W912DS-16-B-0015_Sampling.pdf

E-5

E-4

E-3

E-2 E-1

OPC B-9

OPC B-8

OPC B-7

OPC B-6

OPC B-5

OPC B-4

OPC B-3

OPC B-2

OPC_B-1

OPC B-10

µ0 500 1,000250 Feet

Old Place Creek Environmental Sampling Locations

LOCATION OPC-B-1-SO-0.0-201311190922 OPC-B-1-SO-2.0-201311190925 OPC-B-1-SO-4.0-201311190935 OPC-B-1-SO-6.0-201311191020 OPC-B1-SO-COMP-10-201311191040 OPC-B1-SO-COMP-12-201311191055 OPC-B1-SO-COMP-14-201311191110 OPC-B1-SO-COMP-8-201311191030 OPC-B-3_ENV-SO-0.-201311191245 OPC-B-3_ENV-SO-10-201311191415 OPC-B-3_ENV-SO-12-201311191430 OPC-B-3_ENV-SO-14-201311191440 OPC-B-3_ENV-SO-2.-201311191255 OPC-B-3_ENV-SO-4.-201311191325 OPC-B-3_ENV-SO-6.-201311191340 OPC-B-3_ENV-SO-8.-201311191400 SAMPLING DATE 19-NOV-13 19-NOV-13 19-NOV-13 19-NOV-13 19-NOV-13 19-NOV-13 19-NOV-13 19-NOV-13 19-NOV-13 19-NOV-13 19-NOV-13 19-NOV-13 19-NOV-13 19-NOV-13 19-NOV-13 19-NOV-13 LAB SAMPLE ID L1323690-01 L1323690-02 L1323690-03 L1323690-04 L1323690-05 L1323690-06 L1323690-07 L1323690-08 L1323690-09 L1323690-10 L1323690-11 L1323690-12 L1323690-13 L1323690-14 L1323690-15 L1323690-16

Units Qual Qual Qual Qual Qual Qual Qual Qual Qual Qual Qual Qual Qual Qual Qual Qual

General Chemistry - Westborough Lab

Chromium, Trivalent mg/kg 23 39 100 23 30 16 8.8 40 18 6.1 9.4 10 38 8.2 8.3 6.6 Solids, Total % 77.3 72.3 33.7 18.5 43.4 51.2 77.4 44.6 41.4 81.6 86.2 83.7 21.6 54.7 79.1 83.4 Cyanide, Total mg/kg 5.5 U 10 U 4.4 U 3.6 U 2.4 U 4.3 U 4.6 U 2.3 U 2.2 U 1.1 U 4.3 U 1.8 U 1.2 U 1.1 U pH (H) SU 3.8 3.5 7.1 7.2 7.4 7.5 7.8 7.7 6 7.6 7.4 7.1 6.8 6.7 7.4 7.4 Chromium, Hexavalent mg/kg 1 U 1.1 U 2.4 U 4.3 U 1.8 U 1.6 U 1 U 1.8 U 1.9 U 0.98 U 0.93 U 0.96 U 3.7 U 1.5 U 1 U 0.96 U Chromium, SPLP Hexavalent mg/kg 0.01 U 0.004 J 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.005 J 0.005 J 0.005 J 0.01 U 0.01 U Cyanide, Reactive mg/kg 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U Sulfide, Reactive mg/kg 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U 10 U Ignitability of Solids - Westborough Lab

Ignitability - NI NI NI NI NI NI NI NI NI NI NI NI NI NI Total Metals - Westborough Lab

Aluminum, Total mg/kg 8000 8900 14000 8900 15000 7900 3600 16000 4700 2600 3900 4400 10000 5100 3600 2800 Antimony, Total mg/kg 0.52 J 0.97 5 0.69 J 0.33 J 0.17 J 0.1 J 0.4 J 0.81 J 0.08 J 0.12 J 0.24 J 7.1 0.16 J 0.11 J 0.1 J Arsenic, Total mg/kg 11 20 67 10 22 9.9 4 14 15 1.4 1.4 2.6 38 4.4 6.4 1.8 Barium, Total mg/kg 32 47 160 42 31 34 13 39 24 5.6 18 17 180 7.1 4 6.3 Beryllium, Total mg/kg 0.21 J 0.26 J 0.83 J 0.95 J 1.1 1 0.4 1.3 0.46 J 0.46 0.52 0.49 0.69 J 0.24 J 0.3 J 0.53 Boron, Total mg/kg 9.1 11 34 41 25 16 4.7 24 13 3.6 2.7 1.6 31 6.2 3.8 3.1 Cadmium, Total mg/kg 0.03 J 0.03 J 0.86 0.2 J 0.21 J 0.09 J 0.08 J 0.11 J 0.12 J 0.23 U 0.04 J 0.09 J 1.4 0.35 U 0.24 U 0.23 U Calcium, Total mg/kg 530 400 2400 3600 1800 1700 360 1700 1700 100 170 360 2500 700 170 120 Chromium, Total mg/kg 23 39 100 23 30 16 8.8 40 18 6.1 9.4 10 38 8.2 8.3 6.6 Cobalt, Total mg/kg 3.6 4.1 11 7.3 26 8.2 2.2 14 2.8 2.2 3.9 7.5 6.4 2.3 2.6 3.6 Copper, Total mg/kg 25 42 270 17 17 10 6 26 37 4 7.4 9.7 100 5.6 4.7 4.8 Iron, Total mg/kg 31000 30000 20000 18000 42000 29000 6400 33000 11000 4300 6100 6600 16000 12000 8900 5500 Lead, Total mg/kg 27 71 190 16 15 8.1 4.5 25 35 2.9 5.9 6.8 90 5.9 4.3 3.2 Magnesium, Total mg/kg 2800 3100 6300 6300 6200 3300 1300 7100 2500 720 1400 1800 5500 1200 770 850 Manganese, Total mg/kg 99 100 400 200 350 180 48 610 50 18 53 72 100 39 30 27 Mercury, Total mg/kg 0.05 J 0.43 3.6 0.42 U 0.15 U 0.14 U 0.09 U 0.14 J 0.26 0.08 U 0.09 U 0.09 U 0.36 0.04 J 0.08 U 0.08 U Nickel, Total mg/kg 11 13 42 19 29 12 5.4 32 9.9 3.7 8.3 15 39 4.5 4.4 4.6 Potassium, Total mg/kg 3600 3100 2800 2100 2600 1200 560 3000 950 510 530 460 2400 580 530 500 Selenium, Total mg/kg 0.84 J 1.2 J 4.9 J 1.3 J 1.4 J 0.99 J 0.28 J 1.3 J 1.2 J 0.16 J 0.33 J 0.79 J 2.6 J 0.73 J 0.36 J 0.22 J Silver, Total mg/kg 0.29 J 0.34 J 0.99 J 0.28 J 0.14 J 0.17 J 0.04 J 0.13 J 0.25 J 0.57 U 0.54 U 0.58 U 0.44 J 0.06 J 0.61 U 0.58 U Sodium, Total mg/kg 1400 2400 11000 24000 8100 6600 1800 7300 8900 980 650 610 16000 4000 1200 1100 Thallium, Total mg/kg 0.12 J 0.14 J 0.22 J 0.11 J 0.15 J 0.07 J 0.04 J 0.15 J 0.06 J 0.02 J 0.03 J 0.03 J 0.4 J 0.11 J 0.04 J 0.02 J Vanadium, Total mg/kg 44 46 56 31 46 30 12 48 21 13 17 17 44 12 12 13 Zinc, Total mg/kg 46 44 190 60 81 35 23 96 33 18 30 42 160 13 J 17 22 TCLP Metals by EPA 1311 - Westborough Lab

Arsenic, TCLP mg/l 0.1 J 1 U 0.03 J 1 U 1 U 1 U 1 U 1 U 1 U 1 U 0.1 J 1 U 0.05 J 1 U Barium, TCLP mg/l 0.2 J 0.17 J 0.11 J 0.12 J 0.11 J 0.09 J 0.11 J 0.1 J 0.24 J 0.17 J 0.23 J 0.13 J 0.1 J 0.15 J Cadmium, TCLP mg/l 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U Chromium, TCLP mg/l 0.2 U 0.2 U 0.2 U 0.2 U 0.2 U 0.2 U 0.2 U 0.2 U 0.2 U 0.2 U 0.2 U 0.04 J 0.2 U 0.2 U Lead, TCLP mg/l 0.05 J 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.04 J 0.03 J 0.5 U 0.5 U 0.02 J 0.5 U 0.02 J Mercury, TCLP mg/l 0.001 U 0.001 U 0.001 U 0.001 U 0.001 U 0.001 U 0.001 U 0.001 U 0.001 U 0.001 U 0.001 U 0.001 U 0.001 U 0.001 U Selenium, TCLP mg/l 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U Silver, TCLP mg/l 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U 0.1 U SPLP Metals by EPA 1312 - Westborough Lab

