2024 Profile 02002P Reports.pdf

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Attached to
Hazmat Recycling Services Federal contract opportunity
Solicitation number
FA813224Q0005
Issued by
Department of the Air Force Materiel Command Air Force Sustainment Center

About this file

This document is a series of Sample Analysis Reports from the Tinker Air Force Base Environmental Laboratory (72ABW/CEIEA) for waste characterization samples, all assigned to ODEQ ID: OK00091 and Profile Number 02002P. The reports document environmental testing of metal treatment rework grinding dust and debris samples collected from June 2024 through November 2024, with five separate analyses performed on different sample batches (WCS identifiers: LI0033, LI0033A, LI0043, LI0036, and LI0008).

Each report presents comprehensive metals data analyzed using EPA methods (EPA 6010B for metals analysis, EPA 3010 for digestion, EPA 1311 for TCLP, and EPA 7473 for mercury). The samples consistently show multi-layered solid waste with dust and debris containing various metal concentrations. Detected metals include barium (ranging 0.25–2.90 ppm), cadmium (0.25–>5 ppm), chromium (0.20–>5 ppm), copper (0.44–1.84 ppm), manganese (0.40–>5 ppm), nickel (2.05 ppm), zinc (1.40–>5 ppm), antimony (0.65–>5 ppm), and molybdenum (0.22 ppm), with most other tested elements below reporting limits. Physical data shows negative halogen screening, no flashpoint detection, and pH results marked as not tested. All organic screens indicate dust/debris with trace isopropyl alcohol or petroleum distillates. Reports are reviewed by Danny Mathis, Chemist, with dates ranging from July 2024 through December 2024. Laboratory contact: 405.736.5871.

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72ABW/CEIEA TINKER ENVIRONMENTAL LABORATORY

Sample Analysis Report

ODEQ ID: OK00091

Methods of Analysis Sample Description Analyst Date 202305115

NAT 11/25/2024 02002P

SH 11/22/2024 LI0033

NAT 11/21/2024 10/25/2024

SRC 11/26/2024 PROFILE DESCRIPTION:

Headspace Screen DM 11/13/2024

Metals Data Physical Data Element Reporting

Limit Data (ppm)

Silver 0.20 ppm BRL Arsenic 0.20 ppm BRL Barium 0.20 ppm 0.25 Beryllium 0.20 ppm BRL Cadmium 0.20 ppm BRL Cobalt 0.20 ppm BRL Chromium 0.20 ppm 0.20 Copper 0.20 ppm 1.84 Manganese 0.20 ppm 0.78 Molybdenum 0.20 ppm 0.22 Nickel 0.20 ppm BRL Lead 0.20 ppm BRL Antimony 0.20 ppm BRL Selenium 0.20 ppm BRL Thallium 0.20 ppm BRL Vanadium 0.20 ppm BRL Zinc 0.20 ppm 4.00 Mercury 0.10 ppm BRL

Data Reviewed by Danny Mathis, Chemist Date: 12/3/2024

NT: NOT TESTED BRL: BELOW REPORTING LIMIT

Metals Data reported in ppm unless otherwise specified.

Data

Layers

NT

NT

NEGATIVE

SOLID

MULTI

Analysis pH Flashpoint

DUST/DEBRIS, NO SOLVENTS DETECTED

Laboratory Comments Only

Organic Screen Narritive

Halogens Physical State

TCLP (EPA 1311)

Mercury (EPA 7473)

METAL TREATMENT REWORK - GRINDING

DUST AND DEBRIS

DRUM

PROFILE NUMBER

WCS

DATE RECEIVED

GC/MS Screen FTIR Screen Flash Point pH (EPA 9040B)

Method Metals (EPA 6010B) Digestion (EPA 3010)

The Tinker Air Force Base Environmental Laboratory is committed to providing the highest quality analytical data to our customers. If you have questions please contact the laboratory at 405.736.5871.

