Attachment 3 E QAPS.pdf

TABLE I, Sample Retention1

LOCATION MINIMUM QUANTITY RETENTION PERIOD 1

Bulk Tank Cars/Tank Truck/Intermodal Container

Fuels 1 gallon (4 liters) 2 15 days for fuels Lubricating Oils 0.25 gallons (1 liter) 2 45 days for lubricating oils

Drums4 2 gallons (8 liter) (multi-drum composite) 3 45 days

Shipping Tank(s)

2 gallons (8 liters) for Aviation Turbine Fuels 1 gallon (4 liters) for all other Fuels, Lubricating Oils, and Additives

45 days

Tanker/Barge/Pipeline (Composite Line at Custody Transfer Point)

5 gallon (20 liters) for all fuel types 45 days

Tanker/Barge (Composite)

F.O.B. Origin 2 gallons (8 liters) for Aviation Turbine Fuels 1 gallon (4 liters) for all other fuels

45 days

F.O.B. Destination 2 gallons (8 liters) Until shore tests on-specification Tanker/Barge (Each Compartment)

F.O.B. Origin 0.25 gallon (1 liter) 45 days F.O.B. Destination 0.25 gallon (1 liter) Until shore test on-specification

NOTES:

1. Unless otherwise noted in this document or applicable contract, the retention period shall be for the stated number of days after the sample has been taken from the location indicated.

2. If the conveyance is compartmentalized, a proportional sample shall be taken from each compartment.

3. An 8-liter composite sample of each product lot shall be taken from a predetermined number of randomly selected drums IAW Table III of API MPSM, Chapter 8.1 (ASTM D 4057).

4. Applies to DLA Energy managed procurements of products shipped in drums. Does not apply to DLA Aviation managed procurements for packaged products.

T A

B L

E I

I, M in im um S am p lin g an d

T es ti n g R eq ui re m en ts f or

P et ro le um P ro d uc ts

Se ri es

, t an k er s an d ba rg es

IT

E

M W

H E

N T

O S

A M

P L

E L

O C

A T

IO

N

O F

S A

M P

L E

T Y

P E

O F

S A

M P

L E

T

E

ST

R E

Q U

IR

E

D

1.

a

Prior to Loading

B ef or e ac ce pt an ce o f ne w m at er ie l an d af te r es ta bl is hm en t o f ne w ba tc h4

E ac h sh or e st or ag e ta nk

Si ng le T an k

C om po si te o r A ll

L ev el s

A 5, 1.

b

A ft er li ne p ac k bu t p ri or to lo ad in g A s cl os e to th e cu st od y tr an sf er po in t a s po ss ib le e

Sa m pl e

C 7, D ed ic at ed

S ys te m

B

-1 N on -D ed ic at ed

S ys te m

1.

c

During Loading

Im m ed ia te ly a ft er s ta rt o f lo ad in g/ sh ip m en t A s cl os e to th e cu st od y tr an t a s po ss ib le

L in e Sa m pl e C

1.

d

A ft er f ir st

V es se l c ar go c om pa rt m en t( s)

Sp ot

C 7, 1.

e

D ur in g lo ad g s cl os e to th e cu st od y tr an t a s po ss e

Sa m pl e

H ou rl y

V is ua l6, 8 , R et ai n10

1.

f

After Loading ft er lo ad h ve ss el c ar go c om pa rt m en t

A ll

L ev el

C om bi ne

A ll

L ev el s in to o ol um et ri c C om po si te

S am pl e13

C 6, , 1

1, R em ai nd er o f B

(R et ai n fu el f or

B -1 r ef er ee te st g)

N O

T E

S

1.

A dd iti on al r eq ui re m en ts to in cl ud e re ta in s am pl es m ay b e re qu ir ed

Se e

Q ua lit y

A ss ur an ce P ro vi si on s (C o r

E -Q

A P fo r fu rt he r de ta il s.

2.

ef er to A

ST

M

I nt er na tio na l D f or s am pl in g pr oc ed ur es

3.

T es t r es ul ts s ha ll be c om pa re d ag ai ns t t he q ua lit y re le as e ce rt if ic at e.