Aluminum, SPLP mg/kg 0.748 2.26 1.04 3.92 1.32 6.84 3.15 0.949 23.4 7.29 7.07 1.58 2.92 3.28 7.77 Antimony, SPLP mg/kg 0.0145 J 0.0115 J 0.05 U 0.05 U 0.05 U 0.05 U 0.0121 J 0.05 U 0.05 U 0.05 U 0.05 U 0.0169 J 0.05 U 0.05 U 0.05 U Arsenic, SPLP mg/kg 0.005 U 0.0237 0.005 U 0.005 U 0.005 U 0.0039 J 0.005 U 0.005 U 0.0056 0.005 0.0061 0.0389 0.005 U 0.005 U 0.005 U Barium, SPLP mg/kg 0.0357 0.0833 0.0936 0.0757 0.0487 0.0725 0.0703 J 0.0777 0.209 0.0761 0.0667 0.0809 0.0542 0.0219 0.0469 Beryllium, SPLP mg/kg 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.0036 J 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.002 J Boron, SPLP mg/kg 0.343 0.468 0.378 0.638 0.464 0.287 0.61 0.283 0.144 0.19 0.173 0.247 0.199 0.202 0.146 Cadmium, SPLP mg/kg 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U Calcium, SPLP mg/kg 2.75 4.98 4.44 4.66 3.93 1.98 5.39 4.51 2.03 1.87 1.94 3.44 4.32 2.27 3.02 Chromium, SPLP mg/kg 0.0054 J 0.016 0.004 J 0.01 0.0043 J 0.01 0.0077 J 0.0039 J 0.042 0.016 0.015 0.0032 J 0.0046 J 0.0086 J 0.016 Cobalt, SPLP mg/kg 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.011 0.01 U 0.005 J 0.01 U 0.01 U 0.01 U 0.006 J Copper, SPLP mg/kg 0.0095 J 0.0306 0.004 J 0.0037 J 0.0034 J 0.0102 0.0042 J 0.0121 0.045 0.03 0.0236 0.0089 J 0.01 U 0.0037 J 0.0278 Iron, SPLP mg/kg 1.35 1.58 0.553 B 2.99 0.713 3.29 2.62 1.39 19.4 5.92 6.18 0.832 2.3 2.96 6.26 Lead, SPLP mg/kg 0.0051 J 0.0195 0.0034 J 0.0043 J 0.0038 J 0.0055 J 0.0026 J 0.0048 J 0.0235 0.0147 0.0145 0.006 J 0.0023 J 0.0041 J 0.0122 Magnesium, SPLP mg/kg 4.01 11.4 12.5 8.76 8.54 3 9.77 11.9 6.82 4.21 4.29 10.3 11.2 3.96 7.84 Manganese, SPLP mg/kg 0.0031 J 0.0161 0.0082 J 0.0323 0.0063 J 0.0128 0.0296 0.0046 J 0.0595 0.0209 0.026 0.0029 J 0.0072 J 0.0059 J 0.0261 Mercury, SPLP mg/kg 0.001 U 0.001 U 0.001 U 0.001 U 0.001 U 0.001 U 0.001 U 0.001 U 0.001 U 0.001 U 0.001 U 0.001 U 0.001 U 0.001 U 0.001 U Nickel, SPLP mg/kg 0.0053 J 0.0076 J 0.0044 J 0.0057 J 0.025 U 0.0047 J 0.0041 J 0.025 U 0.0226 J 0.0067 J 0.0113 J 0.025 U 0.025 U 0.025 U 0.0072 J Potassium, SPLP mg/kg 4.86 9.3 9.05 13 9.07 5.38 13.6 9.9 7.45 6.46 5.7 8.14 5.97 4.07 5.8 Selenium, SPLP mg/kg 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U Silver, SPLP mg/kg 0.007 U 0.007 U 0.007 U 0.007 U 0.007 U 0.007 U 0.007 U 0.007 U 0.007 U 0.007 U 0.007 U 0.007 U 0.007 U 0.007 U 0.007 U Sodium, SPLP mg/kg 80.5 186 220 189 157 77.8 202 185 55.2 84.5 84.5 160 124 53.4 90.3 Thallium, SPLP mg/kg 0.02 U 0.02 U 0.0042 J 0.02 U 0.02 U 0.0044 J 0.02 U 0.02 U 0.02 U 0.02 U 0.02 U 0.02 U 0.02 U 0.02 U 0.02 U Vanadium, SPLP mg/kg 0.0025 J 0.0199 0.0224 0.0133 0.0206 0.0823 0.0084 J 0.0049 J 0.162 0.0854 0.0841 0.073 0.0092 J 0.0179 0.0937 Zinc, SPLP mg/kg 0.0207 J 0.0312 J 0.0197 J 0.029 J 0.0132 J 0.0358 J 0.0262 J 0.0142 J 0.144 0.0472 J 0.0537 0.0147 J 0.0174 J 0.0128 J 0.0604 TCLP Pesticides by EPA 1311 - Westborough Lab

Chlordane mg/l 0.001 U 0.001 U 0.001 U 0.001 U 0.001 U 0.001 U 0.001 U 0.001 U 0.001 U 0.001 U 0.001 U 0.001 U 0.001 U 0.001 U Endrin mg/l 0.0002 U 0.0002 U 0.0002 U 0.0002 U 0.0002 U 0.0002 U 0.0002 U 0.0002 U 0.0002 U 0.0002 U 0.0002 U 0.0002 U 0.0002 U 0.0002 U Heptachlor mg/l 0.0001 U 0.0001 U 0.0001 U 0.0001 U 0.0001 U 0.0001 U 0.0001 U 0.0001 U 0.0001 U 0.0001 U 0.0001 U 0.0001 U 0.0001 U 0.0001 U Heptachlor epoxide mg/l 0.0001 U 0.0001 U 0.0001 U 0.0001 U 0.0001 U 0.0001 U 0.0001 U 0.0001 U 0.0001 U 0.0001 U 0.0001 U 0.0001 U 0.0001 U 0.0001 U Lindane mg/l 0.0001 U 0.0001 U 0.0001 U 0.0001 U 0.0001 U 0.0001 U 0.0001 U 0.0001 U 0.0001 U 0.0001 U 0.0001 U 0.0001 U 0.0001 U 0.0001 U Methoxychlor mg/l 0.001 U 0.001 U 0.001 U 0.001 U 0.001 U 0.001 U 0.001 U 0.001 U 0.001 U 0.001 U 0.001 U 0.001 U 0.001 U 0.001 U Toxaphene mg/l 0.001 U 0.001 U 0.001 U 0.001 U 0.001 U 0.001 U 0.001 U 0.001 U 0.001 U 0.001 U 0.001 U 0.001 U 0.001 U 0.001 U Chlorinated Herbicides by GC - Westborough Lab

2,4,5-T mg/kg 0.212 U 0.225 U 0.479 U 0.874 U 0.377 U 0.322 U 0.212 U 0.363 U 0.393 U 0.202 U 0.188 U 0.197 U 0.758 U 0.297 U 0.204 U 0.197 U 2,4,5-TP (Silvex) mg/kg 0.212 U 0.225 U 0.479 U 0.874 U 0.377 U 0.322 U 0.212 U 0.363 U 0.393 U 0.202 U 0.188 U 0.197 U 0.758 U 0.297 U 0.204 U 0.197 U 2,4-D mg/kg 0.212 U 0.225 U 0.479 U 0.874 U 0.377 U 0.322 U 0.212 U 0.363 U 0.393 U 0.202 U 0.188 U 0.197 U 0.758 U 0.297 U 0.204 U 0.197 U Dinoseb mg/kg 0.0425 U 0.0451 U 0.0958 U 0.175 U 0.0755 U 0.0644 U 0.0424 U 0.0726 U 0.0786 U 0.0404 U 0.0377 U 0.0394 U 0.152 U 0.0595 U 0.0408 U 0.0394 U Volatile Organics by GC/MS - Westborough Lab

