079308.00+PART 2+DCSpec_Rev_02-19.pdf

PDF 6 MB Posted Jun 13, 2019

Attached to: 761/18283. SAR Former Salzburg Cleaners Remediation
Solicitation number: RFQ-171-190000000458-4
Issued by: Bay County, Michigan

View the file

Other files

File	Type	Posted
Adverisement - 1906 South Erie Street Bay City MI.pdf	PDF	Jun 13, 2019
079308.00+PART 3+DCSpec_Rev_02-19.pdf	PDF	Jun 13, 2019
Addendum No. 2-061019.pdf	PDF	Jun 13, 2019
Addendum No. 3.pdf	PDF	Jun 13, 2019
079308.00+PART 1+DCSpec_Rev_02-19.pdf	PDF	Jun 13, 2019
Addendum 1 18283.pdf	PDF	Jun 13, 2019

On GovTribe

Work with this file

Download the original file
Contacts named in this file
Similar government files
Ask GovTribe AI about this file

Try for free Login

Text version

The file's text, extracted by GovTribe without its formatting.

Bidding and Contract Document (R 2/19) Project Name: Former Salzburg Cleaners File No. 761/18283.SAR

APPENDIX VII

REFERENCE REPORTS

205 W IVY AVE

1900 S

ERIE ST 107 W IVY AVE

S ERIE ST

1904 S

WENONA AVE

SALZBURG

AVE

SALZBURG

AVE

1907 S

CHILSON ST

SALZBURG

AVE

207 W IVY AVE

SALZBURG

AVE

Date: 12/11/2018

G!. Fire Hydrants

Watermain

Water Service in ch in ch in ch

205 W IVY AVE

1900 S

ERIE ST 107 W IVY AVE

1906 S

ERIE ST

1904 S

WENONA AVE

SALZBURG

AVE

SALZBURG

AVE

1907 S

CHILSON ST

SALZBURG

AVE

207 W

IVY AVE

SALZBURG

AVE

Catch Basin

Manhole Combined

Sanitary

Storm

Lateral Line Combination

Domestic

Storm

Commercial

Industrial

Gravity Main Combined

Sanitary

Storm

Interceptor

Date: 12/11/2018

P.O. Box 30270

Lansing, MI 48909

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

MDEQ-RRD-SAGINAW BAY

RE: SALZBURG CLEANERS

Bay City, MI 48708

401 Ketchum St., Suite B

Melissa Yuvan

I certify that the analyses performed by the MDEQ Environmental Laboratory were conducted by methods approved by the U.S. Environmental Protection Agency and other appropriate regulatory agencies .

Sincerely, 27 November 2018 Work Order: 1810151

Price: $7,410.00

Kirby Shane

Laboratory Director

Lab Work Order # 1810151

Page 1 of 104Page 1 of 105

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

Project:

Project Manager:

Reported:

MDEQ-RRD-SAGINAW BAY

401 Ketchum St., Suite B

Melissa Yuvan

SALZBURG CLEANERS

Bay City MI, 48708

Site Code: 079308-00 11/27/2018

Sample ID Laboratory ID Date SampledMatrix Date Received

Analytical Report for Samples

Qualifier

1810151-01 Soil/Sediment 10/16/2018SB1 (2-3) 10/10/2018

1810151-02 Soil/Sediment 10/16/2018SB1 (3.5-4) 10/10/2018

1810151-03 Soil/Sediment 10/16/2018SB1 (15.5-16) 10/10/2018

1810151-04 Soil/Sediment 10/16/2018SB2 (3-3.5) 10/10/2018

1810151-05 Soil/Sediment 10/16/2018SB2 (8.5-9) 10/10/2018

1810151-06 Soil/Sediment 10/16/2018SB2 (14-14.5) 10/10/2018

1810151-07 Soil/Sediment 10/16/2018SB3 (3.5-4) 10/10/2018

1810151-08 Soil/Sediment 10/16/2018SB3 (6.5-7) 10/10/2018

1810151-09 Soil/Sediment 10/16/2018SB3 (14.5-15) 10/10/2018

1810151-10 Soil/Sediment 10/16/2018SB4 (0.5-1) 10/10/2018

1810151-11 Soil/Sediment 10/16/2018SB4 (2.5-3) 10/10/2018

1810151-12 Soil/Sediment 10/16/2018SB4 (14-14.5) 10/10/2018

1810151-13 Soil/Sediment 10/16/2018SB5 (0.5-1) 10/10/2018

1810151-14 Soil/Sediment 10/16/2018SB5 (9-9.5) 10/10/2018

1810151-15 Soil/Sediment 10/16/2018SB5 (14.5-15) 10/10/2018

1810151-16 Soil/Sediment 10/16/2018SB6 (2-2.5) 10/10/2018

1810151-17 Soil/Sediment 10/16/2018SB6 (11-11.5) 10/10/2018

1810151-18 Soil/Sediment 10/16/2018SB6 (14-14.5) 10/10/2018

1810151-19 Soil/Sediment 10/16/2018SB7 (3-3.5) 10/10/2018

1810151-20 Soil/Sediment 10/16/2018SB7 (10-10.5) 10/10/2018

Page 2 of 104Page 2 of 105

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

Notes and Definitions

Y21 Reporting Limits (RL) raised due to matrix interference.

Y20 Reporting Limits (RL) raised due to matrix.

Y17 Probable petroleum product(s) present.

Y11 Unidentified peaks present in sample.

X Methods 8260 & 624 are used to analyze volatile organics that have boiling points below 200 ºC. 2-Methylnaphthalene & naphthalene have boiling points above 200 ºC and are better suited to analysis by methods 8270 & 625 as semivolatile organics.

V Value not available due to dilution.

T Reported value is less than the reporting limit (RL). Result is estimated.

N Result is estimated due to Non-homogeneous sample.

A11 Result is estimated due to high initial verification standard criteria failure.

A05 Result and reporting limit are estimated due to low continuing calibration standard criteria failure.

A04 Result is estimated due to high matrix spike recovery.

Reporting LimitRL

Indicates compound analyzed for but not detectedND dry Sample results reported on a dry weight basis

Not ApplicableNA

Page 3 of 104Page 3 of 105

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1810151-01

RLCAS #

Client ID: SB1 (2-3)

