TU002_GW_January_2020.pdf

LABORATORIES, INC.

1835 W. 205th Street Torrance, CA 9050 1 Tel: (310) 618-8889

Date: 01-22-2020 EMAX Batch No.: 20A093

Attn: Bryan Jones

CH2M Hill 2525 Airpark Drive Redding CA 96001

Subject: Laboratory Report Project: BEALE AFB LTO&M TU002 2020

Enclosed is the Laboratory report for samples received on 01/16/20.

The data reported relate only to samples listed below

Sample ID Control # Col Date Matrix

TU02_MW-11_0120 A093-01 01/13/20 WATER

TU02_MW-11_0120MS A093-01M 01/13/20 WATER

TU02_MW-11_0120MSD A093-01S 01/13/20 WATER

TU02_TB01-0120 A093-02 01/13/20 WATER

TU02_MW-1_0120 A093-03 01/14/20 WATER

TU02_MW-13_0120 A093-04 01/14/20 WATER

TU02_MW-6_0120 A093-05 01/14/20 WATER

TU02_MW-23_0120 A093-06 01/15/20 WATER

The results are summarized on the following pages.

Please feel free to call if you have any questions concerning these results.

Sincerely yours, _ API I )

Caspar J. Pang Laboratory Director

Analysis

VOLATILE ORGANICS BY GC/MS

VOLATILE ORGANICS BY GC/MS

VOLATILE ORGANICS BY GC/MS

VOLATILE ORGANICS BY GC/MS

VOLATILE ORGANICS BY GC/MS

VOLATILE ORGANICS BY GC/MS

VOLATILE ORGANICS BY GC/MS

VOLATILE ORGANICS BY GC/MS

This report is confidential and intended solely for the use of the individual or entity to whom it is addressed. This report shall not be reproduced except in full or without the written approval of EMAX.

EMAX certifies that results included in this report meets all TNI & DOD requirements unless noted in the Case Narrative.

NELAP Accredited Certificate Number CA002912018-15 ANAB Accredited DoD ELAP and ISO/IEC 17025 Certificate Number L2278 Testing California ELAP Accredited Certificate Number 2672

REPORT ID: 20A093 Page 1 of 253

Z00r0C13

.JACOBS ch~ CHAIN OF CUSTODY RECORD 11151202010:33:26 AM Page 1 OF 1

Project Name BAFB Container: 40 mL Glass

Location BealeAFB 4'C Preservatives:

Project Number 456998.09.23.CM.RA.20

Project Manager Ben Dykstra Filtered: NA

Sample Manager Kevin Roberts Holding Time: 7

(530) 604-4129 OJ

I -I

Task Order 00075 ~ Project BEALE AFB L TO&M TU002 2020 OJ:'; z m» t:

Turnaround Time 7 Days ~;;: 3 .... men atg~ 0-

Shipping Date: 1/15/2020 '< -u J\)

::T m ", Q, COC Number: EMXT207 o~o

0 C::m IJJ =.» 0

~m ::J or -oj 5' m ~ ';;: C/J

DATE TIME Matrix -I COMMENTS

TU02_MW-11_0120 1/13/2020 13:42 Water X 3 ( TU02_MW-11_0120MS 1/13/2020 13:42 Water X 3 I

\ TU02_MW-11_0120SD 1/13/2020 13:42 Water X 3 ~ TU02_TB01-0120 1/13/2020 7:00 Water X 3 ~ TU02_MW-1_0120 1/14/2020 6:02 Water X 3 , TU02_MW-13_0120 1/14/2020 5:38 Water X 3 , TU02_MW-6_0120 1/14/2020 6:25 Water X 3 I

Ufru02_MW-23_0120 I 1/15/202() I 8:40 I Water r X 1- -- --- I 3 I

I TOTAL NUMBER OF CONTAINERS 1 241

Signatures Date/Time Shipping Details Special Instructions:

Approved by ATTN:

... ILL....-~ MethOdBhiPment: Fed Ex Sampled by '''"'"""'-.. . 1>1 zo 070()

'cll"."lsh" by 1 ~ r; ="" N!Pi:> o~ I~, y~ "0 S,m •• C"""dy Received by 1['. , I ').- q' ~ Alrblll No. and v • • [..i,...,;> - > 0 . Report Copy to Relinquished by Lab Name: EMAX LaboratOries, Inc. Andy Mai bryan.jones10@jacobs.com

Received by Lab Phone: (310) 618-8889 (530) 229-3350 ttm?· 2->lu REPORT ID: 20A093 Page 2 of 253

SAMPLE RECEIPT FORM 1

'~Fedex Type of DclivelY AU'billl Tracking Number o UPS o GSO o Others "':}1"1-'1 ~U401 .J-vtSO n EMAX Courier o Client Delivery

COC INSPECTION

.$Client Name WClient PMlFC ~~mpler Name r;;l'$ampling Daterrime

0""Address 9'Tclll / Fax II ~ouricr Signatllre !:}Analysis Required

Safety Issues (ifany) o High concentrations expected o From Superfund Site ORad screening required

Note:

PACKAGING INSPECTION

Container yr'l:ooler o Box o Other

Condition o Custody Seal o Intact o Damaged

Packaging ¢'~bble Pack o Styrofoam o Popcom

Tcn1peratures ~ooler 11. ,\.I °c o Cooler 2 ---°c o Cooler 3 --- °c (Cool, :-:6 °C but not [TOZCJl) o Cooler 6 °c o Cooler 7 °c o Cooler 8 °c

(!)SIN IGiZ3ffli\:JLj

Thermometer: B-SIN C-SIN Iq l?'«,j '-Ilol.

Comments: o Temperature is out of range. PM was informed IMMEDIATELY.

Note:

DISCREPANCIES

LabSamplelD LabSampleContainerlD Code ClientSample Label lD / Information

.,-... -"~-' .- .v."",~ .• ",,,~~,.,, '""_·.· .. ~.~m_ '--..

/.,...-r

(' -- It/II / ·If\Ill~..;.t)

Reference: EMAX-SM02 Rev.ll

Form: SM02Fl

ECN 'LO A(2g~ , Reeipicllt!?:O-S1 e CA1Ztz.,llo Date , IllOlLO Time [.1, ~

~a;nple ID -erMatrix o Preservative (if any) ~AT o Sufficient 0 o Cooler 4 °c o Cooler 5 °c --- ---o Cooler 9 °c o Cooler 10 °c --- .. --~

D-SIN

Con'ecti ve Action o pH holdmg hme reql1ll"ement for water samples IS 15 mlns. Water samples for pH analYSIS are receIved beyond 15 mlJlutes from sampllJlg lIme.

NOTES/OBSERVA TlONS:

LEGEND:

Code Description- Sample Management

Dl Analysis is not indicated in ____ ~

D2 Analysis mismatch COC vs label

D3 Sample lD mismatch COC vs label

D4 Sample lD is not indicated in ___ _

DS Container -[improper] [leaking] [broken]

D6 Date/Time is not indicated in ___ _

D7 Daterrime mismatch COC vs label

D8 Sample listed in COC is not received

D9 Sample received is not listed in COC

DIO No initial/date on con'ections in COClJabel

Dl I Container count mismatch COC vs received

DI2 Container size mismatch coe vs received

REVIEWS:

S amp Ie La beli ng -\.-\"t-r7'lL.U~'-'-+'--+' Date --'-I-'-..:L..\...!::..:'C..-+-..:.;t.!L

Code Description-Sample Management

DB Out of Holding Time

D14 Bubble is >6mm

DIS No trip blank in cooler

D16 Preservation not indicated in ____ _

D17 Preservation mismatch COC vs label

D18 Insufficient chemical preservative

D19 Insufficient Sample

D20 No filtration info for dissolved analysis

D21 No sample for moisture detennination

D22 ------------------------------------- 023 -------------------------------------

SRF ____ 1Y++~r==--- Date _____ -f~~~~ ____ _ o Continue to next page.

