Detected
108-86-1 Bromobenzene 1 1.0Not Detected
74-97-5 Bromochloromethane 1 1.0Not Detected
75-27-4 Bromodichloromethane 1 1.0Not Detected
75-25-2 Bromoform 1 1.0Not Detected
74-83-9 Bromomethane 5 1.0Not Detected
75-15-0 Carbon disulfide 1 1.0Not Detected
56-23-5 Carbon tetrachloride 1 1.0Not Detected
108-90-7 Chlorobenzene 1 1.0Not Detected
75-00-3 Chloroethane 5 1.0Not Detected
67-66-3 Chloroform 1 1.0Not Detected
74-87-3 Chloromethane 5 1.0Not Detected
156-59-2 cis-1,2-Dichloroethylene 1 1.0Not Detected
CAS# : Chemical Abstract Service Registry Number
RL : Reporting Limit
ND : Not Detected ug / L : microgram / liter (ppb) mg / L : milligram / liter (ppm) ug / Kg : microgram / kilogram (ppb) mg / Kg : milligram / kilogram (ppm)
Laboratory Contacts
Inorganic Unit Mgr: Sandy Gregg
Organic Unit Mgr: Carol Smith
Page 2 of 891200046Lab Work Order #:
P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
Sample Number: AB47458 WASTE (SOIL DRUM)
TCLP Volatile Leachate
Compound
Date Tested:
RL
Analytical Method:
CAS #
8260 Analyst:
Qualifier
12/15/2009 KCL
Extraction Method: Extraction Date: 12/03/20091311 Qualifier:
Dilution FactorResult ug/L
10061-01-5 cis-1,3-Dichloropropylene 1 1.0Not Detected
110-82-7 Cyclohexane 5 1.0Not Detected
124-48-1 Dibromochloromethane 1 1.0Not Detected
74-95-3 Dibromomethane 1 1.0Not Detected
75-71-8 Dichlorodifluoromethane 5 1.0Not Detected
60-29-7 Diethyl ether 5 1.0Not Detected
108-20-3 Diisopropyl Ether 5 1.0Not Detected
100-41-4 Ethylbenzene 1 1.0Not Detected
637-92-3 Ethyltertiarybutylether 5 1.0Not Detected
67-72-1 Hexachloroethane 5 1.0Not Detected
98-82-8 Isopropylbenzene 1 1.0Not Detected
108383,106423 m & p - Xylene 2 1.0Not Detected
74-88-4 Methyl iodide 1 1.0Not Detected
75-09-2 Methylene chloride 5 1.0Not Detected
1634-04-4 Methyltertiarybutylether 1 1.0Not Detected
91-20-3 Naphthalene X5 1.0Not Detected
104-51-8 n-Butylbenzene 1 1.0Not Detected
103-65-1 n-Propylbenzene 1 1.0Not Detected
95-47-6 o-Xylene 1 1.0Not Detected
99-87-6 p-Isopropyl toluene 1 1.0Not Detected
135-98-8 sec-Butylbenzene 1 1.0Not Detected
100-42-5 Styrene 1 1.0Not Detected
98-06-6 tert-Butylbenzene 1 1.0Not Detected
75-65-0 tertiary Butyl Alcohol 50 1.0Not Detected
994-05-8 tertiaryAmylmethylether 5 1.0Not Detected
127-18-4 Tetrachloroethylene 1 1.0Not Detected
109-99-9 Tetrahydrofuran 5 1.0Not Detected
108-88-3 Toluene 1 1.0Not Detected
156-60-5 trans-1,2-Dichloroethylene 1 1.0Not Detected
10061-02-6 trans-1,3-Dichloropropylene 1 1.0Not Detected
110-57-6 trans-1,4-Dichloro-2-butene Z5 1.0Not Detected
79-01-6 Trichloroethylene 1 1.0Not Detected
75-69-4 Trichlorofluoromethane 1 1.0Not Detected
75-01-4 Vinyl chloride 1 1.0Not Detected
TCLP Base Neutral Acid Compounds
Compound
Date Tested:
RL
Analytical Method:
CAS #
8270 Analyst:
Qualifier
12/15/2009 SMH
Extraction Method: Extraction Date: 12/10/20093510 Qualifier:
Dilution FactorResult ug/L
CAS# : Chemical Abstract Service Registry Number
RL : Reporting Limit
ND : Not Detected ug / L : microgram / liter (ppb) mg / L : milligram / liter (ppm) ug / Kg : microgram / kilogram (ppb) mg / Kg : milligram / kilogram (ppm)
Laboratory Contacts
Inorganic Unit Mgr: Sandy Gregg
Organic Unit Mgr: Carol Smith