QC Batch

Organics-Volatiles See note Y11

5300 ug/kg dry 2000 82601,1,1,2-Tetrachloroethane630-20-6 10/18/18ND B8J1812

5300 ug/kg dry 2000 82601,1,1-Trichloroethane71-55-6 10/18/18ND B8J1812

5300 ug/kg dry 2000 82601,1,2,2-Tetrachloroethane79-34-5 10/18/18ND B8J1812

5300 ug/kg dry 2000 82601,1,2-Trichloroethane79-00-5 10/18/18ND B8J1812

5300 ug/kg dry 2000 82601,1-Dichloroethane75-34-3 10/18/18ND B8J1812

5300 ug/kg dry 2000 82601,1-Dichloroethylene75-35-4 10/18/18ND B8J1812

27000 ug/kg dry 2000 82601,2,3-Trichlorobenzene87-61-6 10/18/18ND B8J1812

5300 A05ug/kg dry 2000 82601,2,3-Trichloropropane96-18-4 10/18/18ND B8J1812

5300 ug/kg dry 2000 82601,2,3-Trimethylbenzene526-73-8 10/18/186700 B8J1812

27000 ug/kg dry 2000 82601,2,4-Trichlorobenzene120-82-1 10/18/18ND B8J1812

5300 ug/kg dry 2000 82601,2,4-Trimethylbenzene95-63-6 10/18/18ND B8J1812

5300 ug/kg dry 2000 82601,2-Dibromoethane106-93-4 10/18/18ND B8J1812

5300 ug/kg dry 2000 82601,2-Dichlorobenzene95-50-1 10/18/18ND B8J1812

5300 ug/kg dry 2000 82601,2-Dichloroethane107-06-2 10/18/18ND B8J1812

5300 ug/kg dry 2000 82601,2-Dichloropropane78-87-5 10/18/18ND B8J1812

5300 ug/kg dry 2000 82601,3,5-Trimethylbenzene108-67-8 10/18/1810000 B8J1812

5300 ug/kg dry 2000 82601,3-Dichlorobenzene541-73-1 10/18/18ND B8J1812

5300 ug/kg dry 2000 82601,4-Dichlorobenzene106-46-7 10/18/18ND B8J1812

27000 ug/kg dry 2000 82602,2,4-Trimethylpentane540-84-1 10/18/1843000 B8J1812

27000 ug/kg dry 2000 82602-Butanone (MEK)78-93-3 10/18/18ND B8J1812

27000 Xug/kg dry 2000 82602-Methylnaphthalene91-57-6 10/18/1889000 B8J1812

110000 ug/kg dry 2000 82602-Propanone (acetone)67-64-1 10/18/18ND B8J1812

27000 ug/kg dry 2000 82604-Methyl-2-pentanone (MIBK)108-10-1 10/18/18ND B8J1812

27000 ug/kg dry 2000 8260Acrylonitrile107-13-1 10/18/18ND B8J1812

5300 ug/kg dry 2000 8260Benzene71-43-2 10/18/18ND B8J1812

5300 ug/kg dry 2000 8260Bromochloromethane74-97-5 10/18/18ND B8J1812

5300 ug/kg dry 2000 8260Bromodichloromethane75-27-4 10/18/18ND B8J1812

5300 ug/kg dry 2000 8260Bromoform75-25-2 10/18/18ND B8J1812

21000 ug/kg dry 2000 8260Bromomethane74-83-9 10/18/18ND B8J1812

5300 ug/kg dry 2000 8260Carbon disulfide75-15-0 10/18/18ND B8J1812

5300 ug/kg dry 2000 8260Carbon tetrachloride56-23-5 10/18/18ND B8J1812

5300 ug/kg dry 2000 8260Chlorobenzene108-90-7 10/18/18ND B8J1812

27000 ug/kg dry 2000 8260Chloroethane75-00-3 10/18/18ND B8J1812

5300 ug/kg dry 2000 8260Chloroform67-66-3 10/18/18ND B8J1812

27000 ug/kg dry 2000 8260Chloromethane74-87-3 10/18/18ND B8J1812

5300 ug/kg dry 2000 8260cis-1,2-Dichloroethylene156-59-2 10/18/18ND B8J1812

5300 ug/kg dry 2000 8260cis-1,3-Dichloropropylene10061-01-5 10/18/18ND B8J1812

27000 ug/kg dry 2000 8260Cyclohexane110-82-7 10/18/1834000 B8J1812

5300 ug/kg dry 2000 8260Dibromochloromethane124-48-1 10/18/18ND B8J1812

5300 ug/kg dry 2000 8260Dibromomethane74-95-3 10/18/18ND B8J1812

Page 4 of 104Page 4 of 105

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1810151-01

RLCAS #

Client ID: SB1 (2-3)

QC Batch

Organics-Volatiles See note Y11

27000 ug/kg dry 2000 8260Dichlorodifluoromethane75-71-8 10/18/18ND B8J1812

21000 ug/kg dry 2000 8260Diethyl ether60-29-7 10/18/18ND B8J1812

27000 ug/kg dry 2000 8260Diisopropyl Ether108-20-3 10/18/18ND B8J1812

5300 ug/kg dry 2000 8260Ethylbenzene100-41-4 10/18/18200000 B8J1812

27000 ug/kg dry 2000 8260Ethyltertiarybutylether637-92-3 10/18/18ND B8J1812

27000 ug/kg dry 2000 8260Hexachloroethane67-72-1 10/18/18ND B8J1812

5300 ug/kg dry 2000 8260Hexane110-54-3 10/18/1843000 B8J1812

5300 ug/kg dry 2000 8260Isopropylbenzene98-82-8 10/18/1826000 B8J1812

11000 ug/kg dry 2000 8260m & p - Xylene1330-20-7 10/18/1818000 B8J1812

11000 ug/kg dry 2000 8260Methylene chloride75-09-2 10/18/18ND B8J1812

5300 ug/kg dry 2000 8260Methyltertiarybutylether1634-04-4 10/18/18ND B8J1812

27000 Xug/kg dry 2000 8260Naphthalene91-20-3 10/18/18110000 B8J1812

5300 ug/kg dry 2000 8260n-Butylbenzene104-51-8 10/18/1829000 B8J1812

5300 ug/kg dry 2000 8260n-Propylbenzene103-65-1 10/18/18100000 B8J1812

5300 ug/kg dry 2000 8260o-Xylene95-47-6 10/18/18ND B8J1812

5300 ug/kg dry 2000 8260sec-Butylbenzene135-98-8 10/18/187800 B8J1812

5300 ug/kg dry 2000 8260Styrene100-42-5 10/18/18ND B8J1812

5300 ug/kg dry 2000 8260tert-Butylbenzene98-06-6 10/18/18ND B8J1812

270000 ug/kg dry 2000 8260tertiary Butyl Alcohol75-65-0 10/18/18ND B8J1812

27000 ug/kg dry 2000 8260tertiaryAmylmethylether994-05-8 10/18/18ND B8J1812

5300 ug/kg dry 2000 8260Tetrachloroethylene127-18-4 10/18/18ND B8J1812

27000 ug/kg dry 2000 8260Tetrahydrofuran109-99-9 10/18/18ND B8J1812

5300 ug/kg dry 2000 8260Toluene108-88-3 10/18/18ND B8J1812

5300 ug/kg dry 2000 8260trans-1,2-Dichloroethylene156-60-5 10/18/18ND B8J1812

5300 ug/kg dry 2000 8260trans-1,3-Dichloropropylene10061-02-6 10/18/18ND B8J1812

5300 ug/kg dry 2000 8260Trichloroethylene79-01-6 10/18/18ND B8J1812

5300 ug/kg dry 2000 8260Trichlorofluoromethane75-69-4 10/18/18ND B8J1812

5300 ug/kg dry 2000 8260Vinyl chloride75-01-4 10/18/18ND B8J1812

V40.3-194Not ApplicableSurrogate: Bromofluorobenzene 826010/18/18 B8J1812

V52.1-217Not ApplicableSurrogate: Dibromofluoromethane 826010/18/18 B8J1812

V55.4-196Not ApplicableSurrogate: Toluene-d8 826010/18/18 B8J1812

Page 5 of 104Page 5 of 105

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1810151-01

RLCAS #

Client ID: SB1 (2-3)