A ny d is cr ep an ci es s ha ll be id en ti fi ed , i nv es ti ga te d, a nd r es ol ve d.

4.

U po n pr oc ur em en t a t r ef in er ie s, b le nd in g in st al la tio ns , e tc . a nd a t m ai n in st al la tio ns in cl ud in g na tio na l d ep ot s o ce an im po rt in g po in ts o n es ta bl is hm en t o f ne w b at ch es

5.

P ri or to p er fo rm in g A

-l ev el te st in g, th e ho m og en ei ty o f ea ch b at ch s ha ll be d et er m in ed

. R ef er to p ar ag ra ph

b) (1 ii

i) (C of th is d oc um en t f or a dd it io na l d et ai ls

6.

T es t f or F

SI

I an d

SD

A o nl y if li ne in je ct ed

7.

I f sa m pl e fa il s ap pe ar an ce

, p er fo rm p ar tic ul at e m at te r us in g ap pr ov ed m et ho ds a s ou tli ne d in th e ap pl ic ab le s pe ci fi ca tio n.

8.

ub ri ci ty a ls o re qu ir ed f or F

-7 on ly if li ne in je ct ed , o r de te rm in e

L

IA

c on ce nt ra tio n by v ol um et ri c m ea su re m en t/ ca lc ul at io

9.

F ir st in s ha ll be d on e af te r on e (1

) m et er o r af te r lin e di sp la ce m en t w hi ch ev er is th e gr ea r.

Fo r al l t an ke r an d ba rg e, a f lo w -p ro po rt io na l s am pl e ta ke n in a cc or da nc e w ith M

PM

S

C ha pt er

, S ec tio n 2, is p re fe rr ed a t t he c us to dy tr an sf er p oi nt

. H ow ev er

, m an ua l s am pl es ta ke n in a cc or da nc e w ith M

PM

S

C ha pt

8, S ec tio n ar e ac ce pt ab le if th ey a re ta ke n ho ur ly th ro ug ho ut th e sh ip m en t a nd th at th e qu an ti ty o f th e co m po si te s am pl e m ee ts th e re qu ir em en ts in T ab le

I

B es t p ra ct ic e is f or B

-1 te st c om pl et io n fo r

FO

B O ri gi n Pr oc ur em en ts or T yp e

A le ve l t es tin g w he n sp ec if ie d in c on tr ac t f or

F O

B D es tin at io n Pr oc ur em en ts pr io r to v es se l r el ea se

B as ed o n Q

A R d ec is io n, v es se l m ay l a ft er

C T es ts to m ee t s ch ed ul e re qu ir em en ts in cl ud in g to a vo id p re di ct ed w ea th er

; r em ai nd er o f B

-1 te st s to b e co m pl et ed b ef or e ar ri va l a t n ex t l oa d or d is ch ar ge p or t.

T es t r ep or t w ill b e pr ov id ed to d es ig na d di sc ha rg e po rt

T yp e

A le ve l t es tin g re qu ir ed f or F

O B

D es tin at io n

Pr oc ur em en ts un le ss o th er w is e sp ec if ie d by c on tr ac t)

A s de fi ne d by A

PI

M

P M

S C ha pt er

-1 , s ec ti on

.2

Fo r pr od uc t v er if ic at io n pu rp os es . R es ul ts o f C

-t es t m us t f al l w ith in r ep ro du ci bi lit y of s ou rc e ta nk

A -l ev el r es ul ts

N ew c ar go f ro m s am e ba tc h, w ith in da ys

, w ill o nl y re qu ir e B

-1 te st in g to v er if y pr ev io us

A -l ev el te st r es ul ts

. B -1 le ve l v er if ic at io n te st r es ul ts s ho ul d fa ll w ith in g re pr od uc ib ili ty o f so ur ce ta nk A

-l ev el r es ul ts

A

B L

E I

I, M in im um S am p lin g an d

T es ti n g R eq ui re m en ts f or

P et ro le um P ro d uc

Se ri es

, p ip el in e, t an k tr u ck s, t an k ca rs

, i so

-c on ta in er s1, IT

E

M W

H E

N T

O S

A M

P L

E L

O C

A T

IO

N

O F

S A

M P

L E

T Y

P E

O F

S A

M P

L E

T

E

ST

R E

Q U

IR

E

D

2.

