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DEFENSE LOGISTICS AGENCY ENERGY Page 1 of 6

8725 JOHN J. KINGMAN ROAD

FORT BELVOIR, VIRGINIA 22060-6222

DISTRIBUTION STATEMENT – A: APPROVED FOR PUBLIC RELEASE. DISTRIBUTION IS UNLIMITED

C16.23 FUEL, NAVAL DISTILLATE (F-76) (DLA ENERGY AUGUST 2022)

NATIONAL STOCK NUMBER PRODUCT NOMENCLATURE DLA ENERGY PRODUCT CODE

9140-00-273-2377 Fuel, Naval Distillate F76

For supplies delivered under this contract, the Contractor shall conform to all International, Federal, State, and local environmental requirements applicable to the geographic location of the receiving activity on the date of delivery. The Contractor shall also comply with all applicable International Agreements, Treaties, Conventions, and the like to which the United States is a signatory or with whose terms the receiving activity has otherwise agreed to comply, including but not limited to, the requirements of MARPOL 73/78 Annex VI Regulations 14 and 18. The Contractor shall be responsible for determining the existence of all such requirements prior to the time deliveries are made. This includes delivery of fuel and documentation in a manner consistent with any existing or after-imposed Title V (Clean Air Act) Permits. The list of such requirements contained in this contract is not intended to be a complete list, and the Contractor shall be responsible for determining the existence of all such requirements. In the event that an International, Federal, State, and/or local environmental requirement, as identified above, is more stringent than a requirement contained in this contract, the Contractor shall deliver product(s) that complies with the more stringent requirement. Product(s) that fails to meet the more stringent requirement will be considered nonconforming supply. Product(s) to be supplied shall fully meet the requirements of the applicable specification(s). In the event that compliance with the more stringent requirement causes the contractor to incur additional costs, the contractor may request an equitable adjustment.

Unless otherwise indicated by the Contractor in writing, prior to award, the product offered shall be required to fully meet all applicable specifications. The supplier shall provide to the receiving vessel a “Statutory Sample” of at least 400 mL in volume, taken from the receiving vessel’s inlet bunker manifold, together with a Bunker Delivery Note (BDN). This sample will be sealed and carry a sample tag that provides the documentation required per MARPOL 73/78, Annex VI Regulation 18.

a) Naval Distillate Fuel (F-76) shall conform to the requirements of Military specification MIL-DTL-16884P dated 26 Sept 2017.

Nomenclature for Naval Distillate Fuel (F-76) is shown above.

b) SPECIFICATION MODIFICATIONS:

1) Flash Point: All batches of F-76 that are presented for Government acceptance at origin shall meet a minimum flash point requirement of 62.5 degrees Celsius (°C).

2) F-76 offered from a location other than where refined (excludes synthesized material as defined in section 3.2.2 and 3.2.3 of MIL- DTL-16884P) requires testing for FAME content by test method ASTM D7963, BS EN 14078, or IP 579. ASTM D7963 is considered to be the referee test method.

3) In Australia, all deliveries of F-76 shall have a minimum Flash Point of 62.5°C at the custody transfer point.

4) Ash, mass%: All batches of F-76 shall not exceed 0.010% Ash by ASTM D482.

c) MATERIALS: The F-76 supplied under this contract shall not contain un-hydrotreated light cycle oils or contain any stabilizer additives, or any other additive or material not explicitly allowed per section 3.2 of MIL-DTL-16884P.

For F-76 containing a synthetic component, the synthetic component shall be certified to Tables A-I and A-II of MIL-DTL-16884P; for synthesized iso-paraffins, the synthetic component shall be certified to Tables B-I and B-II of MIL-DTL-16884P. It is not necessary to analyze each batch of the synthetic component for compliance with Table A-II (or Table B-II, as applicable) once it is demonstrated that the process scheme is adequately controlled and if no significant changes to existing production operations have been made, such as a turnaround event on a refinery unit used to produce the synthetic component or a change in feedstock material. The signed F-76 synthetic component certification page shall be supplied for each shipment which includes synthetic paraffinic materials attesting that no changes to the production process have been made and certifying that the last certificate of analysis, dated and including Table A-II (or Table B-II, as applicable) results, is still valid.

d) ADDITIVES:

1) Lubricity Improver Additive (LIA) – Lubricity additives are allowed in F-76. The LIA additive(s) used shall conform to MIL-PRF-

32490A, Performance Specification, Additive, Lubricity Improver, Distillate Fuel, dated 24 May 2019 and found in ASSIST and shall

DEFENSE LOGISTICS AGENCY ENERGY Page 2 of 6 be listed in the electronic Qualified Products List (QPL)-32490, located in the Qualified Products Database (QPD) found at https://assist.dla.mil/ (or http://quicksearch.dla.mil) . Instructions on how to use ASSIST are located in QAP C1.02. Either Grade A.

Grade B, or Grade C material is suitable for treatment of de-sulfurized F-76. Additive concentration shall not exceed the maximum allowable concentration applicable to the specific additive selected for inclusion in finished F-76.

2) Information pertaining to qualification of additives not currently listed on QPL-32490 may be obtained from Commander, Naval Sea Systems Command, ATTN: SEA 05S, 1333 Isaac Hull Avenue, SE, Stop 5160, Washington Navy Yard, DC 20376-5160, USA, or by e-mailing CommandStandards@navy.mil.

3) Dyes and Markers - Red dye required in off-highway diesel fuel in accordance with 40 CFR Part 80 as modified by the Environmental Protection Agency's interim final rule published in the Federal Register dated July 14, 1994 shall not be added to F-

76. The finished product shall show no visual evidence of red dye. This F-76 product is for military, off-highway use only and must be segregated at all times from any diesel fuel used on-highway. NOTE: Red dye does not apply to Atlantic/Europe/Mediterranean or Western Pacific Overseas Bulk purchase programs unless offering refinery is located in the United States or one of its possessions.

e) BATCH SAMPLING: The Contractor shall provide one 20 mL sample per each individual tank in a procurement batch.

For each 20 mL sample provided by the Contractor, the Contractor shall also submit a Refinery Certificate of Quality (RCQ), or Certificate of Analysis (CoA), as applicable, with the F-76 sample when submitting to the US Naval Research Laboratory.