Page 3 of 891200046Lab Work Order #:
P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
Sample Number: AB47458 WASTE (SOIL DRUM)
TCLP Base Neutral Acid Compounds
Compound
Date Tested:
RL
Analytical Method:
CAS #
8270 Analyst:
Qualifier
12/15/2009 SMH
Extraction Method: Extraction Date: 12/10/20093510 Qualifier:
Dilution FactorResult ug/L
SURROGATE #2 - Fluorobiphenyl# 70.1
SURROGATE #2,4,6-Tribromophenol# 78.6
SURROGATE #2-Fluorophenol# 29.2
SURROGATE #Nitrobenzene - D5# 85.1
SURROGATE #Phenol - D6# 19.2
SURROGATE #p-Terphenyl-d14# 84.5
120-82-1 1,2,4-Trichlorobenzene 2 1.0Not Detected
95-95-4 2,4,5-Trichlorophenol 5.1 1.0Not Detected
88-06-2 2,4,6-Trichlorophenol 4 1.0Not Detected
120-83-2 2,4-Dichlorophenol 10 1.0Not Detected
105-67-9 2,4-Dimethylphenol 5.1 1.0Not Detected
51-28-5 2,4-Dinitrophenol 25 1.0Not Detected
121-14-2 2,4-Dinitrotoluene 5.1 1.0Not Detected
606-20-2 2,6-Dinitrotoluene 5.1 1.0Not Detected
91-58-7 2-Chloronaphthalene 2 1.0Not Detected
95-57-8 2-Chlorophenol 10 1.0Not Detected
534-52-1 2-Methyl-4,6-dinitrophenol 20 1.0Not Detected
91-57-6 2-Methylnaphthalene 5.1 1.0Not Detected
95-48-7 2-Methylphenol (o-Cresol) 10 1.0Not Detected
88-74-4 2-Nitroaniline 20 1.0Not Detected
88-75-5 2-Nitrophenol 5.1 1.0Not Detected
108394,106445 3 & 4-Methylphenol 20 1.0Not Detected
99-09-2 3-Nitroaniline 20 1.0Not Detected
101-55-3 4-Bromophenyl phenyl ether 2 1.0Not Detected
59-50-7 4-Chloro-3-methyl-phenol 5.1 1.0Not Detected
7005-72-3 4-Chlorodiphenylether 1 1.0Not Detected
100-01-6 4-Nitroaniline 20 1.0Not Detected
100-02-7 4-Nitrophenol 25 1.0Not Detected
83-32-9 Acenaphthene 1 1.01.7
208-96-8 Acenaphthylene 1 1.0Not Detected
62-53-3 Aniline 4 1.0Not Detected
120-12-7 Anthracene 1 1.0Not Detected
103-33-3 Azobenzene 2 1.0Not Detected
56-55-3 Benzo[a]anthracene 1 1.0Not Detected
50-32-8 Benzo[a]pyrene 1 1.0Not Detected
205-99-2 Benzo[b]fluoranthene 1 1.0Not Detected
191-24-2 Benzo[g,h,i]perylene 51 1.0Not Detected
207-08-9 Benzo[k]fluoranthene 1 1.0Not Detected
100-51-6 Benzyl Alcohol 51 1.0Not Detected
111-91-1 Bis(2-chloroethoxy)methane 2 1.0Not Detected
111-44-4 Bis(2-chloroethyl)ether 1 1.0Not Detected
CAS# : Chemical Abstract Service Registry Number
RL : Reporting Limit
ND : Not Detected ug / L : microgram / liter (ppb) mg / L : milligram / liter (ppm) ug / Kg : microgram / kilogram (ppb) mg / Kg : milligram / kilogram (ppm)
Laboratory Contacts
Inorganic Unit Mgr: Sandy Gregg
Organic Unit Mgr: Carol Smith
Page 4 of 891200046Lab Work Order #:
P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
Sample Number: AB47458 WASTE (SOIL DRUM)
TCLP Base Neutral Acid Compounds
Compound
Date Tested:
RL
Analytical Method:
CAS #
8270 Analyst:
Qualifier
12/15/2009 SMH
Extraction Method: Extraction Date: 12/10/20093510 Qualifier:
Dilution FactorResult ug/L
108-60-1 Bis(2-chloroisopropyl)ether 1 1.0Not Detected
117-81-7 Bis(2-ethylhexyl)phthalate 5.1 1.0Not Detected
85-68-7 Butyl benzyl phthalate 5.1 1.0Not Detected
86-74-8 Carbazole 5.1 1.0Not Detected
218-01-9 Chrysene 1 1.0Not Detected
53-70-3 Dibenz[a,h]anthracene 52 1.0Not Detected
132-64-9 Dibenzofuran 4 1.0Not Detected
84-66-2 Diethylphthalate 5.1 1.0Not Detected
