App VI RI Report - Part 2.pdf

Chuck’s Corner

Facility ID No. 00006430

Remedial Investigation Report

EnviroSolutions, Inc. June 2016

APPENDIX E

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

MDEQ-RRD-CADILLAC

RE: CHUCK'S CORNERS. OSCEOLA COUNTY

Cadillac, MI 49601-2158

120 W. Chapin Street

Ann Emington

I certify that the analyses performed by the MDEQ Environmental Laboratory were conducted by methods approved by the U.S. Environmental Protection Agency and other appropriate regulatory agencies .

Sincerely, 15 September 2015 Work Order: 1508239

Price: $360.00

George Krisztian

Laboratory Director

Lab Work Order # 1508239

Page 1 of 7Page 1 of 7

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

Project:

Project Manager:

Reported:

MDEQ-RRD-CADILLAC

120 W. Chapin Street

Ann Emington

CHUCK'S CORNERS. OSCEOLA COUNTY

Cadillac MI, 49601-2158

Site Code: 67000151 09/15/2015

Sample ID Laboratory ID Date SampledMatrix Date Received

Analytical Report for Samples

Qualifier

1508239-01 Air 08/28/2015Sub Slab #1 (SE) 08/26/2015

1508239-02 Air 08/28/2015Sub Slab #2 (NW) 08/26/2015

Notes and Definitions

Y11 Unidentified peaks present in sample.

T Reported value is less than the reporting limit (RL). Result is estimated.

A05 Result and reporting limit are estimated due to low continuing calibration standard criteria failure.

Reporting LimitRL

Indicates compound analyzed for but not detectedND

Not ApplicableNA

Page 2 of 7Page 2 of 7

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1508239-01

RLCAS #

Client ID: Sub Slab #1 (SE)

QC Batch

Organics-Volatiles See note Y11

1.6 ug/m3 1 TO-151,1,1-Trichloroethane71-55-6 09/11/15ND B5I1411

2.0 ug/m3 1 TO-151,1,2,2-Tetrachloroethane79-34-5 09/11/15ND B5I1411

2.3 ug/m3 1 TO-151,1,2-Trichloro-1,2,2-trifluoroethane76-13-1 09/11/15ND B5I1411

1.6 ug/m3 1 TO-151,1,2-Trichloroethane79-00-5 09/11/15ND B5I1411

1.2 ug/m3 1 TO-151,1-Dichloroethane75-34-3 09/11/15ND B5I1411

1.2 ug/m3 1 TO-151,1-Dichloroethylene75-35-4 09/11/15ND B5I1411

2.2 ug/m3 1 TO-151,2,4-Trichlorobenzene120-82-1 09/11/15ND B5I1411

1.4 ug/m3 1 TO-151,2,4-Trimethylbenzene95-63-6 09/11/1520 B5I1411

2.3 ug/m3 1 TO-151,2-Dibromoethane106-93-4 09/11/15ND B5I1411

2.1 ug/m3 1 TO-151,2-Dichloro-1,1,2,2-Tetrafluoroethane76-14-2 09/11/15ND B5I1411

1.8 ug/m3 1 TO-151,2-Dichlorobenzene95-50-1 09/11/15ND B5I1411

1.2 ug/m3 1 TO-151,2-Dichloroethane107-06-2 09/11/15ND B5I1411

1.4 ug/m3 1 TO-151,2-Dichloropropane78-87-5 09/11/15ND B5I1411

1.4 ug/m3 1 TO-151,3,5-Trimethylbenzene108-67-8 09/11/155.9 B5I1411

0.65 ug/m3 1 TO-151,3-Butadiene106-99-0 09/11/15ND B5I1411

1.8 ug/m3 1 TO-151,3-Dichlorobenzene541-73-1 09/11/15ND B5I1411

1.8 ug/m3 1 TO-151,4-Dichlorobenzene106-46-7 09/11/15ND B5I1411

1.4 ug/m3 1 TO-152,2,4-Trimethylpentane540-84-1 09/11/1513 B5I1411

14 ug/m3 1 TO-152-Butanone (MEK)78-93-3 09/11/15ND B5I1411

1.1 ug/m3 1 TO-152-Chloro-1,3-butadiene126-99-8 09/11/15ND B5I1411

4.0 ug/m3 1 TO-154-Methyl-2-pentanone (MIBK)108-10-1 09/11/15ND B5I1411

1.6 A05ug/m3 1 TO-15Acetonitrile75-05-8 09/11/15ND B5I1411

1.1 ug/m3 1 TO-15Acrylonitrile107-13-1 09/11/15ND B5I1411

0.94 ug/m3 1 TO-15Benzene71-43-2 09/11/1515 B5I1411

2.0 ug/m3 1 TO-15Bromodichloromethane75-27-4 09/11/15ND B5I1411

3.0 ug/m3 1 TO-15Bromoform75-25-2 09/11/15ND B5I1411

1.1 ug/m3 1 TO-15Bromomethane74-83-9 09/11/15ND B5I1411

1.9 ug/m3 1 TO-15Carbon tetrachloride56-23-5 09/11/15ND B5I1411

1.4 ug/m3 1 TO-15Chlorobenzene108-90-7 09/11/15ND B5I1411

0.78 ug/m3 1 TO-15Chloroethane75-00-3 09/11/15ND B5I1411

1.4 ug/m3 1 TO-15Chloroform67-66-3 09/11/1584 B5I1411

0.61 ug/m3 1 TO-15Chloromethane74-87-3 09/11/150.86 B5I1411

1.2 ug/m3 1 TO-15cis-1,2-Dichloroethylene156-59-2 09/11/15ND B5I1411

1.3 ug/m3 1 TO-15cis-1,3-Dichloropropylene10061-01-5 09/11/15ND B5I1411

2.5 ug/m3 1 TO-15Dibromochloromethane124-48-1 09/11/15ND B5I1411

1.5 ug/m3 1 TO-15Dichlorodifluoromethane75-71-8 09/11/153.9 B5I1411

1.3 ug/m3 1 TO-15Ethylbenzene100-41-4 09/11/156.2 B5I1411

3.1 ug/m3 1 TO-15Hexachlorobutadiene87-68-3 09/11/15ND B5I1411

3.5 ug/m3 1 TO-15Hexane110-54-3 09/11/15ND B5I1411

1.3 ug/m3 1 TO-15m & p - Xylene1330-20-7 09/11/1525 B5I1411

Page 3 of 7Page 3 of 7

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1508239-01

RLCAS #

Client ID: Sub Slab #1 (SE)

QC Batch

Organics-Volatiles See note Y11

1.0 ug/m3 1 TO-15Methylene chloride75-09-2 09/11/1510 B5I1411

1.8 ug/m3 1 TO-15Methyltertiarybutylether1634-04-4 09/11/15ND B5I1411

1.3 ug/m3 1 TO-15o-Xylene95-47-6 09/11/159.5 B5I1411

1.3 ug/m3 1 TO-15Styrene100-42-5 09/11/15ND B5I1411

2.0 ug/m3 1 TO-15Tetrachloroethylene127-18-4 09/11/1536 B5I1411

1.1 ug/m3 1 TO-15Toluene108-88-3 09/11/1552 B5I1411

1.2 ug/m3 1 TO-15trans-1,2-Dichloroethylene156-60-5 09/11/15ND B5I1411

1.3 ug/m3 1 TO-15trans-1,3-Dichloropropylene10061-02-6 09/11/15ND B5I1411

1.6 ug/m3 1 TO-15Trichloroethylene79-01-6 09/11/15ND B5I1411

1.7 ug/m3 1 TO-15Trichlorofluoromethane75-69-4 09/11/152.0 B5I1411

0.75 ug/m3 1 TO-15Vinyl chloride75-01-4 09/11/15ND B5I1411

Page 4 of 7Page 4 of 7

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1508239-02

RLCAS #

Client ID: Sub Slab #2 (NW)

QC Batch

Organics-Volatiles See note Y11

1.6 ug/m3 1 TO-151,1,1-Trichloroethane71-55-6 09/11/15ND B5I1411

2.0 ug/m3 1 TO-151,1,2,2-Tetrachloroethane79-34-5 09/11/15ND B5I1411

2.3 ug/m3 1 TO-151,1,2-Trichloro-1,2,2-trifluoroethane76-13-1 09/11/15ND B5I1411

1.6 ug/m3 1 TO-151,1,2-Trichloroethane79-00-5 09/11/15ND B5I1411

1.2 ug/m3 1 TO-151,1-Dichloroethane75-34-3 09/11/15ND B5I1411

1.2 ug/m3 1 TO-151,1-Dichloroethylene75-35-4 09/11/15ND B5I1411

2.2 ug/m3 1 TO-151,2,4-Trichlorobenzene120-82-1 09/11/15ND B5I1411

1.4 ug/m3 1 TO-151,2,4-Trimethylbenzene95-63-6 09/11/157.2 B5I1411

2.3 ug/m3 1 TO-151,2-Dibromoethane106-93-4 09/11/15ND B5I1411

2.1 ug/m3 1 TO-151,2-Dichloro-1,1,2,2-Tetrafluoroethane76-14-2 09/11/15ND B5I1411