The RCQ or CoA for each individual tank shall be representative of Level A testing for the F-76 product.

NOTE: This sample is in addition to those required in accordance with Quality Assurance Provision (QAP) E1

QUANTITY OF SAMPLE WHEN SAMPLED SUBMISSION PERIOD

20 mL Upon completion of each individual procurement batch

Shipped within 30 days of delivery of

“Batch” Definition in accordance with MIL-STD-3004-1A, 3.1.9: A specific quantity of product that is processed or utilized as a single unit and tested to meet test criteria and specifications.

The sample from each tank/batch shall be either an all-level sample or a composite of upper, middle, and lower samples. A copy of the full-specification test report shall accompany each sample. The sample container will be any 20 mL amber borosilicate vial with a polytetrafluoroethylene (PTFE) lined screw cap. A tracking number for the samples shall be provided to: Thomas Loegel at Thomas.loegel@nrl.navy.mil or (202) 404-1157. Samples shall be shipped to:

US Naval Research Laboratory ATTN: Thomas Loegel, Code 6181 F76 Component Analysis Forensic Project 4555 Overlook Ave., S.W.

Washington D.C. 20375-5320

The paperwork provided with these samples shall include the following information:

Contract Number Contractor’s Name Product Refinery Location Quantity of Tank/Batch Full-Specification Test Report https://assist.dla.mil/ https://assist.dla.mil/ https://assist.dla.mil/ https://assist.dla.mil/ https://assist.dla.mil/ http://quicksearch.dla.mil/ http://quicksearch.dla.mil/

DEFENSE LOGISTICS AGENCY ENERGY Page 3 of 6

For samples containing synthetic components, include the following additional information:

Manufacturer of synthetic component Batch Number Date of Test Report Quantity of Tank/Batch Percent Composition Production Process of Synthetic Component Feedstock Full-Specification Test Report

f) TRACEABILITY:

1) F-76 fuel supplied under this contract shall maintain traceability with respect to additives and materials, which is defined as the ability to trace the individual batch of fuel back to the original point of manufacture through documentation.

2) All traceability documentation shall be sufficient to guarantee that at no point have any unauthorized materials or additives been blended into the final product or any of its associated blend components per section 3.2 Material of MIL-DTL-16884P.

3) For all F-76 supplied, the traceability documentation shall consist of statement(s) attesting to the materials composition, which includes materials derived from non-petroleum sources, additives and their concentration levels. Additives and concentrations to be reported include LIAs outlined in section d.1 above and any trace additives resulting from existing tank heels, product trail-back in a multiproduct system, all product blending operations, etc.

4) If F-76 is produced by means of blending, the traceability requirement and documentation for additives and materials shall apply to each blending component used from the point of manufacture through the blend operation. Materials composition, additives and their concentration levels shall be included. The requirement and intent of traceability for blend components is not to obtain full certificates of analysis of each individual blend component, but for certification that no unapproved additives or materials are present in blend components used.

5) The form titled: “F-76 Traceability Signature Page” (attached below) shall be used to document conformance with the provisions of this traceability paragraph. The offeror/supplier shall comply with this requirement utilizing one of the three options below and notification shall be provided to both the contracting office and QT@dla.mil during the pre-award phase which option was chosen for compliance. Documents provided in conjunction with individual shipments shall be uploaded into Wide Area Work Flow as attachments under the quality tab.

i) OPTION 1 – As part of the offeror submission package the offeror shall provide the traceability signature page from each entity in the supply chain providing and/or handling F-76 product and/or blending components all the way back to the point of manufacture. For each individual shipment, the supplier will submit a traceability page signed only by the awardee.

ii) OPTION 2 – As part of the offer submission package the offeror shall provide the traceability signature page, signed only by the offeror. Upon award and prior to the first shipment the awardee shall provide the signed traceability signature page from each entity in the supply chain providing and/or handling F-76 product and/or blending components all the way back to the point of manufacture. For each individual shipment, the supplier will submit a traceability page signed only by the awardee.

iii) OPTION 3 – As part of the offeror submission package, the offeror shall provide the traceability signature page, signed only by the offeror. For each individual shipment, the awardee shall provide the signed traceability signature page from each entity in the supply chain providing and/or handling F-76 product and/or blending components all the way back to the point of manufacture.

Regardless of the option chosen, the traceability sheet signed by offeror shall be submitted to both the contracting office and to QT@dla.mil during pre-award phase.

For OPTION 1 or OPTION 2, the purpose of the awardee submitting a signed traceability page with each shipment is to confirm that the initial traceability certification is still valid at the time of F-76 product shipment.

mailto:QT@dla.mil

DEFENSE LOGISTICS AGENCY ENERGY Page 4 of 6

6) If at any point during the contract period the traceability information provided under OPTION 1 or OPTION 2 becomes invalid (i.e.

the supply chain is altered or the source of F-76 product or a blending component changes), the supplier shall notify both the contracting office and QT@dla.mil and updated documentation shall be provided.

Signature

Prepared by:

Quality / Technical Directorate Approval:

Contracting Approval:

DEFENSE LOGISTICS AGENCY ENERGY Page 5 of 6

F-76 Traceability Signature Page

Contract or Solicitation Number:

CLIN:

Order Number:

Shipment Number:

Traceability OPTION selected per paragraph e.5 (circle or otherwise indicate which one of the three options is chosen):

OPTION 1 OPTION 2 OPTION 3

F-76 fuel supplied under the above contract, CLIN, order number and shipment number maintains traceability with respect the materials composition, additives and their concentration levels. This signed statement certifies that at no point have any unauthorized un- hydrotreated light cycle oils, other unauthorized materials, or additives been blended into the final product or any of its associated blend components per the most recent revision of MIL-DTL-16884 at date of contract award. All materials and additives are listed below. The percentage of each material as defined in sections 3.2, 3.2.2, and 3.2.3 (i.e. refined hydrocarbon distillate fuel, Fischer-Tropsch, Hydroprocessed Renewable Diesel, etc.) and the concentration level for each additive are also shown. For the purposes of the offeror submission this signed statement attests that no unapproved additives or materials will be added to batches or components of batches of F-76 for delivery under government contracts.