1,1,1-Trichloroethane mg/kg 0.0014 U 1,1,1-Trichloroethane mg/kg 0.0013 U 0.0014 U 0.003 U 0.0054 U 0.0023 U 0.002 U 0.0013 U 0.0022 U 0.0024 U 0.0012 U 0.0012 U 0.0012 U 0.0046 U 0.0018 U 0.0013 U 0.0012 U 1,1,2,2-Tetrachloroethane mg/kg 0.0014 U 1,1,2,2-Tetrachloroethane mg/kg 0.0013 U 0.0014 U 0.003 U 0.0054 U 0.0023 U 0.002 U 0.0013 U 0.0022 U 0.0024 U 0.0012 U 0.0012 U 0.0012 U 0.0046 U 0.0018 U 0.0013 U 0.0012 U 1,1,2-Trichloroethane mg/kg 0.0021 U 1,1,2-Trichloroethane mg/kg 0.0019 U 0.0021 U 0.0044 U 0.0081 U 0.0034 U 0.0029 U 0.0019 U 0.0034 U 0.0036 U 0.0018 U 0.0017 U 0.0018 U 0.0069 U 0.0027 U 0.0019 U 0.0018 U 1,1-Dichloroethane mg/kg 0.0021 U 1,1-Dichloroethane mg/kg 0.0019 U 0.0021 U 0.0044 U 0.0081 U 0.0034 U 0.0029 U 0.0019 U 0.0034 U 0.0036 U 0.0018 U 0.0017 U 0.0018 U 0.0069 U 0.0027 U 0.0019 U 0.0018 U 1,1-Dichloroethene mg/kg 0.0014 U 1,1-Dichloroethene mg/kg 0.0013 U 0.0014 U 0.003 U 0.0054 U 0.0023 U 0.002 U 0.0013 U 0.0022 U 0.0024 U 0.0012 U 0.0012 U 0.0012 U 0.0046 U 0.0018 U 0.0013 U 0.0012 U 1,2,3-Trichlorobenzene mg/kg 0.0069 U 1,2,3-Trichlorobenzene mg/kg 0.0065 U 0.0069 U 0.015 U 0.027 U 0.012 U 0.0098 U 0.0064 U 0.011 U 0.012 U 0.0061 U 0.0058 U 0.006 U 0.023 U 0.0091 U 0.0063 U 0.006 U 1,2,4-Trichlorobenzene mg/kg 0.0069 U 1,2,4-Trichlorobenzene mg/kg 0.0065 U 0.0069 U 0.015 U 0.027 U 0.012 U 0.0098 U 0.0064 U 0.011 U 0.012 U 0.0061 U 0.0058 U 0.006 U 0.023 U 0.0091 U 0.0063 U 0.006 U 1,2,4-Trimethylbenzene mg/kg 0.0069 U 1,2,4-Trimethylbenzene mg/kg 0.0065 U 0.0069 U 0.015 U 0.027 U 0.012 U 0.0098 U 0.0064 U 0.011 U 0.012 U 0.0061 U 0.0058 U 0.006 U 0.023 U 0.0091 U 0.0063 U 0.006 U 1,2-Dibromo-3-chloropropane mg/kg 0.0069 U 1,2-Dibromo-3-chloropropane mg/kg 0.0065 U 0.0069 U 0.015 U 0.027 U 0.012 U 0.0098 U 0.0064 U 0.011 U 0.012 U 0.0061 U 0.0058 U 0.006 U 0.023 U 0.0091 U 0.0063 U 0.006 U 1,2-Dibromoethane mg/kg 0.0055 U 1,2-Dibromoethane mg/kg 0.0052 U 0.0055 U 0.012 U 0.022 U 0.0092 U 0.0078 U 0.0052 U 0.009 U 0.0097 U 0.0049 U 0.0046 U 0.0048 U 0.018 U 0.0073 U 0.005 U 0.0048 U 1,2-Dichlorobenzene mg/kg 0.0069 U 1,2-Dichlorobenzene mg/kg 0.0065 U 0.0069 U 0.015 U 0.027 U 0.012 U 0.0098 U 0.0064 U 0.011 U 0.012 U 0.0061 U 0.0058 U 0.006 U 0.023 U 0.0091 U 0.0063 U 0.006 U 1,2-Dichloroethane mg/kg 0.0014 U 1,2-Dichloroethane mg/kg 0.0013 U 0.0014 U 0.003 U 0.0054 U 0.0023 U 0.002 U 0.0013 U 0.0022 U 0.0024 U 0.0012 U 0.0012 U 0.0012 U 0.0046 U 0.0018 U 0.0013 U 0.0012 U 1,2-Dichloropropane mg/kg 0.0048 U 1,2-Dichloropropane mg/kg 0.0045 U 0.0048 U 0.01 U 0.019 U 0.0081 U 0.0068 U 0.0045 U 0.0078 U 0.0084 U 0.0043 U 0.0041 U 0.0042 U 0.016 U 0.0064 U 0.0044 U 0.0042 U 1,3,5-Trimethylbenzene mg/kg 0.0069 U 1,3,5-Trimethylbenzene mg/kg 0.0065 U 0.0069 U 0.015 U 0.027 U 0.012 U 0.0098 U 0.0064 U 0.011 U 0.012 U 0.0061 U 0.0058 U 0.006 U 0.023 U 0.0091 U 0.0063 U 0.006 U 1,3-Dichlorobenzene mg/kg 0.0069 U 1,3-Dichlorobenzene mg/kg 0.0065 U 0.0069 U 0.015 U 0.027 U 0.012 U 0.0098 U 0.0064 U 0.011 U 0.012 U 0.0061 U 0.0058 U 0.006 U 0.023 U 0.0091 U 0.0063 U 0.006 U 1,4-Dichlorobenzene mg/kg 0.0069 U 1,4-Dichlorobenzene mg/kg 0.0065 U 0.0069 U 0.015 U 0.027 U 0.012 U 0.0098 U 0.0064 U 0.011 U 0.012 U 0.0061 U 0.0058 U 0.006 U 0.023 U 0.0091 U 0.0063 U 0.006 U 1,4-Dioxane mg/kg 0.14 U 1,4-Dioxane mg/kg 0.13 U 0.14 U 0.3 U 0.54 U 0.23 U 0.2 U 0.13 U 0.22 U 0.24 U 0.12 U 0.12 U 0.12 U 0.46 U 0.18 U 0.13 U 0.12 U 2-Butanone mg/kg 0.014 U 2-Butanone mg/kg 0.013 U 0.014 U 0.11 0.054 U 0.0053 J 0.0048 J 0.013 U 0.022 U 0.024 U 0.012 U 0.012 U 0.012 U 0.046 U 0.018 U 0.013 U 0.012 U 2-Hexanone mg/kg 0.014 U 2-Hexanone mg/kg 0.013 U 0.014 U 0.03 U 0.054 U 0.023 U 0.02 U 0.013 U 0.022 U 0.024 U 0.012 U 0.012 U 0.012 U 0.046 U 0.018 U 0.013 U 0.012 U 4-Methyl-2-pentanone mg/kg 0.014 U 4-Methyl-2-pentanone mg/kg 0.013 U 0.014 U 0.03 U 0.054 U 0.023 U 0.02 U 0.013 U 0.022 U 0.024 U 0.012 U 0.012 U 0.012 U 0.046 U 0.018 U 0.013 U 0.012 U Acetone mg/kg 0.014 U Acetone mg/kg 0.013 U 0.014 U 0.12 0.032 J 0.027 0.038 0.0064 J 0.022 U 0.024 U 0.012 U 0.012 U 0.012 U 0.018 J 0.039 0.0081 J 0.012 U Benzene mg/kg 0.0014 U Benzene mg/kg 0.0013 U 0.0014 U 0.003 U 0.0054 U 0.0023 U 0.002 U 0.0013 U 0.0022 U 0.0024 U 0.0012 U 0.0012 U 0.0012 U 0.0046 U 0.0018 U 0.0013 U 0.0012 U Bromochloromethane mg/kg 0.0069 U Bromochloromethane mg/kg 0.0065 U 0.0069 U 0.015 U 0.027 U 0.012 U 0.0098 U 0.0064 U 0.011 U 0.012 U 0.0061 U 0.0058 U 0.006 U 0.023 U 0.0091 U 0.0063 U 0.006 U Bromodichloromethane mg/kg 0.0014 U Bromodichloromethane mg/kg 0.0013 U 0.0014 U 0.003 U 0.0054 U 0.0023 U 0.002 U 0.0013 U 0.0022 U 0.0024 U 0.0012 U 0.0012 U 0.0012 U 0.0046 U 0.0018 U 0.0013 U 0.0012 U Bromoform mg/kg 0.0055 U Bromoform mg/kg 0.0052 U 0.0055 U 0.012 U 0.022 U 0.0092 U 0.0078 U 0.0052 U 0.009 U 0.0097 U 0.0049 U 0.0046 U 0.0048 U 0.018 U 0.0073 U 0.005 U 0.0048 U Bromomethane mg/kg 0.0028 U Bromomethane mg/kg 0.0026 U 0.0028 U 0.0059 U 0.011 U 0.0046 U 0.0039 U 0.0026 U 0.0045 U 0.0048 U 0.0024 U 0.0023 U 0.0024 U 0.0092 U 0.0036 U 0.0025 U 0.0024 U Carbon disulfide mg/kg 0.014 U Carbon disulfide mg/kg 0.013 U 0.014 U 0.03 U 0.054 U 0.021 J 0.044 0.011 J 0.025 0.024 U 0.012 U 0.012 U 0.012 U 0.022 J 0.0076 J 0.0031 J 0.012 U Carbon tetrachloride mg/kg 0.0014 U Carbon tetrachloride mg/kg 0.0013 U 0.0014 U 0.003 U 0.0054 U 0.0023 U 0.002 U 0.0013 U 0.0022 U 0.0024 U 0.0012 U 0.0012 U 0.0012 U 0.0046 U 0.0018 U 0.0013 U 0.0012 U Chlorobenzene mg/kg 0.0014 U Chlorobenzene mg/kg 0.0013 U 0.0014 U 0.003 U 0.0054 U 0.0023 U 0.002 U 0.0013 U 0.0022 U 0.0024 U 0.0012 U 0.0012 U 0.0012 U 0.0046 U 0.0018 U 0.0013 U 0.0012 U Chloroethane mg/kg 0.0028 U