Code Description-Sample Management

Rl Proceed as indicated in 0 COC 0 Label

R2 Refer to attached instruction

R3 Cancel the analysis

R4 Use vial with smallest bubble fjr>l

RS Log-in with latest sampling date and time+ I min

R6 Adjust pH as necessary

R7 Filter and preserved as necessary

R8 ------------------------------------ I~ ______________________________ ___

RIO

RII __________________________________ __

RIZ __________________________________ __

PM --=:h;.,..,--""=...".....------~ Date -,1'-/cpq...Y..:th"-i-/_1D __ _

ENIAX Laboratories, Inc. J 8:1S 'vY. 20Sth St., Torrance, Ca 90501

REPORT ID: 20A093 Page 3 of 253

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REPORT ID: 20A093 Page 4 of 253

REPORTING CONVENTIONS

OAT A QUALIFIERS:

Lab Qualifier AFCEE Qualifier Description

J F Indicates that the analyte is positively identified and the result is less than LOQ/RL but greater than LOD/MDLlDL.

N Indicates presumptive evidence of a compound.

B B Indicates that the analyte is found in the associated method blank as well as in the sample at above QC level.

E J Indicates that the result is above the maximum calibration range or estimated value.

* * Out of QC limit.

Note: The above qualifiers are used to flag the results unless the project requires a different set of qualification criteria.

ACRONYMS AND ABBREVIATIONS:

CRDL Contract Required Detection Limit RL Reporting Limit MRL Method Reporting Limit MOL Method Detection Limit DL Detection Limit LOD Limit of Detection LOQ Limit of Quantitation DO Diluted out

DATES

The date and time information for leaching and preparation reflect the beginning date and time of the procedure unless the method, protocol, or project specifically requires otherwise.

REPORT ID: 20A093 Page 5 of 253

SUMMARY PACKAGE

VOLATILE ORGANICS

REPORT ID: 20A093 Page 6 of 253

CASE NARRATIVE

Client : CH2M HILL

Project: BEALE AFB LTO&M TU002 2020

SDG 20A093

METHOD SW5030B/8260B

VOLATILE ORGANICS BY GC/MS

A total of six(6) water samples were received on 01/16/20 to be analyzed for Volatile Organics by GC/MS in accordance with Method SW5030B/8260B and project specific requirements.

Holding Time Samples were analyzed within the prescribed holding time.

Instrument Performance and Calibration Instrument tune check was performed prior to calibration. Result was within acceptance criteria. Multi-calibration points were generated to establish initial calibration (ICAL). ICAL was verified using secondary source (ICV).

Continuing calibration (CCV) was carried out at a frequency required by the project. There were four(4)CCVs (Data file IDs: RAC351, RAC376, RAC395 and RAC421) associated with this SDG. All calibration requirements were satisfied.

Refer to calibration summary forms of ICAL, ICV and CCV for details.

Method Blank Method blank was prepared and analyzed at the frequency required by the project.

For this SDG, two(2) method blanks were analyzed. V067A12B and V067A13B were compliant to project requirement. Refer to sample result summary forms for details.

Lab Control Sample Lab control sample was prepared and analyzed at a frequency required by the project. For this SDG, two(2) sets of LCS/LCD were analyzed. V067A12L/V067A12C and V067A13L/V067A13C were within LCS limits. Refer to LCS summary forms for details.

Matrix QC Sample Matrix spike sample was prepared and analyzed at a frequency required by the project. For this SDG, one (1) set of MS/MSD was analyzed. A093-01M/A093-01S -all analytes were within MS QC limits. Refer to Matrix QC summary form for details.

Surrogate Surrogates were added on QC and field samples. All surrogate recoveries were within QC limits. Refer to sample result summary forms for details.

Sample Analysis Samples were analyzed according to prescribed analytical procedures. Results were evaluated in accordance to project requirements. For this SDG, all quality control requirements were met.

REPORT ID: 20A093 Page 7 of 253

LAB CHRONICLE

VOLATILE ORGANICS BY GC/MS

Cl ient Project

CH2M HILL

BEALE AFB LTO&M TU002 2020

SDG NO. 20A093

Instrument ID 67

WATER

Cl ient Laboratory Di luti on % Analysis Extraction Sample Calibration Prep.

Sample ID Sample ID Factor Moist DateTime DateTime Data FN Data FN Batch Notes MBLK1W V067A12B NA 01/17/2012:47 01/17/2012:47 RAC355 RAC301 V067A12 Method Blank LCS1W V067A12L NA 01/17/2011:29 01/17/2011:29 RAC352 RAC301 V067A12 Lab Control Sample (LCS) LCD1W V067A12C NA 01/17/2011:56 01/17/2011:56 RAC353 RAC301 V067A12 LCS Duplicate TU02_MW-11_0120 A093-01 NA 01/17/2017:04 01/17/2017:04 RAC365 RAC301 V067A12 Field Sample TU02_TB01-0120 A093-02 NA 01/17/2017:30 01/17/2017:30 RAC366 RAC301 V067A12 Field Sample TU02_MW-11_0120MS A093-01M NA 01/17/2017:55 01/17/2017:55 RAC367 RAC301 V067A12 Matrix Spike Sample (MS) TU02_MW-11_0120MSD A093-01S NA 01/17/2018:21 01/17/2018:21 RAC368 RAC301 V067A12 MS Duplicate (MSD) TU02_MW-1_0120 A093-03 NA 01/17/2019:14 01/17/2019:14 RAC370 RAC301 V067A12 Field Sample TU02_MW-13_0120 A093-04 NA 01/17/2019:40 01/17/2019:40 RAC371 RAC301 V067A12 Field Sample TU02_MW-6_0120 A093-05 NA 01/17/2020:05 01/17/2020:05 RAC372 RAC301 V067A12 Field Sample TU02_MW-23_0120 A093-06 NA 01/17/2020:31 01/17/2020:31 RAC373 RAC301 V067A12 Field Sample MBLK2W V067A13B NA 01/21/2013:05 01/21/2013:05 RAC399 RAC301 V067A13 Method Blank LCS2W V067A13L NA 01/21/2011:49 01/21/2011:49 RAC396 RAC301 V067A13 Lab Control Sample (LCS) LCD2W V067A13C 1 NA 01/21/2012:15 01/21/2012:15 RAC397 RAC301 V067A13 LCS Duplicate TU02_MW-23_0120DL A093-06I 5 NA 01/21/2013:31 01/21/2013:31 RAC400 RAC301 V067A13 Diluted Sample

FN - Filename % Moist - Percent Moisture

REPORT ID: 20A093 Page 8 of 253

SAMPLE RESULTS

REPORT ID: 20A093 Page 9 of 253

METHOD SW5030B/8260B

============================================================================== Client CH2M HILL Date Collected: 01/13/20 Project BEALE AFB LTO&M TU002 2020 Date Received: 01/16/20 Batch No. 20A093 Date Extracted: 01/17/20 17:04 Sample ID: TU02 MW-11 - 0120 Date Analyzed: 01/17/20 17:04 Lab Samp ID: A093-=-01 Dilution Factor: 1 Lab Fi le ID: RAC365 Matrix WATER Ext Btch ID: V067A12 % Moisture NA Cal ib. Ref.: RAC301 Instrument ID 67 ==============================================================================

RESULTS LOQ DL LOD PARAMETERS (ug/L) (ug/L) (ug/L) (ug/L) ---------- BENZENE ND 1.0 0.10 0.20 ETHYLBENZENE ND 1.0 0.10 0.20 M,P-XYLENES ND 2.0 0.21 0.40 TERT-BUTYL METHYL ETHER 0.70J 1.0 0.13 0.20 O-XYLENE ND 1.0 0.10 0.20 TOLUENE ND 1.0 0.10 0.20 XYLENES, TOTAL ND 2.0 0.10 0.20 TERT-AMYL METHYL ETHER ND 1.0 0.11 0.20 ETHYL TERT-BUTYL ETHER ND 1.0 0.11 0.20 TERT-BUTYL ALCOHOL ND 10 2.5 5.0 ISOPROPYL ETHER ND 1.0 0.11 0.20