131-11-3 Dimethyl phthalate 5.1 1.0Not Detected
84-74-2 Di-n-butyl phthalate 5.1 1.0Not Detected
117-84-0 Di-n-octyl phthalate 5.1 1.0Not Detected
206-44-0 Fluoranthene 1 1.0Not Detected
86-73-7 Fluorene 1 1.01.1
118-74-1 Hexachlorobenzene 1 1.0Not Detected
87-68-3 Hexachlorobutadiene 1 1.0Not Detected
77-47-4 Hexachlorocyclopentadiene 5Z10 1.0Not Detected
67-72-1 Hexachloroethane 1 1.0Not Detected
193-39-5 Indeno(1,2,3-c,d)pyrene 2 1.0Not Detected
78-59-1 Isophorone 1 1.0Not Detected
91-20-3 Naphthalene 1 1.0Not Detected
98-95-3 Nitrobenzene 2 1.0Not Detected
67-75-9 N-Nitrosodimethylamine 5.1 1.0Not Detected
621-64-7 N-Nitrosodi-n-propylamine 2 1.0Not Detected
86-30-6 N-Nitrosodiphenylamine 2 1.0Not Detected
87-86-5 Pentachlorophenol 20 1.0Not Detected
85-01-8 Phenanthrene 1 1.0Not Detected
108-95-2 Phenol 5.1 1.0Not Detected
129-00-0 Pyrene 1 1.0Not Detected
110-86-1 Pyridine 20 1.0Not Detected
Probable petroleum product(s) present.
TCLP Pesticide Compounds
Compound
Date Tested:
RL
Analytical Method:
CAS #
8081 Analyst:
Qualifier
12/16/2009 MF
Extraction Method: Extraction Date: 12/08/20093510 Qualifier:
Dilution FactorResult ug/L
SURROGATE #Decachlorobiphenyl# 61.7
SURROGATE #Tetrachloro-m-xylene# 45.3
72-54-8 4,4'-DDD 0.03 1.0Not Detected
72-55-9 4,4'-DDE 0.02 1.0Not Detected
50-29-3 4,4'-DDT 0.05 1.0Not Detected
CAS# : Chemical Abstract Service Registry Number
RL : Reporting Limit
ND : Not Detected ug / L : microgram / liter (ppb) mg / L : milligram / liter (ppm) ug / Kg : microgram / kilogram (ppb) mg / Kg : milligram / kilogram (ppm)
Laboratory Contacts
Inorganic Unit Mgr: Sandy Gregg
Organic Unit Mgr: Carol Smith
Page 5 of 891200046Lab Work Order #:
P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
Sample Number: AB47458 WASTE (SOIL DRUM)
TCLP Pesticide Compounds
Compound
Date Tested:
RL
Analytical Method:
CAS #
8081 Analyst:
Qualifier
12/16/2009 MF
Extraction Method: Extraction Date: 12/08/20093510 Qualifier:
Dilution FactorResult ug/L
319-84-6 a-BHC 0.02 1.0Not Detected
5103-71-9 a-Chlordane 0.01 1.0Not Detected
309-00-2 Aldrin 0.01 1.0Not Detected
319-85-7 b-BHC 0.02 1.0Not Detected
319-86-8 d-BHC 0.02 1.0Not Detected
60-57-1 Dieldrin 0.02 1.0Not Detected
959-98-8 Endosulfan I 0.02 1.0Not Detected
33213-65-9 Endosulfan II 0.03 1.0Not Detected
1031-07-8 Endosulfan sulfate 0.05 1.0Not Detected
72-20-8 Endrin 0.02 1.0Not Detected
7421-93-4 Endrin aldehyde 0.02 1.0Not Detected
53494-70-5 Endrin ketone 0.02 1.0Not Detected
58-89-9 g-BHC (Lindane) 0.02 1.0Not Detected
5103-74-2 g-Chlordane 0.01 1.0Not Detected
76-44-8 Heptachlor 0.01 1.0Not Detected
1024-57-3 Heptachlor epoxide K0.02 1.0Not Detected
87-82-1 Hexabromobenzene 0.02 1.0Not Detected
72-43-5 Methoxychlor 0.05 1.0Not Detected
2385-85-5 Mirex 0.02 1.0Not Detected
59080-40-9 PBB (BP-6) 0.05 1.0Not Detected
8001-35-2 Toxaphene 0.1 1.0Not Detected
CAS# : Chemical Abstract Service Registry Number
RL : Reporting Limit
ND : Not Detected ug / L : microgram / liter (ppb) mg / L : milligram / liter (ppm) ug / Kg : microgram / kilogram (ppb) mg / Kg : milligram / kilogram (ppm)
Laboratory Contacts
Inorganic Unit Mgr: Sandy Gregg
Organic Unit Mgr: Carol Smith
Page 6 of 891200046Lab Work Order #:
P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
Sample Number: AB47458 WASTE (SOIL DRUM)
Date TestedAnalyte Name MethodCAS# QualifierResult AnalystRLUnit
7440-38-2 Arsenic - TCLP LAV706012/22/2009µg/LND 10
7782-49-2 Selenium - TCLP LAV774012/14/2009µg/LND 10
7440-22-4 Silver - TCLP LAV776112/10/2009µg/LND 5
Ignitability of Solids KS103001/13/2010FlammableNO
7439-97-6 Mercury - TCLP TS747012/18/2009µg/LND 0.4
Mercury Digestion - TCLP TS747012/17/2009Completed
7440-39-3 Barium - TCLP M 95 WN601012/14/2009µg/L620 10
7440-43-9 Cadmium - TCLP WN601012/14/2009µg/LND 20
7440-47-3 Chromium - TCLP WN601012/14/2009µg/LND 50
7440-50-8 Copper - TCLP WN601012/14/2009µg/LND 20
7439-92-1 Lead - TCLP WN601012/14/2009µg/LND 100
7440-66-6 Zinc - TCLP M 31 WN601012/14/2009µg/L130 20 pH - Sediment LU904512/18/2009pH8.22
Digestion - TCLP BB301012/11/2009Completed
Extraction - TCLP BB1131112/07/2009Completed
Extraction - TCLP Organics BB131112/07/2009Completed
Florisil Cleanup DT362012/15/2009Completed
Gel Permeation Cleanup DT364012/14/2009Completed
CAS# : Chemical Abstract Service Registry Number
RL : Reporting Limit
ND : Not Detected ug / L : microgram / liter (ppb) mg / L : milligram / liter (ppm) ug / Kg : microgram / kilogram (ppb) mg / Kg : milligram / kilogram (ppm)
Laboratory Contacts
Inorganic Unit Mgr: Sandy Gregg
Organic Unit Mgr: Carol Smith
Page 7 of 891200046Lab Work Order #:
P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
Qualifier DescriptionQualifier Code
1 Result(s) and RL(s) are estimated due to low surrogate recovery.
2 Result is estimated due to high surrogate recovery.
3 Result(s) and RL(s) are estimated due to low matrix spike recovery.
4 Result is estimated due to high matrix spike recovery.
5 Result and RL are estimated due to low continuing calibration standard criteria failure.
6 Result is estimated due to high continuing calibration standard criteria failure.
7 Result(s) and RL(s) are estimated due to poor precision.
8 Result(s) and RL(s) are estimated due to low recovery of batch QC.
9 Result outside QC acceptance criteria.
A Value reported is the mean of two or more determinations.
C Value calculated from other independent parameters.
D Analyte value quantified from a dilution(s); reporting limit (RL) raised.
E Result is estimated due to high recovery of batch QC.
F Amenable cyanide was not analyzed due to low level of total cyanide.
G Result and RL are estimated due to initial calibration standard criteria failure.
H Recommended laboratory holding time was exceeded.
I Dilution required due to matrix interference; reporting limit (RL) raised.
J Analyte was positively identified. Value is an estimate.
JA Result is estimated due to multiple Aroclors present.
JC Result is estimated since confirmation analysis did not meet acceptance criteria
JD Due to severe degradation, specific Aroclor identification is difficult and quantitation is estimated.
K RL(s) raised due to matrix interferences.
KR RL(s) raised due to low sample volume submitted.
KS RL(s) raised due to low total solids.
KW RL(s) raised due to light sample weight.
LB Reported library search compounds are tentative…
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