Chloroethane mg/kg 0.0026 U 0.0028 U 0.0059 U 0.011 U 0.0046 U 0.0039 U 0.0026 U 0.0045 U 0.0048 U 0.0024 U 0.0023 U 0.0024 U 0.0092 U 0.0036 U 0.0025 U 0.0024 U Chloroform mg/kg 0.0021 U Chloroform mg/kg 0.0019 U 0.0021 U 0.0044 U 0.0081 U 0.0034 U 0.0029 U 0.0019 U 0.0034 U 0.0036 U 0.0018 U 0.0017 U 0.0018 U 0.0069 U 0.0027 U 0.0019 U 0.0018 U Chloromethane mg/kg 0.0069 U Chloromethane mg/kg 0.0065 U 0.0069 U 0.015 U 0.027 U 0.012 U 0.0098 U 0.0064 U 0.011 U 0.012 U 0.0061 U 0.0058 U 0.006 U 0.023 U 0.0091 U 0.0063 U 0.006 U cis-1,2-Dichloroethene mg/kg 0.0014 U cis-1,2-Dichloroethene mg/kg 0.0013 U 0.0014 U 0.003 U 0.0054 U 0.0023 U 0.002 U 0.0013 U 0.0022 U 0.0024 U 0.0012 U 0.0012 U 0.0012 U 0.0046 U 0.0018 U 0.0013 U 0.0012 U cis-1,3-Dichloropropene mg/kg 0.0014 U cis-1,3-Dichloropropene mg/kg 0.0013 U 0.0014 U 0.003 U 0.0054 U 0.0023 U 0.002 U 0.0013 U 0.0022 U 0.0024 U 0.0012 U 0.0012 U 0.0012 U 0.0046 U 0.0018 U 0.0013 U 0.0012 U Cyclohexane mg/kg 0.028 U Cyclohexane mg/kg 0.026 U 0.028 U 0.059 U 0.11 U 0.046 U 0.039 U 0.026 U 0.045 U 0.048 U 0.024 U 0.023 U 0.024 U 0.092 U 0.036 U 0.025 U 0.024 U Dibromochloromethane mg/kg 0.0014 U Dibromochloromethane mg/kg 0.0013 U 0.0014 U 0.003 U 0.0054 U 0.0023 U 0.002 U 0.0013 U 0.0022 U 0.0024 U 0.0012 U 0.0012 U 0.0012 U 0.0046 U 0.0018 U 0.0013 U 0.0012 U Dichlorodifluoromethane mg/kg 0.014 U Dichlorodifluoromethane mg/kg 0.013 U 0.014 U 0.03 U 0.054 U 0.023 U 0.02 U 0.013 U 0.022 U 0.024 U 0.012 U 0.012 U 0.012 U 0.046 U 0.018 U 0.013 U 0.012 U Ethylbenzene mg/kg 0.0014 U Ethylbenzene mg/kg 0.0013 U 0.0014 U 0.003 U 0.0054 U 0.0023 U 0.002 U 0.0013 U 0.0022 U 0.0024 U 0.0012 U 0.0012 U 0.0012 U 0.0046 U 0.0018 U 0.0013 U 0.0012 U Freon-113 mg/kg 0.028 U Freon-113 mg/kg 0.026 U 0.028 U 0.059 U 0.11 U 0.046 U 0.039 U 0.026 U 0.045 U 0.048 U 0.024 U 0.023 U 0.024 U 0.092 U 0.036 U 0.025 U 0.024 U Isopropylbenzene mg/kg 0.0014 U Isopropylbenzene mg/kg 0.0013 U 0.0014 U 0.003 U 0.0054 U 0.0023 U 0.002 U 0.0013 U 0.0022 U 0.0024 U 0.0012 U 0.0012 U 0.0012 U 0.0046 U 0.0018 U 0.0013 U 0.0012 U Methyl Acetate mg/kg 0.028 U Methyl Acetate mg/kg 0.026 U 0.028 U 0.059 U 0.11 U 0.046 U 0.039 U 0.026 U 0.045 U 0.048 U 0.024 U 0.023 U 0.024 U 0.092 U 0.036 U 0.025 U 0.024 U Methyl cyclohexane mg/kg 0.0055 U Methyl cyclohexane mg/kg 0.0052 U 0.0055 U 0.012 U 0.022 U 0.0092 U 0.0078 U 0.0052 U 0.009 U 0.0097 U 0.0049 U 0.0046 U 0.0048 U 0.018 U 0.0073 U 0.005 U 0.0048 U Methyl tert butyl ether mg/kg 0.0028 U Methyl tert butyl ether mg/kg 0.0026 U 0.0028 U 0.0059 U 0.011 U 0.0046 U 0.0039 U 0.0026 U 0.0045 U 0.0048 U 0.0024 U 0.0023 U 0.0024 U 0.0092 U 0.0036 U 0.0025 U 0.0024 U Methylene chloride mg/kg 0.014 U Methylene chloride mg/kg 0.013 U 0.014 U 0.03 U 0.054 U 0.023 U 0.02 U 0.013 U 0.022 U 0.024 U 0.012 U 0.012 U 0.012 U 0.046 U 0.018 U 0.013 U 0.012 U n-Butylbenzene mg/kg 0.0014 U n-Butylbenzene mg/kg 0.0013 U 0.0014 U 0.003 U 0.0054 U 0.0023 U 0.002 U 0.0013 U 0.0022 U 0.0024 U 0.0012 U 0.0012 U 0.0012 U 0.0046 U 0.0018 U 0.0013 U 0.0012 U n-Propylbenzene mg/kg 0.0014 U n-Propylbenzene mg/kg 0.0013 U 0.0014 U 0.003 U 0.0054 U 0.0023 U 0.002 U 0.0013 U 0.0022 U 0.0024 U 0.0012 U 0.0012 U 0.0012 U 0.0046 U 0.0018 U 0.0013 U 0.0012 U o-Xylene mg/kg 0.0028 U o-Xylene mg/kg 0.0026 U 0.0028 U 0.0059 U 0.011 U 0.0046 U 0.0039 U 0.0026 U 0.0045 U 0.0048 U 0.0024 U 0.0023 U 0.0024 U 0.0092 U 0.0036 U 0.0025 U 0.0024 U p/m-Xylene mg/kg 0.0028 U p/m-Xylene mg/kg 0.0026 U 0.0028 U 0.0059 U 0.011 U 0.0046 U 0.0039 U 0.0026 U 0.0045 U 0.0048 U 0.0024 U 0.0023 U 0.0024 U 0.0092 U 0.0036 U 0.0025 U 0.0024 U sec-Butylbenzene mg/kg 0.0014 U sec-Butylbenzene mg/kg 0.0013 U 0.0014 U 0.003 U 0.0054 U 0.0023 U 0.002 U 0.0013 U 0.0022 U 0.0024 U 0.0012 U 0.0012 U 0.0012 U 0.0046 U 0.0018 U 0.0013 U 0.0012 U Styrene mg/kg 0.0028 U Styrene mg/kg 0.0026 U 0.0028 U 0.0059 U 0.011 U 0.0046 U 0.0039 U 0.0026 U 0.0045 U 0.0048 U 0.0024 U 0.0023 U 0.0024 U 0.0092 U 0.0036 U 0.0025 U 0.0024 U tert-Butylbenzene mg/kg 0.0069 U tert-Butylbenzene mg/kg 0.0065 U 0.0069 U 0.015 U 0.027 U 0.012 U 0.0098 U 0.0064 U 0.011 U 0.012 U 0.0061 U 0.0058 U 0.006 U 0.023 U 0.0091 U 0.0063 U 0.006 U Tetrachloroethene mg/kg 0.0014 U Tetrachloroethene mg/kg 0.0013 U 0.0014 U 0.003 U 0.0054 U 0.0023 U 0.002 U 0.0013 U 0.0022 U 0.0024 U 0.0012 U 0.0012 U 0.0012 U 0.0046 U 0.0018 U 0.0013 U 0.0012 U Toluene mg/kg 0.0021 U Toluene mg/kg 0.0019 U 0.0021 U 0.0044 U 0.0081 U 0.0034 U 0.0029 U 0.0019 U 0.0034 U 0.0036 U 0.0018 U 0.0017 U 0.0018 U 0.0069 U 0.0027 U 0.0019 U 0.0018 U trans-1,2-Dichloroethene mg/kg 0.0021 U trans-1,2-Dichloroethene mg/kg 0.0019 U 0.0021 U 0.0044 U 0.0081 U 0.0034 U 0.0029 U 0.0019 U 0.0034 U 0.0036 U 0.0018 U 0.0017 U 0.0018 U 0.0069 U 0.0027 U 0.0019 U 0.0018 U trans-1,3-Dichloropropene mg/kg 0.0014 U trans-1,3-Dichloropropene mg/kg 0.0013 U 0.0014 U 0.003 U 0.0054 U 0.0023 U 0.002 U 0.0013 U 0.0022 U 0.0024 U 0.0012 U 0.0012 U 0.0012 U 0.0046 U 0.0018 U 0.0013 U 0.0012 U Trichloroethene mg/kg 0.0014 U Trichloroethene mg/kg 0.0013 U 0.0014 U 0.003 U 0.0054 U 0.0023 U 0.002 U 0.0013 U 0.0022 U 0.0024 U 0.0012 U 0.0012 U 0.0012 U 0.0046 U 0.0018 U 0.0013 U 0.0012 U Trichlorofluoromethane mg/kg 0.0069 U Trichlorofluoromethane mg/kg 0.0065 U 0.0069 U 0.015 U 0.027 U 0.012 U 0.0098 U 0.0064 U 0.011 U 0.012 U 0.0061 U 0.0058 U 0.006 U 0.023 U 0.0091 U 0.0063 U 0.006 U Vinyl chloride mg/kg 0.0028 U Vinyl chloride mg/kg 0.0026 U 0.0028 U 0.0059 U 0.011 U 0.0046 U 0.0039 U 0.0026 U 0.0045 U 0.0048 U 0.0024 U 0.0023 U 0.0024 U 0.0092 U 0.0036 U 0.0025 U 0.0024 U No Tentatively Identified Compounds - TIC () mg/kg 0 U 0 U 0 U 0 U 0 U 0 U 0 U 0 U 0 U 0 U 0 U 0 U 0 U 0 U 0 U No Tentatively Identified Compounds - TIC () mg/kg 0 U 0 U 0 U 0 U 0 U 0 U 0 U 0 U 0 U 0 U 0 U 0 U 0 U 0 U 0 U Unknown - TIC (11.654) mg/kg 0.0028 J 0.0035 J SPLP Semivolatiles by EPA 1312 - Westborough Lab