1.8 ug/m3 1 TO-151,2-Dichlorobenzene95-50-1 09/11/15ND B5I1411

1.2 ug/m3 1 TO-151,2-Dichloroethane107-06-2 09/11/15ND B5I1411

1.4 ug/m3 1 TO-151,2-Dichloropropane78-87-5 09/11/15ND B5I1411

1.4 ug/m3 1 TO-151,3,5-Trimethylbenzene108-67-8 09/11/151.9 B5I1411

0.65 ug/m3 1 TO-151,3-Butadiene106-99-0 09/11/15ND B5I1411

1.8 ug/m3 1 TO-151,3-Dichlorobenzene541-73-1 09/11/15ND B5I1411

1.8 ug/m3 1 TO-151,4-Dichlorobenzene106-46-7 09/11/15ND B5I1411

1.4 Tug/m3 1 TO-152,2,4-Trimethylpentane540-84-1 09/11/151.2 B5I1411

14 ug/m3 1 TO-152-Butanone (MEK)78-93-3 09/11/15ND B5I1411

1.1 ug/m3 1 TO-152-Chloro-1,3-butadiene126-99-8 09/11/15ND B5I1411

4.0 ug/m3 1 TO-154-Methyl-2-pentanone (MIBK)108-10-1 09/11/15ND B5I1411

1.6 A05ug/m3 1 TO-15Acetonitrile75-05-8 09/11/15ND B5I1411

1.1 ug/m3 1 TO-15Acrylonitrile107-13-1 09/11/15ND B5I1411

0.94 ug/m3 1 TO-15Benzene71-43-2 09/11/152.0 B5I1411

2.0 ug/m3 1 TO-15Bromodichloromethane75-27-4 09/11/15ND B5I1411

3.0 ug/m3 1 TO-15Bromoform75-25-2 09/11/15ND B5I1411

1.1 ug/m3 1 TO-15Bromomethane74-83-9 09/11/15ND B5I1411

1.9 ug/m3 1 TO-15Carbon tetrachloride56-23-5 09/11/15ND B5I1411

1.4 ug/m3 1 TO-15Chlorobenzene108-90-7 09/11/15ND B5I1411

0.78 ug/m3 1 TO-15Chloroethane75-00-3 09/11/15ND B5I1411

1.4 ug/m3 1 TO-15Chloroform67-66-3 09/11/15160 B5I1411

0.61 ug/m3 1 TO-15Chloromethane74-87-3 09/11/150.93 B5I1411

1.2 ug/m3 1 TO-15cis-1,2-Dichloroethylene156-59-2 09/11/15ND B5I1411

1.3 ug/m3 1 TO-15cis-1,3-Dichloropropylene10061-01-5 09/11/15ND B5I1411

2.5 ug/m3 1 TO-15Dibromochloromethane124-48-1 09/11/15ND B5I1411

1.5 ug/m3 1 TO-15Dichlorodifluoromethane75-71-8 09/11/156.1 B5I1411

1.3 ug/m3 1 TO-15Ethylbenzene100-41-4 09/11/152.3 B5I1411

3.1 ug/m3 1 TO-15Hexachlorobutadiene87-68-3 09/11/15ND B5I1411

3.5 ug/m3 1 TO-15Hexane110-54-3 09/11/15ND B5I1411

1.3 ug/m3 1 TO-15m & p - Xylene1330-20-7 09/11/1513 B5I1411

Page 5 of 7Page 5 of 7

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1508239-02

RLCAS #

Client ID: Sub Slab #2 (NW)

QC Batch

Organics-Volatiles See note Y11

1.0 ug/m3 1 TO-15Methylene chloride75-09-2 09/11/152.2 B5I1411

1.8 ug/m3 1 TO-15Methyltertiarybutylether1634-04-4 09/11/15ND B5I1411

1.3 ug/m3 1 TO-15o-Xylene95-47-6 09/11/153.4 B5I1411

1.3 ug/m3 1 TO-15Styrene100-42-5 09/11/15ND B5I1411

2.0 ug/m3 1 TO-15Tetrachloroethylene127-18-4 09/11/1557 B5I1411

1.1 ug/m3 1 TO-15Toluene108-88-3 09/11/1516 B5I1411

1.2 ug/m3 1 TO-15trans-1,2-Dichloroethylene156-60-5 09/11/15ND B5I1411

1.3 ug/m3 1 TO-15trans-1,3-Dichloropropylene10061-02-6 09/11/15ND B5I1411

1.6 ug/m3 1 TO-15Trichloroethylene79-01-6 09/11/15ND B5I1411

1.7 ug/m3 1 TO-15Trichlorofluoromethane75-69-4 09/11/152.2 B5I1411

0.75 ug/m3 1 TO-15Vinyl chloride75-01-4 09/11/15ND B5I1411

Page 6 of 7Page 6 of 7

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

MDEQ-RRD-CADILLAC

RE: CHUCK'S CORNERS. OSCEOLA COUNTY

Cadillac, MI 49601-2158

120 W. Chapin Street

Ann Emington

I certify that the analyses performed by the MDEQ Environmental Laboratory were conducted by methods approved by the U.S. Environmental Protection Agency and other appropriate regulatory agencies .

Sincerely, 25 May 2016 Work Order: 1605126

Price: $360.00

George Krisztian

Laboratory Director

Lab Work Order # 1605126

Page 1 of 7Page 1 of 7

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

Project:

Project Manager:

Reported:

MDEQ-RRD-CADILLAC

120 W. Chapin Street

Ann Emington

CHUCK'S CORNERS. OSCEOLA COUNTY

Cadillac MI, 49601-2158

Site Code: 67000151 05/25/2016

Sample ID Laboratory ID Date SampledMatrix Date Received

Analytical Report for Samples

Qualifier

1605126-01 Air 05/12/2016SS-1 05/11/2016

1605126-02 Air 05/12/2016SS-2 05/11/2016

Notes and Definitions

A10 Result and reporting limit are estimated due to low initial verification standard criteria failure.

Reporting LimitRL

Indicates compound analyzed for but not detectedND

Not ApplicableNA

Page 2 of 7Page 2 of 7

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1605126-01

RLCAS #

Client ID: SS-1

QC Batch

Organics-Volatiles

16 ug/m3 10 TO-151,1,1-Trichloroethane71-55-6 05/14/16ND B6E1712

20 ug/m3 10 TO-151,1,2,2-Tetrachloroethane79-34-5 05/14/16ND B6E1712

23 ug/m3 10 TO-151,1,2-Trichloro-1,2,2-trifluoroethane76-13-1 05/14/16ND B6E1712

16 ug/m3 10 TO-151,1,2-Trichloroethane79-00-5 05/14/16ND B6E1712

12 ug/m3 10 TO-151,1-Dichloroethane75-34-3 05/14/16ND B6E1712

12 ug/m3 10 TO-151,1-Dichloroethylene75-35-4 05/14/16ND B6E1712

22 ug/m3 10 TO-151,2,4-Trichlorobenzene120-82-1 05/14/16ND B6E1712

15 ug/m3 10 TO-151,2,4-Trimethylbenzene95-63-6 05/14/1632 B6E1712

23 ug/m3 10 TO-151,2-Dibromoethane106-93-4 05/14/16ND B6E1712

21 ug/m3 10 TO-151,2-Dichloro-1,1,2,2-Tetrafluoroethane76-14-2 05/14/16ND B6E1712