Signature:

Printed Name:

Title:

Company Name:

Date:

Material Percent

Additive Concentration Responsible Party for Injection

DEFENSE LOGISTICS AGENCY ENERGY Page 6 of 6

F-76 Synthetic Component Certification

Contract or Solicitation Number:

CLIN:

Order Number:

Shipment Number:

Synthetic paraffinic materials supplied as indicated with the above contract, CLIN, order number, and shipment number is derived from either Fischer-Tropsch (FT) or Hydroprocessed Renewable Diesel (HRD) methods. This signed statement certifies that since the last certificate of analysis (COA), including table A-II or B-II results of MIL-DTL-16884P, Appendix A or B, no changes, including feedstock material, production location, or production processes have been made. In addition, no turnaround events have been executed on any units utilized to produce the synthetic paraffinic materials since the last COA, including table A-II or B-II, properties were tested. Please supply the date of the most recent COA and an identifying number for that report in the space provided below.

DATE OF COA: _

LAB REPORT ID NUMBER

Signature:

Printed Name:

Title:

Company Name:

2022-08-10T12:41:46-0400

GRIECO.DAVID.FRANK.1385613233

2022-08-11T12:32:31-0400

BANISZEWSKI.DANIEL.J.1287388698

2022-08-17T15:47:37-0400

RALPH.ERIN.S.1229663042

PDF (DLA)DLA FORM 1889, OCT 2011

SUPPLEMENTAL QUALITY ASSURANCE PROVISION (SQAP)

SHEET 1 OF 2PREVIOUS EDITION IS USABLE Add Continuation Page

Print Form Email Form Clear Export Data Import Data About Check for Newer Version Contact Us

REV DESCRIPTION DATE APPROVED

NEW DLA ENERGY QAP E40.01

REVISIONS

QAP E40.01 MATERIAL INSPECTION AND RECEIVING REPORT (MIRR)/WIDE AREA WORKFLOW

(WAWF) ENERGY RECEIVING REPORT (ERR) (BULK FUEL/DIRECT DELIVERY AVIATION FUEL).

Required in all bulk fuel solicitations/contracts and direct delivery aviation fuel solicitations/contracts. DLA FORM 1889 dated .

QAP E40.01 MATERIAL INSPECTION AND RECEIVING REPORT (MIRR)/WIDE AREA WORKFLOW

(WAWF) ENERGY RECEIVING REPORT (ERR) (BULK FUEL/DIRECT DELIVERY AVIATION FUEL)

(DLA ENERGY JUL 2014)

(a) The requirements listed in paragraphs (b) and (c) are in addition to the other Wide Area Workflow (WAWF) requirements included in this contract. Whenever access to the WAWF system is limited or not available (i.e., during an extended loss of internet connectivity), the Contractor shall notify the Contracting Officer and request permission to submit documents manually until the WAWF system is again available for use. Manual documentation shall be completed in accordance with DFARS Appendix F.

(b) Test reports shall be entered into the WAWF system by means of the Statement of Quality tab.

Instructions for entering test information into the Statement of Quality Tab can be found in the WAWF Vendor Energy Receiving Report (ERR)/Combo Desktop Reference which can be downloaded at https://wawftraining.eb.mil/xhtml/ unauth/web/wbt/wawfra/vendor/VendorIndex.xhtml.

(c) Use the guidelines below for the submission of fuel quality testing data and supporting documentation for each ERR/Combo.

(1) MARINE SHIPMENTS. Submit a completed ERR/Combo and test reports via the Statement of Quality tab for all products shipped. If more than one shipping tank was used for the lift, a complete laboratory analysis for each shipping tank must be entered in the Statement of Quality tab. Also, clearly indicate the quantity of product shipped from each tank in the block titled “Quantity shipped from this tank”. Upload scanned copies, via the Attachments tab, of quantity determination documents and other shipping documents requested by the Quality Assurance Representative (QAR).

(2) PIPELINE SHIPMENTS. Submit a completed ERR/Combo and input the test results via the Statement of Quality tab for the total quantity of product shipped from each shipping tank used to fill the order. If more than one shipping tank was used for the shipment, a complete laboratory analysis for each shipping tank must be entered in the Statement of Quality tab. Also, clearly indicate the quantity of product shipped from each tank in the block titled “Quantity shipped from this tank”. Upload scanned copies, via the Attachments tab, of quantity determination documents and other shipping documents requested by the QAR.

(3) TRUCK, RAIL CAR AND INTERMODAL CONTAINER SHIPMENTS. When loading from source tank has finished for each shipment, submit a completed ERR/Combo and input test results via the Statement of Quality tab, for product received from that source tank. If only one shipment is made from a shipping tank, enter that quantity in the “Quantity shipped from this tank” block located on the Statement of Quality tab. If more than one shipment is made from the same shipping tank, the “Quantity shipped from this tank” block can either be left blank or be annotated with the quantity shipped during each individual shipment. Upload scanned copies, via the Attachments tab, of quantity determination documents and other shipping documents requested by the QAR.

DISTRIBUTION

STATEMENT - A

APPROVED FOR

PUBLIC RELEASE

DISTRIBUTION IS

"UNLIMITED"

DATE

07/08/2014

APPROVED BY

07/08/2014

REVIEWED BY

07/07/2014

PREPARED BY

DRAWING NUMBERSCALE

CODE ID NO.

52838

SIZE

NSN

MULTIPLE

ITEM

DLA ENERGY QAP E40.01

DLA Land & Maritime DLA Troop Support DLA Aviation clear

DEFENSE LOGISTICS AGENCY ENERGY

8725 JOHN J. KINGMAN RD

DLA Energy

SHEET 2 OF 2PREVIOUS EDITION IS USABLE Add Continuation Page

NEW DLA ENERGY QAP E40.01

THIS PAGE INTENTIONALLY LEFT BLANK

DISTRIBUTION STATEMENT - A

APPROVED FOR PUBLIC RELEASE

DISTRIBUTION IS "UNLIMITED"

SUPPLEMENTAL QUALITY ASSURANCE PROVISION

(SQAP)

DRAWING NUMBERSCALE CODE ID NO.