SURROGATE PARAMETERS RESULTS SPK_AMT % RECOVERY QC LIMIT -------------------- ---------- --------1,2-DICHLOROETHANE-D4 9.05 10.00 90.5 81-118 BROMOFLUOROBENZENE 9.83 10.00 98.3 85-114 TOLUENE-D8 9.80 10.00 98.0 89-112 DIBROMOFLUOROMETHANE 9.30 10.00 93.0 80-119

REPORT ID: 20A093 Page 10 of 253

Cl ient CH2M HILL Date Collected: 01/13/20 Project BEALE AFB LTO&M TU002 2020 Date Received: 01/16/20 Batch No. 20A093 Date Extracted: 01/17/20 17:30 Sample ID: TU02_TB01-0120 Date Analyzed: 01/17/20 17:30 Lab Samp 10: A093-02 Dilution Factor: 1 Lab Fi le ID: RAC366 Matrix WATER Ext Btch ID: V067A12 % Moisture NA Cal ib. Ref. : RAC301 Instrument ID 67

RESULTS LOQ DL LOD

PARAMETERS (ug/L) (ug/L) (ug/l) (ug/L)

BENZENE NO 1.0 0.10 0.20

ET HYLBENZENE NO 1.0 0.10 0.20

M,P-XYLENES NO 2.0 0.21 0.40

TERT-BUTYL METHYL ETHER NO 1.0 0.13 0.20

O-XYLENE NO 1.0 0.10 0.20

TOLUENE NO 1.0 0.10 0.20

XYLENES, TOTAL NO 2.0 0.10 0.20

TERT-AMYL METHYL ETHER NO 1.0 0.11 0.20

ETHYL TERT-BUTYL ETHER NO 1.0 0.11 0.20

TERT-BUTYL ALCOHOL NO 10 2.5 5.0

ISOPROPYL ETHER NO 1.0 0.11 0.20

SURROGATE PARAMETERS RESULTS SPK_AMT % RECOVERY QC LIMIT

1,2-DICHLOROETHANE-D4 9.48 10.00 94.8 81-118

BROMOFLUOROBENZENE 9.74 10.00 97.4 85-114

TOLUENE-D8 9.73 10.00 97.3 89-112

DIBROMOFLUOROMETHANE 9.46 10.00 94.6 80-119

REPORT ID: 20A093 Page 11 of 253

Cl ient CH2M HILL Date Collected: 01/14/20 Project BEALE AFB LTO&M TU002 2020 Date Received: 01/16/20 Batch No. 20A093 Date Extracted: 01/17/20 19: 14 Sample ID: TU02 MW-1 0120 Date Analyzed: 01/17/20 19:14 Lab Samp ID: A093-=-03 - Dilution Factor: 1 Lab Fi le ID: RAC370 Matrix WATER Ext Btch ID: V067A12 % Moisture NA Calib. Ref.: RAC301 Instrument ID 67

RESULTS LOa DL LOD PARAMETERS (ug/L) (ug/L) ( ug/L) (ug/L)

BENZENE ND 1.0 0.10 0.20

ETHYLBENZENE ND 1.0 0.10 0.20

M,P-XYLENES ND 2.0 0.21 0.40

TERT-BUTYL METHYL ETHER 38 1.0 0.13 0.20

O-XYLENE ND 1.0 0.10 0.20

TOLUENE ND 1.0 0.10 0.20

XYLENES, TOTAL ND 2.0 0.10 0.20

TERT-AMYL METHYL ETHER ND 1.0 0.11 0.20

ETHYL TERT-BUTYL ETHER ND 1.0 0.11 0.20

TERT-BUTYL ALCOHOL ND 10 2.5 5.0

ISOPROPYL ET HER ND 1.0 0.11 0.20

SURROGATE PARAMETERS RESULTS SPK AMT % RECOVERY ac LIMIT

1,2-DICHLOROETHANE-D4 9.67 10.00 96.7 81-118

BROMOFLUOROBENZENE 9.63 10.00 96.3 85 -114

TOLUENE-D8 9.55 10.00 95.5 89-112

DIBROMOFLUOROMETHANE 9.61 10.00 96.1 80-119

REPORT ID: 20A093 Page 12 of 253

Client CH2M HILL Date Collected: 01/14/20 Project BEALE AFB LTO&M TU002 2020 Date Received: 01/16/20 Batch No. 20A093 Date Extracted: 01/17/20 19:40 Sample ID: TU02 MW-13 0120 Date Analyzed: 01/17/20 19:40 Lab Samp ID: A093:04 - Dilution Factor: 1 Lab Fi le ID: RAC371 Matrix WATER Ext Btch ID: V067A12 % Moisture NA Cal ib. Ref. : RAC301 Instrument ID 67

RESULTS LOO DL LOD

PARAMETERS (ug/L) (ug/L) ( ug/l) (ug/L)

BENZENE ND 1.0 0.10 0.20

ETHYL BENZENE ND 1.0 0.10 0.20

M,P-XYLENES ND 2.0 0.21 0.40

TERT-BUTYL METHYL ETHER 83 1.0 0.13 0.20

O-XYLENE ND 1.0 0.10 0.20

TOLUENE ND 1.0 0.10 0.20

XYLENES, TOTAL ND 2.0 0.10 0.20

TERT-AMYL METHYL ETHER 0.12J 1.0 0.11 0.20

ETHYL TERT-BUTYL ETHER ND 1.0 0.11 0.20

TERT-BUTYL ALCOHOL ND 10 2.5 5.0

ISOPROPYL ETHER ND 1.0 0.11 0.20

SURROGATE PARAMETERS RESULTS SPK AMT % RECOVERY OC LIMIT

1,2-DICHLOROETHANE-D4 9.60 10.00 96.0 81-118

BROMOFLUOROBENZENE 9.46 10.00 94.6 85-114

TOLUENE-D8 9.64 10.00 96.4 89-112

DIBROMOFLUOROMETHANE 9.52 10.00 95.2 80-119

REPORT ID: 20A093 Page 13 of 253

METHOD SWS030B/8260B

Cl ient CH2M HILL Date Collected: 01/14/20 Project BEALE AFB LTO&M TU002 2020 Date Received: 01/16/20 Batch No. 20A093 Date Extracted: 01/17/20 20:0S Sample ID: TU02 MW-6 0120 Date Analyzed: 01/17/20 20:0S Lab Samp ID: A093-=-OS - Dilution Factor: 1 Lab Fi le ID: RAC372 Matrix WATER Ext Btch ID: V067A12 % Moisture NA Cal ib. Ref. : RAC301 Instrument ID 67

RESULTS LOQ DL LOD

PARAMETERS (ug/L) (ug/L) (ug/L) (ug/L)

BENZENE ND 1.0 0.10 0.20

ETHYL BENZENE ND 1.0 0.10 0.20

M,P-XYLENES ND 2.0 0.21 0.40

TERT-BUTYL METHYL ETHER 1.7 1.0 0.13 0.20

O-XYLENE ND 1.0 0.10 0.20

TOLUENE ND 1.0 0.10 0.20

XYLENES, TOTAL ND 2.0 0.10 0.20

TERT-AMYL METHYL ETHER ND 1.0 0.11 0.20

ETHYL TERT-BUTYL ETHER ND 1.0 0.11 0.20

TERT-BUTYL ALCOHOL ND 10 2.S S.O

ISOPROPYL ETHER ND 1.0 0.11 0.20

SURROGATE PARAMETERS RESULTS SPK AMT % RECOVERY QC LIMIT

1,2-DICHLOROETHANE-D4 9.78 10.00 97.8 81-118

BROMOFLUOROBENZENE 9.60 10.00 96.0 8S-114

TOLUENE-D8 9.6S 10.00 96.S 89-112

DIBROMOFLUOROMETHANE 9.64 10.00 96.4 80-119

REPORT ID: 20A093 Page 14 of 253

Cl ient CH2M HILL Date Collected: 01/15/20 Project BEALE AFB LTO&M TU002 2020 Date Received: 01/16/20 Batch No. 20A093 Date Extracted: 01/17/20 20:31 # 01/21/20 13:31 Sample ID: TU02 MW-23 0120 Date Analyzed: 01/17/20 20:31 # 01/21/20 13:31 Lab Samp ID: A093~06 #A093-06I Dilution Factor: 1 # 5 Lab Fi le ID: RAC373 #RAC400 Matrix WATER Ext Btch ID: V067A12 #V067A13 % Moisture NA Cal ib. Ref.: RAC301 #RAC301 Instrument ID 67