18 ug/m3 10 TO-151,2-Dichlorobenzene95-50-1 05/14/16ND B6E1712

12 ug/m3 10 TO-151,2-Dichloroethane107-06-2 05/14/16ND B6E1712

14 ug/m3 10 TO-151,2-Dichloropropane78-87-5 05/14/16ND B6E1712

15 ug/m3 10 TO-151,3,5-Trimethylbenzene108-67-8 05/14/16ND B6E1712

6.5 ug/m3 10 TO-151,3-Butadiene106-99-0 05/14/16ND B6E1712

18 ug/m3 10 TO-151,3-Dichlorobenzene541-73-1 05/14/16ND B6E1712

18 ug/m3 10 TO-151,4-Dichlorobenzene106-46-7 05/14/16ND B6E1712

14 ug/m3 10 TO-152,2,4-Trimethylpentane540-84-1 05/14/16300 B6E1712

150 ug/m3 10 TO-152-Butanone (MEK)78-93-3 05/14/16ND B6E1712

11 ug/m3 10 TO-152-Chloro-1,3-butadiene126-99-8 05/14/16ND B6E1712

40 ug/m3 10 TO-154-Methyl-2-pentanone (MIBK)108-10-1 05/14/16ND B6E1712

17 A10ug/m3 10 TO-15Acetonitrile75-05-8 05/14/16ND B6E1712

11 ug/m3 10 TO-15Acrylonitrile107-13-1 05/14/16ND B6E1712

9.4 ug/m3 10 TO-15Benzene71-43-2 05/14/1615 B6E1712

20 ug/m3 10 TO-15Bromodichloromethane75-27-4 05/14/16ND B6E1712

31 ug/m3 10 TO-15Bromoform75-25-2 05/14/16ND B6E1712

11 ug/m3 10 TO-15Bromomethane74-83-9 05/14/16ND B6E1712

19 ug/m3 10 TO-15Carbon tetrachloride56-23-5 05/14/16ND B6E1712

14 ug/m3 10 TO-15Chlorobenzene108-90-7 05/14/16ND B6E1712

7.8 ug/m3 10 TO-15Chloroethane75-00-3 05/14/16ND B6E1712

14 ug/m3 10 TO-15Chloroform67-66-3 05/14/16ND B6E1712

6.1 ug/m3 10 TO-15Chloromethane74-87-3 05/14/16ND B6E1712

12 ug/m3 10 TO-15cis-1,2-Dichloroethylene156-59-2 05/14/16ND B6E1712

13 ug/m3 10 TO-15cis-1,3-Dichloropropylene10061-01-5 05/14/16ND B6E1712

25 ug/m3 10 TO-15Dibromochloromethane124-48-1 05/14/16ND B6E1712

15 ug/m3 10 TO-15Dichlorodifluoromethane75-71-8 05/14/16ND B6E1712

13 ug/m3 10 TO-15Ethylbenzene100-41-4 05/14/1659 B6E1712

31 ug/m3 10 TO-15Hexachlorobutadiene87-68-3 05/14/16ND B6E1712

35 ug/m3 10 TO-15Hexane110-54-3 05/14/16ND B6E1712

13 ug/m3 10 TO-15m & p - Xylene1330-20-7 05/14/16210 B6E1712

Page 3 of 7Page 3 of 7

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1605126-01

RLCAS #

Client ID: SS-1

QC Batch

Organics-Volatiles

10 ug/m3 10 TO-15Methylene chloride75-09-2 05/14/16ND B6E1712

18 ug/m3 10 TO-15Methyltertiarybutylether1634-04-4 05/14/16ND B6E1712

13 ug/m3 10 TO-15o-Xylene95-47-6 05/14/1650 B6E1712

13 ug/m3 10 TO-15Styrene100-42-5 05/14/16ND B6E1712

20 ug/m3 10 TO-15Tetrachloroethylene127-18-4 05/14/16ND B6E1712

11 ug/m3 10 TO-15Toluene108-88-3 05/14/16770 B6E1712

12 ug/m3 10 TO-15trans-1,2-Dichloroethylene156-60-5 05/14/16ND B6E1712

13 ug/m3 10 TO-15trans-1,3-Dichloropropylene10061-02-6 05/14/16ND B6E1712

16 ug/m3 10 TO-15Trichloroethylene79-01-6 05/14/16ND B6E1712

17 ug/m3 10 TO-15Trichlorofluoromethane75-69-4 05/14/16ND B6E1712

7.5 ug/m3 10 TO-15Vinyl chloride75-01-4 05/14/16ND B6E1712

Page 4 of 7Page 4 of 7

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1605126-02

RLCAS #

Client ID: SS-2

QC Batch

Organics-Volatiles

16 ug/m3 10 TO-151,1,1-Trichloroethane71-55-6 05/14/16ND B6E1712

20 ug/m3 10 TO-151,1,2,2-Tetrachloroethane79-34-5 05/14/16ND B6E1712

23 ug/m3 10 TO-151,1,2-Trichloro-1,2,2-trifluoroethane76-13-1 05/14/16ND B6E1712

16 ug/m3 10 TO-151,1,2-Trichloroethane79-00-5 05/14/16ND B6E1712

12 ug/m3 10 TO-151,1-Dichloroethane75-34-3 05/14/16ND B6E1712

12 ug/m3 10 TO-151,1-Dichloroethylene75-35-4 05/14/16ND B6E1712

22 ug/m3 10 TO-151,2,4-Trichlorobenzene120-82-1 05/14/16ND B6E1712

15 ug/m3 10 TO-151,2,4-Trimethylbenzene95-63-6 05/14/1638 B6E1712

23 ug/m3 10 TO-151,2-Dibromoethane106-93-4 05/14/16ND B6E1712

21 ug/m3 10 TO-151,2-Dichloro-1,1,2,2-Tetrafluoroethane76-14-2 05/14/16ND B6E1712

18 ug/m3 10 TO-151,2-Dichlorobenzene95-50-1 05/14/16ND B6E1712

12 ug/m3 10 TO-151,2-Dichloroethane107-06-2 05/14/16ND B6E1712

14 ug/m3 10 TO-151,2-Dichloropropane78-87-5 05/14/16ND B6E1712

15 ug/m3 10 TO-151,3,5-Trimethylbenzene108-67-8 05/14/16ND B6E1712

6.5 ug/m3 10 TO-151,3-Butadiene106-99-0 05/14/16ND B6E1712

18 ug/m3 10 TO-151,3-Dichlorobenzene541-73-1 05/14/16ND B6E1712

18 ug/m3 10 TO-151,4-Dichlorobenzene106-46-7 05/14/16ND B6E1712

14 ug/m3 10 TO-152,2,4-Trimethylpentane540-84-1 05/14/16230 B6E1712

150 ug/m3 10 TO-152-Butanone (MEK)78-93-3 05/14/16ND B6E1712

11 ug/m3 10 TO-152-Chloro-1,3-butadiene126-99-8 05/14/16ND B6E1712

40 ug/m3 10 TO-154-Methyl-2-pentanone (MIBK)108-10-1 05/14/16ND B6E1712

17 A10ug/m3 10 TO-15Acetonitrile75-05-8 05/14/16ND B6E1712

11 ug/m3 10 TO-15Acrylonitrile107-13-1 05/14/16ND B6E1712

9.4 ug/m3 10 TO-15Benzene71-43-2 05/14/1613 B6E1712

20 ug/m3 10 TO-15Bromodichloromethane75-27-4 05/14/16ND B6E1712

31 ug/m3 10 TO-15Bromoform75-25-2 05/14/16ND B6E1712

11 ug/m3 10 TO-15Bromomethane74-83-9 05/14/16ND B6E1712

19 ug/m3 10 TO-15Carbon tetrachloride56-23-5 05/14/16ND B6E1712

14 ug/m3 10 TO-15Chlorobenzene108-90-7 05/14/16ND B6E1712

7.8 ug/m3 10 TO-15Chloroethane75-00-3 05/14/16ND B6E1712

14 ug/m3 10 TO-15Chloroform67-66-3 05/14/1631 B6E1712

6.1 ug/m3 10 TO-15Chloromethane74-87-3 05/14/16ND B6E1712

12 ug/m3 10 TO-15cis-1,2-Dichloroethylene156-59-2 05/14/16ND B6E1712

13 ug/m3 10 TO-15cis-1,3-Dichloropropylene10061-01-5 05/14/16ND B6E1712

25 ug/m3 10 TO-15Dibromochloromethane124-48-1 05/14/16ND B6E1712

15 ug/m3 10 TO-15Dichlorodifluoromethane75-71-8 05/14/16ND B6E1712

13 ug/m3 10 TO-15Ethylbenzene100-41-4 05/14/1666 B6E1712

31 ug/m3 10 TO-15Hexachlorobutadiene87-68-3 05/14/16ND B6E1712

35 ug/m3 10 TO-15Hexane110-54-3 05/14/16ND B6E1712

13 ug/m3 10 TO-15m & p - Xylene1330-20-7 05/14/16230 B6E1712

Page 5 of 7Page 5 of 7

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1605126-02

RLCAS #

Client ID: SS-2

QC Batch

Organics-Volatiles

10 ug/m3 10 TO-15Methylene chloride75-09-2 05/14/16ND B6E1712

18 ug/m3 10 TO-15Methyltertiarybutylether1634-04-4 05/14/16ND B6E1712

13 ug/m3 10 TO-15o-Xylene95-47-6 05/14/1659 B6E1712

13 ug/m3 10 TO-15Styrene100-42-5 05/14/16ND B6E1712

20 ug/m3 10 TO-15Tetrachloroethylene127-18-4 05/14/1640 B6E1712

11 ug/m3 10 TO-15Toluene108-88-3 05/14/16810 B6E1712

12 ug/m3 10 TO-15trans-1,2-Dichloroethylene156-60-5 05/14/16ND B6E1712

13 ug/m3 10 TO-15trans-1,3-Dichloropropylene10061-02-6 05/14/16ND B6E1712

16 ug/m3 10 TO-15Trichloroethylene79-01-6 05/14/16ND B6E1712

17 ug/m3 10 TO-15Trichlorofluoromethane75-69-4 05/14/16ND B6E1712

7.5 ug/m3 10 TO-15Vinyl chloride75-01-4 05/14/16ND B6E1712

Page 6 of 7Page 6 of 7

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

MDEQ-RRD-CADILLAC

RE: CHUCK'S CORNERS. OSCEOLA COUNTY

Cadillac, MI 49601-2158

120 W. Chapin Street

Ann Emington

I certify that the analyses performed by the MDEQ Environmental Laboratory were conducted by methods approved by the U.S. Environmental Protection Agency and other appropriate regulatory agencies .

Sincerely, 03 June 2016 Work Order: 1605125

Price: $1,067.00

George Krisztian

Laboratory Director

Lab Work Order # 1605125

Page 1 of 19Page 1 of 19

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

Project:

Project Manager:

Reported:

MDEQ-RRD-CADILLAC

120 W. Chapin Street

Ann Emington

CHUCK'S CORNERS. OSCEOLA COUNTY

Cadillac MI, 49601-2158

Site Code: 67000151 06/03/2016

Sample ID Laboratory ID Date SampledMatrix Date Received

Analytical Report for Samples

Qualifier

1605125-01 Water 05/12/2016MW-105s 05/11/2016

1605125-02 Water 05/12/2016MW-105D 05/11/2016

1605125-03 Water 05/12/2016MW-107 05/11/2016

1605125-04 Water 05/12/2016MW-114 05/11/2016

1605125-05 Water 05/12/2016MW-116D 05/11/2016

1605125-06 Water 05/12/2016MW-117 05/11/2016

1605125-07 Water 05/12/2016Field Blank 05/11/2016

Notes and Definitions

Y11 Unidentified peaks present in sample.

X Methods 8260 & 624 are used to analyze volatile organics that have boiling points below 200 ºC. 2-Methylnaphthalene & naphthalene have boiling points above 200 ºC and are better suited to analysis by methods 8270 & 625 as semivolatile organics.

A11 Result is estimated due to high initial verification standard criteria failure.

A09 Result is estimated due to high recovery of batch quality control.

A08 Result(s) and reporting limits(s) are estimated due to low recovery of batch QC.

A07 Result(s) and reporting limit(s) are estimated due to poor precision.

A06 Result is estimated due to high continuing calibration standard criteria failure.

A05 Result and reporting limit are estimated due to low continuing calibration standard criteria failure.

A04 Result is estimated due to high matrix spike recovery.

A03 Result(s) and reporting limit(s) are estimated due to low matrix spike recovery.