a

Prior to Shipment

B ef or e ac ce pt an ce o f ne w m at er ie l a nd af r es ta bl is hm en t o f ne w b at ch h Sh ip m en t S to ra ge T an k

Si ng le T an k

C om po si or ll L ev el s A

9, 2.

b

A ft er li ne p ac k bu t p ri to lo ad in g/ sh ip m en t A s cl os e to th e cu st od y tr an sf er p oi nt a s po ss e

Sa m pl e

C 5, D ed ic at ed

S ys te m

B -1

N on

-D ed ic at ed S ys te m

2.

c

During Shipment

Im m ed ia te ly a ft er s ta rt o f lo ad in g/ sh ip m en t A s cl os e to th e cu st od y tr an sf er p oi nt a s po ss ib le a nd d ow ns tr ea m o f th e fi lte r se pa ra to r

(i f eq ui pp ed

L in e

Sa m pl e

C 5, 2.

d

Pi pe li ne

O nl y:

H ou rl y af te r st ar t o f lo ad in g or s hi pm en t10 cl os e to th e cu st od y tr an sf er p oi nt a s po ss ib le a nd d ow ns tr ea m o f th e fi lte r se pa ra to r (i f eq ui pp ed

L in e Sa m pl e A pp er an ce

5, (R et ai n fu el f or

B -1 r ef ee in g)

2.

e

D ai ly o n fi rs t f il l a nd a ny tim e a ne w ta nk is pl ed o n is su e

(a ft er li ne d is pl ac em t)

, T C

, I

SO

, R ef ue le rs o r ot he r ov er th e ro ad tr an sp or ta tio n m od es o nl y cl os e to th e cu st od y tr an sf er p oi nt a s po ss ib le

L oa di ng

R ac k or

F ill

P oi nt an d do w ns tr ea m o f th e fi lt er s ep ar at or if eq ui pp ed

L in e Sa m pl e C ol or by v is ua l m et ho d) an

A pp ea ra nc e5 .

If v is ua l f ai ls p er fo rm C

2.

f

After Loading

D ai ly f or e ac h co nv ey an ce m od e

(N r eq ui re d fo r pi pe li ne o pe ra ti on s) h

C ar go C om pa rt m en t o r an ot he r po in t th at p ro vi de s a re pr es en ta tiv e sa m pl e A ll L el pp ea ra nc e on e ac h co m pa rt m t n co m po si te

,6

,8

D ru m s

Sa m pl e of e ac h lo t o f pr od uc t s ha ll b e ta ke n fr om a p re de te rm ed nu be r of r an do m ly s el ec te d dr um s14 M ul ti

-d ru m C om po

N O

T E

S:

1.

A dd iti on al c on tr ac tu al r eq ui re m en ts to in cl ud e re ta in s am pl es m ay b e re qu ir ed

S ee C on tr ac t Q ua lit y A ss ur an ce

P la ns

C o r E

-Q A

P s) f or f ur th er d et ai ls

2.

R ef er to

A

ST

M I nt er na tio na l D f or s am pl in g pr oc ed ur es

3.

T es t r es ul ts s ha ll be c om pa re d ag ai ns t t he q ua lit y re le as e ce rt if ic at e.

A ny d is cr ep an ci es s ha ll be id en ti fi ed

, i nv es ti ga te d, a nd r es ol ve

U po n pr oc ur em en t a t r ef in er ie s, b le nd in g in st al la tio ns

, e tc an d at m ai n in st al la tio ns in cl ud in g na ti on al d ep ot s o ce an im po rt in g po in ts o n es ta bl is hm en t o f ne w b at ch es

5.

T es t f or

F

SI

I an d

SD

A o nl y if li ne in je ct ed

6.

I f sa m pl e fa il s ap pe ar an ce , p er fo rm p ar tic ul at e m at te r us in g ap pr ov ed m et ho ds a s ou tli ne d in th e ap pl ic ab le s pe ci fi ca ti on

7.