ODEQ ID: OK00091

Analyst Date

NAT 9/18/2024

SH 9/16/2024

GF 9/11/2024

SRC 9/11/2024

Headspace Screen DM 9/11/2024

Element Reporting Limit (ppm)

Data (ppm)

Silver 0.20 BRL Arsenic 0.20 BRL Barium 0.20 BRL Beryllium 0.20 BRL Cadmium 0.20 BRL Cobalt 0.20 BRL Chromium 0.20 BRL Copper 0.20 0.44 Manganese 0.20 0.40 Molybdenum 0.20 BRL Nickel 0.20 BRL Lead 0.20 BRL Antimony 0.20 BRL Selenium 0.20 BRL Thallium 0.20 BRL Vanadium 0.20 BRL Zinc 0.20 2.44 Mercury 0.10 BRL

Data Reviewed by Danny Mathis, Chemist Date: 9/27/2024

NT: NOT TESTED BRL: BELOW REPORTING LIMIT

Data

Physical Data

Layers

NT

NT

NEGATIVE

SOLID

MULTI

Analysis pH (EPA 9040B) Flashpoint

DUST/DEBRIS WITH A TRACE OF ISOPROPYL ALCOHOL

Laboratory Comments Only

Organic Screen Narritive

Halogens Physical State

METAL TREATMENT REWORK - GRINDING

DUST AND DEBRIS

PROFILE DESCRIPTION:

Sample Data Metals Data

Sample Description

DRUM

PROFILE NUMBER

WCS

DATE RECEIVED

202303057 02002P

LI0033A

8/23/2024

GC/MS Screen FTIR Screen Flash Point pH (EPA 9040B)

Methods of Analysis Method

Metals (EPA 6010B) Digestion (EPA 3010)

TCLP (EPA 1311)

Mercury (EPA 7473)

The Tinker Air Force Base Environmental Laboratory is committed to providing the highest quality analytical data to our

ODEQ ID: OK00091

Analyst Date

GF 7/30/2024

SH 7/26/2024

GF 7/24/2024

SRC 7/24/2024

Headspace Screen DM 7/25/2024

Element Reporting Limit (ppm)

Data (ppm)

Silver 0.20 BRL Arsenic 0.20 BRL Barium 0.20 1.77 Beryllium 0.20 BRL Cadmium 0.20 0.25 Cobalt 0.20 BRL Chromium 0.20 >5 Copper 0.20 BRL Manganese 0.20 BRL Molybdenum 0.20 BRL Nickel 0.20 BRL Lead 0.20 BRL Antimony 0.20 >5 Selenium 0.20 BRL Thallium 0.20 BRL Vanadium 0.20 BRL Zinc 0.20 1.40 Mercury 0.10 BRL

Data Reviewed by Danny Mathis, Chemist Date: 8/7/2024

NT: NOT TESTED BRL: BELOW REPORTING LIMIT

Data

Physical Data

Layers

NT

NT

NEGATIVE

SOLID

MULTI

Analysis pH (EPA 9040B) Flashpoint

DUST/DEBRIS WITH TRACE OF ISOPROPYL ALCOHOL

Laboratory Comments Only

Organic Screen Narritive

Halogens Physical State

METAL TREATMENT REWORK - GRINDING

DUST AND DEBRIS

PROFILE DESCRIPTION:

Sample Data Metals Data

Sample Description

DRUM

PROFILE NUMBER

WCS

DATE RECEIVED

202403858 02002P

LI0043

7/5/2024

GC/MS Screen FTIR Screen Flash Point pH (EPA 9040B)

Methods of Analysis Method

Metals (EPA 6010B) Digestion (EPA 3010)

TCLP (EPA 1311)

Mercury (EPA 7473)

The Tinker Air Force Base Environmental Laboratory is committed to providing the highest quality analytical data to our