Reporting LimitRL

Indicates compound analyzed for but not detectedND

Not ApplicableNA

Page 2 of 19Page 2 of 19

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1605125-01

RLCAS #

Client ID: MW-105s

QC Batch

Organics-Volatiles See note Y11

1.0 ug/L 1 82601,1,1,2-Tetrachloroethane630-20-6 05/16/16ND B6E1608

1.0 ug/L 1 82601,1,1-Trichloroethane71-55-6 05/16/16ND B6E1608

1.0 ug/L 1 82601,1,2,2-Tetrachloroethane79-34-5 05/16/16ND B6E1608

1.0 ug/L 1 82601,1,2-Trichloroethane79-00-5 05/16/16ND B6E1608

1.0 ug/L 1 82601,1-Dichloroethane75-34-3 05/16/16ND B6E1608

1.0 ug/L 1 82601,1-Dichloroethylene75-35-4 05/16/16ND B6E1608

5.0 ug/L 1 82601,2,3-Trichlorobenzene87-61-6 05/16/16ND B6E1608

1.0 ug/L 1 82601,2,3-Trichloropropane96-18-4 05/16/16ND B6E1608

1.0 ug/L 1 82601,2,3-Trimethylbenzene526-73-8 05/16/169.8 B6E1608

5.0 ug/L 1 82601,2,4-Trichlorobenzene120-82-1 05/16/16ND B6E1608

1.0 ug/L 1 82601,2,4-Trimethylbenzene95-63-6 05/16/1646 B6E1608

5.0 ug/L 1 82601,2-Dibromo-3-chloropropane96-12-8 05/16/16ND B6E1608

1.0 ug/L 1 82601,2-Dibromoethane106-93-4 05/16/16ND B6E1608

1.0 ug/L 1 82601,2-Dichlorobenzene95-50-1 05/16/16ND B6E1608

1.0 ug/L 1 82601,2-Dichloroethane107-06-2 05/16/16ND B6E1608

1.0 ug/L 1 82601,2-Dichloropropane78-87-5 05/16/16ND B6E1608

1.0 ug/L 1 82601,3,5-Trimethylbenzene108-67-8 05/16/1613 B6E1608

1.0 ug/L 1 82601,3-Dichlorobenzene541-73-1 05/16/16ND B6E1608

1.0 ug/L 1 82601,4-Dichlorobenzene106-46-7 05/16/16ND B6E1608

5.0 ug/L 1 82602-Butanone (MEK)78-93-3 05/16/16ND B6E1608

5.0 ug/L 1 82602-Hexanone591-78-6 05/16/16ND B6E1608

5.0 Xug/L 1 82602-Methylnaphthalene91-57-6 05/16/167.7 B6E1608

20 ug/L 1 82602-Propanone (acetone)67-64-1 05/16/16ND B6E1608

5.0 ug/L 1 82604-Methyl-2-pentanone (MIBK)108-10-1 05/16/16ND B6E1608

5.0 ug/L 1 8260Acrylonitrile107-13-1 05/16/16ND B6E1608

1.0 ug/L 1 8260Benzene71-43-2 05/16/16ND B6E1608

1.0 ug/L 1 8260Bromobenzene108-86-1 05/16/16ND B6E1608

1.0 ug/L 1 8260Bromochloromethane74-97-5 05/16/16ND B6E1608

1.0 ug/L 1 8260Bromodichloromethane75-27-4 05/16/16ND B6E1608

1.0 ug/L 1 8260Bromoform75-25-2 05/16/16ND B6E1608

5.0 ug/L 1 8260Bromomethane74-83-9 05/16/16ND B6E1608

1.0 ug/L 1 8260Carbon disulfide75-15-0 05/16/16ND B6E1608

1.0 ug/L 1 8260Carbon tetrachloride56-23-5 05/16/16ND B6E1608

1.0 ug/L 1 8260Chlorobenzene108-90-7 05/16/16ND B6E1608

5.0 ug/L 1 8260Chloroethane75-00-3 05/16/16ND B6E1608

1.0 ug/L 1 8260Chloroform67-66-3 05/16/16ND B6E1608

5.0 ug/L 1 8260Chloromethane74-87-3 05/16/16ND B6E1608

1.0 ug/L 1 8260cis-1,2-Dichloroethylene156-59-2 05/16/16ND B6E1608

1.0 ug/L 1 8260cis-1,3-Dichloropropylene10061-01-5 05/16/16ND B6E1608

5.0 ug/L 1 8260Cyclohexane110-82-7 05/16/165.9 B6E1608

Page 3 of 19Page 3 of 19

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1605125-01

RLCAS #

Client ID: MW-105s

QC Batch

Organics-Volatiles See note Y11

1.0 ug/L 1 8260Dibromochloromethane124-48-1 05/16/16ND B6E1608

1.0 ug/L 1 8260Dibromomethane74-95-3 05/16/16ND B6E1608

5.0 ug/L 1 8260Dichlorodifluoromethane75-71-8 05/16/16ND B6E1608

5.0 ug/L 1 8260Diethyl ether60-29-7 05/16/16ND B6E1608

5.0 ug/L 1 8260Diisopropyl Ether108-20-3 05/16/16ND B6E1608

1.0 ug/L 1 8260Ethylbenzene100-41-4 05/16/1611 B6E1608

5.0 ug/L 1 8260Ethyltertiarybutylether637-92-3 05/16/16ND B6E1608

5.0 ug/L 1 8260Hexachloroethane67-72-1 05/16/16ND B6E1608

1.0 ug/L 1 8260Isopropylbenzene98-82-8 05/16/161.8 B6E1608

2.0 ug/L 1 8260m & p - Xylene1330-20-7 05/16/1643 B6E1608

1.0 ug/L 1 8260Methyl iodide74-88-4 05/16/16ND B6E1608

5.0 ug/L 1 8260Methylene chloride75-09-2 05/16/16ND B6E1608

1.0 ug/L 1 8260Methyltertiarybutylether1634-04-4 05/16/16ND B6E1608

5.0 Xug/L 1 8260Naphthalene91-20-3 05/16/169.5 B6E1608

1.0 ug/L 1 8260n-Butylbenzene104-51-8 05/16/164.6 B6E1608

1.0 ug/L 1 8260n-Propylbenzene103-65-1 05/16/167.9 B6E1608

1.0 ug/L 1 8260o-Xylene95-47-6 05/16/166.3 B6E1608

1.0 ug/L 1 8260p-Isopropyl toluene99-87-6 05/16/16ND B6E1608

1.0 ug/L 1 8260sec-Butylbenzene135-98-8 05/16/16ND B6E1608

1.0 ug/L 1 8260Styrene100-42-5 05/16/16ND B6E1608

1.0 ug/L 1 8260tert-Butylbenzene98-06-6 05/16/16ND B6E1608

50 ug/L 1 8260tertiary Butyl Alcohol75-65-0 05/16/16ND B6E1608

5.0 ug/L 1 8260tertiaryAmylmethylether994-05-8 05/16/16ND B6E1608

1.0 ug/L 1 8260Tetrachloroethylene127-18-4 05/16/16ND B6E1608

5.0 ug/L 1 8260Tetrahydrofuran109-99-9 05/16/16ND B6E1608

1.0 ug/L 1 8260Toluene108-88-3 05/16/161.4 B6E1608

1.0 ug/L 1 8260trans-1,2-Dichloroethylene156-60-5 05/16/16ND B6E1608

1.0 ug/L 1 8260trans-1,3-Dichloropropylene10061-02-6 05/16/16ND B6E1608

5.0 A05ug/L 1 8260trans-1,4-Dichloro-2-butene110-57-6 05/16/16ND B6E1608

1.0 ug/L 1 8260Trichloroethylene79-01-6 05/16/16ND B6E1608

1.0 ug/L 1 8260Trichlorofluoromethane75-69-4 05/16/16ND B6E1608

1.0 ug/L 1 8260Vinyl chloride75-01-4 05/16/16ND B6E1608

85-115100 %Surrogate: Bromofluorobenzene 826005/16/16 B6E1608

82.7-11592.8 %Surrogate: Dibromofluoromethane 826005/16/16 B6E1608

85-11598.4 %Surrogate: Toluene-d8 826005/16/16 B6E1608

Page 4 of 19Page 4 of 19

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1605125-01

RLCAS #

Client ID: MW-105s

QC Batch

Inorganics-Metals

1.0 ug/L 1 6020/200.8Arsenic7440-38-2 05/27/166.3 B6E2505

5.0 ug/L 1 6020/200.8Barium7440-39-3 05/27/1662 B6E2505

0.2 ug/L 1 6020/200.8Cadmium7440-43-9 05/27/16ND B6E2505

1.0 ug/L 1 6020/200.8Chromium7440-47-3 05/27/16ND B6E2505

1.0 ug/L 1 6020/200.8Copper7440-50-8 05/27/16ND B6E2505

1.0 ug/L 1 6020/200.8Lead7439-92-1 05/27/16ND B6E2505

0.2 ug/L 1 7470/245.1Mercury7439-97-6 05/18/16ND B6E1704

1.0 ug/L 1 6020/200.8Selenium7782-49-2 05/27/16ND B6E2505

0.2 ug/L 1 6020/200.8Silver7440-22-4 05/27/16ND B6E2505

5.0 ug/L 1 6020/200.8Zinc7440-66-6 05/27/16ND B6E2505

Page 5 of 19Page 5 of 19

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1605125-02

RLCAS #

Client ID: MW-105D

QC Batch

Organics-Volatiles See note Y11

1.0 ug/L 1 82601,1,1,2-Tetrachloroethane630-20-6 05/16/16ND B6E1608