1,2,4,5-Tetrachlorobenzene mg/kg 0.02 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 2,3,4,6-Tetrachlorophenol mg/kg 0.01 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 2,4,5-Trichlorophenol mg/kg 0.01 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 2,4,6-Trichlorophenol mg/kg 0.01 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 2,4-Dichlorophenol mg/kg 0.02 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 2,4-Dimethylphenol mg/kg 0.01 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 2,4-Dinitrophenol mg/kg 0.04 U 0.02 U 0.02 U 0.02 U 0.02 U 0.02 U 0.02 U 0.02 U 0.02 U 0.02 U 0.02 U 0.02 U 0.02 U 0.02 U 0.02 U 0.02 U 2,4-Dinitrotoluene mg/kg 0.01 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 2,6-Dinitrotoluene mg/kg 0.01 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 2-Chloronaphthalene mg/kg 0.004 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 2-Chlorophenol mg/kg 0.004 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 2-Methylnaphthalene mg/kg 0.004 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 2-Methylphenol mg/kg 0.01 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 2-Nitroaniline mg/kg 0.01 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 2-Nitrophenol mg/kg 0.02 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 3,3'-Dichlorobenzidine mg/kg 0.01 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 3-Methylphenol/4-Methylphenol mg/kg 0.01 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 3-Nitroaniline mg/kg 0.01 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 4,6-Dinitro-o-cresol mg/kg 0.02 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 4-Bromophenyl phenyl ether mg/kg 0.004 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 4-Chloroaniline mg/kg 0.01 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 4-Chlorophenyl phenyl ether mg/kg 0.004 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 4-Nitroaniline mg/kg 0.01 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 4-Nitrophenol mg/kg 0.02 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U Acenaphthene mg/kg 0.004 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U Acenaphthylene mg/kg 0.004 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U Acetophenone mg/kg 0.01 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U Anthracene mg/kg 0.004 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U Atrazine mg/kg 0.02 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U Benzaldehyde mg/kg 0.01 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U Benzo(a)anthracene mg/kg 0.004 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U Benzo(a)pyrene mg/kg 0.004 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U Benzo(b)fluoranthene mg/kg 0.004 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U Benzo(ghi)perylene mg/kg 0.004 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U Benzo(k)fluoranthene mg/kg 0.004 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U Biphenyl mg/kg 0.004 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U Bis(2-chloroethoxy)methane mg/kg 0.01 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U Bis(2-chloroethyl)ether mg/kg 0.004 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U Bis(2-chloroisopropyl)ether mg/kg 0.004 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U Bis(2-ethylhexyl)phthalate mg/kg 0.0029 J 0.0098 0.0079 0.019 0.0018 J 0.0013 J 0.0023 J 0.0069 0.003 U 0.00096 J 0.0019 J 0.0026 J 0.003 U 0.003 U 0.003 U 0.0011 J Butyl benzyl phthalate mg/kg 0.01 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U Caprolactam mg/kg 0.02 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U Carbazole mg/kg 0.004 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U Chrysene mg/kg 0.004 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U Di-n-butylphthalate mg/kg 0.01 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U Di-n-octylphthalate mg/kg 0.01 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U Dibenzo(a,h)anthracene mg/kg 0.004 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U Dibenzofuran mg/kg 0.004 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U Diethyl phthalate mg/kg 0.01 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U Dimethyl phthalate mg/kg 0.01 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U Fluoranthene mg/kg 0.004 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U Fluorene mg/kg 0.004 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U Hexachlorobenzene mg/kg 0.004 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U Hexachlorobutadiene mg/kg 0.004 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U Hexachlorocyclopentadiene mg/kg 0.04 U 0.02 U 0.02 U 0.02 U 0.02 U 0.02 U 0.02 U 0.02 U 0.02 U 0.02 U 0.02 U 0.02 U 0.02 U 0.02 U 0.02 U 0.02 U Hexachloroethane mg/kg 0.004 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U Indeno(1,2,3-cd)pyrene mg/kg 0.004 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U Isophorone mg/kg 0.01 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U n-Nitrosodi-n-propylamine mg/kg 0.01 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U Naphthalene mg/kg 0.004 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U NDPA/DPA mg/kg 0.004 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U Nitrobenzene mg/kg 0.004 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U p-Chloro-m-cresol mg/kg 0.004 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U Pentachlorophenol mg/kg 0.02 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U 0.01 U Phenanthrene mg/kg 0.004 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U Phenol mg/kg 0.01 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U 0.005 U Pyrene mg/kg 0.004 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U 0.002 U Semivolatile Organics by GC/MS - Mansfield Lab

1,2,4,5-Tetrachlorobenzene mg/kg 0.0862 U 0.0906 U 0.194 U 0.353 U 0.15 U 0.127 U 0.0844 U 0.148 U 0.157 U 0.0798 U 0.0773 U 0.078 U 0.304 U 0.122 U 0.0821 U 0.0793 U 2,3,4,6-Tetrachlorophenol mg/kg 0.172 U 0.181 U 0.388 U 0.705 U 0.299 U 0.254 U 0.169 U 0.295 U 0.315 U 0.16 U 0.154 U 0.156 U 0.608 U 0.244 U 0.164 U 0.159 U 2,4,5-Trichlorophenol mg/kg 0.0862 U 0.0906 U 0.194 U 0.353 U 0.15 U 0.127 U 0.0844 U 0.148 U 0.157 U 0.0798 U 0.0773 U 0.078 U 0.304 U 0.122 U 0.0821 U 0.0793 U 2,4,6-Trichlorophenol mg/kg 0.0862 U 0.0906 U 0.194 U 0.353 U 0.15 U 0.127 U 0.0844 U 0.148 U 0.157 U 0.0798 U 0.0773 U 0.078 U 0.304 U 0.122 U 0.0821 U 0.0793 U 2,4-Dichlorophenol mg/kg 0.0862 U 0.0906 U 0.194 U 0.353 U 0.15 U 0.127 U 0.0844 U 0.148 U 0.157 U 0.0798 U 0.0773 U 0.078 U 0.304 U 0.122 U 0.0821 U 0.0793 U 2,4-Dimethylphenol mg/kg 0.0862 U 0.0906 U 0.194 U 0.353 U 0.15 U 0.127 U 0.0844 U 0.148 U 0.157 U 0.0798 U 0.0773 U 0.078 U 0.304 U 0.122 U 0.0821 U 0.0793 U 2,4-Dinitrophenol mg/kg 0.517 U 0.544 U 1.16 U 2.12 U 0.898 U 0.762 U 0.507 U 0.886 U 0.945 U 0.478 U 0.464 U 0.468 U 1.82 U 0.73 U 0.492 U 0.476 U 2,4-Dinitrotoluene mg/kg 0.129 U 0.136 U 0.291 U 0.529 U 0.224 U 0.191 U 0.127 U 0.222 U 0.236 U 0.12 U 0.116 U 0.117 U 0.456 U 0.183 U 0.123 U 0.119 U 2,6-Dinitrotoluene mg/kg 0.0431 U 0.0453 U 0.0971 U 0.176 U 0.0748 U 0.0635 U 0.0422 U 0.0738 U 0.0787 U 0.0399 U 0.0386 U 0.039 U 0.152 U 0.0609 U 0.041 U 0.0396 U 2-Chloronaphthalene mg/kg 0.0862 U 0.0906 U 0.194 U 0.353 U 0.15 U 0.127 U 0.0844 U 0.148 U 0.157 U 0.0798 U 0.0773 U 0.078 U 0.304 U 0.122 U 0.0821 U 0.0793 U 2-Chlorophenol mg/kg 0.0431 U 0.0453 U 0.0971 U 0.176 U 0.0748 U 0.0635 U 0.0422 U 0.0738 U 0.0787 U 0.0399 U 0.0386 U 0.039 U 0.152 U 0.0609 U 0.041 U 0.0396 U 2-Methylphenol mg/kg 0.0862 U 0.0906 U 0.194 U 0.353 U 0.15 U 0.127 U 0.0844 U 0.148 U 0.157 U 0.0798 U 0.0773 U 0.078 U 0.304 U 0.122 U 0.0821 U 0.0793 U 2-Nitroaniline mg/kg 0.0431 U 0.0453 U 0.0971 U 0.176 U 0.0748 U 0.0635 U 0.0422 U 0.0738 U 0.0787 U 0.0399 U 0.0386 U 0.039 U 0.152 U 0.0609 U 0.041 U 0.0396 U 2-Nitrophenol mg/kg 0.0862 U 0.0906 U 0.194 U 0.353 U 0.15 U 0.127 U 0.0844 U 0.148 U 0.157 U 0.0798 U 0.0773 U 0.078 U 0.304 U 0.122 U 0.0821 U 0.0793 U 3,3'-Dichlorobenzidine mg/kg 0.129 U 0.136 U 0.291 U 0.529 U 0.224 U 0.191 U 0.127 U 0.222 U 0.236 U 0.12 U 0.116 U 0.117 U 0.456 U 0.183 U 0.123 U 0.119 U 3-Nitroaniline mg/kg 0.0431 U 0.0453 U 0.0971 U 0.176 U 0.0748 U 0.0635 U 0.0422 U 0.0738 U 0.0787 U 0.0399 U 0.0386 U 0.039 U 0.152 U 0.0609 U 0.041 U 0.0396 U 4,6-Dinitro-2-methylphenol mg/kg 0.431 U 0.453 U 0.971 U 1.76 U 0.748 U 0.635 U 0.422 U 0.738 U 0.787 U 0.399 U 0.386 U 0.39 U 1.52 U 0.609 U 0.41 U 0.396 U 4-Bromophenyl-phenylether mg/kg 0.0862 U 0.0906 U 0.194 U 0.353 U 0.15 U 0.127 U 0.0844 U 0.148 U 0.157 U 0.0798 U 0.0773 U 0.078 U 0.304 U 0.122 U 0.0821 U 0.0793 U 4-Chloro-3-methylphenol mg/kg 0.129 U 0.136 U 0.291 U 0.529 U 0.224 U 0.191 U 0.127 U 0.222 U 0.236 U 0.12 U 0.116 U 0.117 U 0.456 U 0.183 U 0.123 U 0.119 U 4-Chloroaniline mg/kg 0.0431 U 0.0453 U 0.0971 U 0.176 U 0.0748 U 0.0635 U 0.0422 U 0.0738 U 0.0787 U 0.0399 U 0.0386 U 0.039 U 0.152 U 0.0609 U 0.041 U 0.0396 U 4-Chlorophenyl-phenylether mg/kg 0.0431 U 0.0453 U 0.0971 U 0.176 U 0.0748 U 0.0635 U 0.0422 U 0.0738 U 0.0787 U 0.0399 U 0.0386 U 0.039 U 0.152 U 0.0609 U 0.041 U 0.0396 U 4-Methylphenol mg/kg 0.0862 U 0.0906 U 0.194 U 0.353 U 0.15 U 0.127 U 0.0844 U 0.148 U 0.157 U 0.0798 U 0.0773 U 0.078 U 0.304 U 0.122 U 0.0821 U 0.0793 U 4-Nitroaniline mg/kg 0.0431 U 0.0453 U 0.0971 U 0.176 U 0.0748 U 0.0635 U 0.0422 U 0.0738 U 0.0787 U 0.0399 U 0.0386 U 0.039 U 0.152 U 0.0609 U 0.041 U 0.0396 U 4-Nitrophenol mg/kg 0.862 U 0.906 U 1.94 U 3.53 U 1.5 U 1.27 U 0.844 U 1.48 U 1.57 U 0.798 U 0.773 U 0.78 U 3.04 U 1.22 U 0.821 U 0.793 U Acetophenone mg/kg 0.0862 U 0.08 J 0.194 U 0.353 U 0.15 U 0.127 U 0.0844 U 0.148 U 0.157 U 0.0798 U 0.0773 U 0.078 U 0.304 U 0.122 U 0.0821 U 0.0793 U Atrazine mg/kg 0.0862 U 0.0906 U 0.194 U 0.353 U 0.15 U 0.127 U 0.0844 U 0.148 U 0.157 U 0.0798 U 0.0773 U 0.078 U 0.304 U 0.122 U 0.0821 U 0.0793 U Benzaldehyde mg/kg 0.646 U 0.68 U 1.46 U 2.64 U 1.12 U 0.953 U 0.633 U 1.11 U 1.18 U 0.598 U 0.58 U 0.585 U 2.28 U 0.913 U 0.616 U 0.595 U