T yp e

A le ve l t es tin g re qu ir ed f or F

O B

D es tin at io n

Pr oc ur em en ts un le ss o th er w is e sp ec if ie d by c on tr ac t)

8.

I f th e co nv ey an ce is c om pa rt m en ta li ze d, a p ro po rt io na l s am pl e sh al l b e ta ke n fr om e ac h co m pa rt m en t s uc h th at a to ta l o f on e li te r is c ol le ct ed f ro m th e co nv ey an ce

9.

F ilt ra ti on ti m e te st in g is r eq ui re d fo r

JP

-5

J P-an d sh al l m ee t c on tr ac t r eq ui re m en t.

Fo r pi pe lin e sh ip m en ts , a f lo w -p ro po rt io na l s am pl e ta ke n in a cc or da nc e w it h

M

PM

S C ha pt er

, S ec tio n

2, is p re fe rr ed a t t he c us to dy tr an sf er p oi nt . H ow ev er , m an ua l s am pl es ta ke n in a cc or da nc e w ith

M

PM

S C ha pt er

Se ct io n ar e ac ce pt ab le if th ey a re ta ke n ho ur ly th ro ug ho ut th e sh ip m en t a nd th at th e qu an tit y of th e co m po si te s am pl e m ee ts th e re qu ir em en ts in T ab le

I

. P ri or to p er fo rm in g A

-l ev el te st in g, th e ho m og en ei ty o f ea ch b at ch s ha ll be d et er m in ed

. R ef er to p ar ag ra ph

b) (1 ii

i) (C of th is d oc um en t f or a dd iti on al d et ai ls

L ub ri ci ty a ls o re qu ir ed f or

F -7 on ly if li ne in je ct ed o r de te rm in e L

IA

c on ce nt ra tio n by v ol um et ri c m ea su re m en t/ ca lc ul at

Fo r pr od uc t v er if ic at io n pu rp os es . R es ul ts o f C

-t es t m us t f al l w ith in r ep ro du ci bi lit y of s ou rc e ta nk r es ul ts

. A co m po si te s am pl e of ga llo ns lit er s) f or

A vi at io n T ur bi ne F ue ls an d ga llo n

(4 li te rs fo r al l o th er f ue ls fo r ea ch lo t o f pr od uc t s ha ll be ta ke n fr om a p re de te rm in ed n um be r of r an do m ly s el ec te d dr um s.

T he to ta l nu m be r of d ru m s sa m pl ed p er lo t s ha ll, a t a m in im um , b e th at c ite d in T ab le

I

II

of A

P I

M

PM

S ch ap te r 8.

(A

ST

M d b ut m ay b e in cr ea se d at th e go ve rn m en t's o pt

A

B L

E I

I, M in im um S am p lin g an d

T es ti n g R eq ui re m en ts f or

P et ro le um P ro d es

, p ro d uc t re ce ip t an d d is ch ar ge s fo r ta n ke rs a n d b ar ge s (F

O B

D es ti n at io n

IT

M

W H

E N

T O

S A

M P

L E

L O

C A

T

IO

N O

F S

A M

P L

E T

Y P

E O

F S

A M

P L

E T

E

ST

R E

Q U

IR

E

D

3.

a

Prior to Discharge

Pr io r to d is ch ar ge

Fr om e ac h ve ss el c ar go c om pa rt m en t

A ll

L pp ea ra nc e an d

D en si ty

3.

b

F ro m e ac h ve ss el c ar go c om pa rt m en t

A ll

L ev el (C om bi ne A ll L ev el s in to ol um et ri c

C om po

Sa pl e)

3.

During Discharge

W ith in m in ut es a ft er s ta rt a nd e ac h ho ur a ft er u nt il c om pl et

D oc k/

D is ch ar ge M an if ol d

H ea de r

L in e Sa m pl e / R et ai n Pe rf or m A pp ea ra nc e te st 2, an d th en r et ai n fu el f ef er ee te st in g

3.

e

After Discharge

If r em ai nd er o f fu el w il l b e sh ip pe he r

D

FS

P h ve ss el c om pa rt m en t w it h fu re ai ni ng o n bo ar d

A ll

L ai n un til d is ch ar ge at de in at io n

N O

T E

S:

1.