QC Batch

Organics-Semivolatiles See note Y17, Y20

740 ug/kg dry 1 82701,2,4-Trichlorobenzene120-82-1 10/24/18ND B8J2215

1200 ug/kg dry 1 82702,4,5-Trichlorophenol95-95-4 10/24/18ND B8J2215

1200 ug/kg dry 1 82702,4,6-Trichlorophenol88-06-2 10/24/18ND B8J2215

1200 ug/kg dry 1 82702,4-Dichlorophenol120-83-2 10/24/18ND B8J2215

1200 ug/kg dry 1 82702,4-Dimethylphenol105-67-9 10/24/18ND B8J2215

6300 ug/kg dry 1 82702,4-Dinitrophenol51-28-5 10/24/18ND B8J2215

930 ug/kg dry 1 82702,4-Dinitrotoluene121-14-2 10/24/18ND B8J2215

930 ug/kg dry 1 82702,6-Dinitrotoluene606-20-2 10/24/18ND B8J2215

740 ug/kg dry 1 82702-Chloronaphthalene91-58-7 10/24/18ND B8J2215

1200 ug/kg dry 1 82702-Chlorophenol95-57-8 10/24/18ND B8J2215

6300 ug/kg dry 1 82702-Methyl-4,6-dinitrophenol534-52-1 10/24/18ND B8J2215

9300 ug/kg dry 10 82702-Methylnaphthalene91-57-6 10/26/18160000 B8J2215

1200 ug/kg dry 1 82702-Methylphenol (o-Cresol)95-48-7 10/24/18ND B8J2215

1900 ug/kg dry 1 82702-Nitroaniline88-74-4 10/24/18ND B8J2215

1200 ug/kg dry 1 82702-Nitrophenol88-75-5 10/24/18ND B8J2215

2400 ug/kg dry 1 82703 & 4-Methylphenol108394,106445 10/24/18ND B8J2215

1900 ug/kg dry 1 82703-Nitroaniline99-09-2 10/24/18ND B8J2215

740 ug/kg dry 1 82704-Bromophenyl phenyl ether101-55-3 10/24/18ND B8J2215

740 ug/kg dry 1 82704-Chloro-3-methyl-phenol59-50-7 10/24/18ND B8J2215

370 ug/kg dry 1 82704-Chlorodiphenylether7005-72-3 10/24/18ND B8J2215

1900 ug/kg dry 1 82704-Nitroaniline100-01-6 10/24/18ND B8J2215

6300 A05ug/kg dry 1 82704-Nitrophenol100-02-7 10/24/18ND B8J2215

370 ug/kg dry 1 8270Acenaphthene83-32-9 10/24/18600 B8J2215

370 ug/kg dry 1 8270Acenaphthylene208-96-8 10/24/18ND B8J2215

370 ug/kg dry 1 8270Anthracene120-12-7 10/24/18ND B8J2215

740 ug/kg dry 1 8270Azobenzene103-33-3 10/24/18ND B8J2215

370 ug/kg dry 1 8270Benz[a]anthracene56-55-3 10/24/18ND B8J2215

740 ug/kg dry 1 8270Benzo[a]pyrene50-32-8 10/24/18ND B8J2215

740 ug/kg dry 1 8270Benzo[b]fluoranthene205-99-2 10/24/18ND B8J2215

740 ug/kg dry 1 8270Benzo[g,h,i]perylene191-24-2 10/24/18ND B8J2215

740 ug/kg dry 1 8270Benzo[k]fluoranthene207-08-9 10/24/18ND B8J2215

9300 ug/kg dry 1 8270Benzyl Alcohol100-51-6 10/24/18ND B8J2215

740 ug/kg dry 1 8270Bis(2-chloroethoxy)methane111-91-1 10/24/18ND B8J2215

370 ug/kg dry 1 8270Bis(2-chloroethyl)ether111-44-4 10/24/18ND B8J2215

370 A05ug/kg dry 1 8270Bis(2-chloroisopropyl)ether108-60-1 10/24/18ND B8J2215

930 ug/kg dry 1 8270Bis(2-ethylhexyl)phthalate117-81-7 10/24/181200 B8J2215

930 ug/kg dry 1 8270Butyl benzyl phthalate85-68-7 10/24/18ND B8J2215

930 ug/kg dry 1 8270Carbazole86-74-8 10/24/18ND B8J2215

370 ug/kg dry 1 8270Chrysene218-01-9 10/24/18ND B8J2215

740 ug/kg dry 1 8270Dibenz[a,h]anthracene53-70-3 10/24/18ND B8J2215

Page 6 of 104Page 6 of 105

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1810151-01

RLCAS #

Client ID: SB1 (2-3)

QC Batch

Organics-Semivolatiles See note Y17, Y20

930 ug/kg dry 1 8270Dibenzofuran132-64-9 10/24/18ND B8J2215

930 ug/kg dry 1 8270Diethylphthalate84-66-2 10/24/18ND B8J2215

930 ug/kg dry 1 8270Dimethyl phthalate131-11-3 10/24/18ND B8J2215

930 ug/kg dry 1 8270Di-n-butyl phthalate84-74-2 10/24/18ND B8J2215

930 ug/kg dry 1 8270Di-n-octyl phthalate117-84-0 10/24/18ND B8J2215

370 ug/kg dry 1 8270Fluoranthene206-44-0 10/24/18ND B8J2215

370 ug/kg dry 1 8270Fluorene86-73-7 10/24/18730 B8J2215

740 ug/kg dry 1 8270Hexachlorobenzene118-74-1 10/24/18ND B8J2215

370 ug/kg dry 1 8270Hexachlorobutadiene87-68-3 10/24/18ND B8J2215

3700 ug/kg dry 1 8270Hexachlorocyclopentadiene77-47-4 10/24/18ND B8J2215

370 ug/kg dry 1 8270Hexachloroethane67-72-1 10/24/18ND B8J2215

740 ug/kg dry 1 8270Indeno(1,2,3-c,d)pyrene193-39-5 10/24/18ND B8J2215

370 ug/kg dry 1 8270Isophorone78-59-1 10/24/18ND B8J2215

3700 ug/kg dry 10 8270Naphthalene91-20-3 10/26/18150000 B8J2215

740 ug/kg dry 1 8270Nitrobenzene98-95-3 10/24/18ND B8J2215

930 ug/kg dry 1 8270N-Nitrosodimethylamine67-75-9 10/24/18ND B8J2215

740 ug/kg dry 1 8270N-Nitrosodi-n-propylamine621-64-7 10/24/18ND B8J2215

740 ug/kg dry 1 8270N-Nitrosodiphenylamine86-30-6 10/24/18ND B8J2215

6300 ug/kg dry 1 8270Pentachlorophenol87-86-5 10/24/18ND B8J2215

370 ug/kg dry 1 8270Phenanthrene85-01-8 10/24/181300 B8J2215

1200 ug/kg dry 1 8270Phenol108-95-2 10/24/18ND B8J2215

370 ug/kg dry 1 8270Pyrene129-00-0 10/24/18ND B8J2215

20.3-11589.0 %Surrogate: 2,4,6-Tribromophenol 827010/24/18 B8J2215

32.9-11564.2 %Surrogate: 2-Fluorobiphenyl 827010/24/18 B8J2215

23.7-11572.2 %Surrogate: 2-Fluorophenol 827010/24/18 B8J2215

31.8-11561.0 %Surrogate: Nitrobenzene-d5 827010/24/18 B8J2215

29.3-11587.2 %Surrogate: Phenol-d6 827010/24/18 B8J2215

38.5-11583.3 %Surrogate: p-Terphenyl-d14 827010/24/18 B8J2215

Page 7 of 104Page 7 of 105

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1810151-01

RLCAS #

Client ID: SB1 (2-3)

QC Batch

Inorganics-General Chemistry

0.1 % 1 2540 B% Total SolidsTS 10/23/1853.9 B8J1904

Page 8 of 104Page 8 of 105

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1810151-02

RLCAS #

Client ID: SB1 (3.5-4)