SIZE

8725 JOHN J. KINGMAN RD

PDF (DLA)

DLA FORM 1889, OCT 2011

SUPPLEMENTAL QUALITY ASSURANCE PROVISION (SQAP)

SHEET OF

PREVIOUS EDITION IS USABLE

REV

DESCRIPTION

DATE

APPROVED

REVISIONS

REV

DESCRIPTION

DATE

APPROVED

REVISIONS

DISTRIBUTION STATEMENT - A

APPROVED FOR PUBLIC RELEASE

DISTRIBUTION IS "UNLIMITED"

SUPPLEMENTAL QUALITY ASSURANCE PROVISION (SQAP)

Supplemental Quality Assurance Provision (SQAP)

DSCC Form 2291, Feb 2004 online none standard

Quality Assurance

DLA

1 +

No

Tech Qual Deskbook n/a

No

Supplemental Quality Assurance Provision (SQAP) interactive

October 2011 (added Energy; updated supply center names)

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rev: NEW description: DLA ENERGY QAP E40.01 revdate:

revapproved:

revcomments:

apprdate: 07/08/2014 apprBy:

reviewdate: 2014-07-08 revBy:

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totInstances: 1.00000000

C16.01 TURBINE FUEL, AVIATION (JP5) (DLA ENERGY DEC 2022)

NATIONAL STOCK NUMBER PRODUCT NOMENCLATURE DLA ENERGY PRODUCT

9130-00-273-2379 Turbine Fuel, Aviation, JP-5 JP5 9130-01-499-9521 Turbine Fuel, Aviation, JP-5 (Bunker fuel overseas locations only) JP5

Product shall meet MIL-DTL-5624W, Turbine Fuel, Aviation, Grade JP-5, dated March 28, 2016, revalidated December 31, 2020.

(a) SPECIFICATION MODIFICATION: The requirements of Table I in the specification are modified as follows:

a. FILTRATION TIME TESTING. Round upwards when reporting the filtration time, in minutes. For example, a filtration time of 4 minutes, 22 seconds, would be reported as 5 minutes.

b. FLASH POINT TESTING. The referee procedure for performing flash point testing of JP-5 shall be the manual method of the latest revision of ASTM D93, as opposed to the automated version of ASTM D93.

c. FLASH POINT.

i. All batches of JP-5 that are presented for Government acceptance at origin and for subsequent shipment through a multiproduct pipeline, shall meet a minimum flash point requirement of 62.5°C. This requirement is meant to address multiproduct commercial pipelines and does not apply to multiproduct systems within a facility.

ii. In the U.S. all JP-5 deliveries in California, Oregon, and Washington shall have a minimum Flash Point of 62.5 oC at the custody transfer point.

iii. In Australia all JP-5 deliveries shall have a minimum Flash Point of 61.5°C at the custody transfer point.

d. ACID NUMBER. For JP-5 delivered to Kodiak Island, Alaska, the maximum total acid number shall be 0.020 mg KOH/g.

e. MICRO-SEPAROMETER (MSEP) REQUIREMENTS.

i. Prior to initial production under this contract, the Contractor shall elect, on a one-time basis, which MSEP limit to meet for the balance of the contract. If the Contractor introduces Fuel System Icing Inhibitor (FSII) and/or Corrosion Inhibitor/Lubricity Improver (CI/LI) after verification of product conformance with the MSEP requirement, the product is not required to meet a fixed limit on subsequent MSEP tests.

ii. If the Contractor elects to verify conformance with the MSEP requirement on a sample of product that does not contain FSII and CI/LI, an additional MSEP test shall be performed on a hand blend containing jet fuel, FSII, CI/LI, and Antioxidant (only if required). The FSII shall be added to this hand blend at a concentration range between 0.08 volume percent minimum and 0.11 volume percent maximum. The amount of the CI/LI added to this hand blend shall be within the concentration range specified in QPL-25017.

f. ADDITIONAL REQUIREMENT APPLICABLE TO DEEP FREEZE PROGRAM ONLY. The Deep Freeze Program is for Antarctic operations of the Department of Defense and other federal agencies; whereby JP-5 sulfur content shall not exceed 0.0015 mass-percent (15 ppm).

(b) ADDITIVES.

a. Additives are required for deliveries of JP-5, per MIL-DTL-5624W, dated March 28, 2016, revalidated December 31, 2020, unless addition is excluded by specific solicitation line item, applicable contract clause, or another contractual requirement. FSII included in jet fuel shall conform to MIL-DTL- 85470B, Inhibitor, Icing, Fuel System, High Flash, Notice 1 dated June 15, 1999, and revalidated August 28, 2019.

b. The CI/LI additive(s) used shall conform to MIL-PRF-25017H Inhibitor, Corrosion/Lubricity Improver, Fuel Soluble, w/Amendment 1, dated August 4, 2011, and revalidated May 25, 2021,

c. Line injection of additives (FSII and CI/LI) from shipping tank to delivery conveyance or other free on board (FOB) point is permitted under the following conditions:

i. Additives must be proportionately injected throughout the entire loading process to ensure the additive is homogeneously blended into the jet fuel. The Contractor shall maintain records evidencing the homogeneous blending of all line injected additives. Such methods may include meter or tank gauge readings or test results taken at intervals to provide confidence in the injection process.

ii. When FSII is required, additive concentration must be verified based on a representative sample from each shipping conveyance.

(c) Conformance to specification requirements at the custody transfer point is required, however, prior to shipment, a laboratory hand blend of JP-5 fuel with all additives required by this contract shall be tested to verify compliance with the required specification (except for MSEP). MSEP analysis shall be performed per the Contractor’s election in MIL-DTL-5624W, dated March 28, 2016, and revalidated December 31, 2020.

(d) BATCH SAMPLING: The Contractor shall provide one 20 mL sample per each individual tank in a procurement batch.

For each 20 mL sample provided by the Contractor, the Contractor shall also submit a Refinery Certificate of Quality (RCQ), or Certificate of Analysis (CoA), as applicable, with the JP-5 sample when submitting to the US Naval Research Laboratory. The RCQ or CoA for each individual tank shall be representative of Level A testing for the JP-5 product.