ODEQ ID: OK00091

Analyst Date

GF 7/24/2024

SH 7/22/2024

GF 7/16/2024

SRC 7/24/2024

Headspace Screen DM 7/16/2024

Element Reporting Limit (ppm)

Data (ppm)

Silver 0.20 BRL Arsenic 0.20 BRL Barium 0.20 2.90 Beryllium 0.20 BRL Cadmium 0.20 >5 Cobalt 0.20 BRL Chromium 0.20 >5 Copper 0.20 BRL Manganese 0.20 >5 Molybdenum 0.20 BRL Nickel 0.20 BRL Lead 0.20 BRL Antimony 0.20 0.65 Selenium 0.20 BRL Thallium 0.20 BRL Vanadium 0.20 BRL Zinc 0.20 >5 Mercury 0.10 BRL

Data Reviewed by Danny Mathis, Chemist Date: 7/26/2024

NT: NOT TESTED BRL: BELOW REPORTING LIMIT

pH (EPA 9040B)

Methods of Analysis Method

Metals (EPA 6010B) Digestion (EPA 3010)

TCLP (EPA 1311)

Mercury (EPA 7473)

METAL TREATMENT REWORK - GRINDING

DUST AND DEBRIS

PROFILE DESCRIPTION:

Sample Data Metals Data

Sample Description

DRUM

PROFILE NUMBER

WCS

DATE RECEIVED

202402572 02002P

LI0036

7/5/2024

GC/MS Screen FTIR Screen Flash Point

RAGS/DEBRI, METAL SHAVINGS, NO SOLVENTS

DETECTED

Laboratory Comments Only

Organic Screen Narritive

Halogens Physical State

Data

Physical Data

Layers

NT

NT

NEGATIVE

SOLID

MULTI

Analysis pH (EPA 9040B) Flashpoint

The Tinker Air Force Base Environmental Laboratory is committed to providing the highest quality analytical data to our

ODEQ ID: OK00091

Analyst Date

GF 7/3/2024

GF 7/3/2024

GF 7/2/2024

SRC 7/9/2024

Headspace Screen DM 7/2/2024

Element Reporting Limit (ppm)

Data (ppm)

Silver 0.20 BRL Arsenic 0.20 BRL Barium 0.20 1.29 Beryllium 0.20 BRL Cadmium 0.20 4.42 Cobalt 0.20 BRL Chromium 0.20 >5 Copper 0.20 BRL Manganese 0.20 1.34 Molybdenum 0.20 BRL Nickel 0.20 2.05 Lead 0.20 BRL Antimony 0.20 >5 Selenium 0.20 BRL Thallium 0.20 BRL Vanadium 0.20 BRL Zinc 0.20 >5 Mercury 0.10 BRL

Data Reviewed by Danny Mathis, Chemist Date: 7/15/2024

NT: NOT TESTED BRL: BELOW REPORTING LIMIT

Data

Physical Data

Layers

NT

NT

NEGATIVE

SOLID

MULTI

Analysis pH (EPA 9040B) Flashpoint

RAGS/DEBRIS WITH A TRACE OF PETROLEUM

DISTILLATES

Laboratory Comments Only

Organic Screen Narritive

Halogens Physical State

METAL TREATMENT REWORK - GRINDING

DUST AND DEBRIS

PROFILE DESCRIPTION:

Sample Data Metals Data

Sample Description

DRUM

PROFILE NUMBER

WCS

DATE RECEIVED

202400233 02002P

LI0008

6/21/2024

GC/MS Screen FTIR Screen Flash Point pH (EPA 9040B)

Methods of Analysis Method

Metals (EPA 6010B) Digestion (EPA 3010)

TCLP (EPA 1311)

Mercury (EPA 7473)

The Tinker Air Force Base Environmental Laboratory is committed to providing the highest quality analytical data to our

202305115.pdf
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202303057.pdf
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202403858.pdf
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202402572.pdf
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202400233.pdf
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