T es t f or f la sh p oi nt o n hi gh f la sh c ar go ta nk s if lo w a nd h ig h fl as h ca rg oe s ar e ca rr ie d to ge th er a bo ar d th e sa m e ve ss el w ith ou t s eg re ga te d ve nt in g sy st em or a vi at io n fu el d el iv er y, F

SI

I an d

SD

A s ha ll b e te st ed o nl y if li ne in je ct ed

T hi s re qu ir es a n ad di tio na l q ua rt s am pl e.

es t f or a dd iti ve s if li ne in je ct ed d ow ns tr ea m o f th e in je ct or

If li ne in je ct in g

L

IA

in to

F -7

6, te st f or lu br ic it y.

B L

E I

I, M in im um S am p lin g an d

T es ti n g R eq ui re m en ts f or

P et ro le um P ro d es

, p ro d uc t re ce ip t fr om p ip el in e (F

O B

D es ti na ti

)1

IT

M

W H

E N

T O

S A

M P

L E

L O

C A

T

IO

N O

F S

A M

P L

E T

Y P

E O

F S

A M

P L

E T

E

ST

R E

Q U

IR

E

D

4.

c

During Receipt

D ur in g pi pe li ne r ec ei pt us to dy tr an sf er p oi nt e

Sa m pl e/

R et ai n

G al lo n M in im um

4.

d

D ur in g pi pe li ne r ec ei pt

, i m m ed ia te ly a ft t, M id po in t a nd h ou r pr io r co pl et n3 cl os e to th e cu st od y tr an sf er p oi nt a s po ss e

After Receipt

A ft er r ec ei pt o f fu h re ce ip t t an k A ll le ve l

T

S:

1.

ef er to A

ST

M

I nt er na ti on al D f or s am pl in g pr oc ed ur es

2.

R et ai n fo r re fe re e te st in g in th e ev en t a f ai lu re o cc ur s on r ec ei pt ta nk . R et ai n sa m pl e fo r d ay s.

S am pl in g is I

A W

A

PI

M

PM

S C ha pt er

3.

F ue l f ro m a n ew b at ch w ill b e co ns id er ed a n ew r ec ei pt f or q ua li ty c on tr ol p ur po se

TABLE III, Definitions of Test Series I. TYPE A: Includes all specification quality conformance tests plus any additional contractual requirements.

II. TYPE B-1 & C: As shown in the table below for each product. Properties and test methods will be in accordance with the product specification for each grade identified in the solicitation/contract.

AVGAS

AVIATION

TURBINE MOGAS

DIESEL/

KEROSENE/

NAVAL DISTILLATE LUBE OIL

TEST PROPERTIES B-1 C B-1 C B-1 C B-1 C B-1 C

Appearance/ workmanship

Particulate content * *8 *1 *8

Filtration Time *

Color (visual) * * * * * * * * *

Density/API Gravity/ Specific Gravity

Distillation * * * *

Corrosion, Copper Strip * *

Existent Gum * *

Carbon Residue *1

Vapor Pressure * *

Lead Content * *3

Freeze Point *

Flash Point * * * * *

FSII Content *

MSEP (JP-8, F-24, F-27,

Jet A & Jet A-1)

Conductivity (JP-5 & JP- 8, F-24, F-27 & Jet A-1)

*4

Thermal stability (B-1 requirement applies to JPTS and marine/multi-product mode receipt tank sample)

Sediment & Water

Total Sediment aged

Viscosity *7

Water Content * *8 *2

Emulsion *2

Foam Test *

Knock Rating (RON / MON) *6

Lubricity *1

FAME *5 *1

Solid Contaminants *2

* The procedure to be used for conducting these tests will be as stated in the appropriate product specification and/or contract. For any products not covered under this table, contact Quality Assurance Representative for guidance.

NOTES:

1. F76 only.

2. Only if the specification has this requirement.

3. If contamination with leaded fuels is suspected.

4. If fuel contains conductivity additive, wait approximately 2 minutes after obtaining sample for charges in the fuel to dissipate before performing CU testing.