QC Batch

Organics-Volatiles See note Y11

620 ug/kg dry 400 82601,1,1,2-Tetrachloroethane630-20-6 10/19/18ND B8J2913

620 ug/kg dry 400 82601,1,1-Trichloroethane71-55-6 10/19/18ND B8J2913

620 ug/kg dry 400 82601,1,2,2-Tetrachloroethane79-34-5 10/19/18ND B8J2913

620 ug/kg dry 400 82601,1,2-Trichloroethane79-00-5 10/19/18ND B8J2913

620 ug/kg dry 400 82601,1-Dichloroethane75-34-3 10/19/18ND B8J2913

620 ug/kg dry 400 82601,1-Dichloroethylene75-35-4 10/19/18ND B8J2913

3100 ug/kg dry 400 82601,2,3-Trichlorobenzene87-61-6 10/19/18ND B8J2913

620 ug/kg dry 400 82601,2,3-Trichloropropane96-18-4 10/19/18ND B8J2913

620 ug/kg dry 400 82601,2,3-Trimethylbenzene526-73-8 10/19/182200 B8J2913

3100 ug/kg dry 400 82601,2,4-Trichlorobenzene120-82-1 10/19/18ND B8J2913

620 ug/kg dry 400 82601,2,4-Trimethylbenzene95-63-6 10/19/184900 B8J2913

620 ug/kg dry 400 82601,2-Dibromoethane106-93-4 10/19/18ND B8J2913

620 ug/kg dry 400 82601,2-Dichlorobenzene95-50-1 10/19/18ND B8J2913

620 ug/kg dry 400 82601,2-Dichloroethane107-06-2 10/19/18ND B8J2913

620 ug/kg dry 400 82601,2-Dichloropropane78-87-5 10/19/18ND B8J2913

620 ug/kg dry 400 82601,3,5-Trimethylbenzene108-67-8 10/19/181400 B8J2913

620 ug/kg dry 400 82601,3-Dichlorobenzene541-73-1 10/19/18ND B8J2913

620 ug/kg dry 400 82601,4-Dichlorobenzene106-46-7 10/19/18ND B8J2913

3100 ug/kg dry 400 82602,2,4-Trimethylpentane540-84-1 10/19/1892000 B8J2913

3100 ug/kg dry 400 82602-Butanone (MEK)78-93-3 10/19/18ND B8J2913

3100 Xug/kg dry 400 82602-Methylnaphthalene91-57-6 10/19/1841000 B8J2913

12000 ug/kg dry 400 82602-Propanone (acetone)67-64-1 10/19/18ND B8J2913

3100 ug/kg dry 400 82604-Methyl-2-pentanone (MIBK)108-10-1 10/19/18ND B8J2913

3100 ug/kg dry 400 8260Acrylonitrile107-13-1 10/19/18ND B8J2913

620 ug/kg dry 400 8260Benzene71-43-2 10/19/181200 B8J2913

620 ug/kg dry 400 8260Bromochloromethane74-97-5 10/19/18ND B8J2913

620 ug/kg dry 400 8260Bromodichloromethane75-27-4 10/19/18ND B8J2913

620 ug/kg dry 400 8260Bromoform75-25-2 10/19/18ND B8J2913

2500 ug/kg dry 400 8260Bromomethane74-83-9 10/19/18ND B8J2913

620 ug/kg dry 400 8260Carbon disulfide75-15-0 10/19/18ND B8J2913

620 ug/kg dry 400 8260Carbon tetrachloride56-23-5 10/19/18ND B8J2913

620 ug/kg dry 400 8260Chlorobenzene108-90-7 10/19/18ND B8J2913

3100 ug/kg dry 400 8260Chloroethane75-00-3 10/19/18ND B8J2913

620 ug/kg dry 400 8260Chloroform67-66-3 10/19/18ND B8J2913

3100 ug/kg dry 400 8260Chloromethane74-87-3 10/19/18ND B8J2913

620 ug/kg dry 400 8260cis-1,2-Dichloroethylene156-59-2 10/19/18ND B8J2913

620 ug/kg dry 400 8260cis-1,3-Dichloropropylene10061-01-5 10/19/18ND B8J2913

3100 ug/kg dry 400 8260Cyclohexane110-82-7 10/19/1834000 B8J2913

620 ug/kg dry 400 8260Dibromochloromethane124-48-1 10/19/18ND B8J2913

620 ug/kg dry 400 8260Dibromomethane74-95-3 10/19/18ND B8J2913

Page 9 of 104Page 9 of 105

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1810151-02

RLCAS #

Client ID: SB1 (3.5-4)

QC Batch

Organics-Volatiles See note Y11

3100 ug/kg dry 400 8260Dichlorodifluoromethane75-71-8 10/19/18ND B8J2913

2500 ug/kg dry 400 8260Diethyl ether60-29-7 10/19/18ND B8J2913

3100 ug/kg dry 400 8260Diisopropyl Ether108-20-3 10/19/18ND B8J2913

620 ug/kg dry 400 8260Ethylbenzene100-41-4 10/19/1819000 B8J2913

3100 ug/kg dry 400 8260Ethyltertiarybutylether637-92-3 10/19/18ND B8J2913

3100 ug/kg dry 400 8260Hexachloroethane67-72-1 10/19/18ND B8J2913

620 ug/kg dry 400 8260Hexane110-54-3 10/19/1856000 B8J2913

620 ug/kg dry 400 8260Isopropylbenzene98-82-8 10/19/1811000 B8J2913

1200 ug/kg dry 400 8260m & p - Xylene1330-20-7 10/19/183800 B8J2913

1200 ug/kg dry 400 8260Methylene chloride75-09-2 10/19/18ND B8J2913

620 ug/kg dry 400 8260Methyltertiarybutylether1634-04-4 10/19/18ND B8J2913

3100 Xug/kg dry 400 8260Naphthalene91-20-3 10/19/1842000 B8J2913

620 ug/kg dry 400 8260n-Butylbenzene104-51-8 10/19/1818000 B8J2913

620 ug/kg dry 400 8260n-Propylbenzene103-65-1 10/19/1847000 B8J2913

620 ug/kg dry 400 8260o-Xylene95-47-6 10/19/18ND B8J2913

620 ug/kg dry 400 8260sec-Butylbenzene135-98-8 10/19/185600 B8J2913

620 ug/kg dry 400 8260Styrene100-42-5 10/19/18ND B8J2913

620 ug/kg dry 400 8260tert-Butylbenzene98-06-6 10/19/18ND B8J2913

31000 ug/kg dry 400 8260tertiary Butyl Alcohol75-65-0 10/19/18ND B8J2913

3100 ug/kg dry 400 8260tertiaryAmylmethylether994-05-8 10/19/18ND B8J2913

620 ug/kg dry 400 8260Tetrachloroethylene127-18-4 10/19/18ND B8J2913

3100 ug/kg dry 400 8260Tetrahydrofuran109-99-9 10/19/18ND B8J2913

620 ug/kg dry 400 8260Toluene108-88-3 10/19/18ND B8J2913

620 ug/kg dry 400 8260trans-1,2-Dichloroethylene156-60-5 10/19/18ND B8J2913

620 ug/kg dry 400 8260trans-1,3-Dichloropropylene10061-02-6 10/19/18ND B8J2913

620 ug/kg dry 400 8260Trichloroethylene79-01-6 10/19/18ND B8J2913

620 ug/kg dry 400 8260Trichlorofluoromethane75-69-4 10/19/18ND B8J2913

620 ug/kg dry 400 8260Vinyl chloride75-01-4 10/19/18ND B8J2913

V40.3-194Not ApplicableSurrogate: Bromofluorobenzene 826010/19/18 B8J2913

V52.1-217Not ApplicableSurrogate: Dibromofluoromethane 826010/19/18 B8J2913

V55.4-196Not ApplicableSurrogate: Toluene-d8 826010/19/18 B8J2913

Page 10 of 104Page 10 of 105

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1810151-02

RLCAS #

Client ID: SB1 (3.5-4)