NOTE: This sample is in addition to those required in accordance with Quality Assurance Provision (QAP) E1

QUANTITY OF SAMPLE WHEN SAMPLED SUBMISSION PERIOD

20 mL Upon completion of each individual

Shipped within 30 days of procurement batch delivery

“Batch” Definition in accordance with MIL-STD-3004-1A, 3.1.9: A specific quantity of product that is processed or utilized as a single unit and tested to meet test criteria and specifications.

The sample from each tank/batch shall be either an all-level sample or a composite of upper, middle, and lower samples. A copy of the batch’s full-specification test report shall accompany each sample. The sample container shall be any 20 mL amber borosilicate vial with a polytetrafluoroethylene (PTFE) lined screw cap. A tracking number for the samples shall be provided to: Thomas Loegel at thomas.loegel@nrl.navy.mil or (202) 767-1716. Samples shall be shipped to:

US Naval Research Laboratory ATTN: Thomas Loegel, Code 6181

JP-5 Component Analysis Library Project 4555 Overlook Ave., S.W.

Washington D.C. 20375-5320

The paperwork provided with these samples shall include the following information:

• Contract Number

• Contractor’s Name

• Product

• Refinery Location

• Quantity of Tank/Batch

• Full-Specification Test Report

For samples containing synthetic components, include the following additional information:

• Manufacturer of synthetic component

• Batch Number

• Date of Test Report

• Quantity of Tank/Batch

• Percent Composition

• Production Process of Synthetic Component

• Feedstock

• Full-Specification Test Report

Prepared by

Quality Technical Support Office Approval

Contracting Approval mailto:Robert.morris@nrl.navy.mil

C16.01 TURBINE FUEL, AVIATION (JP5) (DLA ENERGY DECJUL 2022APRIL 2018)

c. FLASH POINT.

e. MICRO-SEPAROMETER (MSEP) REQUIREMENTS.

(b) ADDITIVES.

NOTE: This sample is in addition to those required in accordance with Quality Assurance Provision (QAP) E1

2022-12-20T10:32:42-0500

RALPH.ERIN.S.1229663042

2022-12-22T13:27:12-0500

BANISZEWSKI.DANIEL.J.1287388698

2022-12-27T09:36:58-0500

MACLANE.SKYLLAR.BRYANNA.1252141827

DEFENSE LOGISTICS AGENCY ENERGY Page 1 of 1

Quality/Technical Support

Office Approval:

Contracting Approval:

C1.02 ASSIST DATABASE OF SPECIFICATIONS (DEC 2016)

Unless otherwise specified, current versions of defense or federal specifications and standards, military handbooks, commercial item descriptions, qualified product lists, and other related technical documents cited in this solicitation/contract can be accessed from the Department of Defense (DoD) Acquisition Streamlining and Standardization Information System

(ASSIST) database at https://assist.dla.mil under ASSIST-Quick Search or http://quicksearch.dla.mil. ASSIST is the official source for all Defense Standardization Program documents and contains the most current information on documents prepared by DoD, as well as information on how to acquire referenced non-Government standards that have been adopted for

DoD use. Note that commercial or foreign specifications are not located on ASSIST and must be obtained from the relevant sponsoring organization (e.g. ASTM, SAE, API, ISO, etc.). Registered ASSIST account holders may establish profiles to receive automatic E-mail alerts when changes are planned or made to documents of interest by selecting criteria on the [Alert

Portal Profile Maintenance] screens accessed from the [User Profile] menu. Users may also view or download a bi-monthly summary of changes to the ASSIST database under the [ASSIST Update] menu.

Basic instructions on how to use ASSIST:

1. Go to http://quicksearch.dla.mil/.

2. Type in the numeric portion of the specification or Qualified Product List (QPL) and click on the Search button.

3. Look through the search results to find the desired document and click on the Document ID.

a. For specifications: click on the .pdf link under Media.

b. For QPL information: click on the View Qualified Product Database (QPD) data link to open the QPD

i. Click on the link in the “Govt Designation” Column to view qualified products

1. To view qualified source plants, click on the Source Plants link under the Related Links column

2017-08-07T09:00:32-0400

TAYLOR.LORI.L.1391585080

2017-08-07T09:22:23-0400

SHEPHERD.SANDRA.S.1012568459

2017-11-20T09:19:52-0500

BANISZEWSKI.DANIEL.J.1287388698

STURGEON.STEVEN.A

LAN.JR.1009816565

Digitally signed by

STURGEON.STEVEN.ALAN.JR.1009816565

Date: 2022.03.28 15:50:06 -04'00'

MILLS.KEITH.10501831

MILLS.KEITH.1050183110

Date: 2022.03.28 15:34:49 -04'00'

HEIDBREDER.MICHAE

L.G.1139641082

HEIDBREDER.MICHAEL.G.1139641082

Date: 2022.03.28 15:27:41 -04'00'

(March 2022)

TABLE I, Sample Retention1

LOCATION MINIMUM QUANTITY RETENTION PERIOD 1

Bulk Tank Cars/Tank Truck/Intermodal Container

Additives 0.5-gallon (2 liters)2 Until receipt and quality verification of each lot/batch

Fuels 1 gallon (3 liters) 2 15 days for fuels/45 days for lubricating oils

Lubricating Oils 0.25 gallons (1 liter) 2

AVGAS Drums 0,25 gallons (1 liter) (multi-drum composite) 3 45 days

Shipping Tank(s)

2 gallons (8 liters) for Aviation Turbine Fuels 1 gallon (3 liters) for all other Fuels, Lubricating Oils, and Additives

45 days

Tanker/Barge/Pipeline (Composite Line at Custody Transfer Point)

2 gallon (8 liters) for Aviation Turbine

1 gallon (3 liters) for all other Fuels

Tanker/Barge (Composite)

F.O.B. Origin 2 gallons (8 liters) for Aviation Turbine

1 gallon (3 liters) for all other fuels

F.O.B. Destination 2 gallons (8 liters) Until shore tests on-specification Tanker/Barge (Each Compartment)

F.O.B. Origin 1 gallon (3 liters) 45 days F.O.B. Destination 1 gallon (3 liters) Until shore test on-specification

NOTES:

1. Unless otherwise noted in this document or applicable contract, the retention period shall be for the stated number of days after the sample has been taken from the location indicated.