RESULTS LOQ DL LOD

PARAMETERS (ug/L) (ug/L) (ug/L) (ug/L)

BENZENE ND 1.0 0.10 0.20

ETHYL BENZENE ND 1.0 0.10 0.20

M,P-XYLENES ND 2.0 0.21 0.40

# TERT-BUTYL METHYL ETHER 150 5.0 0.65 1.0

O-XYLENE ND 1.0 0.10 0.20

TOLUENE ND 1.0 0.10 0.20

XYLENES, TOTAL ND 2.0 0.10 0.20

TERT-AMYL METHYL ETHER 0.17J 1.0 0.11 0.20

ETHYL TERT-BUTYL ETHER ND 1.0 0.11 0.20

TERT-BUTYL ALCOHOL ND 10 2.5 5.0

ISOPROPYL ETHER ND 1.0 0.11 0.20

SURROGATE PARAMETERS RESULTS SPK_AMT % RECOVERY QC LIMIT

1,2-DICHLOROETHANE-D4 9.95 10.00 99.5 81-118

BROMOFLUOROBENZENE 9.33 10.00 93.3 85-114

TOLUENE-D8 9.54 10.00 95.4 89-112

DIBROMOFLUOROMETHANE 9.66 10.00 96.6 80-119

# 1,2-DICHLOROETHANE-D4 46.3 50.00 92.7 81-118

# BROMOFLUOROBENZENE 48.2 50.00 96.5 85-114

# TOLUENE-D8 48.1 50.00 96.2 89-112

# DIBROMOFLUOROMETHANE 47.7 50.00 95.4 80-119

# Members of the Associated File

REPORT ID: 20A093 Page 15 of 253

CL ient CH2M HILL Date CoLLected: 01/15/20 Project BEALE AFB LTO&M TU002 2020 Date Received: 01/16/20 Batch No. 20A093 Date Extracted: 01/17/20 20:31 SampLe ID: TU02 MW-23 0120 Date AnaLyzed: 01/17/20 20:31 Lab Samp ID: A093-=-06 - DiLution Factor: 1 Lab Fi Le ID: RAC373 Matrix WATER Ext Btch ID: V067A12 % Moisture NA CaL ib. Ref. : RAC301 Instrument ID 67

RESULTS LOQ DL LOD

PARAMETERS (ug/L) (ug/L) (ug/L) (ug/L)

BENZENE ND 1.0 0.10 0.20

ETHYL BENZENE ND 1.0 0.10 0.20

M,P-XYLENES ND 2.0 0.21 0.40

TERT-BUTYL METHYL ETHER 170E 1.0 0.13 0.20

O-XYLENE ND 1.0 0.10 0.20

TOLUENE ND 1.0 0.10 0.20

XYLENES, TOTAL ND 2.0 0.10 0.20

TERT-AMYL METHYL ETHER 0.17J 1.0 0.11 0.20

ETHYL TERT-BUTYL ETHER ND 1.0 0.11 0.20

TERT-BUTYL ALCOHOL ND 10 2.5 5.0

ISOPROPYL ETHER ND 1.0 0.11 0.20

SURROGATE PARAMETERS RESULTS SPK_AMT % RECOVERY QC LIMIT

1,2-DICHLOROETHANE-D4 9.95 10.00 99.5 81-118

BROMOFLUOROBENZENE 9.33 10.00 93.3 85-114

TOLUENE-D8 9.54 10.00 95.4 89-112

DIBROMOFLUOROMETHANE 9.66 10.00 96.6 80-119

REPORT ID: 20A093 Page 16 of 253

Cl ient CH2M HILL Date Collected: 01/15/20 Project BEALE AFB LTO&M TU002 2020 Date Received: 01/16/20 Batch No. 20A093 Date Extracted: 01/21/20 13:31 Sample ID: TU02 MW-23 0120DL Date Analyzed: 01/21/20 13:31 Lab Samp ID: A093-=-06I - Dilution Factor: 5 Lab Fi le ID: RAC400 Matrix WATER Ext Btch ID: V067A13 % Moisture NA Cal ib. Ref. : RAC301 Instrument ID 67

RESULTS LOQ DL LOD

PARAMETERS (ug/L) (ug/L) (ug/L) (ug/L)

BENZENE ND 5.0 0.50 1.0

ETHYL BENZENE ND 5.0 0.50 1.0

M,P-XYLENES ND 10 1.0 2.0

TERT-BUTYL METHYL ETHER 150 5.0 0.65 1.0

O-XYLENE ND 5.0 0.50 1.0

TOLUENE NO 5.0 0.50 1.0

XYLENES, TOTAL NO 10 0.50 1.0

TERT-AMYL METHYL ETHER NO 5.0 0.55 1.0

ETHYL TERT-BUTYL ETHER NO 5.0 0.55 1.0

TERT-BUTYL ALCOHOL ND 50 12 25

ISOPROPYL ETHER ND 5.0 0.55 1.0

SURROGATE PARAMETERS RESULTS SPK_AMT % RECOVERY QC LIMIT

1,2-DICHLOROETHANE-D4 46.3 50.00 92.7 81-118

BROMOFLUOROBENZENE 48.2 50.00 96.5 85-114

TOLUENE-D8 48.1 50.00 96.2 89-112

DIBROMOFLUOROMETHANE 47.7 50.00 95.4 80-119

REPORT ID: 20A093 Page 17 of 253

QC SUMMARIES

REPORT ID: 20A093 Page 18 of 253

Cl i ent CH2M HILL Date Collected: NA Project BEALE AFB LTO&M TU002 2020 Date Received: 01/17/20 Batch No. 20A093 Date Extracted: 01/17/20 12:47 Sample ID: MBLK1W Date Analyzed: 01/17/20 12:47 Lab Samp ID: V067A12B Di lution Factor: 1 Lab Fi le ID: RAC355 Matrix WATER Ext Btch ID: V067A12 % Moisture NA Cal ib. Ref. : RAC301 Instrument ID 67

RESULTS LOQ DL LOD

PARAMETERS (ug/L) (ug/L) (ug/L) (ug/L)

BENZENE ND 1.0 0.10 0.20

ETHYL BENZENE ND 1.0 0.10 0.20

M,P-XYLENES ND 2.0 0.21 0.40

TERT-BUTYL METHYL ETHER ND 1.0 0.13 0.20

O-XYLENE ND 1.0 0.10 0.20

TOLUENE ND 1.0 0.10 0.20

XYLENES, TOTAL ND 2.0 0.10 0.20

TERT-AMYL METHYL ETHER ND 1.0 0.11 0.20

ETHYL TERT-BUTYL ETHER ND 1.0 0.11 0.20

TERT-BUTYL ALCOHOL ND 10 2.5 5.0

ISOPROPYL ETHER ND 1.0 0.11 0.20

SURROGATE PARAMETERS RESULTS SPK_AMT % RECOVERY QC LIMIT

1,2-DICHLOROETHANE-D4 9.49 10.00 94.9 81-118

BROMOFLUOROBENZENE 9.58 10.00 95.8 85-114

TOLUENE-D8 9.67 10.00 96.7 89-112

DIBROMOFLUOROMETHANE 9.40 10.00 94.0 80-119

REPORT ID: 20A093 Page 19 of 253

CLI ENT:

PROJECT:

BATCH NO.:

METHOD:

CH2M HILL

BEALE AFB LTO&M TU002 2020

20A093

SW5030B/8260B

EMAX QUALITY CONTROL DATA

LCS/LCD ANALYSIS

MATRIX: WATER % MOISTURE: NA

DILUTION FACTOR: 1

SAMPLE ID: MBLK1W

LAB SAMP ID: V067A12B V067A12L V067A12C

LAB FILE ID: RAC355 RAC352 RAC353

DA TE EXTRACTED: 01/17/2012:47 01/17/2011:29 01/17/2011:56 DATE COLLECTED: NA

DATE ANALYZED: 01/17/2012:47 01/17/2011 :29 01/17/2011:56 DATE RECEIVED: 01/17/20

PREP. BATCH: V067A12 V067A12 V067A12

CALIB. REF: RAC301 RAC301 RAC301

ACCESSION:

BLNK RSLT SPIKE AMT BS RSLT BS SPIKE AMT BSD RSLT BSD RPD QC LIMIT

PARAMETER (ug/L) (ug/L) (ug/L) % REC (ug/L) (ug/L) % REC ( % ) ( % ) Benzene ND 10.0 9.92 99 10.0 10.2 102 3 79·120 Ethylbenzene ND 10.0 9.25 92 10.0 9.52 95 3 79-121 m,p-Xylenes ND 20.0 18.7 94 20.0 19.1 95 2 80-121 tert-butyl Methyl ether ND 10.0 9.27 93 10.0 9.95 99 7 71-124 o-Xylene ND 10.0 9.64 -;6 10.0 9.88 99 2 78-122 Toluene ND 10.0 9.44 94 10.0 9.62 96 2 80-121 Xylenes, Total ND 30.0 28.3 94 30.0 28.9 96 2 79-121 tert-Amyl methyl ether ND 10.0 9.72 97 10.0 10.4 104 7 68-128 Ethyl tert-butyl ether ND 10.0 9.04 90 10.0 9.51 95 5 70-127 tert-butyl alcohol ND 250 234 94 250 271 108 14 68-129 isopropyl Ether ND 10.0 9.88 99 10.0 10.4 104 5 67-128

SPIKE AMT BS RSLT BS SPIKE AMT BSD RSlT BSD QC LIMIT SURROGATE PARAMETER (ug/L) (ug/l) % REC (ug/l) (ug/l) % REC ( % ) 1,2-Dichloroethane-d4 10.0 9.42 94 10.0 9.83 98 81-118 Bromofluorobenzene 10.0 9.52 95 10.0 9.51 95 85-114 Toluene-d8 10.0 9.65 97 10.0 9.57 96 89-112 Dibromofluoromethane 10.0 9.55 95 10.0 9.61 96 80-119

MAX RPD

REPORT ID: 20A093 Page 20 of 253

Cl ient CH2M HILL Date Collected: NA Project BEALE AFB LTO&M TU002 2020 Date Received: 01/21/20 Batch No. 20A093 Date Extracted: 01/21/20 13:0S Sample ID: MBLK2W Date Analyzed: 01/21/20 13:0S Lab Samp ID: V067A13B Dilution Factor: 1 Lab Fi le ID: RAC399 Matrix WATER Ext Btch ID: V067A13 % Moisture NA Cal ib. Ref. : RAC301 Instrument ID 67

RESULTS LOQ DL LOD

PARAMETERS (ug/L) (ug/L) (ug/L) (ug/L)

BENZENE ND 1.0 0.10 0.20

ETHYLBENZENE ND 1.0 0.10 0.20

M,P-XYLENES ND 2.0 0.21 0.40

TERT-BUTYL METHYL ETHER ND 1.0 0.13 0.20

O-XYLENE ND 1.0 0.10 0.20

TOLUENE ND 1.0 0.10 0.20

XYLENES, TOTAL ND 2.0 0.10 0.20

TERT-AMYL METHYL ETHER ND 1.0 0.11 0.20

ETHYL TERT-BUTYL ETHER ND 1.0 0.11 0.20

TERT-BUTYL ALCOHOL ND 10 2.S S.O

ISOPROPYL ETHER ND 1.0 0.11 0.20

SURROGATE PARAMETERS RESULTS SPK AMT % RECOVERY QC LIMIT

1,2-DICHLOROETHANE-D4 9.S0 10.00 9S.0 81-118

BROMOFLUOROBENZENE 9.54 10.00 95.4 8S-114

TOLUENE-D8 9.S6 10.00 9S.6 89-112

DIBROMOFLUOROMETHANE 9.S3 10.00 9S.3 80-119

REPORT ID: 20A093 Page 21 of 253

BATCH NO.:

METHOD:

CH2M HILL

BEALE AFB LTO&M TU002 2020

20A093

SW5030B/8260B

EMAX QUALITY CONTROL DATA

LCS/LCD ANALYSIS

MATRIX: WATER % MOISTURE: NA

DILUTION FACTOR: 1

SAMPLE ID: MBLK2W

LAB SAMP ID: V067A13B V067A13L V067A13C

LAB FILE 10: RAC399 RAC396 RAC397

DATE EXTRACTED: 01/21/2013:05 01/21/2011:49 01/21/2012:15 DATE COLLECTED: NA

DATE ANALYZED: 01/21/2013:05 01/21/2011:49 01/21/2012:15 DATE RECEIVED: 01/21/20

PREP. BATCH: V067A13 V067A13 V067A13

CALIB. REF: RAC301 RAC301 RAC301

ACCESSION:

BLNK RSLT SPIKE AMT BS RSLT BS SPIKE AMT BSD RSLT BSD RPD QC LIMIT

PARAMETER (ug/L) (ug/L) (ug/L) % REC (ug/L) (ug/L) % REC ( % ) ( % ) Benzene ND 10.0 10.5 105 10.0 10.3 103 1 79-120 Ethylbenzene ND 10.0 9.72 97 10.0 9.63 96 1 79-121 m,p-Xylenes ND 20.0 19.8 99 20.0 19.5 97 1 80-121 tert-butyl Methyl ether ND 10.0 9.40 94 10.0 9.29 93 1 71-124 o-Xylene ND 10.0 10.2 102 10.0 10.1 101 1 78-122 Toluene ND 10.0 9.87 99 10.0 9.84 98 0 80-121 Xylenes, Total ND 30.0 29.9 100 30.0 29.5 98 1 79-121 tert-Amyl methyl ether ND 10.0 10.0 100 10.0 9.99 100 0 68-128 Ethyl tert-butyl ether ND 10.0 9.28 93 10.0 9.10 91 2 70-127 tert-butyl alcohol ND 250 243 97 250 245 98 1 68-129 isopropyl Ether ND 10.0 10.3 103 10.0 10.2 102 1 67-128

SPIKE AMT BS RSLT BS SPIKE AMT BSD RSLT BSD QC LIMIT

SURROGATE PARAMETER (ug/L) (ug/L) % REC (ug/L) (ug/L) % REC ( % ) 1,2-Dichloroethane-d4 10.0 9.47 95 10.0 9.57 96 81-118 Bromofluorobenzene 10.0 9.61 96 10.0 9.37 94 85-114 Toluene-d8 10.0 9.56 96 10.0 9.72 97 89-112 Dibromofluoromethane 10.0 9.52 95 10.0 9.52 95 80-119

MAX RPD

REPORT ID: 20A093 Page 22 of 253

BATCH NO.:

METHOD:

CH2M HILL

BEALE AFB LTO&M TU002 2020

20A093

SW5030B/8260B

EMAX QUALITY CONTROL DATA

MS/MSD ANALYSIS

MATRIX: WATER % MOISTURE: NA

DILUTION FACTOR: 1 1

SAMPLE ID: TU02 MW-11 0120 -

LAB SAMP ID: A093-=-01 A093-01M A093-01S

LAB FILE ID: RAC365 RAC367 RAC368

DATE EXTRACTED: 01/17/2017:04 01/17/2017:55 01/17/2018:21 DATE COLLECTED: 01/13/20

DATE ANALYZED: 01/17/2017:04 01/17/2017:55 01/17/2018:21 DATE RECEIVED: 01/16/20

PREP. BATCH: V067A12 V067A12 V067A12

CALIB. REF: RAC301 RAC301 RAC301

ACCESSION:

SMPL RSLT SPIKE AMT MS RSLT MS SPIKE AMT MSD RSLT MSD RPD QC LIMIT

PARAMETER (ug/L) (ug/L) (ug/L) % REC (ug/L) (ug/L) % REC ( % ) ( % ) Benzene ND 10.0 10.5 105 10.0 10.0 100 4 79-120 Ethylbenzene ND 10.0 9.48 95 10.0 9.29 93 2 79-121 m,p-Xylenes ND 20.0 19.2 96 20.0 19.0 95 1 80-121 tert-butyl Methyl ether 0.701J 10.0 10.8 101 10.0 10.2 95 6 71-124 o-Xylene ND 10.0 10.0 100 10.0 9.68 97 3 78-122 Toluene ND 10.0 9.64 96 10.0 9.51 95 1 80-121 Xylenes, Total ND 30.0 29.2 97 30.0 28.7 96 2 79-121 tert-Amyl methyl ether ND 10.0 10.5 105 10.0 10.1 101 4 68-128 Ethyl tert-butyl ether ND 10.0 9.89 99 10.0 9.43 94 5 70-127 tert-butyl alcohol ND 250 254 102 250 243 97 5 68-129 isopropyl Ether ND 10.0 10.8 108 10.0 10.3 103 4 67-128

SPIKE AMT MS RSLT MS SPIKE AMT MSD RSLT MSD QC LIMIT

SURROGATE PARAMETER (ug/L) (ug/L) % REC (ug/L) (ug/L) % REC ( % ) 1,2-Dichloroethane-d4 10.0 9.71 97 10.0 9.66 97 81-118 Bromofluorobenzene 10.0 9.30 93 10.0 9.49 95 85-114 Toluene-d8 10.0 9.46 95 10.0 9.54 95 89-112 Dibromofluoromethane 10.0 9.75 98 10.0 9.53 95 80-119

MAX RPD

REPORT ID: 20A093 Page 23 of 253

INITIAL CALIBRATION

REPORT ID: 20A093 Page 24 of 253

5A

VOLATILE ORGANIC INSTRUMENT PERFORMANCE CHECK

BROMOFLUOROBENZENE (BFB)

Lab Name: EMAX Inc Contract: BEALE AFB LTO&M TU002 2020 Lab Code: EMXT Case No.:

Lab File ID: RAC295 Instrument ID: 67 GC Column:RTX502.2ID:0.25mm (mm) m/e ION ABUNDANCE CRITERIA

SAS No.: SDG No.: 20A093 BFB Injection Date: 01/15/20 BFB Injection Time: 18:08 Heated Purge: (Y/N) N

% RELATIVE

ABUNDANCE

50 15.0 - 40.0% of mass 95 18.48 75 30.0 - 60.0% of mass 95 45.05 95 Base peak, 100% relative abundance 100.00 --96 5.0 - 9.0% of mass 95 6.48

173 Less than 2.0% of mass 174 O.OO( 0.0)1 174 Greater than 50% of mass 95 77.80 175 5.0 - 9.0% of mass 174 6.30( 8.1)1 176 95.0 - 101.0% of mass 174 75.53( 97.1)1 177 5.0 - 9.0% of mass 176 5.07( 6.7)2

1-Value 1S % mass 174 2-Value 1S % mass 176

THIS CHECK APPLIES TO THE FOLLOWING SAMPLES, MS, MSD,BLANKS, AND STANDARDS:

EPA

SAMPLE NO.

VSTDO.3

VSTDO.5

VSTD01

VSTD02

VSTD05

VSTD010

VSTD020

VSTD030

VSTD050

VSTD100

LAB

SAMPLE ID

V067A151 V067A152 V067A153 V067A154 V067A155 V067A156 V067A157 V067A158 V067A159 V067A1510

FORM V VOA

LAB DATE TIME

FILE ID ANALYZED ANALYZED

RAC296 01/15/20 18:40

RAC297 01/15/20 19:06

RAC298 01/15/20 19:31

RAC299 01/15/20 19:57

RAC300 01/15/20 20:22

RAC301 01/15/20 20:48

RAC302 01/15/20 21 :13

RAC303 01/15/20 21 :39

RAC304 01/15/20 22:04

RAC305 01/15/20 22:30

OLM02.0

REPORT ID: 20A093 Page 25 of 253

Instrument ID :67 Beginning DateTime :01/15/20 18:40 Spike Units :PPB IC File :RAC301

M lOX Parameters

1 1,4-DIFLUOROBENZENE

2 Dichlorodifluoromethane 3 Dichlorotetrafluoroethane 4 Chloromethane 5 Vinyl chloride 6 Bromomethane 7 Chtoroethane 8 DichLorofluoromethane 9 Trichlorofluoromethane

10 sec-Propyl alcohol 5 11 Acrolein

12 1,1,2'Trichloro-1,2,2-trifluoroethane 5 13 Acetone

14 1,1-Dichloroethene 25 15 tert-Butyl alcohol

16 Methyl acetate 17 Iodomethane

10 18 Acetonitrile 19 Methylene chloride 20 Carbon disulfide

5 21 Acrylonitrile 22 tert-Butyl methyl ether (MTBE) 23 trans-1,2-Dichloroethene 24 Isopropyl ether (DIPE) 25 1,'-Dichloroethane 26 Vinyl acetate

25 27 2-Butanol 28 tert-Butyl ethyl ether (ETBE)

5 29 2-Butanone 30 2,2-Dichloropropane 31 cis-1,2-Dichloroethene 32 Chloroform 33 Bromochloromethane

5 34 tert-Amyl alcohol 35 Dibromofluoromethane 36 Tetrahydrofuran 37 1,1,1-Trichloroethane 38 Cyclohexane 39 2,2,4'Trimethylpentane 40 1,'-Dichloropropene 41 Carbon tetrachloride 42 tert-Amyl methyl ether (TAME) 43 1,2-Dichloroethane-d4 44 1,2-Dichloroethane 45 Benzene 46 Trichloroethene 47 Methylcyclohexane 48 1,2-Dichtoropropane

INITIAL CALIBRATION - RELATIVE RESPONSE_FACTOR

.3 .5 1 2 5 10 20 18:40 19:06 19:31 19:57 20:22 20:48 21:13

RAC296 RAC297 RAC298 RAC299 RAC300 RAC301 RAC302

1 1 1 1 1 1 1

- .. ---- 0.276 0.263 0.276 0.288 0.293 0.267 ------ ------ ------ ---_ .. Oo ............. ----- .. ... _----

0.462 0.515 0.505 0.499 0.499 0.503 0.440 ............. 0.427 0.416 0.429 0.442 0.449 0.396

0.239 0.339 0.293 0.320 0.327 0.337 0.310

0.207 0.265 0.266 0.271 0.279 0.288 0.260

0.593 0.632 0.614 0.589 0.614 0.607 0.537

------ 0.416 0.396 0.430 0.440 0.452 0.404

- .. ---- _ .. _--- 0.025 0.025 0.023 0.023 0.019

0.218 0.233 0.220 0.214 0.229 0.223 0.199

------ ---- .... ------ 0.039 0.035 0.033 0.028

0.516 0.555 0.523 0.508 0.533 0.528 0.469

0.012 0.011 0.011 0.010 0.010 0.010 0.009

---_ ... - 0.119 0.107 0.124 0.117 0.116 0.112

0.475 0.515 0.503 0.488 0.511 0.510 0.454 ............... .......... - ------ ----- .. --........ - ------ ...... ----

------ ------ 0.565 0.490 0.463 0.444 0.392

0.999 1.252 1.2'15 1.268 1.289 1.348 1.269

------ 0.043 0.043 0.045 0.045 0.046 0.041

0.476 0.470 0.465 0.462 0.466 0.459 0.406

0.343 0.358 0.351 0.343 0.355 0.355 0.320

1.092 1.161 1.139 1. 101 1.138 1.125 1.003

0.614 0.638 0.635 0.613 0.634 0.627 0.565 -... _ ... -- 0.363 0.349 0.406 0.403 0.443 0.406

------ 0.010 0.010 0.010 0.010 0.011 0.011 ------ 0.947 0.856 0.802 0.771 0.744 0.663 -_ ......... 0.010 0.011 0.011 0.011 0.012 0.011