1.0 ug/L 1 82601,1,1-Trichloroethane71-55-6 05/16/16ND B6E1608

1.0 ug/L 1 82601,1,2,2-Tetrachloroethane79-34-5 05/16/16ND B6E1608

1.0 ug/L 1 82601,1,2-Trichloroethane79-00-5 05/16/16ND B6E1608

1.0 ug/L 1 82601,1-Dichloroethane75-34-3 05/16/16ND B6E1608

1.0 ug/L 1 82601,1-Dichloroethylene75-35-4 05/16/16ND B6E1608

5.0 ug/L 1 82601,2,3-Trichlorobenzene87-61-6 05/16/16ND B6E1608

1.0 ug/L 1 82601,2,3-Trichloropropane96-18-4 05/16/16ND B6E1608

1.0 ug/L 1 82601,2,3-Trimethylbenzene526-73-8 05/16/169.4 B6E1608

5.0 ug/L 1 82601,2,4-Trichlorobenzene120-82-1 05/16/16ND B6E1608

1.0 ug/L 1 82601,2,4-Trimethylbenzene95-63-6 05/16/1617 B6E1608

5.0 ug/L 1 82601,2-Dibromo-3-chloropropane96-12-8 05/16/16ND B6E1608

1.0 ug/L 1 82601,2-Dibromoethane106-93-4 05/16/16ND B6E1608

1.0 ug/L 1 82601,2-Dichlorobenzene95-50-1 05/16/16ND B6E1608

1.0 ug/L 1 82601,2-Dichloroethane107-06-2 05/16/16ND B6E1608

1.0 ug/L 1 82601,2-Dichloropropane78-87-5 05/16/16ND B6E1608

1.0 ug/L 1 82601,3,5-Trimethylbenzene108-67-8 05/16/168.8 B6E1608

1.0 ug/L 1 82601,3-Dichlorobenzene541-73-1 05/16/16ND B6E1608

1.0 ug/L 1 82601,4-Dichlorobenzene106-46-7 05/16/16ND B6E1608

5.0 ug/L 1 82602-Butanone (MEK)78-93-3 05/16/165.5 B6E1608

5.0 ug/L 1 82602-Hexanone591-78-6 05/16/16ND B6E1608

5.0 Xug/L 1 82602-Methylnaphthalene91-57-6 05/16/16ND B6E1608

20 ug/L 1 82602-Propanone (acetone)67-64-1 05/16/16ND B6E1608

5.0 ug/L 1 82604-Methyl-2-pentanone (MIBK)108-10-1 05/16/16ND B6E1608

5.0 ug/L 1 8260Acrylonitrile107-13-1 05/16/16ND B6E1608

5.0 ug/L 5 8260Benzene71-43-2 05/17/16360 B6E1608

1.0 ug/L 1 8260Bromobenzene108-86-1 05/16/16ND B6E1608

1.0 ug/L 1 8260Bromochloromethane74-97-5 05/16/16ND B6E1608

1.0 ug/L 1 8260Bromodichloromethane75-27-4 05/16/16ND B6E1608

1.0 ug/L 1 8260Bromoform75-25-2 05/16/16ND B6E1608

5.0 ug/L 1 8260Bromomethane74-83-9 05/16/16ND B6E1608

1.0 ug/L 1 8260Carbon disulfide75-15-0 05/16/16ND B6E1608

1.0 ug/L 1 8260Carbon tetrachloride56-23-5 05/16/16ND B6E1608

1.0 ug/L 1 8260Chlorobenzene108-90-7 05/16/16ND B6E1608

5.0 ug/L 1 8260Chloroethane75-00-3 05/16/16ND B6E1608

1.0 ug/L 1 8260Chloroform67-66-3 05/16/16ND B6E1608

5.0 ug/L 1 8260Chloromethane74-87-3 05/16/16ND B6E1608

1.0 ug/L 1 8260cis-1,2-Dichloroethylene156-59-2 05/16/16ND B6E1608

1.0 ug/L 1 8260cis-1,3-Dichloropropylene10061-01-5 05/16/16ND B6E1608

5.0 ug/L 1 8260Cyclohexane110-82-7 05/16/1652 B6E1608

Page 6 of 19Page 6 of 19

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1605125-02

RLCAS #

Client ID: MW-105D

QC Batch

Organics-Volatiles See note Y11

1.0 ug/L 1 8260Dibromochloromethane124-48-1 05/16/16ND B6E1608

1.0 ug/L 1 8260Dibromomethane74-95-3 05/16/16ND B6E1608

5.0 ug/L 1 8260Dichlorodifluoromethane75-71-8 05/16/16ND B6E1608

5.0 ug/L 1 8260Diethyl ether60-29-7 05/16/16ND B6E1608

5.0 ug/L 1 8260Diisopropyl Ether108-20-3 05/16/16ND B6E1608

1.0 ug/L 1 8260Ethylbenzene100-41-4 05/16/1659 B6E1608

5.0 ug/L 1 8260Ethyltertiarybutylether637-92-3 05/16/16ND B6E1608

5.0 ug/L 1 8260Hexachloroethane67-72-1 05/16/16ND B6E1608

1.0 ug/L 1 8260Isopropylbenzene98-82-8 05/16/1619 B6E1608

2.0 ug/L 1 8260m & p - Xylene1330-20-7 05/16/1661 B6E1608

1.0 ug/L 1 8260Methyl iodide74-88-4 05/16/16ND B6E1608

5.0 ug/L 1 8260Methylene chloride75-09-2 05/16/16ND B6E1608

1.0 ug/L 1 8260Methyltertiarybutylether1634-04-4 05/16/163.1 B6E1608

5.0 Xug/L 1 8260Naphthalene91-20-3 05/16/1645 B6E1608

1.0 ug/L 1 8260n-Butylbenzene104-51-8 05/16/16ND B6E1608

1.0 ug/L 1 8260n-Propylbenzene103-65-1 05/16/1632 B6E1608

1.0 ug/L 1 8260o-Xylene95-47-6 05/16/162.5 B6E1608

1.0 ug/L 1 8260p-Isopropyl toluene99-87-6 05/16/16ND B6E1608

1.0 ug/L 1 8260sec-Butylbenzene135-98-8 05/16/16ND B6E1608

1.0 ug/L 1 8260Styrene100-42-5 05/16/16ND B6E1608

1.0 ug/L 1 8260tert-Butylbenzene98-06-6 05/16/16ND B6E1608

50 ug/L 1 8260tertiary Butyl Alcohol75-65-0 05/16/16ND B6E1608

5.0 ug/L 1 8260tertiaryAmylmethylether994-05-8 05/16/16ND B6E1608

1.0 ug/L 1 8260Tetrachloroethylene127-18-4 05/16/16ND B6E1608

5.0 ug/L 1 8260Tetrahydrofuran109-99-9 05/16/16ND B6E1608

1.0 ug/L 1 8260Toluene108-88-3 05/16/169.7 B6E1608

1.0 ug/L 1 8260trans-1,2-Dichloroethylene156-60-5 05/16/16ND B6E1608

1.0 ug/L 1 8260trans-1,3-Dichloropropylene10061-02-6 05/16/16ND B6E1608

5.0 A05ug/L 1 8260trans-1,4-Dichloro-2-butene110-57-6 05/16/16ND B6E1608

1.0 ug/L 1 8260Trichloroethylene79-01-6 05/16/16ND B6E1608

1.0 ug/L 1 8260Trichlorofluoromethane75-69-4 05/16/16ND B6E1608

1.0 ug/L 1 8260Vinyl chloride75-01-4 05/16/16ND B6E1608

85-115103 %Surrogate: Bromofluorobenzene 826005/16/16 B6E1608

82.7-11594.3 %Surrogate: Dibromofluoromethane 826005/16/16 B6E1608

85-11598.9 %Surrogate: Toluene-d8 826005/16/16 B6E1608

Page 7 of 19Page 7 of 19

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1605125-03

RLCAS #

Client ID: MW-107

QC Batch

Organics-Volatiles

1.0 ug/L 1 82601,1,1,2-Tetrachloroethane630-20-6 05/18/16ND B6E1801

1.0 ug/L 1 82601,1,1-Trichloroethane71-55-6 05/18/16ND B6E1801

1.0 ug/L 1 82601,1,2,2-Tetrachloroethane79-34-5 05/18/16ND B6E1801

1.0 ug/L 1 82601,1,2-Trichloroethane79-00-5 05/18/16ND B6E1801

1.0 ug/L 1 82601,1-Dichloroethane75-34-3 05/18/16ND B6E1801

1.0 ug/L 1 82601,1-Dichloroethylene75-35-4 05/18/16ND B6E1801

5.0 ug/L 1 82601,2,3-Trichlorobenzene87-61-6 05/18/16ND B6E1801

1.0 ug/L 1 82601,2,3-Trichloropropane96-18-4 05/18/16ND B6E1801

1.0 ug/L 1 82601,2,3-Trimethylbenzene526-73-8 05/18/16ND B6E1801

5.0 ug/L 1 82601,2,4-Trichlorobenzene120-82-1 05/18/16ND B6E1801

1.0 ug/L 1 82601,2,4-Trimethylbenzene95-63-6 05/18/16ND B6E1801

5.0 ug/L 1 82601,2-Dibromo-3-chloropropane96-12-8 05/18/16ND B6E1801

1.0 ug/L 1 82601,2-Dibromoethane106-93-4 05/18/16ND B6E1801

1.0 ug/L 1 82601,2-Dichlorobenzene95-50-1 05/18/16ND B6E1801

1.0 ug/L 1 82601,2-Dichloroethane107-06-2 05/18/16ND B6E1801

1.0 ug/L 1 82601,2-Dichloropropane78-87-5 05/18/16ND B6E1801

1.0 ug/L 1 82601,3,5-Trimethylbenzene108-67-8 05/18/16ND B6E1801