2. If the conveyance is compartmentalized, a proportional sample shall be taken from each compartment such that a total of one liter is collected from the conveyance.

3. A one-liter composite sample of each product lot shall be taken from a predetermined number of randomly selected drums IAW Table III of API MPSM, Chapter 8.1 (ASTM D 4057).

TABLE II, Minimum Sampling and Testing Requirements for Petroleum Products Series 1, 1,13

ITEM WHEN TO SAMPLE LOCATION OF SAMPLE TYPE OF SAMPLE2 TEST REQUIRED3

1.a Prior to Loading

Before acceptance of new materiel and after establishment of new batch4

(Procurement) Each shore storage tank Single Tank Composite or All

Levels A

1.b Prior to loading (Government Stock) Each shore storage tank Single Tank Composites or All

Levels B-11, 5

1.c After line pack but prior to loading

(Procurement & Government Stock) As close to the custody transfer point as possible Line Sample C6,7 Dedicated System B-1 Non-Dedicated System

1.d In coordination with vessel crew (Procurement & Government Stock) Each vessel cargo compartment Manual method or onboard ship equipment Gauge or Ullage Report (Dry

Tanks) 1.e D uring Loading

After first in 9 (Procurement) Vessel cargo compartment(s) Spot C6,7,8 1.f After first in 9(Government Stock) Vessel cargo compartment(s) Spot Appearance and Density6,7,8

1.g After first in 9

(Replenishment at sea) Each vessel cargo compartment Spot C6,7,8

1.h During loading

As close to the custody transfer point as possible Line Sample Hourly Visual6,8, Retain10

Discard retain after passing 1.j tests

1.i

A fter Loading

After loading

Each vessel cargo compartment

All Level (Combine All Levels into one

Multiple Compartment Composite Sample)

C 6,11

Remainder of B-112

(Retain fuel for B-1 referee testing)

1. Additional requirements to include retain samples may be required. See Quality Assurance Provisions (C or E-QAP) for further details or DFSP QCP.

2. Refer to ASTM International D4057 for sampling procedures.

3. Test results shall be compared against the quality release certificate. Any discrepancies shall be identified, investigated, and resolved.

4. Upon procurement at refineries, blending installations, etc. and at main installations including national depots & ocean importing points on establishment of new batches.

5. Government-owned stocks previously tested at any type B level test within 90 days need only type C (test FSII & SDA if present).

6. Test for FSII and SDA only if line injected.

7. If sample fails appearance (see 5.11.4.3) perform particulate matter IAW 5.2.1.10.1. Maximum particulate IAW Table I.

8. Lubricity also required for F-76 only if line injected.

9. First in shall be done after one (1) meter or after line displacement whichever is the greater.

10. For all tanker, barge, and pipeline shipments, a flow-proportional sample taken in accordance with MPMS Chapter 8, Section 2, is preferred at the custody transfer point. However, manual samples taken in accordance with MPMS Chapter 8, Section 1 are acceptable if they are taken hourly throughout the shipment and that the quantity of the composite sample meets the requirements in QAP E-1. For Government Shipments, pull a 1-quart sample hourly and retain until passing of 1.j B-1 tests.

11. Vessel may sail after “C” Tests; Remainder of B-1 tests to be completed before arrival at next load or discharge port. Test report will be provided to designated discharge port.

12. Type A level testing required for FOB Destination Procurements (unless otherwise specified by contract).

13. If a YON is being used as a barge, the QA requirements for waterborne transfer of petroleum products must be observed.

Series 2, 1,8

ITEM WHEN TO SAMPLE LOCATION OF SAMPLE TYPE OF SAMPLE 2 TEST REQUIRED3

2.a

Prior to Shipm ent

Before acceptance of new materiel and after establishment of new batch4

(Procurement) Each Shipment Storage Tank Single Tank Composite or All Levels A10

2.b Prior to shipment (Government Stock) Each Shipment Storage Tank Single Tank Composite or All Levels B-15

2.c After line pack but prior to loading/shipment

As close to the custody transfer point as possible Line Sample C6,7 Dedicated System

B-1 Non-Dedicated System

2.d

D uring Shipm ent

Immediately after start of loading/shipment

Downstream of the filter separator (if equipped) or closest to the custody transfer point as possible Line Sample C6

2.e Hourly after start of loading or shipment

Pipeline Only point as possible Line Sample

Apperance6

(Retain fuel for B-1 referee testing)

2.f

Daily on first fill and anytime a new tank is placed on issue (after line displacement) TT, TC, ISO, Refuelers or other over the road transportation modes only point as possible (Loading Rack or Fill Point)

Line Sample Color (by visual method) and Appearance6.

If visual fails perform C7

2.g fter Loading

Daily for each conveyance mode *Not required for pipeline operations

Each Cargo Compartment or another point that provides a representative sample All Level

Appearance on each compartment

C on composite 6,7,9

1. Additional contractual requirements to include retain samples may be required. See Contract Quality Assurance Plans (C or E-QAPs) for further details

2. Refer to ASTM International D4057 for sampling procedures.

3. Test results shall be compared against the quality release certificate. Any discrepancies shall be identified, investigated, and resolved.

4. Upon procurement at refineries, blending installations, etc., and at main installations including national depots & ocean importing points on establishment of new batches.

5. Government-owned stocks that have been tested previously at any type B level test within 90 days need only type C (test FSII & SDA if present. Test for lubricity for F-76 when LIA is injected outbound only).

6. Test for FSII and SDA only if line injected.

7. If sample fails appearance (see 5.11.4.3), perform particulate matter IAW ¶ 5.2.1.10.1. Maximum particulate IAW IGRL

8. Type A level testing required for FOB Destination Procurements (unless otherwise specified by contract).

9. Road tank truck vehicles with multiple compartments shall have a 1-quart representative sample obtained from each compartment.

10. Filtration time testing is required for JP-4, JP-5 & JP-8 and shall meet MIL-STD-3004-1 Table I or contract requirement, whichever is more stringent.