0.465 0.452 0.422 0.384 0.386 0.384 0.343

0.329 0.336 0.344 0.341 0.350 0.340 0.314

0.514 0.548 0.535 0.521 0.540 0.539 0.477

0.140 0.153 0.162 0.159 0.162 0.163 0.145 -... _ .... - 0.008 0.008 0.009 0.008 0.009 0.009

0.239 0.255 0.266 0.287 0.287 0.300 0.281

------ ------ 0.046 0.044 0.041 0.040 0.036

0.441 0.461 0.455 0.443 0.464 0.461 0.418

0.498 0.565 0.547 0.553 0.574 0.590 0.544

1.075 1.268 1.295 1.309 1.331 1.402 1.317

0.168 0.174 0.162 0.157 0.168 0.169 0.151

0.367 0.394 0.368 0.361 0.387 0.383 0.345

0.124 0.132 0.126 0.122 0.122 0.123 0.109

0.188 0.191 0.209 0.222 0.215 0.228 0.212

0.242 0.260 0.257 0.255 0.263 0.262 0.232

1.288 1.346 1.314 1.258 1.325 1.309 1.176

0.361 0.378 0.366 0.356 0.376 0.370 0.336

0.563 0.653 0.632 0.641 0.672 0.697 0.637

0.311 0.323 0.321 0.313 0.325 0.326 0.291

21:39

RAC303

0.257

0.427 0.380 0.311 0.263 0.545 0.397

0.020 0.192 0.030 0.471 0.009 0.116 0.470

0.405 1.236 0.044 0.429 0.329 1.060 0.589 0.414 0.011 0.691 0.011 0.337 0.324 0.496 0.152 0.009 0.284 0.037 0.421 0.536 1.245 0.152 0.350 0.116 0.214 0.244 1.219 0.346 0.630 0.303

Column Spec :RTX502.2 ID :0.25MM Ending DateTime :01/15/20 22:30 HPChem Method :V067A15

50 100 22:04 22:30

RAC304 RAC305 AV_RRF % RSD Av_Rt_M

1 1 1 o 10.0697

0.269 0.233 0.269 6.56 1.8600

------ ------ 0.000 0.00 0.0000

0.418 ----- ... 0.474 7.93 2.1029

0.367 .............. 0.413 7.12 2.2212

0.316 0.285 0.308 9.67 2.6178

0.264 0.234 0.260 8.95 2.6662

0.569 0.578 0.588 5.25 2.7359

0.414 ------ 0.419 4.87 2.9842

------ - ... ---- 0.000 0.00 0.0000

0.021 0.022 0.022 9.80 3.4778

0.207 0.201 0.213 6.43 3.5193

0.032 0.034 0.033 10.36 3.5618

0.503 ------ 0.512 5.51 3.7353

0.010 0.011 0.010 8.46 3.8596

0.119 0.110 0.115 4.48 4.2400

0.496 0.515 0.494 4.31 4.1824

------ ------ 0.000 0.00 0.0000

0.419 0.436 0.452 12.27 4.4709

1.300 1.167 1.234 7.79 4.4628

0.047 0.051 0.045 6.09 4.7041

0.437 0.467 0.454 4.95 4.7462

0.344 0.357 0.345 3.66 4.9725

1.109 1.157 1. 108 4.35 5.6283

0.617 0.647 0.618 4.03 5.8152

0.417 0.402 0.400 7.03 5.8741

0.012 0.011 0.011 5.83 6.3545

0.715 0.754 0.771 11.33 6.5508

0.012 0.013 0.011 8.50 6.8300

0.342 ------ 0.391 12.10 7.1107

0.340 0.358 0.338 3.75 7.2261

0.519 0.541 0.523 4.29 7.6073 O. ,61 0.171 0.157 5.92 7.9710

0.010 0.009 0.009 6.24 8.0682

0.291 0.265 0.275 6.78 8.1126

0.039 0.042 0.041 8.32 8.0656

0.438 0.445 0.445 3.66 8.4967

0.550 0.477 0.543 6.19 8.4851

1.289 ------ 1.281 6.95 8.6653

0.161 0.166 0.163 4.66 8.8473

0.371 0.376 0.370 4.22 9.0225

0.120 0.126 0.122 5.02 9.1686

------ ------ 0.210 6.62 9.2137

0.254 0.269 0.254 4.41 9.4139

1.271 ------ 1.278 4.24 9.3940

0.362 0.376 0.363 3.78 10.6481

0.647 ------ 0.641 5.66 10.7311

0.319 0.336 0.317 4.08 11.0088

Sc

\/ 17/,,),0

REPORT ID: 20A093 Page 26 of 253

49 Bromodichloromethane 0.334 0.349 0.352 0.338 0.355 0.357 0.322 0.336 0.351 0.372 0.346 4.14 11.4455 20 50 1,4-Dioxane ------ ------ 0.001 0.001 0.001 0.001 0.001 0.001 0.001 0.001 0.001 8.28 11.5343

51 Dibromomethane 0.106 0.'128 0.129 0.128 0.130 0.131 0.118 0.124 0.131 0.140 0.126 7.09 11.5244 52 2-Chloroethyl vinyl ether 0.074 0.075 0.072 0.076 0.078 0.071 0.077 0.082 ------ 0.076 4.60 12.1202

5 53 4-Methyl-2-pentanone 0.160 0.162 0.161 0.158 0.158 0.157 0.140 0.150 0.161 0.171 0.158 5.11 12.1641 54 cis-1,3-Dichloropropene 0.422 0.455 0.452 0.440 0.455 0.456 0.410 0.426 0.450 0.474 0.444 4.34 12.4927 55 CHLOROBENZENE-D5 1 1 1 1 1 1 1 1 1 1 1 o 15.5145 56 Toluene-d8 1.268 1.319 1.376 1.467 1.495 1.537 1.437 1.449 1.482 .. ----- 1.426 6.15 12.8943 57 Toluene 1.828 1.849 1.773 1.711 1.805 1.770 1.588 1.636 1.705 ---- ... - 1.741 5.05 13.0258 58 Ethyl methacrylate 0.254 0.264 0.273 0.267 0.274 0.274 0.245 0.261 0.276 0.296 0.268 5.24 13.4464 59 trans-1,3-Dichloropropene 0.395 0.386 0.407 0.393 0.403 0.414 0.368 0.386 0.408 0.436 0.400 4.65 13.4055 60 1,1,2-Trichloroethane 0.201 0.206 0.205 0.203 0.206 0.204 0.185 0.193 0.202 0.217 0.202 4.24 13.6684

5 61 2-Hexanone 0.121 0.120 0.119 0.123 0.121 0.120 0.107 0.114 0.123 0.131 0.120 5.20 13.7269 62 1,3-Dichloropropane 0.380 0.388 0.382 0.385 0.393 0.389 0.350 0.367 0.387 0.413 0.384 4.29 14.1066 63 Tetrachloroethene 0.373 0.390 0.359 0.349 0.371 0.364 0.327 0.332 0.351 0.358 0.357 5.27 14.1650 64 o ibromochloromethane 0.239 0.262 0.251 0.255 0.260 0.256 0.232 0.244 0.258 0.276 0.253 4.89 14.5155 65 1,2-Dibromoethane 0.177 0.185 0.189 0.190 0.192 0.192 0.174 0.181 0.192 0.206 0.188 4.90 14.8631 66 1-Chlorohexane 0.700 0.728 0.675 0.660 0.703 0.692 0.625 0.626 0.660 0.667 0.674 4.94 15.1917 67 Chlorobenzene 1.041 1.063 1.032 1.021 1.050 1.042 0.934 0.964 0.998 1.033 1.018 4.01 15.5817 68 1,1,1,2-Tetrachloroethane 0.319 0.327 0.340 0.329 0.340 0.333 0.298 0.312 0.325 0.331 0.325 3.92 15.6693 69 Ethylbenzene 2.114 2.162 2.092 2.012 2.108 2.086 1.869 1.927 1.987 ------ 2.040 4.76 15.6839