1.0 ug/L 1 82601,3-Dichlorobenzene541-73-1 05/18/16ND B6E1801

1.0 ug/L 1 82601,4-Dichlorobenzene106-46-7 05/18/16ND B6E1801

5.0 ug/L 1 82602-Butanone (MEK)78-93-3 05/18/16ND B6E1801

5.0 ug/L 1 82602-Hexanone591-78-6 05/18/16ND B6E1801

5.0 A07, Xug/L 1 82602-Methylnaphthalene91-57-6 05/18/16ND B6E1801

20 ug/L 1 82602-Propanone (acetone)67-64-1 05/18/16ND B6E1801

5.0 ug/L 1 82604-Methyl-2-pentanone (MIBK)108-10-1 05/18/16ND B6E1801

5.0 ug/L 1 8260Acrylonitrile107-13-1 05/18/16ND B6E1801

1.0 ug/L 1 8260Benzene71-43-2 05/18/16ND B6E1801

1.0 ug/L 1 8260Bromobenzene108-86-1 05/18/16ND B6E1801

1.0 ug/L 1 8260Bromochloromethane74-97-5 05/18/16ND B6E1801

1.0 ug/L 1 8260Bromodichloromethane75-27-4 05/18/16ND B6E1801

1.0 ug/L 1 8260Bromoform75-25-2 05/18/16ND B6E1801

5.0 A07ug/L 1 8260Bromomethane74-83-9 05/18/16ND B6E1801

1.0 ug/L 1 8260Carbon disulfide75-15-0 05/18/16ND B6E1801

1.0 ug/L 1 8260Carbon tetrachloride56-23-5 05/18/16ND B6E1801

1.0 ug/L 1 8260Chlorobenzene108-90-7 05/18/16ND B6E1801

5.0 ug/L 1 8260Chloroethane75-00-3 05/18/16ND B6E1801

1.0 ug/L 1 8260Chloroform67-66-3 05/18/16ND B6E1801

5.0 A07ug/L 1 8260Chloromethane74-87-3 05/18/16ND B6E1801

1.0 ug/L 1 8260cis-1,2-Dichloroethylene156-59-2 05/18/16ND B6E1801

1.0 ug/L 1 8260cis-1,3-Dichloropropylene10061-01-5 05/18/16ND B6E1801

5.0 ug/L 1 8260Cyclohexane110-82-7 05/18/16ND B6E1801

1.0 ug/L 1 8260Dibromochloromethane124-48-1 05/18/16ND B6E1801

Page 8 of 19Page 8 of 19

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1605125-03

RLCAS #

Client ID: MW-107

QC Batch

Organics-Volatiles

1.0 ug/L 1 8260Dibromomethane74-95-3 05/18/16ND B6E1801

5.0 ug/L 1 8260Dichlorodifluoromethane75-71-8 05/18/16ND B6E1801

5.0 ug/L 1 8260Diethyl ether60-29-7 05/18/16ND B6E1801

5.0 ug/L 1 8260Diisopropyl Ether108-20-3 05/18/16ND B6E1801

1.0 ug/L 1 8260Ethylbenzene100-41-4 05/18/16ND B6E1801

5.0 ug/L 1 8260Ethyltertiarybutylether637-92-3 05/18/16ND B6E1801

5.0 ug/L 1 8260Hexachloroethane67-72-1 05/18/16ND B6E1801

1.0 ug/L 1 8260Isopropylbenzene98-82-8 05/18/16ND B6E1801

2.0 ug/L 1 8260m & p - Xylene1330-20-7 05/18/16ND B6E1801

1.0 ug/L 1 8260Methyl iodide74-88-4 05/18/16ND B6E1801

5.0 ug/L 1 8260Methylene chloride75-09-2 05/18/16ND B6E1801

1.0 ug/L 1 8260Methyltertiarybutylether1634-04-4 05/18/16ND B6E1801

5.0 Xug/L 1 8260Naphthalene91-20-3 05/18/16ND B6E1801

1.0 ug/L 1 8260n-Butylbenzene104-51-8 05/18/16ND B6E1801

1.0 ug/L 1 8260n-Propylbenzene103-65-1 05/18/16ND B6E1801

1.0 ug/L 1 8260o-Xylene95-47-6 05/18/16ND B6E1801

1.0 ug/L 1 8260p-Isopropyl toluene99-87-6 05/18/16ND B6E1801

1.0 ug/L 1 8260sec-Butylbenzene135-98-8 05/18/16ND B6E1801

1.0 ug/L 1 8260Styrene100-42-5 05/18/16ND B6E1801

1.0 ug/L 1 8260tert-Butylbenzene98-06-6 05/18/16ND B6E1801

50 ug/L 1 8260tertiary Butyl Alcohol75-65-0 05/18/16ND B6E1801

5.0 ug/L 1 8260tertiaryAmylmethylether994-05-8 05/18/16ND B6E1801

1.0 ug/L 1 8260Tetrachloroethylene127-18-4 05/18/16ND B6E1801

5.0 ug/L 1 8260Tetrahydrofuran109-99-9 05/18/16ND B6E1801

1.0 ug/L 1 8260Toluene108-88-3 05/18/16ND B6E1801

1.0 ug/L 1 8260trans-1,2-Dichloroethylene156-60-5 05/18/16ND B6E1801

1.0 ug/L 1 8260trans-1,3-Dichloropropylene10061-02-6 05/18/16ND B6E1801

5.0 A05, A08ug/L 1 8260trans-1,4-Dichloro-2-butene110-57-6 05/18/16ND B6E1801

1.0 ug/L 1 8260Trichloroethylene79-01-6 05/18/16ND B6E1801

1.0 ug/L 1 8260Trichlorofluoromethane75-69-4 05/18/16ND B6E1801

1.0 ug/L 1 8260Vinyl chloride75-01-4 05/18/16ND B6E1801

85-11598.8 %Surrogate: Bromofluorobenzene 826005/18/16 B6E1801

82.7-11596.8 %Surrogate: Dibromofluoromethane 826005/18/16 B6E1801

85-11598.2 %Surrogate: Toluene-d8 826005/18/16 B6E1801

Page 9 of 19Page 9 of 19

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1605125-03

RLCAS #

Client ID: MW-107

QC Batch

Inorganics-Metals

1.0 ug/L 1 6020/200.8Arsenic7440-38-2 05/27/167.6 B6E2505

5.0 ug/L 1 6020/200.8Barium7440-39-3 05/27/16120 B6E2505

0.2 ug/L 1 6020/200.8Cadmium7440-43-9 05/27/16ND B6E2505

1.0 ug/L 1 6020/200.8Chromium7440-47-3 05/27/16ND B6E2505

1.0 ug/L 1 6020/200.8Copper7440-50-8 05/27/1619 B6E2505

1.0 ug/L 1 6020/200.8Lead7439-92-1 05/27/16ND B6E2505

0.2 ug/L 1 7470/245.1Mercury7439-97-6 05/18/16ND B6E1704

1.0 A03ug/L 1 6020/200.8Selenium7782-49-2 05/27/16ND B6E2505

0.2 ug/L 1 6020/200.8Silver7440-22-4 05/27/16ND B6E2505

5.0 ug/L 1 6020/200.8Zinc7440-66-6 05/27/16ND B6E2505

Page 10 of 19Page 10 of 19

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1605125-04

RLCAS #

Client ID: MW-114

QC Batch

Organics-Volatiles

1.0 ug/L 1 82601,1,1,2-Tetrachloroethane630-20-6 05/16/16ND B6E1608

1.0 ug/L 1 82601,1,1-Trichloroethane71-55-6 05/16/16ND B6E1608

1.0 ug/L 1 82601,1,2,2-Tetrachloroethane79-34-5 05/16/16ND B6E1608

1.0 ug/L 1 82601,1,2-Trichloroethane79-00-5 05/16/16ND B6E1608

1.0 ug/L 1 82601,1-Dichloroethane75-34-3 05/16/16ND B6E1608

1.0 ug/L 1 82601,1-Dichloroethylene75-35-4 05/16/16ND B6E1608

5.0 ug/L 1 82601,2,3-Trichlorobenzene87-61-6 05/16/16ND B6E1608

1.0 ug/L 1 82601,2,3-Trichloropropane96-18-4 05/16/16ND B6E1608

1.0 ug/L 1 82601,2,3-Trimethylbenzene526-73-8 05/16/16ND B6E1608

5.0 ug/L 1 82601,2,4-Trichlorobenzene120-82-1 05/16/16ND B6E1608

1.0 ug/L 1 82601,2,4-Trimethylbenzene95-63-6 05/16/16ND B6E1608

5.0 ug/L 1 82601,2-Dibromo-3-chloropropane96-12-8 05/16/16ND B6E1608

1.0 ug/L 1 82601,2-Dibromoethane106-93-4 05/16/16ND B6E1608

1.0 ug/L 1 82601,2-Dichlorobenzene95-50-1 05/16/16ND B6E1608

1.0 ug/L 1 82601,2-Dichloroethane107-06-2 05/16/16ND B6E1608

1.0 ug/L 1 82601,2-Dichloropropane78-87-5 05/16/16ND B6E1608

1.0 ug/L 1 82601,3,5-Trimethylbenzene108-67-8 05/16/16ND B6E1608

1.0 ug/L 1 82601,3-Dichlorobenzene541-73-1 05/16/16ND B6E1608

1.0 ug/L 1 82601,4-Dichlorobenzene106-46-7 05/16/16ND B6E1608

5.0 ug/L 1 82602-Butanone (MEK)78-93-3 05/16/16ND B6E1608

5.0 ug/L 1 82602-Hexanone591-78-6 05/16/16ND B6E1608

5.0 Xug/L 1 82602-Methylnaphthalene91-57-6 05/16/16ND B6E1608