Biphenyl mg/kg 0.0862 U 0.0906 U 0.194 U 0.353 U 0.15 U 0.127 U 0.0844 U 0.148 U 0.157 U 0.0798 U 0.0773 U 0.078 U 0.304 U 0.122 U 0.0821 U 0.0793 U bis(2-Chloroethoxy)methane mg/kg 0.0862 U 0.0906 U 0.194 U 0.353 U 0.15 U 0.127 U 0.0844 U 0.148 U 0.157 U 0.0798 U 0.0773 U 0.078 U 0.304 U 0.122 U 0.0821 U 0.0793 U bis(2-Chloroethyl)ether mg/kg 0.0862 U 0.0906 U 0.194 U 0.353 U 0.15 U 0.127 U 0.0844 U 0.148 U 0.157 U 0.0798 U 0.0773 U 0.078 U 0.304 U 0.122 U 0.0821 U 0.0793 U bis(2-chloroisopropyl)ether mg/kg 0.0862 U 0.0906 U 0.194 U 0.353 U 0.15 U 0.127 U 0.0844 U 0.148 U 0.157 U 0.0798 U 0.0773 U 0.078 U 0.304 U 0.122 U 0.0821 U 0.0793 U bis(2-Ethylhexyl)phthalate mg/kg 0.192 0.57 0.12 J 0.705 U 0.299 U 0.254 U 0.169 U 0.295 U 0.315 U 0.16 U 0.154 U 0.156 U 0.608 U 0.244 U 0.164 U 0.159 U Butylbenzylphthalate mg/kg 0.0862 U 0.0906 U 0.194 U 0.353 U 0.15 U 0.127 U 0.0844 U 0.148 U 0.157 U 0.0798 U 0.0773 U 0.078 U 0.304 U 0.122 U 0.0821 U 0.0793 U Caprolactam mg/kg 0.0862 U 0.0906 U 0.194 U 0.353 U 0.15 U 0.127 U 0.0844 U 0.148 U 0.157 U 0.0798 U 0.0773 U 0.078 U 0.304 U 0.122 U 0.0821 U 0.0793 U Carbazole mg/kg 0.0862 U 0.0906 U 0.194 U 0.353 U 0.15 U 0.127 U 0.0844 U 0.148 U 0.157 U 0.0798 U 0.0773 U 0.078 U 0.304 U 0.122 U 0.0821 U 0.0793 U Di-n-butylphthalate mg/kg 0.0367 J 0.136 U 0.291 U 0.529 U 0.224 U 0.191 U 0.127 U 0.222 U 0.236 U 0.12 U 0.116 U 0.117 U 0.456 U 0.183 U 0.123 U 0.119 U Di-n-octylphthalate mg/kg 0.0862 U 0.0906 U 0.194 U 0.353 U 0.15 U 0.127 U 0.0844 U 0.148 U 0.157 U 0.0798 U 0.0773 U 0.078 U 0.304 U 0.122 U 0.0821 U 0.0793 U Dibenzofuran mg/kg 0.0862 U 0.0906 U 0.194 U 0.353 U 0.15 U 0.127 U 0.0844 U 0.148 U 0.157 U 0.0798 U 0.0773 U 0.078 U 0.304 U 0.122 U 0.0821 U 0.0793 U Diethylphthalate mg/kg 0.0862 U 0.0906 U 0.194 U 0.353 U 0.15 U 0.127 U 0.0844 U 0.148 U 0.157 U 0.0798 U 0.0773 U 0.078 U 0.304 U 0.122 U 0.0821 U 0.0793 U Dimethylphthalate mg/kg 0.0862 U 0.0906 U 0.194 U 0.353 U 0.15 U 0.127 U 0.0844 U 0.148 U 0.157 U 0.0798 U 0.0773 U 0.078 U 0.304 U 0.122 U 0.0821 U 0.0793 U Hexachlorobenzene mg/kg 0.0862 U 0.0906 U 0.194 U 0.353 U 0.15 U 0.127 U 0.0844 U 0.148 U 0.157 U 0.0798 U 0.0773 U 0.078 U 0.304 U 0.122 U 0.0821 U 0.0793 U Hexachlorobutadiene mg/kg 0.0862 U 0.0906 U 0.194 U 0.353 U 0.15 U 0.127 U 0.0844 U 0.148 U 0.157 U 0.0798 U 0.0773 U 0.078 U 0.304 U 0.122 U 0.0821 U 0.0793 U Hexachlorocyclopentadiene mg/kg 0.0431 U 0.0453 U 0.0971 U 0.176 U 0.0748 U 0.0635 U 0.0422 U 0.0738 U 0.0787 U 0.0399 U 0.0386 U 0.039 U 0.152 U 0.0609 U 0.041 U 0.0396 U Hexachloroethane mg/kg 0.0862 U 0.0906 U 0.194 U 0.353 U 0.15 U 0.127 U 0.0844 U 0.148 U 0.157 U 0.0798 U 0.0773 U 0.078 U 0.304 U 0.122 U 0.0821 U 0.0793 U Isophorone mg/kg 0.0862 U 0.0906 U 0.194 U 0.353 U 0.15 U 0.127 U 0.0844 U 0.148 U 0.157 U 0.0798 U 0.0773 U 0.078 U 0.304 U 0.122 U 0.0821 U 0.0793 U N-Nitroso-di-n-propylamine mg/kg 0.0862 U 0.0906 U 0.194 U 0.353 U 0.15 U 0.127 U 0.0844 U 0.148 U 0.157 U 0.0798 U 0.0773 U 0.078 U 0.304 U 0.122 U 0.0821 U 0.0793 U n-Nitrosodiphenylamine mg/kg 0.0862 U 0.0906 U 0.194 U 0.353 U 0.15 U 0.127 U 0.0844 U 0.148 U 0.157 U 0.0798 U 0.0773 U 0.078 U 0.304 U 0.122 U 0.0821 U 0.0793 U Nitrobenzene mg/kg 0.0862 U 0.0906 U 0.194 U 0.353 U 0.15 U 0.127 U 0.0844 U 0.148 U 0.157 U 0.0798 U 0.0773 U 0.078 U 0.304 U 0.122 U 0.0821 U 0.0793 U Pentachlorophenol mg/kg 0.258 U 0.272 U 0.582 U 1.06 U 0.449 U 0.381 U 0.253 U 0.443 U 0.472 U 0.239 U 0.232 U 0.234 U 0.912 U 0.365 U 0.246 U 0.238 U Phenol mg/kg 0.0862 U 0.0906 U 0.194 U 0.353 U 0.15 U 0.127 U 0.0844 U 0.148 U 0.157 U 0.0798 U 0.0773 U 0.078 U 0.304 U 0.122 U 0.0821 U 0.0793 U Campesterol - TIC (19.887) mg/kg 4.94 NJ Campesterol - TIC (19.902) mg/kg 7.72 NJ Campesterol - TIC (19.906) mg/kg 3.05 NJ 0.448 NJ Campesterol - TIC (19.907) mg/kg 4.95 NJ Campesterol - TIC (19.911) mg/kg 0.243 NJ Cyclic Octaatomic Sulfur - TIC (11.691) mg/kg 0.102 NJ Cyclic Octaatomic Sulfur - TIC (11.696) mg/kg 0.65 NJ Cyclic Octaatomic Sulfur - TIC (11.701) mg/kg 0.842 NJ Cyclic Octaatomic Sulfur - TIC (11.711) mg/kg 2.39 NJ 0.964 NJ Cyclic Octaatomic Sulfur - TIC (11.716) mg/kg 1.18 NJ 0.726 NJ Ergostanol - TIC (19.974) mg/kg 1.35 NJ Ergostanol - TIC (20.552) mg/kg 0.913 NJ Ergostanol - TIC (20.561) mg/kg 1.31 NJ Ergostanol - TIC (20.566) mg/kg 1.1 NJ Ergostanol - TIC (20.571) mg/kg 0.895 NJ Ergostanol - TIC (20.59) mg/kg 9.21 NJ Ergostanol - TIC (20.609) mg/kg 6.91 NJ Ergostanol - TIC (20.629) mg/kg 20 NJ Ergostanol - TIC (20.634) mg/kg 17.8 NJ Friedelan-3-one - TIC (21.962) mg/kg 