QC Batch

Organics-Semivolatiles See note Y17, Y20

500 ug/kg dry 1 82701,2,4-Trichlorobenzene120-82-1 10/24/18ND B8J2215

830 ug/kg dry 1 82702,4,5-Trichlorophenol95-95-4 10/24/18ND B8J2215

830 ug/kg dry 1 82702,4,6-Trichlorophenol88-06-2 10/24/18ND B8J2215

830 ug/kg dry 1 82702,4-Dichlorophenol120-83-2 10/24/18ND B8J2215

830 ug/kg dry 1 82702,4-Dimethylphenol105-67-9 10/24/18ND B8J2215

4300 ug/kg dry 1 82702,4-Dinitrophenol51-28-5 10/24/18ND B8J2215

630 ug/kg dry 1 82702,4-Dinitrotoluene121-14-2 10/24/18ND B8J2215

630 ug/kg dry 1 82702,6-Dinitrotoluene606-20-2 10/24/18ND B8J2215

500 ug/kg dry 1 82702-Chloronaphthalene91-58-7 10/24/18ND B8J2215

830 ug/kg dry 1 82702-Chlorophenol95-57-8 10/24/18ND B8J2215

4300 ug/kg dry 1 82702-Methyl-4,6-dinitrophenol534-52-1 10/24/18ND B8J2215

6300 ug/kg dry 10 82702-Methylnaphthalene91-57-6 10/26/1838000 B8J2215

830 ug/kg dry 1 82702-Methylphenol (o-Cresol)95-48-7 10/24/18ND B8J2215

1300 ug/kg dry 1 82702-Nitroaniline88-74-4 10/24/18ND B8J2215

830 ug/kg dry 1 82702-Nitrophenol88-75-5 10/24/18ND B8J2215

1700 ug/kg dry 1 82703 & 4-Methylphenol108394,106445 10/24/18ND B8J2215

1300 ug/kg dry 1 82703-Nitroaniline99-09-2 10/24/18ND B8J2215

500 ug/kg dry 1 82704-Bromophenyl phenyl ether101-55-3 10/24/18ND B8J2215

500 ug/kg dry 1 82704-Chloro-3-methyl-phenol59-50-7 10/24/18ND B8J2215

250 ug/kg dry 1 82704-Chlorodiphenylether7005-72-3 10/24/18ND B8J2215

1300 ug/kg dry 1 82704-Nitroaniline100-01-6 10/24/18ND B8J2215

4300 A05ug/kg dry 1 82704-Nitrophenol100-02-7 10/24/18ND B8J2215

250 ug/kg dry 1 8270Acenaphthene83-32-9 10/24/18ND B8J2215

250 ug/kg dry 1 8270Acenaphthylene208-96-8 10/24/18ND B8J2215

250 ug/kg dry 1 8270Anthracene120-12-7 10/24/18ND B8J2215

500 ug/kg dry 1 8270Azobenzene103-33-3 10/24/18ND B8J2215

250 ug/kg dry 1 8270Benz[a]anthracene56-55-3 10/24/18ND B8J2215

500 ug/kg dry 1 8270Benzo[a]pyrene50-32-8 10/24/18ND B8J2215

500 ug/kg dry 1 8270Benzo[b]fluoranthene205-99-2 10/24/18ND B8J2215

500 ug/kg dry 1 8270Benzo[g,h,i]perylene191-24-2 10/24/18ND B8J2215

500 ug/kg dry 1 8270Benzo[k]fluoranthene207-08-9 10/24/18ND B8J2215

6300 ug/kg dry 1 8270Benzyl Alcohol100-51-6 10/24/18ND B8J2215

500 ug/kg dry 1 8270Bis(2-chloroethoxy)methane111-91-1 10/24/18ND B8J2215

250 ug/kg dry 1 8270Bis(2-chloroethyl)ether111-44-4 10/24/18ND B8J2215

250 A05ug/kg dry 1 8270Bis(2-chloroisopropyl)ether108-60-1 10/24/18ND B8J2215

630 ug/kg dry 1 8270Bis(2-ethylhexyl)phthalate117-81-7 10/24/18ND B8J2215

630 ug/kg dry 1 8270Butyl benzyl phthalate85-68-7 10/24/18ND B8J2215

630 ug/kg dry 1 8270Carbazole86-74-8 10/24/18ND B8J2215

250 ug/kg dry 1 8270Chrysene218-01-9 10/24/18ND B8J2215

500 ug/kg dry 1 8270Dibenz[a,h]anthracene53-70-3 10/24/18ND B8J2215

Page 11 of 104Page 11 of 105

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1810151-02

RLCAS #

Client ID: SB1 (3.5-4)

QC Batch

Organics-Semivolatiles See note Y17, Y20

630 ug/kg dry 1 8270Dibenzofuran132-64-9 10/24/18ND B8J2215

630 ug/kg dry 1 8270Diethylphthalate84-66-2 10/24/18ND B8J2215

630 ug/kg dry 1 8270Dimethyl phthalate131-11-3 10/24/18ND B8J2215

630 ug/kg dry 1 8270Di-n-butyl phthalate84-74-2 10/24/18ND B8J2215

630 ug/kg dry 1 8270Di-n-octyl phthalate117-84-0 10/24/18ND B8J2215

250 ug/kg dry 1 8270Fluoranthene206-44-0 10/24/18300 B8J2215

250 ug/kg dry 1 8270Fluorene86-73-7 10/24/18ND B8J2215

500 ug/kg dry 1 8270Hexachlorobenzene118-74-1 10/24/18ND B8J2215

250 ug/kg dry 1 8270Hexachlorobutadiene87-68-3 10/24/18ND B8J2215

2500 ug/kg dry 1 8270Hexachlorocyclopentadiene77-47-4 10/24/18ND B8J2215

250 ug/kg dry 1 8270Hexachloroethane67-72-1 10/24/18ND B8J2215

500 ug/kg dry 1 8270Indeno(1,2,3-c,d)pyrene193-39-5 10/24/18ND B8J2215

250 ug/kg dry 1 8270Isophorone78-59-1 10/24/18ND B8J2215

2500 ug/kg dry 10 8270Naphthalene91-20-3 10/26/1831000 B8J2215

500 ug/kg dry 1 8270Nitrobenzene98-95-3 10/24/18ND B8J2215

630 ug/kg dry 1 8270N-Nitrosodimethylamine67-75-9 10/24/18ND B8J2215

500 ug/kg dry 1 8270N-Nitrosodi-n-propylamine621-64-7 10/24/18ND B8J2215

500 ug/kg dry 1 8270N-Nitrosodiphenylamine86-30-6 10/24/18ND B8J2215

4300 ug/kg dry 1 8270Pentachlorophenol87-86-5 10/24/18ND B8J2215

250 ug/kg dry 1 8270Phenanthrene85-01-8 10/24/18560 B8J2215

830 ug/kg dry 1 8270Phenol108-95-2 10/24/18ND B8J2215

250 ug/kg dry 1 8270Pyrene129-00-0 10/24/18370 B8J2215

20.3-11592.6 %Surrogate: 2,4,6-Tribromophenol 827010/24/18 B8J2215

32.9-11567.2 %Surrogate: 2-Fluorobiphenyl 827010/24/18 B8J2215

23.7-11563.4 %Surrogate: 2-Fluorophenol 827010/24/18 B8J2215

31.8-11569.1 %Surrogate: Nitrobenzene-d5 827010/24/18 B8J2215

29.3-11571.6 %Surrogate: Phenol-d6 827010/24/18 B8J2215

38.5-11585.8 %Surrogate: p-Terphenyl-d14 827010/24/18 B8J2215

Page 12 of 104Page 12 of 105

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1810151-02

RLCAS #

Client ID: SB1 (3.5-4)

QC Batch

Inorganics-General Chemistry

0.1 N% 1 2540 B% Total SolidsTS 10/23/1879.2 B8J1904

Page 13 of 104Page 13 of 105

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1810151-03

RLCAS #

Client ID: SB1 (15.5-16)