20 ug/L 1 82602-Propanone (acetone)67-64-1 05/16/16ND B6E1608

5.0 ug/L 1 82604-Methyl-2-pentanone (MIBK)108-10-1 05/16/16ND B6E1608

5.0 ug/L 1 8260Acrylonitrile107-13-1 05/16/16ND B6E1608

1.0 ug/L 1 8260Benzene71-43-2 05/16/16ND B6E1608

1.0 ug/L 1 8260Bromobenzene108-86-1 05/16/16ND B6E1608

1.0 ug/L 1 8260Bromochloromethane74-97-5 05/16/16ND B6E1608

1.0 ug/L 1 8260Bromodichloromethane75-27-4 05/16/16ND B6E1608

1.0 ug/L 1 8260Bromoform75-25-2 05/16/16ND B6E1608

5.0 ug/L 1 8260Bromomethane74-83-9 05/16/16ND B6E1608

1.0 ug/L 1 8260Carbon disulfide75-15-0 05/16/16ND B6E1608

1.0 ug/L 1 8260Carbon tetrachloride56-23-5 05/16/16ND B6E1608

1.0 ug/L 1 8260Chlorobenzene108-90-7 05/16/16ND B6E1608

5.0 ug/L 1 8260Chloroethane75-00-3 05/16/16ND B6E1608

1.0 ug/L 1 8260Chloroform67-66-3 05/16/16ND B6E1608

5.0 ug/L 1 8260Chloromethane74-87-3 05/16/16ND B6E1608

1.0 ug/L 1 8260cis-1,2-Dichloroethylene156-59-2 05/16/16ND B6E1608

1.0 ug/L 1 8260cis-1,3-Dichloropropylene10061-01-5 05/16/16ND B6E1608

5.0 ug/L 1 8260Cyclohexane110-82-7 05/16/16ND B6E1608

1.0 ug/L 1 8260Dibromochloromethane124-48-1 05/16/16ND B6E1608

Page 11 of 19Page 11 of 19

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1605125-04

RLCAS #

Client ID: MW-114

QC Batch

Organics-Volatiles

1.0 ug/L 1 8260Dibromomethane74-95-3 05/16/16ND B6E1608

5.0 ug/L 1 8260Dichlorodifluoromethane75-71-8 05/16/16ND B6E1608

5.0 ug/L 1 8260Diethyl ether60-29-7 05/16/16ND B6E1608

5.0 ug/L 1 8260Diisopropyl Ether108-20-3 05/16/16ND B6E1608

1.0 ug/L 1 8260Ethylbenzene100-41-4 05/16/16ND B6E1608

5.0 ug/L 1 8260Ethyltertiarybutylether637-92-3 05/16/16ND B6E1608

5.0 ug/L 1 8260Hexachloroethane67-72-1 05/16/16ND B6E1608

1.0 ug/L 1 8260Isopropylbenzene98-82-8 05/16/16ND B6E1608

2.0 ug/L 1 8260m & p - Xylene1330-20-7 05/16/16ND B6E1608

1.0 ug/L 1 8260Methyl iodide74-88-4 05/16/16ND B6E1608

5.0 ug/L 1 8260Methylene chloride75-09-2 05/16/16ND B6E1608

1.0 ug/L 1 8260Methyltertiarybutylether1634-04-4 05/16/1611 B6E1608

5.0 Xug/L 1 8260Naphthalene91-20-3 05/16/16ND B6E1608

1.0 ug/L 1 8260n-Butylbenzene104-51-8 05/16/16ND B6E1608

1.0 ug/L 1 8260n-Propylbenzene103-65-1 05/16/16ND B6E1608

1.0 ug/L 1 8260o-Xylene95-47-6 05/16/16ND B6E1608

1.0 ug/L 1 8260p-Isopropyl toluene99-87-6 05/16/16ND B6E1608

1.0 ug/L 1 8260sec-Butylbenzene135-98-8 05/16/16ND B6E1608

1.0 ug/L 1 8260Styrene100-42-5 05/16/16ND B6E1608

1.0 ug/L 1 8260tert-Butylbenzene98-06-6 05/16/16ND B6E1608

50 ug/L 1 8260tertiary Butyl Alcohol75-65-0 05/16/16ND B6E1608

5.0 ug/L 1 8260tertiaryAmylmethylether994-05-8 05/16/16ND B6E1608

1.0 ug/L 1 8260Tetrachloroethylene127-18-4 05/16/16ND B6E1608

5.0 ug/L 1 8260Tetrahydrofuran109-99-9 05/16/16ND B6E1608

1.0 ug/L 1 8260Toluene108-88-3 05/16/161.3 B6E1608

1.0 ug/L 1 8260trans-1,2-Dichloroethylene156-60-5 05/16/16ND B6E1608

1.0 ug/L 1 8260trans-1,3-Dichloropropylene10061-02-6 05/16/16ND B6E1608

5.0 A05ug/L 1 8260trans-1,4-Dichloro-2-butene110-57-6 05/16/16ND B6E1608

1.0 ug/L 1 8260Trichloroethylene79-01-6 05/16/16ND B6E1608

1.0 ug/L 1 8260Trichlorofluoromethane75-69-4 05/16/16ND B6E1608

1.0 ug/L 1 8260Vinyl chloride75-01-4 05/16/16ND B6E1608

85-11599.5 %Surrogate: Bromofluorobenzene 826005/16/16 B6E1608

82.7-11596.1 %Surrogate: Dibromofluoromethane 826005/16/16 B6E1608

85-11599.8 %Surrogate: Toluene-d8 826005/16/16 B6E1608

Page 12 of 19Page 12 of 19

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1605125-05

RLCAS #

Client ID: MW-116D

QC Batch

Organics-Volatiles

1.0 ug/L 1 82601,1,1,2-Tetrachloroethane630-20-6 05/16/16ND B6E1608

1.0 ug/L 1 82601,1,1-Trichloroethane71-55-6 05/16/16ND B6E1608

1.0 ug/L 1 82601,1,2,2-Tetrachloroethane79-34-5 05/16/16ND B6E1608

1.0 ug/L 1 82601,1,2-Trichloroethane79-00-5 05/16/16ND B6E1608

1.0 ug/L 1 82601,1-Dichloroethane75-34-3 05/16/16ND B6E1608

1.0 ug/L 1 82601,1-Dichloroethylene75-35-4 05/16/16ND B6E1608

5.0 ug/L 1 82601,2,3-Trichlorobenzene87-61-6 05/16/16ND B6E1608

1.0 ug/L 1 82601,2,3-Trichloropropane96-18-4 05/16/16ND B6E1608

1.0 ug/L 1 82601,2,3-Trimethylbenzene526-73-8 05/16/16ND B6E1608

5.0 ug/L 1 82601,2,4-Trichlorobenzene120-82-1 05/16/16ND B6E1608

1.0 ug/L 1 82601,2,4-Trimethylbenzene95-63-6 05/16/16ND B6E1608

5.0 ug/L 1 82601,2-Dibromo-3-chloropropane96-12-8 05/16/16ND B6E1608

1.0 ug/L 1 82601,2-Dibromoethane106-93-4 05/16/16ND B6E1608

1.0 ug/L 1 82601,2-Dichlorobenzene95-50-1 05/16/16ND B6E1608

1.0 ug/L 1 82601,2-Dichloroethane107-06-2 05/16/16ND B6E1608

1.0 ug/L 1 82601,2-Dichloropropane78-87-5 05/16/16ND B6E1608

1.0 ug/L 1 82601,3,5-Trimethylbenzene108-67-8 05/16/16ND B6E1608

1.0 ug/L 1 82601,3-Dichlorobenzene541-73-1 05/16/16ND B6E1608

1.0 ug/L 1 82601,4-Dichlorobenzene106-46-7 05/16/16ND B6E1608

5.0 ug/L 1 82602-Butanone (MEK)78-93-3 05/16/16ND B6E1608

5.0 ug/L 1 82602-Hexanone591-78-6 05/16/16ND B6E1608

5.0 Xug/L 1 82602-Methylnaphthalene91-57-6 05/16/16ND B6E1608

20 ug/L 1 82602-Propanone (acetone)67-64-1 05/16/16ND B6E1608

5.0 ug/L 1 82604-Methyl-2-pentanone (MIBK)108-10-1 05/16/16ND B6E1608

5.0 ug/L 1 8260Acrylonitrile107-13-1 05/16/16ND B6E1608

1.0 ug/L 1 8260Benzene71-43-2 05/16/16ND B6E1608

1.0 ug/L 1 8260Bromobenzene108-86-1 05/16/16ND B6E1608

1.0 ug/L 1 8260Bromochloromethane74-97-5 05/16/16ND B6E1608

1.0 ug/L 1 8260Bromodichloromethane75-27-4 05/16/16ND B6E1608

1.0 ug/L 1 8260Bromoform75-25-2 05/16/16ND B6E1608

5.0 ug/L 1 8260Bromomethane74-83-9 05/16/16ND B6E1608

1.0 ug/L 1 8260Carbon disulfide75-15-0 05/16/16ND B6E1608

1.0 ug/L 1 8260Carbon tetrachloride56-23-5 05/16/16ND B6E1608

1.0 ug/L 1 8260Chlorobenzene108-90-7 05/16/16ND B6E1608

5.0 ug/L 1 8260Chloroethane75-00-3 05/16/16ND B6E1608

1.0 ug/L 1 8260Chloroform67-66-3 05/16/161.1 B6E1608

5.0 ug/L 1 8260Chloromethane74-87-3 05/16/16ND B6E1608

1.0 ug/L 1 8260cis-1,2-Dichloroethylene156-59-2 05/16/16ND B6E1608

1.0 ug/L 1 8260cis-1,3-Dichloropropylene10061-01-5 05/16/16ND B6E1608