2.94 NJ Friedelan-3-one - TIC (22.3) mg/kg 0.671 NJ Friedelan-3-one - TIC (22.314) mg/kg 0.984 NJ Friedelan-3-one - TIC (22.324) mg/kg 0.884 NJ Friedelan-3-one - TIC (22.338) mg/kg 2.4 NJ Friedelan-3-one - TIC (22.348) mg/kg 5.63 NJ No Tentatively Identified Compounds - TIC () mg/kg 0 U Stigmast-4-en-3-one - TIC (21.129) mg/kg 6.77 NJ Stigmast-4-en-3-one - TIC (21.409) mg/kg 0.364 NJ Stigmast-4-en-3-one - TIC (21.423) mg/kg 0.558 NJ Stigmast-4-en-3-one - TIC (21.428) mg/kg 9.57 NJ Stigmast-4-en-3-one - TIC (21.447) mg/kg 14.8 NJ Stigmast-4-en-3-one - TIC (21.452) mg/kg 9.71 NJ 5.93 NJ Stigmast-4-en-3-one - TIC (21.5) mg/kg 0.222 NJ Stigmasterol - TIC (19.824) mg/kg 4.01 NJ Stigmasterol - TIC (20.065) mg/kg 5.84 NJ Stigmasterol - TIC (20.08) mg/kg 6.69 NJ 4.08 NJ 0.263 NJ Sulfur - TIC (7.979) mg/kg 0.284 NJ 0.3 NJ 0.136 NJ Unknown - TIC (12.072) mg/kg 0.227 J Unknown - TIC (13.776) mg/kg 1.39 J Unknown - TIC (14.321) mg/kg 6.47 J 15.5 J Unknown - TIC (14.87) mg/kg 0.862 J Unknown - TIC (14.889) mg/kg 0.363 J Unknown - TIC (14.927) mg/kg 0.377 J Unknown - TIC (15.693) mg/kg 0.477 J Unknown - TIC (15.712) mg/kg 1.76 J Unknown - TIC (15.731) mg/kg 0.251 J Unknown - TIC (15.799) mg/kg 0.281 J Unknown - TIC (15.809) mg/kg 0.727 J Unknown - TIC (15.958) mg/kg 2.44 J Unknown - TIC (16.223) mg/kg 20.7 J Unknown - TIC (16.43) mg/kg 2.4 J 5.3 J Unknown - TIC (16.434) mg/kg 4.72 J Unknown - TIC (16.435) mg/kg 11.4 J Unknown - TIC (16.439) mg/kg 12.9 J 7.26 J 8.61 J Unknown - TIC (16.444) mg/kg 1.54 J Unknown - TIC (16.473) mg/kg 6.4 J Unknown - TIC (16.478) mg/kg 0.327 J 5.17 J 0.838 J Unknown - TIC (16.488) mg/kg 0.178 J 0.456 J Unknown - TIC (16.545) mg/kg 0.106 J Unknown - TIC (16.935) mg/kg 4.81 J Unknown - TIC (17.147) mg/kg 0.913 J Unknown - TIC (17.181) mg/kg 2.1 J Unknown - TIC (17.186) mg/kg 0.536 J 1.83 J Unknown - TIC (17.195) mg/kg 0.287 J Unknown - TIC (17.2) mg/kg 5.97 J Unknown - TIC (17.412) mg/kg 3.51 J Unknown - TIC (17.821) mg/kg 4.21 J Unknown - TIC (17.826) mg/kg 5.7 J Unknown - TIC (18.101) mg/kg 0.446 J Unknown - TIC (18.486) mg/kg 4.05 J Unknown - TIC (18.693) mg/kg 0.637 J Unknown - TIC (18.794) mg/kg 2.67 J Unknown - TIC (18.871) mg/kg 9.22 J Unknown - TIC (19.064) mg/kg 0.552 J Unknown - TIC (19.073) mg/kg 0.91 J 1.88 J Unknown - TIC (19.078) mg/kg 2.71 J 2.04 J Unknown - TIC (19.083) mg/kg 2.22 J Unknown - TIC (19.131) mg/kg 0.489 J Unknown - TIC (19.15) mg/kg 0.468 J Unknown - TIC (19.155) mg/kg 0.502 J Unknown - TIC (19.333) mg/kg 1.62 J Unknown - TIC (19.459) mg/kg 3.65 J Unknown - TIC (19.675) mg/kg 7.45 J Unknown - TIC (19.68) mg/kg 2.48 J Unknown - TIC (19.69) mg/kg 2.25 J 0.581 J Unknown - TIC (19.694) mg/kg 4.82 J 1.78 J Unknown - TIC (19.695) mg/kg 6.86 J 3.74 J Unknown - TIC (19.81) mg/kg 0.118 J Unknown - TIC (19.887) mg/kg 0.344 J Unknown - TIC (19.954) mg/kg 0.334 J Unknown - TIC (19.983) mg/kg 0.143 J Unknown - TIC (19.984) mg/kg 1.04 J Unknown - TIC (19.993) mg/kg 1.63 J 1.53 J 0.431 J 0.954 J Unknown - TIC (19.998) mg/kg 6.42 J Unknown - TIC (20.003) mg/kg 1.98 J Unknown - TIC (20.06) mg/kg 11.2 J Unknown - TIC (20.085) mg/kg 11.2 J Unknown - TIC (20.099) mg/kg 0.667 J Unknown - TIC (20.166) mg/kg 4.51 J Unknown - TIC (20.171) mg/kg 3.96 J Unknown - TIC (20.181) mg/kg 10.8 J 2.98 J Unknown - TIC (20.186) mg/kg 0.679 J Unknown - TIC (20.191) mg/kg 0.146 J Unknown - TIC (20.234) mg/kg 34.1 J Unknown - TIC (20.253) mg/kg 2.72 J Unknown - TIC (20.34) mg/kg 3.81 J Unknown - TIC (20.383) mg/kg 0.955 J Unknown - TIC (20.45) mg/kg 0.0856 J Unknown - TIC (20.456) mg/kg 3.07 J Unknown - TIC (20.465) mg/kg 3.03 J Unknown - TIC (20.479) mg/kg 3.11 J Unknown - TIC (20.484) mg/kg 39.8 J Unknown - TIC (20.494) mg/kg 53.1 J 21.6 J Unknown - TIC (20.508) mg/kg 42.7 J Unknown - TIC (20.513) mg/kg 64.7 J Unknown - TIC (20.561) mg/kg 0.939 J Unknown - TIC (20.566) mg/kg 6.27 J Unknown - TIC (20.585) mg/kg 0.314 J Unknown - TIC (20.595) mg/kg 0.0999 J 0.755 J Unknown - TIC (20.672) mg/kg 4.47 J Unknown - TIC (20.706) mg/kg 2.63 J Unknown - TIC (20.71) mg/kg 2.59 J Unknown - TIC (20.715) mg/kg 1.96 J Unknown - TIC (20.72) mg/kg 1.3 J Unknown - TIC (20.73) mg/kg 0.414 J Unknown - TIC (20.744) mg/kg 2.7 J Unknown - TIC (20.749) mg/kg 38.8 J Unknown - TIC (20.759) mg/kg 19.5 J Unknown - TIC (20.788) mg/kg 62.8 J Unknown - TIC (20.792) mg/kg 0.105 J Unknown - TIC (20.793) mg/kg 95.3 J Unknown - TIC (20.807) mg/kg 1.82 J Unknown - TIC (20.812) mg/kg 0.34 J Unknown - TIC (20.817) mg/kg 0.199 J Unknown - TIC (20.826) mg/kg 0.633 J