Series 3, product receipt and discharges for tankers and barges6, 7, 8, 10

ITEM WHEN TO SAMPLE LOCATION OF SAMPLE TYPE OF SAMPLE TEST REQUIRED

3.a

Prior to D ischarge

Prior to discharge (Multi Product Cargo)

From each vessel cargo compartment All Level Appearance and Density1,2

3.b From each vessel cargo compartment

(Combine All Levels into one

B-13

3.c (Single Product Cargo) (Procurement & Government Stock) From each vessel cargo compartment

(Combine All Levels into one

C4,5

3.d D uring

Within 30 minutes after start and each hour after until completion

Dock/Discharge Manifold Header Line Sample / Retain

Perform Appearance test5,9 and then retain fuel for

Referee testing

3.e At 1 hour after start, Midpoint and 1 hour prior to completion

Dock/Discharge Manifold Header Line Sample Particulate (if applicable)

3.f A fter

After receipt by waterborne vessel (Procurement & Government Stock) Receipt tank All Level B-1

3.g If remainder of fuel will be shipped to another DFSP

Each vessel compartment with fuel remaining on board All Level Retain until discharged at next destination

1. Test for flash point on high flash cargo tanks if low and high flash cargoes are carried together aboard the same vessel without segregated venting systems

2. If on-spec, discharge is authorized.

3. It is preferred that B-1 testing is completed before discharge. In the event capabilities do not exist or time does not allow, the vessel can be discharged once appearance and density testing is completed on each compartment per Table IX 3.a, and C5 testing on the volumetric composite in 3.b. If B-1 testing is not completed prior to discharge, volumetric composite for 3b. shall be retained until receiving tank testing passes. Once discharging is completed, a B-1 test will be performed on the receiving tanks per Table IX 3.i. If receiving tank fails, a B-1 will be performed on retained fuel.

4. Discharge is authorized after conformance with type C tests, and the provisions of Section 5.1.3.1 are met. Retain composite sample until the receiving tank analysis is complete. If product fails, perform B-1 tests on retain composite to help determine the cause of the off-specification problem.

5. For aviation fuel delivery, FSII and SDA shall be tested only if line injected. This requires an additional quart sample.

6. Refer to ASTM International D4057 for sampling procedures.

7. Flash Point at the receiving point is not required for product used by the U.S. Army. This fuel is tested IAW Petroleum Laboratory Operations (TM 4-43.31)

8. Type A level testing required for FOB Destination Procurements (unless otherwise specified by contract).

9. Test for additives if line injected downstream of the injector. (If line injecting LIA into F-76, test for lubricity.)

10. If a YON is being used as a barge, the QA requirements for waterborne transfer of petroleum products must be observed.

TABLE III, Tests required aviation gasoline3

PROPERTIES B-1 TEST B-2 TEST B-3 TEST C TEST

Appearance 1,2 X X X X

Color (Visual) X X X X Density or API gravity X X X X Distillation X X X Copper strip corrosion X X X Existent gum X X Vapor pressure X X Free water determination2 X X X Lead content X X Potential gum X Color (Saybolt)

Freeze Point

Knock Value Total Sulfur Oxidation Stability

1. Obtain sample in a clear round 1 quart glass bottle, swirl the bottle vigorously so a vortex is formed. Visually check for sediment at the point of the vortex. If sediment is visible, an investigation is necessary in order to determine the source of the contaminant (a spot larger than 3 mm diameter indicates corrective action may be required to prevent the delivery of contaminated fuel).

2. AVGAS samples shall be checked for particulate and water. Particulate shall be determined visually upstream of filter separators and/or by the particle assessment method downstream of the filter separator. Free water shall be determined downstream of filter separator using a water detector (AEL Aqua-Glo test method or Hydro-Light).

3. For determining correct testing results (rounding protocol) see 4.2.2.2.1 Testing Rounding Protocol

TABLE IV, Tests required for aviation turbine 7

Appearance 1 X X X X Color (visual) X X X X Density or API gravity X X X X Particulate matter X X X Distillation X X X Copper strip corrosion X X X Freezing point X X X Existent gum X X X Vapor pressure (JP-4 only) X X X Flash point (except JP-4) 11 X X X X Water reaction2 Lead content (If contaminated with leaded fuels suspected)

X X X

Fuel system icing inhibitor 3 X X X Filtration time X X X

MSEP (JP-4, JP-8, F-24, F-27, Jet A & Jet A-1) 4,5

Conductivity (JP-4 and JP-8, F-24, F-27 & Jet A-1) 6

Thermal stability (B-1 requirement applies only to JPTS and marine/multi-product mode receipt tank sample)10

X X

Color (Saybolt) X

Acid number X

Peroxide Number 8 X

Fatty Acid Methyl Ester (FAME) 9 X X X

1. Obtain sample in a clear round 1 quart glass bottle, swirl the bottle vigorously so a vortex is formed. Visually check for sediment at the point of the vortex. If sediment is visible, an investigation is necessary to determine the source of the contaminant (a spot larger than 3 mm diameter indicates corrective action may be required to prevent the delivery of contaminated fuel).

2. Optional or at the request of Service Control Point.

3. If product contains FSII, product shall be checked on delivery into a bulk storage tank and every month thereafter.

4. If the capability does not exist to perform this test at the terminal, send sample to the nearest Service laboratory that has capability. In the event operational necessity dictates issue of product before results are obtained from the Service laboratory, shipments may be made, however, when laboratory results indicate failure, notify DLA Energy Quality Operations Division.

5. In all cases where MSEP is measured, conductivity will also be measured using ASTM D2624. For unadditized Jet A that is injected outbound of a facility an MSEP shall be performed using either D7224 or D8073 where possible. If either method is not available testing may be conducted with D3948. Passing results for D3948 will be considered acceptable. Failing fuels shall be retested using D7224 or D8073. If the fuel passes D7224 with a minimum limit of 85 or D8073 with a limit of 88 the fuel is considered to be acceptable with no further action. If the fuel fails D7224 or D8073, an investigation shall be performed.

6. If fuel contains conductivity additive, wait approximately 2 minutes after obtaining sample for charges in the fuel to dissipate before performing CU testing.