QC Batch

Organics-Volatiles

64 ug/kg dry 50 82601,1,1,2-Tetrachloroethane630-20-6 10/18/18ND B8J1812

64 ug/kg dry 50 82601,1,1-Trichloroethane71-55-6 10/18/18ND B8J1812

64 ug/kg dry 50 82601,1,2,2-Tetrachloroethane79-34-5 10/18/18ND B8J1812

64 ug/kg dry 50 82601,1,2-Trichloroethane79-00-5 10/18/18ND B8J1812

64 ug/kg dry 50 82601,1-Dichloroethane75-34-3 10/18/18ND B8J1812

64 ug/kg dry 50 82601,1-Dichloroethylene75-35-4 10/18/18ND B8J1812

320 ug/kg dry 50 82601,2,3-Trichlorobenzene87-61-6 10/18/18ND B8J1812

64 A05ug/kg dry 50 82601,2,3-Trichloropropane96-18-4 10/18/18ND B8J1812

64 ug/kg dry 50 82601,2,3-Trimethylbenzene526-73-8 10/18/18ND B8J1812

320 ug/kg dry 50 82601,2,4-Trichlorobenzene120-82-1 10/18/18ND B8J1812

64 ug/kg dry 50 82601,2,4-Trimethylbenzene95-63-6 10/18/18ND B8J1812

64 ug/kg dry 50 82601,2-Dibromoethane106-93-4 10/18/18ND B8J1812

64 ug/kg dry 50 82601,2-Dichlorobenzene95-50-1 10/18/18ND B8J1812

64 ug/kg dry 50 82601,2-Dichloroethane107-06-2 10/18/18ND B8J1812

64 ug/kg dry 50 82601,2-Dichloropropane78-87-5 10/18/18ND B8J1812

64 ug/kg dry 50 82601,3,5-Trimethylbenzene108-67-8 10/18/18ND B8J1812

64 ug/kg dry 50 82601,3-Dichlorobenzene541-73-1 10/18/18ND B8J1812

64 ug/kg dry 50 82601,4-Dichlorobenzene106-46-7 10/18/18ND B8J1812

320 ug/kg dry 50 82602,2,4-Trimethylpentane540-84-1 10/18/18ND B8J1812

320 ug/kg dry 50 82602-Butanone (MEK)78-93-3 10/18/18ND B8J1812

320 Xug/kg dry 50 82602-Methylnaphthalene91-57-6 10/18/18ND B8J1812

1300 ug/kg dry 50 82602-Propanone (acetone)67-64-1 10/18/18ND B8J1812

320 ug/kg dry 50 82604-Methyl-2-pentanone (MIBK)108-10-1 10/18/18ND B8J1812

320 ug/kg dry 50 8260Acrylonitrile107-13-1 10/18/18ND B8J1812

64 ug/kg dry 50 8260Benzene71-43-2 10/18/18ND B8J1812

64 ug/kg dry 50 8260Bromochloromethane74-97-5 10/18/18ND B8J1812

64 ug/kg dry 50 8260Bromodichloromethane75-27-4 10/18/18ND B8J1812

64 ug/kg dry 50 8260Bromoform75-25-2 10/18/18ND B8J1812

260 ug/kg dry 50 8260Bromomethane74-83-9 10/18/18ND B8J1812

64 ug/kg dry 50 8260Carbon disulfide75-15-0 10/18/18ND B8J1812

64 ug/kg dry 50 8260Carbon tetrachloride56-23-5 10/18/18ND B8J1812

64 ug/kg dry 50 8260Chlorobenzene108-90-7 10/18/18ND B8J1812

320 ug/kg dry 50 8260Chloroethane75-00-3 10/18/18ND B8J1812

64 ug/kg dry 50 8260Chloroform67-66-3 10/18/18ND B8J1812

320 ug/kg dry 50 8260Chloromethane74-87-3 10/18/18ND B8J1812

64 ug/kg dry 50 8260cis-1,2-Dichloroethylene156-59-2 10/18/18ND B8J1812

64 ug/kg dry 50 8260cis-1,3-Dichloropropylene10061-01-5 10/18/18ND B8J1812

320 ug/kg dry 50 8260Cyclohexane110-82-7 10/18/18ND B8J1812

64 ug/kg dry 50 8260Dibromochloromethane124-48-1 10/18/18ND B8J1812

64 ug/kg dry 50 8260Dibromomethane74-95-3 10/18/18ND B8J1812

Page 14 of 104Page 14 of 105

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1810151-03

RLCAS #

Client ID: SB1 (15.5-16)

QC Batch

Organics-Volatiles

320 ug/kg dry 50 8260Dichlorodifluoromethane75-71-8 10/18/18ND B8J1812

260 ug/kg dry 50 8260Diethyl ether60-29-7 10/18/18ND B8J1812

320 ug/kg dry 50 8260Diisopropyl Ether108-20-3 10/18/18ND B8J1812

64 ug/kg dry 50 8260Ethylbenzene100-41-4 10/18/18ND B8J1812

320 ug/kg dry 50 8260Ethyltertiarybutylether637-92-3 10/18/18ND B8J1812

320 ug/kg dry 50 8260Hexachloroethane67-72-1 10/18/18ND B8J1812

64 ug/kg dry 50 8260Hexane110-54-3 10/18/18ND B8J1812

64 ug/kg dry 50 8260Isopropylbenzene98-82-8 10/18/18ND B8J1812

130 ug/kg dry 50 8260m & p - Xylene1330-20-7 10/18/18ND B8J1812

130 ug/kg dry 50 8260Methylene chloride75-09-2 10/18/18ND B8J1812

64 ug/kg dry 50 8260Methyltertiarybutylether1634-04-4 10/18/18ND B8J1812

320 Xug/kg dry 50 8260Naphthalene91-20-3 10/18/18ND B8J1812

64 ug/kg dry 50 8260n-Butylbenzene104-51-8 10/18/18ND B8J1812

64 ug/kg dry 50 8260n-Propylbenzene103-65-1 10/18/18ND B8J1812

64 ug/kg dry 50 8260o-Xylene95-47-6 10/18/18ND B8J1812

64 ug/kg dry 50 8260sec-Butylbenzene135-98-8 10/18/18ND B8J1812

64 ug/kg dry 50 8260Styrene100-42-5 10/18/18ND B8J1812

64 ug/kg dry 50 8260tert-Butylbenzene98-06-6 10/18/18ND B8J1812

3200 ug/kg dry 50 8260tertiary Butyl Alcohol75-65-0 10/18/18ND B8J1812

320 ug/kg dry 50 8260tertiaryAmylmethylether994-05-8 10/18/18ND B8J1812

64 ug/kg dry 50 8260Tetrachloroethylene127-18-4 10/18/18ND B8J1812

320 ug/kg dry 50 8260Tetrahydrofuran109-99-9 10/18/18ND B8J1812

64 ug/kg dry 50 8260Toluene108-88-3 10/18/18ND B8J1812

64 ug/kg dry 50 8260trans-1,2-Dichloroethylene156-60-5 10/18/18ND B8J1812

64 ug/kg dry 50 8260trans-1,3-Dichloropropylene10061-02-6 10/18/18ND B8J1812

64 ug/kg dry 50 8260Trichloroethylene79-01-6 10/18/18ND B8J1812

64 ug/kg dry 50 8260Trichlorofluoromethane75-69-4 10/18/18ND B8J1812

64 ug/kg dry 50 8260Vinyl chloride75-01-4 10/18/18ND B8J1812

40.3-19488.4 %Surrogate: Bromofluorobenzene 826010/18/18 B8J1812

52.1-21792.7 %Surrogate: Dibromofluoromethane 826010/18/18 B8J1812

55.4-19691.1 %Surrogate: Toluene-d8 826010/18/18 B8J1812

Page 15 of 104Page 15 of 105

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1810151-03

RLCAS #

Client ID: SB1 (15.5-16)