5. Only for product transported through multi-product systems, including marine transport.

6. Perform only if Lead Content is performed and fails and/or contamination with another product is suspected. In the case of pipeline, this test shall be performed when considered necessary.

7. For MIL-PRF-17331 and MIL-PRF-9000 viscosity is not required unless the tank has been in long term storage for 3 months.

8. Visual check.

B L

E I

V , C on ve rs io n ch ar t fo r ta n k t ru ck s (T

T ta n k c ar s

(T C t an k w ag on s

(T W t an k t ra il er

T R in te rm od al c on ta in er s

(I M

C )1, as t P ro d uc t

C ar

O D

U C

T T

O B

E L

O A

D E

G as ol in es

: M U

R

M U

M , M

U P, E

FM

E

, 1

, 1

, J vi at io n

T ur bi ue ls

: J A

A /A

1, JP

-8

, F -2

4, J

P -5

T

S 1, K S1

/R /N

A vi at io n T ur ue l3 :

J

P T

S

R P

1/

P2

0/ P

F

D ie se l F ue l:

F -7

F

II

ub ri ca tin g O il s

D ie se l F ue ls

D

F 1, D F2

D

S 1, D S2

D

S S

, D S

W

B D

I, M

G O

G as ol in es

M U

R , M

U M

M

U P

, E

FM

, E

, 1

0, J ra in

/E m pt y

S te am /D ry

St ea m m am m m m m vi at io n T ur bi ne F ue ls

4, JA

A

/A 1, J P

-8 , F

-2 4, -5 , T

S 1, K S

1/ R

/N

D ra in /E m pt y D ra in

/E m pt y

St ea m /D ry St ea m

/D ry

S te am /D ry St ea m

/D ry

St ea m /D ry St ea m

/D ry

St ea m /D ry

A vi at io n T ur bi ne F ue l3

JP

T

S D ra in

/E m pt y

D ra in /E m pt y D ra in

/E m pt y

D ra in /E m pt y S te am m m am m

1/ R

P2 St ea m am m ra in

/E m pt y

St ea m am m /D ry St ea m

/D ry

St ea m

J1 0/

PF

-1

St ea m D ry S te am

/D ry

St ea m /D ry St ea m

D ry

D ra in /E m pt y S te am

/D ry

St ea m /D ry St ea m

/D ry

St ea m /D ry P et ro le um

S ol ve nt o r

P nt hi nn er

St ea m am m m am m am m m ie se l F ue l:

F -7

St ea m

/D ry

St ea m /D ry St ea m

/D ry

St ea m /D ry S te am

/D ry

D ra in /E m pt y S te am

/D ry

St ea m /D ry D ra in

/E m pt y

D ie se l F ue ls

D

F 1, D

2, 1, D

S2 , D

SS

, D

S W

M

G O

St ea m /D ry St ea m

/D ry

St ea m

/D ry

St ea m /D ry S te am

/D ry

St ea m /D ry S te am

/D ry

S te am /D ry D ra in

/E m pt y

F S

II

S

IH

D ra in

/E m pt y

D ra in /E m pt y St ea m

/D ry

St ea m /D ry S te am

/D ry

St ea m /D ry D ra in

/E m pt y

St ea m /D ry St ea m

/D ry

N O

L O

A D

N O

L O

A D

N O

L O

A D

N O

L O

A D

N O

L O

A D

N O

L O

A D

N O

L O

A D

St ea m /D ry

St ea m /D ry

D F

1, D

F2 , D

S1 , D

S2 , D

S S

D

S W

St ea m m /D ry

N O

L O

A D

N O

L O

A D

N O

L O

A D

St ea m /D ry S te am

/D ry

S te am /D ry S te am

/D ry

N O

L O

A D

N O

L O

A D

N O

L O

A D

N O

L O

A D

N O

L O

A D

N O

L O

A D

N O

L O

A D

N O

L O

A D

S te am /D ry

N O

L O

A D

N O

L O

A D

N O

L O

A D

N O

L O

A D

N O

L O

A D

N O

L O

A D

N O

L O

A D

N O

L O

A D

St ea m /D ry

D ra in /E m pt y St ea m

/D ry

St ea m /D ry St ea m

/D ry

St ea m /D ry St ea m

/D ry

St ea m /D ry St ea m

/D ry

St ea m

A

B L

E I

V C on ti nu ed

,C on ve rs io n c h ar t fo r ta n k t ru ck s (T

T ta n k c ar s

(T C t an k w ag on s

(T W t an k t ra il er

T R in te rm od al c on ta in er s

(I M

C )1, T E

S

1.