5.0 ug/L 1 8260Cyclohexane110-82-7 05/16/16ND B6E1608

1.0 ug/L 1 8260Dibromochloromethane124-48-1 05/16/16ND B6E1608

Page 13 of 19Page 13 of 19

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1605125-05

RLCAS #

Client ID: MW-116D

QC Batch

Organics-Volatiles

1.0 ug/L 1 8260Dibromomethane74-95-3 05/16/16ND B6E1608

5.0 ug/L 1 8260Dichlorodifluoromethane75-71-8 05/16/16ND B6E1608

5.0 ug/L 1 8260Diethyl ether60-29-7 05/16/16ND B6E1608

5.0 ug/L 1 8260Diisopropyl Ether108-20-3 05/16/16ND B6E1608

1.0 ug/L 1 8260Ethylbenzene100-41-4 05/16/16ND B6E1608

5.0 ug/L 1 8260Ethyltertiarybutylether637-92-3 05/16/16ND B6E1608

5.0 ug/L 1 8260Hexachloroethane67-72-1 05/16/16ND B6E1608

1.0 ug/L 1 8260Isopropylbenzene98-82-8 05/16/16ND B6E1608

2.0 ug/L 1 8260m & p - Xylene1330-20-7 05/16/16ND B6E1608

1.0 ug/L 1 8260Methyl iodide74-88-4 05/16/16ND B6E1608

5.0 ug/L 1 8260Methylene chloride75-09-2 05/16/16ND B6E1608

1.0 ug/L 1 8260Methyltertiarybutylether1634-04-4 05/16/16ND B6E1608

5.0 Xug/L 1 8260Naphthalene91-20-3 05/16/16ND B6E1608

1.0 ug/L 1 8260n-Butylbenzene104-51-8 05/16/16ND B6E1608

1.0 ug/L 1 8260n-Propylbenzene103-65-1 05/16/16ND B6E1608

1.0 ug/L 1 8260o-Xylene95-47-6 05/16/16ND B6E1608

1.0 ug/L 1 8260p-Isopropyl toluene99-87-6 05/16/16ND B6E1608

1.0 ug/L 1 8260sec-Butylbenzene135-98-8 05/16/16ND B6E1608

1.0 ug/L 1 8260Styrene100-42-5 05/16/16ND B6E1608

1.0 ug/L 1 8260tert-Butylbenzene98-06-6 05/16/16ND B6E1608

50 ug/L 1 8260tertiary Butyl Alcohol75-65-0 05/16/16ND B6E1608

5.0 ug/L 1 8260tertiaryAmylmethylether994-05-8 05/16/16ND B6E1608

1.0 ug/L 1 8260Tetrachloroethylene127-18-4 05/16/16ND B6E1608

5.0 ug/L 1 8260Tetrahydrofuran109-99-9 05/16/16ND B6E1608

1.0 ug/L 1 8260Toluene108-88-3 05/16/16ND B6E1608

1.0 ug/L 1 8260trans-1,2-Dichloroethylene156-60-5 05/16/16ND B6E1608

1.0 ug/L 1 8260trans-1,3-Dichloropropylene10061-02-6 05/16/16ND B6E1608

5.0 A05ug/L 1 8260trans-1,4-Dichloro-2-butene110-57-6 05/16/16ND B6E1608

1.0 ug/L 1 8260Trichloroethylene79-01-6 05/16/16ND B6E1608

1.0 ug/L 1 8260Trichlorofluoromethane75-69-4 05/16/16ND B6E1608

1.0 ug/L 1 8260Vinyl chloride75-01-4 05/16/16ND B6E1608

85-115101 %Surrogate: Bromofluorobenzene 826005/16/16 B6E1608

82.7-11599.3 %Surrogate: Dibromofluoromethane 826005/16/16 B6E1608

85-11599.3 %Surrogate: Toluene-d8 826005/16/16 B6E1608

Page 14 of 19Page 14 of 19

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1605125-06

RLCAS #

Client ID: MW-117

QC Batch

Organics-Volatiles

1.0 ug/L 1 82601,1,1,2-Tetrachloroethane630-20-6 05/16/16ND B6E1608

1.0 ug/L 1 82601,1,1-Trichloroethane71-55-6 05/16/16ND B6E1608

1.0 ug/L 1 82601,1,2,2-Tetrachloroethane79-34-5 05/16/16ND B6E1608

1.0 ug/L 1 82601,1,2-Trichloroethane79-00-5 05/16/16ND B6E1608

1.0 ug/L 1 82601,1-Dichloroethane75-34-3 05/16/16ND B6E1608

1.0 ug/L 1 82601,1-Dichloroethylene75-35-4 05/16/16ND B6E1608

5.0 ug/L 1 82601,2,3-Trichlorobenzene87-61-6 05/16/16ND B6E1608

1.0 ug/L 1 82601,2,3-Trichloropropane96-18-4 05/16/16ND B6E1608

1.0 ug/L 1 82601,2,3-Trimethylbenzene526-73-8 05/16/16ND B6E1608

5.0 ug/L 1 82601,2,4-Trichlorobenzene120-82-1 05/16/16ND B6E1608

1.0 ug/L 1 82601,2,4-Trimethylbenzene95-63-6 05/16/16ND B6E1608

5.0 ug/L 1 82601,2-Dibromo-3-chloropropane96-12-8 05/16/16ND B6E1608

1.0 ug/L 1 82601,2-Dibromoethane106-93-4 05/16/16ND B6E1608

1.0 ug/L 1 82601,2-Dichlorobenzene95-50-1 05/16/16ND B6E1608

1.0 ug/L 1 82601,2-Dichloroethane107-06-2 05/16/16ND B6E1608

1.0 ug/L 1 82601,2-Dichloropropane78-87-5 05/16/16ND B6E1608

1.0 ug/L 1 82601,3,5-Trimethylbenzene108-67-8 05/16/16ND B6E1608

1.0 ug/L 1 82601,3-Dichlorobenzene541-73-1 05/16/16ND B6E1608

1.0 ug/L 1 82601,4-Dichlorobenzene106-46-7 05/16/16ND B6E1608

5.0 ug/L 1 82602-Butanone (MEK)78-93-3 05/16/16ND B6E1608

5.0 ug/L 1 82602-Hexanone591-78-6 05/16/16ND B6E1608

5.0 A03, Xug/L 1 82602-Methylnaphthalene91-57-6 05/16/16ND B6E1608

20 ug/L 1 82602-Propanone (acetone)67-64-1 05/16/16ND B6E1608

5.0 ug/L 1 82604-Methyl-2-pentanone (MIBK)108-10-1 05/16/16ND B6E1608

5.0 ug/L 1 8260Acrylonitrile107-13-1 05/16/16ND B6E1608

1.0 ug/L 1 8260Benzene71-43-2 05/16/16ND B6E1608

1.0 ug/L 1 8260Bromobenzene108-86-1 05/16/16ND B6E1608

1.0 ug/L 1 8260Bromochloromethane74-97-5 05/16/16ND B6E1608

1.0 ug/L 1 8260Bromodichloromethane75-27-4 05/16/16ND B6E1608

1.0 ug/L 1 8260Bromoform75-25-2 05/16/16ND B6E1608

5.0 ug/L 1 8260Bromomethane74-83-9 05/16/16ND B6E1608

1.0 ug/L 1 8260Carbon disulfide75-15-0 05/16/16ND B6E1608

1.0 ug/L 1 8260Carbon tetrachloride56-23-5 05/16/16ND B6E1608

1.0 ug/L 1 8260Chlorobenzene108-90-7 05/16/16ND B6E1608

5.0 ug/L 1 8260Chloroethane75-00-3 05/16/16ND B6E1608

1.0 ug/L 1 8260Chloroform67-66-3 05/16/16ND B6E1608

5.0 ug/L 1 8260Chloromethane74-87-3 05/16/16ND B6E1608

1.0 ug/L 1 8260cis-1,2-Dichloroethylene156-59-2 05/16/16ND B6E1608

1.0 ug/L 1 8260cis-1,3-Dichloropropylene10061-01-5 05/16/16ND B6E1608

5.0 ug/L 1 8260Cyclohexane110-82-7 05/16/16ND B6E1608

1.0 ug/L 1 8260Dibromochloromethane124-48-1 05/16/16ND B6E1608

Page 15 of 19Page 15 of 19

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1605125-06

RLCAS #

Client ID: MW-117

QC Batch

Organics-Volatiles

1.0 ug/L 1 8260Dibromomethane74-95-3 05/16/16ND B6E1608

5.0 ug/L 1 8260Dichlorodifluoromethane75-71-8 05/16/16ND B6E1608

5.0 ug/L 1 8260Diethyl ether60-29-7 05/16/16ND B6E1608

5.0 ug/L 1 8260Diisopropyl Ether108-20-3 05/16/16ND B6E1608

1.0 ug/L 1 8260Ethylbenzene100-41-4 05/16/16ND B6E1608

5.0 ug/L 1 8260Ethyltertiarybutylether637-92-3 05/16/16ND B6E1608

5.0 ug/L 1 8260Hexachloroethane67-72-1 05/16/16ND B6E1608

1.0 ug/L 1 8260Isopropylbenzene98-82-8 05/16/16ND B6E1608

2.0 ug/L 1 8260m & p - Xylene1330-20-7 05/16/16ND B6E1608

1.0 ug/L 1 8260Methyl iodide74-88-4 05/16/16ND B6E1608

5.0 ug/L 1 8260Methylene chloride75-09-2 05/16/16ND B6E1608

1.0 ug/L 1 8260Methyltertiarybutylether1634-04-4 05/16/16ND B6E1608

5.0 Xug/L 1 8260Naphthalene91-20-3 05/16/16ND B6E1608

1.0 ug/L 1…