4-Estimated Quantities For Analytical Services.xls

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NIH Chemical and Low Level Radioactive Waste, Collection, Minimization and Disposal Services
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NIHOD2010181
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Estimated Quantities Laboratory Services Required

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Sheet1

ANALYSISEPA METHODESTIMATED QUANTITIES
TTO SemivolatilesEPA 62520-25 annually
TTO VolatileEPA 62420-25 annually
Total CyanideEPA 335.2/9010B15-20 annually
WSSC Total Metals Group - Cadmium, Chromium, Copper, Lead, Nickel, Silver and ZincEPA 200.7/6010B/7000-795015-20 annually
Total MetalEPA 200.7/6010B/7000-795015-20 annually
Total MercuryEPA 7470/7471/7473300-400 annually
TCLP MetalsEPA 1311/EPA 6010B/7000-795010-20 annually
TCLP VolatileEPA 1311/EPA 8260B10-20 annually
TCLP SemivolatilesEPA 1311/EPA 8270C10-20 annually
TCLP Pesticides/HerbicidesEPA 1311/EPA 8081A/8151A10-20 annually
Priority Pollutant List VolatilesEPA 624/8260B1-2 annually
Priority Pollutant List SemivolatilesEPA 625/8270C1-2 annually
Priority Pollutant List Pesticides/PCB'sEPA 608/8081A/80821-2 annually
Priority Pollutant List MetalsEPA 200.0-289.2/200.7/6010B/7000-79501-2 annually
Sewage Sludge AnalysisSee Attachment# 331-2 annually
Total organic carbon (TOC)EPA 415.140-50 annually
Waste water outfall 001 monthly analysisSee Attachment# 4215-20 annually
BTUASTM 328620-40 annually
Flash pointASTM 3828/ EPA 1020A/1010800-1000 annually
pHEPA 150.1/9040B/90454000-5000 annually
PCBScreening Method60-80 annually
PCBEPA 608/808240-50 annually
RadioassayNIH/RSB4000-5000 annually
Water contentVisual appearance200-300 annually
Chloroflurocarbon vapor detectorScreening Method,HCFC5000 annually
Peroxide testScreening Method Using Potassium Iodide Strip25-30 annually
Ambient air analyzer using Miran 1BX analyzerScreening Method, NIH SOP #1120-30 annually, Spill check, etc.
Field test parametersScreening MethodSpill check or in case of emergency or unknown waste
Total organic halide (TOX)Screening Method Using CLOR-D-TECT test kit conforms to SW-846, EPA Method 9077100-120 annually

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Estimated Quantities For Annual Analytical Services Required&R&"Arial,Bold"Attachment 4 Page &P of &N

Sheet2

ANALYSISEPA METHODESTIMATED QUANTITIES
TTO SemivolatilesEPA 62540-50 annually
TTO VolatileEPA 62440-50 annually
Total CyanideEPA 335.235-40 annually
Total MetalEPA 200.740-50 annually
Total MercuryEPA 7470/7471/7473300-400 annually
TCLP MetalsEPA 1311/EPA 200.710-20 annually
TCLP VolatileEPA 1311/EPA 8240/6010-20 annually
TCLP SemivolatilesEPA 1311/EPA 8250/7010-20 annually
Total organic carbon(TOC)EPA 415.140-50 annually
BTUASTM 328620-40 annually
Flash pointASTM 3828/ EPA 1020A/1010800-1000 annually
pHEPA 150.1/9040/90454000-5000 annually
PCBScreening Method60-80 annually
PCBEPA 608/808040-50 annually
RadioassayNIH/RSB4000-5000annually
Water contentVisual appearance200-300 annually
Chloroflurocarbon vapor detectorScreening Method,HCFC5000 annually
Peroxide testScreening Method Using Potassium Iodide Strip25-30 annually
Ambient air analyzer using Miran 1BX analyzerScreening Method, NIH/SOP #1120-30 annually, Spill check,etc
Field test parametersScreening MethodSpill check or in case of emergency or unknown waste
Total organic halide(TOX)Screening Method Using CLOR-D-TECT test kit conforms to SW-846, EPA Method 9077100-120 annually

Sheet3

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