7. For determining correct reporting of test results (rounding protocol) see 4.2.2.2.1 Testing Rounding Protocol

8. Only applicable to Jet A use by the Navy.

9. Only for product transported through multi-product systems, including marine transport.

10. For JPTS: Ellipsometer (ETR) or Interferometer (ITR) IAW QAP C16.08-13. ETR is the referee. For all other fuels, follow specification requirements (excluding MSC chartered/contracted tankers and barges in dedicated/long term service).

11. Flash Point at the receiving point is not required for product used by the U.S. Army. This fuel is tested in accordance with Petroleum Laboratory Operations (TM 4-43.31).

TABLE V, Support for secure fuel 4

JP-5 Jet A Jet A-1 7 JP-8 F-24 Min. Max. Min. Max. Min. Max. Min. Max. Min. Max.

Appearance 2 C&B C&B C&B C&B C&B C&B C&B C&B C&B C&B

Gravity, API @ 60 °F D1298/D4052 36.0 48.0 37.0 51.0 37.0 51.0 37.0 51.0 37.0 51.0

Density at 15°C (kg/m3) 788 845 775 840 775 840 775 840 775 840 Weight: lb/USG Calculated 6.6 7.0 6.5 7.0 6.5 7.0 6.5 7.0 6.5 7.0 Distillation (°C) D86 3

10% Recovered 205 205 205 205 205 20% Recovered Report Report 50% Recovered Report Report Report Report Report 90% Recovered Report Report Report Report Report Final Boiling Point 300 300 300 300 300 Freezing point, °C D5972/D2386

-46

-40

-47

-47

-40

Flash point, °C D93/D56 60 38 38 38 38

Particulate Matter (mg/L) D2276, D5452, MIL- DTL- 83133

0.5

Conductivity (pS/m) D2624 Report Report 50 700 50 700 Copper strip corrosion D130 No.1 No.1 No.1 No.1 No.1 Existent gum (mg/100 mL) D381 7 7 7 7 7 FSII, (vol %) D5006 1 0.07 0.20 0.04 0.15 0.04 0.15 Thermal Stability D3241

Change in pressure drop, mm Hg 25 25 25 25 25 One of the tube deposit rating methods shall be run:

(1) Ellipsometer (ETR) 6 (nm) or Interferometer (ITR) (nm)

(2) Heater tube deposit, Visual Tube Rating

(VTR)

< 3

< 3 < 3 < 3 < 3

Fatty Acid Methyl Ester (FAME) 5

1. Only use FSII meeting specification MIL-DTL-85470, Inhibitor, Icing, Fuel System, High Flash, NATO Code S-1745.

2. Fuel shall be clear, bright, and free of water and sediment on visual examination. Sample will be taken downstream of final filtration on refueler or hydrant servicing equipment.

3. Distillation property criteria are specified in ASTM D86 scale units. ASTM D2887 results shall be converted to estimated D86 results by application of the correlation in Appendix X4, “Correlation for Jet and Diesel Fuel (Procedures A and B)” of D2887 for comparison with the specified property criteria. Distillation residue and loss limits provide control of the distillation process during the D86 test method and do not apply to D2887.

4. Alternate test methods may be performed provided they are authorized by the specification of the product being tested. Referee test methods are preferred.

5. Only for product transported through multi-product systems. FAME (fatty acid methyl esters) is defined as material meeting the limits of EN14214 or ASTM D6751. FAME that fails to meet the biodiesel quality standards are not permitted in aviation turbine fuel.

6. Tube deposit rating shall be measured by ASTM D3241 ETR Ellipsometer (ETR), when available: otherwise, use Interferometer (ITR) or visual (VTR). ETR shall be the referee procedure, otherwise ITR.

7. DEF STAN 91-091, ASTM D1655 and GOST R 52050 are acceptable.

TABLE VI, Tests required for automotive gasoline

Appearance X X X X Color (Visual) X X X X Water and Particulate (Visual Check) X X X X Density or API gravity X X X X Distillation X X X

Vapor pressure X X

Copper strip corrosion X X Unwashed gum/Solvent-washed gum X X 1 Knock rating (RON and MON) X 2 X 2 Oxidation stability X

1. Unwashed gum, without solvent wash, shall not increase by more than 2 mg as compared to the original product. In the event of gum increase exceeding 2 mg, run type A test as defined in the legend.

2. Perform only if Lead Content is performed and fails and/or contamination with another product is suspected. In the case of pipeline, this test shall be performed when considered necessary.

TABLE VII, Tests required for E85 (ASTM D5798) 1, 2

Appearance X X X X Water X X X Ethanol Volume X X X

Vapor Pressure X X X

Sulfur X X Acidity X Solvent Washed Gum X X pH X Unwashed Gum X Copper X X

1. For cleaning see 5.9.4.2

2. In accordance with DOE Handbook for Handling, Storing and Dispensing E85 and Other Ethanol- Gasoline Blends, it is recommended at a minimum to test the following every one to two months: electrical conductivity, particulate content, hydrocarbon content (D5501 with D5798), water content and RVP. The DOE Guidebook link is https://www.afdc.energy.gov/uploads/publication/ethanol_handbook.pdf (May need to save file vs open document) https://www.afdc.energy.gov/uploads/publication/ethanol_handbook.pdf

TABLE VIII, Tests required for diesel fuels and kerosene

Appearance 1 X X X X Color (Visual) X X X X Density X X X X Distillation X X

Flash point X X X X Carbon residue (F-76 only) X X Cloud point X Pour point (F-76 only) X Copper strip corrosion X

Cetane index 2 X Viscosity (F-76 only) X Water & sediment by centrifuge X

Particulate (F-76 only) X X Storage stability (F-76 only) X Sulfur 3, 4 X X

Fatty Acid Methyl Ester (FAME) (F-76 only) X X

Lubricity (F-76 only) X X

1. For NATO F-76, if the sample has no visible particulates, but is otherwise not clear and bright per ASTM D4176, procedure 1, then the product shall meet the requirements of ASTM D2709, 0.05 percent volume of water and sediment, maximum. The fuel is acceptable for appearance if the water and sediment content is

0.05 percent volume or less. If the sample fails ASTM D4176, procedure 1, because it…