F or p re vi ou s ca rg oe s no t l is te d, c on ta ct D

L A

E ne rg y

Q ua lit y

O pe ra tio ns D iv is io n at D

LA

En er gy

Q ua lit yO pe ra tio ns dl a.

m il fo r ac ce pt ab il it y/ cl ea ni ng p ro ce du re

G er al

I ns tr uc ti on s fo r T an k

C ar s an d T ru ck a.

ve ya nc es al l) s ha ll b e dr y an d fr ee f ro m lo os e ru st , s ca le

, a nd d ir t b.

an li ne d eq ui pm en t s ho ul d no t b e st ea m c le an ed ; w at er w as h sh ou ld s uf fi ce c.

ro le um p ro du ct s sh al l n ot b e lo ad ed in to th e co nv ey an ce s w he re th e pr ev io us c ar go w as c au st ic

, a ci d, o r ch lo ri na te d so lv en ts k tr uc ks a nd c ar s in li qu id f er til iz er s er vi ce s ha ll n ot lo ad a vi at io n tu rb in e fu el s di re ct ly b ut s ha ll ca rr y ou t a t l ea st tw o lo ad s of c om m er ci al g as ol in e pr io r to th e av ia ti tu rb in e fu el lo ad ve rs io n of

G ov er nm en t-ow ne d ta nk c ar s fr om li qu id f er ti li ze r se rv ic e to a vi at io n tu rb in e fu el s er vi ce s ha ll o nl y be d on e w he n no o th er a lt er na ti ve e xi st s.

T an k ca rs b ei ng nv er te d fr om li qu id f er ti liz er s er vi ce to a p et ro le um p ro du ct s ha ll be a de qu at el y cl ea ne d to r em ov e al l t ra ce s of li qu id f er ti li ze r.

A t a m in im um , t he e qu ip m en t m us t b e st cl ne d;

d ri ed a nd m us t b e fr ee f ro m lo os e ru st , s ca le

, a nd d ir t.

A ft er c le an in g, b ut b ef or e lo ad in g av ia ti on tu rb in e fu el s, a t l ea st tw o lo ad s of c om m er ci al g as ol in e sh al l b e ca rr ie d pr io r to lo ad in g av ia tio n tu rb in e fu el . E qu ip m en t w ith u nl in ed c om pa rt m en ts s ho ul d ha ve it s co m pa rt m en ts li ne d w it h an a pp ro ve d co at in g at th is ti m e.

C on ve ya nc es c ar ry in g th ei r in it ia l l oa d of a vi at io n tu rb in e fu el f ol lo w in g co nv er si on s ha ll n ot b e re le as ed f ro m th e lo ad in g un ti l t he y ha ve b ee n sa m pl ed a m in im um o f h ou rs a ft er lo ad in g.

I n ac co rd an ce w it h M

IL

-S

T D

-3

4- 1A

, s am pl es s ha ll u nd er go ty pe B

-2 te st in g pl us T he rm al S ta bi lit y

T es t ( if r eq ui re d by th e pr od uc t s pe ci fi ca ti on

A ft er ty pe

B -2 te st s in di ca pl ia nc e w it h sp ec if ic at io n re qu ir em en ts

, t he c on ve ya nc e ca n be r el ea se d pe nd in g re su lt s of th e T he rm al S ta bi li ty te st s.