QC Batch

Organics-Semivolatiles See note Y20

450 ug/kg dry 1 82701,2,4-Trichlorobenzene120-82-1 10/24/18ND B8J2215

740 ug/kg dry 1 82702,4,5-Trichlorophenol95-95-4 10/24/18ND B8J2215

740 ug/kg dry 1 82702,4,6-Trichlorophenol88-06-2 10/24/18ND B8J2215

740 ug/kg dry 1 82702,4-Dichlorophenol120-83-2 10/24/18ND B8J2215

740 ug/kg dry 1 82702,4-Dimethylphenol105-67-9 10/24/18ND B8J2215

3800 ug/kg dry 1 82702,4-Dinitrophenol51-28-5 10/24/18ND B8J2215

560 ug/kg dry 1 82702,4-Dinitrotoluene121-14-2 10/24/18ND B8J2215

560 ug/kg dry 1 82702,6-Dinitrotoluene606-20-2 10/24/18ND B8J2215

450 ug/kg dry 1 82702-Chloronaphthalene91-58-7 10/24/18ND B8J2215

740 ug/kg dry 1 82702-Chlorophenol95-57-8 10/24/18ND B8J2215

3800 ug/kg dry 1 82702-Methyl-4,6-dinitrophenol534-52-1 10/24/18ND B8J2215

560 ug/kg dry 1 82702-Methylnaphthalene91-57-6 10/24/18ND B8J2215

740 ug/kg dry 1 82702-Methylphenol (o-Cresol)95-48-7 10/24/18ND B8J2215

1100 ug/kg dry 1 82702-Nitroaniline88-74-4 10/24/18ND B8J2215

740 ug/kg dry 1 82702-Nitrophenol88-75-5 10/24/18ND B8J2215

1500 ug/kg dry 1 82703 & 4-Methylphenol108394,106445 10/24/18ND B8J2215

1100 ug/kg dry 1 82703-Nitroaniline99-09-2 10/24/18ND B8J2215

450 ug/kg dry 1 82704-Bromophenyl phenyl ether101-55-3 10/24/18ND B8J2215

450 ug/kg dry 1 82704-Chloro-3-methyl-phenol59-50-7 10/24/18ND B8J2215

230 ug/kg dry 1 82704-Chlorodiphenylether7005-72-3 10/24/18ND B8J2215

1100 ug/kg dry 1 82704-Nitroaniline100-01-6 10/24/18ND B8J2215

3800 A05ug/kg dry 1 82704-Nitrophenol100-02-7 10/24/18ND B8J2215

230 ug/kg dry 1 8270Acenaphthene83-32-9 10/24/18ND B8J2215

230 ug/kg dry 1 8270Acenaphthylene208-96-8 10/24/18ND B8J2215

230 ug/kg dry 1 8270Anthracene120-12-7 10/24/18ND B8J2215

450 ug/kg dry 1 8270Azobenzene103-33-3 10/24/18ND B8J2215

230 ug/kg dry 1 8270Benz[a]anthracene56-55-3 10/24/18ND B8J2215

450 ug/kg dry 1 8270Benzo[a]pyrene50-32-8 10/24/18ND B8J2215

450 ug/kg dry 1 8270Benzo[b]fluoranthene205-99-2 10/24/18ND B8J2215

450 ug/kg dry 1 8270Benzo[g,h,i]perylene191-24-2 10/24/18ND B8J2215

450 ug/kg dry 1 8270Benzo[k]fluoranthene207-08-9 10/24/18ND B8J2215

5600 ug/kg dry 1 8270Benzyl Alcohol100-51-6 10/24/18ND B8J2215

450 ug/kg dry 1 8270Bis(2-chloroethoxy)methane111-91-1 10/24/18ND B8J2215

230 ug/kg dry 1 8270Bis(2-chloroethyl)ether111-44-4 10/24/18ND B8J2215

230 A05ug/kg dry 1 8270Bis(2-chloroisopropyl)ether108-60-1 10/24/18ND B8J2215

560 ug/kg dry 1 8270Bis(2-ethylhexyl)phthalate117-81-7 10/24/18ND B8J2215

560 ug/kg dry 1 8270Butyl benzyl phthalate85-68-7 10/24/18ND B8J2215

560 ug/kg dry 1 8270Carbazole86-74-8 10/24/18ND B8J2215

230 ug/kg dry 1 8270Chrysene218-01-9 10/24/18ND B8J2215

450 ug/kg dry 1 8270Dibenz[a,h]anthracene53-70-3 10/24/18ND B8J2215

Page 16 of 104Page 16 of 105

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1810151-03

RLCAS #

Client ID: SB1 (15.5-16)

QC Batch

Organics-Semivolatiles See note Y20

560 ug/kg dry 1 8270Dibenzofuran132-64-9 10/24/18ND B8J2215

560 ug/kg dry 1 8270Diethylphthalate84-66-2 10/24/18ND B8J2215

560 ug/kg dry 1 8270Dimethyl phthalate131-11-3 10/24/18ND B8J2215

560 ug/kg dry 1 8270Di-n-butyl phthalate84-74-2 10/24/18ND B8J2215

560 ug/kg dry 1 8270Di-n-octyl phthalate117-84-0 10/24/18ND B8J2215

230 ug/kg dry 1 8270Fluoranthene206-44-0 10/24/18ND B8J2215

230 ug/kg dry 1 8270Fluorene86-73-7 10/24/18ND B8J2215

450 ug/kg dry 1 8270Hexachlorobenzene118-74-1 10/24/18ND B8J2215

230 ug/kg dry 1 8270Hexachlorobutadiene87-68-3 10/24/18ND B8J2215

2300 ug/kg dry 1 8270Hexachlorocyclopentadiene77-47-4 10/24/18ND B8J2215

230 ug/kg dry 1 8270Hexachloroethane67-72-1 10/24/18ND B8J2215

450 ug/kg dry 1 8270Indeno(1,2,3-c,d)pyrene193-39-5 10/24/18ND B8J2215

230 ug/kg dry 1 8270Isophorone78-59-1 10/24/18ND B8J2215

230 ug/kg dry 1 8270Naphthalene91-20-3 10/24/18ND B8J2215

450 ug/kg dry 1 8270Nitrobenzene98-95-3 10/24/18ND B8J2215

560 ug/kg dry 1 8270N-Nitrosodimethylamine67-75-9 10/24/18ND B8J2215

450 ug/kg dry 1 8270N-Nitrosodi-n-propylamine621-64-7 10/24/18ND B8J2215

450 ug/kg dry 1 8270N-Nitrosodiphenylamine86-30-6 10/24/18ND B8J2215

3800 ug/kg dry 1 8270Pentachlorophenol87-86-5 10/24/18ND B8J2215

230 ug/kg dry 1 8270Phenanthrene85-01-8 10/24/18ND B8J2215

740 ug/kg dry 1 8270Phenol108-95-2 10/24/18ND B8J2215

230 ug/kg dry 1 8270Pyrene129-00-0 10/24/18ND B8J2215

20.3-115104 %Surrogate: 2,4,6-Tribromophenol 827010/24/18 B8J2215

32.9-11585.0 %Surrogate: 2-Fluorobiphenyl 827010/24/18 B8J2215

23.7-11576.8 %Surrogate: 2-Fluorophenol 827010/24/18 B8J2215

31.8-11579.2 %Surrogate: Nitrobenzene-d5 827010/24/18 B8J2215

29.3-11573.3 %Surrogate: Phenol-d6 827010/24/18 B8J2215

38.5-115101 %Surrogate: p-Terphenyl-d14 827010/24/18 B8J2215

Page 17 of 104Page 17 of 105

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1810151-03

RLCAS #

Client ID: SB1 (15.5-16)

QC Batch

Inorganics-General Chemistry

0.1 % 1 2540 B% Total SolidsTS 10/23/1888.7 B8J1904

Page 18 of 104Page 18 of 105

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1810151-04

RLCAS #

Client ID: SB2 (3-3.5)