Unknown - TIC (20.831) mg/kg 0.487 J Unknown - TIC (20.836) mg/kg 0.458 J Unknown - TIC (20.84) mg/kg 5.41 J Unknown - TIC (20.855) mg/kg 5.57 J Unknown - TIC (20.86) mg/kg 2 J 11.6 J Unknown - TIC (20.874) mg/kg 9.46 J Unknown - TIC (20.889) mg/kg 6.26 J Unknown - TIC (20.927) mg/kg 0.561 J Unknown - TIC (20.932) mg/kg 0.159 J Unknown - TIC (20.942) mg/kg 0.979 J 0.958 J Unknown - TIC (20.951) mg/kg 0.506 J Unknown - TIC (20.961) mg/kg 13.8 J Unknown - TIC (20.975) mg/kg 10.6 J 5.83 J Unknown - TIC (21.004) mg/kg 32.1 J Unknown - TIC (21.072) mg/kg 0.594 J Unknown - TIC (21.081) mg/kg 1.01 J Unknown - TIC (21.086) mg/kg 1.01 J Unknown - TIC (21.115) mg/kg 2.74 J Unknown - TIC (21.125) mg/kg 3.56 J Unknown - TIC (21.187) mg/kg 8.26 J Unknown - TIC (21.202) mg/kg 3.28 J Unknown - TIC (21.207) mg/kg 5.89 J Unknown - TIC (21.211) mg/kg 0.0969 J Unknown - TIC (21.221) mg/kg 18.8 J 0.543 J Unknown - TIC (21.274) mg/kg 4.1 J Unknown - TIC (21.365) mg/kg 0.764 J Unknown - TIC (21.404) mg/kg 0.331 J Unknown - TIC (21.471) mg/kg 2.2 J Unknown - TIC (21.674) mg/kg 1.04 J Unknown - TIC (21.775) mg/kg 0.375 J Unknown - TIC (21.784) mg/kg 5.86 J Unknown - TIC (21.789) mg/kg 0.719 J Unknown - TIC (21.794) mg/kg 0.524 J Unknown - TIC (21.866) mg/kg 0.456 J 0.239 J Unknown - TIC (22.102) mg/kg 1.01 J Unknown - TIC (22.121) mg/kg 1.77 J Unknown - TIC (22.126) mg/kg 1.47 J Unknown - TIC (22.189) mg/kg 2.72 J Unknown - TIC (22.247) mg/kg 0.104 J Unknown - TIC (22.295) mg/kg 0.505 J Unknown - TIC (22.3) mg/kg 0.125 J Unknown - TIC (22.309) mg/kg 0.731 J Unknown - TIC (22.333) mg/kg 3 J Unknown - TIC (22.555) mg/kg 0.596 J Unknown - TIC (22.796) mg/kg 1.83 J Unknown - TIC (4.545) mg/kg 1.15 J Unknown - TIC (4.546) mg/kg 0.6 J Unknown - TIC (4.55) mg/kg 0.814 J Unknown - TIC (8.051) mg/kg 0.531 J Unknown - TIC (8.677) mg/kg 0.222 J Unknown Alkane - TIC (10.815) mg/kg 0.196 J Unknown Alkane - TIC (11.378) mg/kg 0.346 J Unknown Alkane - TIC (11.605) mg/kg 0.355 J Unknown Alkane - TIC (11.903) mg/kg 0.282 J Unknown Alkane - TIC (13.228) mg/kg 0.592 J Unknown Alkane - TIC (13.232) mg/kg 0.334 J Unknown Alkane - TIC (14.658) mg/kg 1.53 J Unknown Alkane - TIC (14.879) mg/kg 0.419 J 1.94 J Unknown Alkane - TIC (14.884) mg/kg 0.79 J 1.63 J 0.203 J Unknown Alkane - TIC (14.889) mg/kg 2.9 J 1.8 J Unknown Alkane - TIC (14.894) mg/kg 1.68 J Unknown Alkane - TIC (15.678) mg/kg 0.826 J Unknown Alkane - TIC (15.679) mg/kg 0.384 J 0.967 J Unknown Alkane - TIC (15.683) mg/kg 1.22 J 0.562 J Unknown Alkane - TIC (16.435) mg/kg 0.272 J Unknown Alkane - TIC (16.449) mg/kg 4.29 J Unknown Alkane - TIC (17.138) mg/kg 0.0796 J Unknown Alkane - TIC (17.142) mg/kg 0.396 J Unknown Alkane - TIC (17.147) mg/kg 1.02 J 0.753 J Unknown Alkane - TIC (17.619) mg/kg 27.7 J Unknown Alkane - TIC (17.802) mg/kg 2.97 J 0.328 J Unknown Alkane - TIC (17.812) mg/kg 4.59 J 2.46 J Unknown Alkane - TIC (17.817) mg/kg 6.38 J Unknown Alkane - TIC (17.821) mg/kg 13.5 J 9.3 J Unknown Alkane - TIC (18.428) mg/kg 0.5 J 0.849 J Unknown Alkane - TIC (18.828) mg/kg 13.4 J Unknown Alkane - TIC (19.02) mg/kg 1.15 J 0.232 J Unknown Alkane - TIC (19.025) mg/kg 1.83 J 2.08 J 0.936 J Unknown Alkane - TIC (19.03) mg/kg 3.96 J 1.42 J Unknown Alkane - TIC (19.035) mg/kg 3.27 J Unknown Alkane - TIC (19.088) mg/kg 0.503 J Unknown Alkane - TIC (19.983) mg/kg 2.79 J Unknown Alkane - TIC (20.21) mg/kg 0.366 J Unknown Amide - TIC (8.094) mg/kg 0.784 J Unknown Amide - TIC (8.095) mg/kg 3.39 J Unknown Cholestanol - TIC (19.988) mg/kg 2.94 J Unknown Decanal - TIC (12.626) mg/kg 1.48 J 0.285 J Unknown Decanal - TIC (13.473) mg/kg 3.88 J 0.404 J Unknown Decanal - TIC (14.311) mg/kg 0.511 J Unknown Decanal - TIC (14.316) mg/kg 0.898 J 0.49 J 0.448 J 0.105 J Unknown Decanal - TIC (14.32) mg/kg 3.94 J Unknown Decanal - TIC (14.325) mg/kg 5.08 J Unknown Decanal - TIC (14.34) mg/kg 41.1 J Unknown Decanal - TIC (14.35) mg/kg 0.286 J Unknown Decanal - TIC (15.736) mg/kg 2.27 J Unknown Decanal - TIC (15.948) mg/kg 0.278 J Unknown Decanal - TIC (15.953) mg/kg 0.455 J 0.114 J 0.433 J 0.0825 J Unknown Decanal - TIC (15.958) mg/kg 0.262 J Unknown Decanal - TIC (15.963) mg/kg 4.89 J 3.37 J 14.3 J Unknown Decanal - TIC (15.967) mg/kg 19.4 J Unknown Decanal - TIC (15.996) mg/kg 0.548 J Unknown Decanal - TIC (17.403) mg/kg 0.0936 J 0.135 J Unknown Decanal - TIC (17.407) mg/kg 0.428 J 3.39 J Unknown Decanal - TIC (17.412) mg/kg 1.08 J Unknown Decanal - TIC (17.417) mg/kg 4.93 J 2.33 J Unknown Decanal - TIC (17.455) mg/kg 0.208 J Unknown Decanal - TIC (8.253) mg/kg 0.736 J Unknown Decanal - TIC (8.629) mg/kg 0.37 J Unknown Decanal - TIC (9.264) mg/kg 0.181 J Unknown Decanone - TIC (14.975) mg/kg 0.358 J Unknown Decanone - TIC (14.985) mg/kg 2.63 J Unknown Decanone - TIC (16.55) mg/kg 3.39 J 0.843 J Unknown Decanone - TIC (9.664) mg/kg 0.374 J Unknown Sitosterol - TIC (20.47) mg/kg 2.23 J 0.971 J Unknown Sitosterol - TIC (20.48) mg/kg 1.28 J Unknown Sitosterol - TIC (20.499) mg/kg 0.0936 J Unknown Sitosterol - TIC (20.547) mg/kg 22.2 J PAHs by GC/MS-SIM - Mansfield Lab

2-Methylnaphthalene mg/kg 0.00303 J 0.00574 0.0852 0.0118 J 0.00869 U 0.00738 U 0.00497 U 0.003 J 0.00346 J 0.00458 U 0.00458 U 0.00454 U 0.0144 J…