T he c on ve ya nc e sh al l n ot b e un lo ad ed u nt il th e lo ad in g po in t n ot if ie s th e de st in at io n th at th e T he rm al S ta bi li ty te st w he n re qu ir ed ha s pa ss ed

. W he n th e ab ov e co nd iti on a pp li es

, t he

D D

-2

, W id e A re a

W or kf lo w

W A

W F)

E ne rg y

R ec ei vi ng R ep or t ( E

R R or e qu iv al en t f or m s ha ll be s o no o be lo ad ed o nl y in a lu m in um o r st ai nl es s-st ee l c on ve ya nc e, o r ot he r co nv ey an ce li ne d w ith a n ap pr ov ed e po xy c oa ti ng . I f eq ui pm en t i s co at ed

, c le an w ith h ot f re sh w at er ex ce ed in g

°C

6°

F an d dr y th or ou gh ly

4.

If p re vi ou s ca rg o co nt ai ne d dy e m ar ke r, a ll tr ac es o f co lo r m us t b e re m ov ed

5.

If p ro du ct to b e lo ad ed d oe s no t c on ta in d ye

, t he n th e ve hi cl e sh al l n ot c on ta in a ny tr ac es o f dy e pr io r to lo ad in g.

6.

D ra in

/e m pt y on ly w he n sa m e sp ec if ic at io n pr od uc t i s be in g lo ad ed

7.

P ri or to lo ad in g th e av ia tio n fu el s li st ed

, t he c on ve ya nc e m us t h av e ca rr ie d a pr ev io us n on

-F A

M E c ar go a nd th en b e st ea m c le an ed a nd d ri ed . T ru ck s th at h av e pr ev io us ly c ar od ie se l c re at e a ri sk o f cr os s-co nt am in at io n of a vi at io n tu rb in e fu el w it h re si du al b io di es el c om po ne nt s.

D ie se l f ue l m ay c on ta in u p to

F

A M

E w ith ou t r ep or ti ng it a s bi od ie se l.

B ec au se o f th e di ff ic ul ti es in m ak in g a lo ad -r ac k of th e pr es en ce o f F

A M

E in th e pr ev io us lo ad

, t he m or e st ri ng en t “

S te am /D ry is r eq ui re

8.

ra in a nd e m pt y if lo ad in g bi od ie se l b le nd

9.

C ar go s ca rr yi ng d ye d ke ro se ne s ha ll u se th e st ea m /d ry c le an in g pr oc ed ur

OPPENHEIM.LEE.B.122

9310131

Digitally signed by OPPENHEIM.LEE.B.1229310131 DN: c=US, o=U.S. Government, ou=DoD, ou=PKI, ou=DLA, cn=OPPENHEIM.LEE.B.1229310131 Date: 2015.07.30 16:00:30 -04'00'

SHANNON.MICHAEL.J.

1229294802

Digitally signed by SHANNON.MICHAEL.J.1229294802 DN: c=US, o=U.S. Government, ou=DoD, ou=PKI, ou=DLA, cn=SHANNON.MICHAEL.J.1229294802 Date: 2015.07.30 14:17:00 -04'00'

SHEPHERD.SANDRA.S.

1012568459

Digitally signed by SHEPHERD.SANDRA.S.1012568459 DN: c=US, o=U.S. Government, ou=DoD, ou=PKI, ou=DLA, cn=SHEPHERD.SANDRA.S.1012568459 Date: 2015.07.30 15:38:32 -04'00'

OPPENHEIM.LEE.B.122

9310131

Digitally signed by OPPENHEIM.LEE.B.1229310131 DN: c=US, o=U.S. Government, ou=DoD, ou=PKI, ou=DLA, cn=OPPENHEIM.LEE.B.1229310131 Date: 2015.06.26 13:12:16 -04'00'

SHANNON.MICHAEL.J.

1229294802

Digitally signed by SHANNON.MICHAEL.J.1229294802 DN: c=US, o=U.S. Government, ou=DoD, ou=PKI, ou=DLA, cn=SHANNON.MICHAEL.J.1229294802 Date: 2015.06.26 08:57:05 -04'00'

SHEPHERD.SANDRA.S.

1012568459

Digitally signed by SHEPHERD.SANDRA.S.1012568459 DN: c=US, o=U.S. Government, ou=DoD, ou=PKI, ou=DLA, cn=SHEPHERD.SANDRA.S.1012568459 Date: 2015.06.26 12:47:33 -04'00'

SPE602-25-Q-0702 Exhibit 4