QC Batch

Organics-Volatiles

61 ug/kg dry 50 82601,1,1,2-Tetrachloroethane630-20-6 10/18/18ND B8J1812

61 ug/kg dry 50 82601,1,1-Trichloroethane71-55-6 10/18/18ND B8J1812

61 ug/kg dry 50 82601,1,2,2-Tetrachloroethane79-34-5 10/18/18ND B8J1812

61 ug/kg dry 50 82601,1,2-Trichloroethane79-00-5 10/18/18ND B8J1812

61 ug/kg dry 50 82601,1-Dichloroethane75-34-3 10/18/18ND B8J1812

61 ug/kg dry 50 82601,1-Dichloroethylene75-35-4 10/18/18ND B8J1812

300 ug/kg dry 50 82601,2,3-Trichlorobenzene87-61-6 10/18/18ND B8J1812

61 A05ug/kg dry 50 82601,2,3-Trichloropropane96-18-4 10/18/18ND B8J1812

61 ug/kg dry 50 82601,2,3-Trimethylbenzene526-73-8 10/18/18ND B8J1812

300 ug/kg dry 50 82601,2,4-Trichlorobenzene120-82-1 10/18/18ND B8J1812

61 ug/kg dry 50 82601,2,4-Trimethylbenzene95-63-6 10/18/18ND B8J1812

61 ug/kg dry 50 82601,2-Dibromoethane106-93-4 10/18/18ND B8J1812

61 ug/kg dry 50 82601,2-Dichlorobenzene95-50-1 10/18/18ND B8J1812

61 ug/kg dry 50 82601,2-Dichloroethane107-06-2 10/18/18ND B8J1812

61 ug/kg dry 50 82601,2-Dichloropropane78-87-5 10/18/18ND B8J1812

61 ug/kg dry 50 82601,3,5-Trimethylbenzene108-67-8 10/18/18ND B8J1812

61 ug/kg dry 50 82601,3-Dichlorobenzene541-73-1 10/18/18ND B8J1812

61 ug/kg dry 50 82601,4-Dichlorobenzene106-46-7 10/18/18ND B8J1812

300 ug/kg dry 50 82602,2,4-Trimethylpentane540-84-1 10/18/18ND B8J1812

300 ug/kg dry 50 82602-Butanone (MEK)78-93-3 10/18/18ND B8J1812

300 Xug/kg dry 50 82602-Methylnaphthalene91-57-6 10/18/18ND B8J1812

1200 ug/kg dry 50 82602-Propanone (acetone)67-64-1 10/18/18ND B8J1812

300 ug/kg dry 50 82604-Methyl-2-pentanone (MIBK)108-10-1 10/18/18ND B8J1812

300 ug/kg dry 50 8260Acrylonitrile107-13-1 10/18/18ND B8J1812

61 ug/kg dry 50 8260Benzene71-43-2 10/18/18ND B8J1812

61 ug/kg dry 50 8260Bromochloromethane74-97-5 10/18/18ND B8J1812

61 ug/kg dry 50 8260Bromodichloromethane75-27-4 10/18/18ND B8J1812

61 ug/kg dry 50 8260Bromoform75-25-2 10/18/18ND B8J1812

240 ug/kg dry 50 8260Bromomethane74-83-9 10/18/18ND B8J1812

61 ug/kg dry 50 8260Carbon disulfide75-15-0 10/18/18ND B8J1812

61 ug/kg dry 50 8260Carbon tetrachloride56-23-5 10/18/18ND B8J1812

61 ug/kg dry 50 8260Chlorobenzene108-90-7 10/18/18ND B8J1812

300 ug/kg dry 50 8260Chloroethane75-00-3 10/18/18ND B8J1812

61 ug/kg dry 50 8260Chloroform67-66-3 10/18/18ND B8J1812

300 ug/kg dry 50 8260Chloromethane74-87-3 10/18/18ND B8J1812

61 ug/kg dry 50 8260cis-1,2-Dichloroethylene156-59-2 10/18/18ND B8J1812

61 ug/kg dry 50 8260cis-1,3-Dichloropropylene10061-01-5 10/18/18ND B8J1812

300 ug/kg dry 50 8260Cyclohexane110-82-7 10/18/18ND B8J1812

61 ug/kg dry 50 8260Dibromochloromethane124-48-1 10/18/18ND B8J1812

61 ug/kg dry 50 8260Dibromomethane74-95-3 10/18/18ND B8J1812

Page 19 of 104Page 19 of 105

TEL: (517) 335-9800

FAX: (517) 335-9600

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY

ENVIRONMENTAL LABORATORY

ResultAnalyte

Analyzed

Date Method QualifierDilutionUnits

Lab ID: 1810151-04

RLCAS #

Client ID: SB2 (3-3.5)

QC Batch

Organics-Volatiles

300 ug/kg dry 50 8260Dichlorodifluoromethane75-71-8 10/18/18ND B8J1812

240 ug/kg dry 50 8260Diethyl ether60-29-7 10/18/18ND B8J1812

300 ug/kg dry 50 8260Diisopropyl Ether108-20-3 10/18/18ND B8J1812

61 ug/kg dry 50 8260Ethylbenzene100-41-4 10/18/18ND B8J1812

300 ug/kg dry 50 8260Ethyltertiarybutylether637-92-3 10/18/18ND B8J1812

300 ug/kg dry 50 8260Hexachloroethane67-72-1 10/18/18ND B8J1812

61 ug/kg dry 50 8260Hexane110-54-3 10/18/18ND B8J1812

61 ug/kg dry 50 8260Isopropylbenzene98-82-8 10/18/18ND B8J1812

120 ug/kg dry 50 8260m & p - Xylene1330-20-7 10/18/18ND B8J1812

120 ug/kg dry 50 8260Methylene chloride75-09-2 10/18/18ND B8J1812

61 ug/kg dry 50 8260Methyltertiarybutylether1634-04-4 10/18/18ND B8J1812

300 Xug/kg dry 50 8260Naphthalene91-20-3 10/18/18ND B8J1812

61 ug/kg dry 50 8260n-Butylbenzene104-51-8 10/18/18ND B8J1812

61 ug/kg dry 50 8260n-Propylbenzene103-65-1 10/18/18ND B8J1812

61 ug/kg dry 50 8260o-Xylene95-47-6 10/18/18ND B8J1812

61 ug/kg dry 50 8260sec-Butylbenzene135-98-8 10/18/18ND B8J1812

61 ug/kg dry 50 8260Styrene100-42-5 10/18/18ND B8J1812

61 ug/kg dry 50 8260tert-Butylbenzene98-06-6 10/18/18ND B8J1812

3000 ug/kg dry 50 8260tertiary Butyl Alcohol75-65-0 10/18/18ND B8J1812

300 ug/kg dry 50 8260tertiaryAmylmethylether994-05-8 10/18/18ND B8J1812

61 ug/kg dry 50 8260Tetrachloroethylene127-18-4 10/18/18ND B8J1812

300 ug/kg dry 50 8260Tetrahydrofuran109-99-9 10/18/18ND B8J1812

61 ug/kg dry 50 8260Toluene108-88-3 10/18/18ND B8J1812

61 ug/kg dry 50 8260trans-1,2-Dichloroethylene156-60-5 10/18/18ND B8J1812

61 ug/kg dry 50 8260trans-1,3-Dichloropropylene10061-02-6 10/18/18ND B8J1812

61 ug/kg dry 50 8260Trichloroethylene79-01-6 10/18/18ND B8J1812

61 ug/kg dry 50 8260Trichlorofluoromethane75-69-4 10/18/18ND B8J1812

61 ug/kg dry 50 8260Vinyl chloride75-01-4 10/18/18ND B8J1812

40.3-19495.2 %Surrogate: Bromofluorobenzene 826010/18/18 B8J1812

52.1-21791.6 %Surrogate: Dibromofluoromethane 826010/18/18 B8J1812

55.4-19691.2 %Surrogate: Toluene-d8 826010/18/18 B8J1812

Page 20 of 104Page 20 of 105