2 70 m-Xylene & p-Xylene 1.573 1.604 1.516 1.492 1.566 1.539 1.392 1.417 ------ ------ 1.512 4.98 15.8152 71 o-Xylene 1.526 1.548 1.470 1.436 1.497 1.462 1.330 1.368 1.406 1.390 1.443 4.87 16.5442 72 Styrene 1.087 1.127 1. 111 1.089 1.139 1.121 1.017 1.050 1.080 1.114 1.093 3.44 16.6070 73 lsopropylbenzene 1.862 1.958 1.893 1.838 1.948 1.926 1.740 1.777 1.812 ------ 1.861 4.11 17.1460 74 1,2-DICHLOROBENZENE-D4 1 1 1 1 1 1 1 1 1 1 1 o 19.4228 75 Bromoform 0.325 0.330 0.328 0.339 0.342 0.344 0.313 0.333 0.356 0.392 0.340 6.39 17.1590 76 1,1,2,2-Tetrachloroethane 0.588 0.608 0.588 0.578 0.588 0.600 0.537 0.565 0.608 0.656 0.592 5.25 17.4263 S~ 77 4-Bromofluorobenzene 1.100 1.115 1.155 1.197 1.212 1.271 1.216 1.230 1.267 1.170 1.193 4.88 17.5242 78 1,2,3-Trichloropropane 0.135 0.152 0.146 0.151 0.149 0.149 0.134 0.141 0.152 0.164 0.147 6.10 17.6410

\f/7/-LO 79 trans-1,4-Dichloro-2-butene 0.164 0.164 0.175 0.177 0.178 0.180 0.167 0.171 0.189 0.202 0.177 6.77 17.2467 80 n-Propylbenzene 6.327 6.515 6.325 6.062 6.474 6.444 5.868 6.003 6.024 ------ 6.227 3.84 17.7432 81 Bromobenzene 0.980 0.998 0.966 0.953 0.988 0.996 0.906 0.942 1.000 1.053 0.978 4.06 17.7871 82 1,3,5-Trimethylbenzene 4.077 4.260 4.055 3.959 4.189 4.139 3.795 3.879 3.977 ... ----- 4.037 3.70 17.9623 83 2-Chlorotoluene 4.013 4.155 3.982 3.872 4.027 3.943 3.622 3.621 3.803 ---_oo- 3.893 4.70 17.9769 84 4-Chlorotoluene 3.259 3.355 3.185 3.063 3.314 3.238 2.900 3.131 3.310 ---- _ .. 3.195 4.52 18.0369 85 tert-Butylbenzene 0.963 0.966 0.916 0.898 0.951 0.933 0.860 0.861 0.904 0.910 0.916 4.14 18.4136 86 1,2,4-Trimethylbenzene 4.008 4.198 3.922 3.837 4.043 4.023 3.612 3.709 3.826 ------ 3.909 4.65 18.4540 87 sec-Butyl benzene 5.821 6.016 5.555 5.402 5.830 5.734 5.177 5.217 5.270 ------ 5.558 5.52 18.6633 88 p-Isopropyltoluene 4.647 4.798 4.589 4.505 4.785 4.672 4.291 4.326 4.488 ............. 4.567 3.97 18.8240 89 1,3-Dichlorobenzene 2.047 2.044 2.022 1.947 2.048 2.018 1.847 1.885 1.965 2.021 1.984 3.61 18.9292 90 1,4-Dichlorobenzene 1.961 1.989 1.897 1.890 1.961 1.941 1.770 1.817 1.886 1.928 1.904 3.57 19.0504 91 n-Butylbenzene 4.388 4.597 4.353 4.186 4.535 4.530 4.144 4.141 4.217 ............ 4.344 4.15 19.2670 92 1,2-Dichlorobenzene 1.669 1.680 1.624 1.605 1.662 1.621 1.480 1.510 1.587 1.620 1.606 4.08 19.4521 93 1,2-Dibromo-3-chloropropane 0.083 0.073 0.081 0.082 0.085 0.088 0.080 0.082 0.088 0.094 0.084 6.68 20.2261 94 1,2,4-Trichlorobenzene 0.924 0.947 0.915 0.913 0.956 0.972 0.905 0.912 0.935 0.951 0.933 2.43 21.0732 95 Hexachlorobutadiene 0.708 0.692 0.689 0.670 0.713 0.708 0.649 0.626 0.626 0.593 0.667 6.26 21.1944 96 Naphthalene 1.204 1.229 1.195 1.203 1.254 1.276 1.179 1.210 1.272 1.313 1.233 3.51 21.3405 97 1,2,3-Trichlorobenzene 0.713 0.717 0.694 0.697 0.736 0.739 0.680 0.687 0.705 0.722 0.709 2.82 21.5961

Spike Amount = Nominal Amount * M ------------------------ --- Ave_%RSD : 5.6 Max roRSD 12.3

REPORT ID: 20A093 Page 27 of 253

SECOND SOURCE

VERIFICATION

REPORT ID: 20A093 Page 28 of 253

BROMOFLUOROBENZENE (BFB)

Lab Name: EMAX Inc Contract; BEALE AFB LTO&M TU002 2020 Lab Code: EMXT Case No.:

Lab Fi le ID: RAC315 Instrument ID: 67 GC Column:RTX502.2ID:0.25mm (mm) m/e ION ABUNDANCE CRITERIA

SAS No.: SDG No.: 20A093 BFB Injection Date: 01/16/20 BFB Injection Time: 11:58 Heated Purge: (Y/N) N

% RELATIVE

ABUNDANCE

50 15.0 - 40.0% of mass 95 19.10 75 30.0 - 60.0% of mass 95 44.69 95 Base peak, 100% relative abundance -- 100.00 96 5.0 - 9.0% of mass 95 6.21

173 Less than 2.0% of mass 174 O.OO( 0.0)1 174 Greater than 50% of mass 95 85.43 175 5.0 - 9.0% of mass 174 6.71( 7.9)1 176 95.0 - 101.0% of mass 174 81.66( 95.6)1 177 5.0 - 9.0% of mass 176 5.33( 6.5)2

-- 0 1-Value 1S % mass 174 0 2-Value 1S % mass 176

THIS CHECK APPLIES TO THE FOLLOWING SAMPLES, MS, MSD,BLANKS, AND STANDARDS:

EPA LAB LAB DATE TIME

SAMPLE NO. SAMPLE ID FILE ID ANALYZED ANALYZED

VSTD010 IV067A1502 RAC316 01/16/20 12:50

FORM V VOA OLM02.0

REPORT ID: 20A093 Page 29 of 253

Instrument ID :67 IC Beginning DateTime :01/15/20 18:40 Spike Amount :10 PPB CC/CV File :RAC316 IC FIle :RAC301

CONTINUE_CALIBRATION - CALIBRATION VERIFICATION

Column Spec :RTX502.2 ID :0.25MM IC Ending DateTime :01/15/20 22:30 HPChem Method :V067A15 Date_Time :01/16/20 12:50

I ~=~. ~~~~~~;~~;=========================== =~~=~~~ i ~~~=~ , =~~=~;;~ I ~~~~~ I ~~~~~ ~~=~~~I =~~~;~ ~=~;~ ==~~=~~ ==~~=~~ ==~~=~~ I ~~=~

1 1.4-DIFLUOROBENZENE 10.000 0 1909254 1 1 10.061 10.070 0

23 Djchlorodifluoromethane 10.415 4.2 535365 0.280 0.269 1.858 1.860 6.56

Dlchlorotetrafluoroethane 4 Chloromethane 9.915 -0.8 5 Vinyl chloride 99 •. 36390 -_6,.46 6 Bromomethane 0 9 7 Chloroethane 9.406 -5 9 8 Dichlorofluoromethane 10.248 2:5 9 Trichlorofluoromethane 10.205 2.0

10 sec-Propy alcohol 11 Acrolein 43.559 -12.9

12 1,1 f 2-Trichloro-1,2,2-trifluoroethane 9.118 -8.8

13 Ace one 45.999 -8.0 14 1,1-Dichloroethene 2239.'910690 _1-08 •. 44

25 15 tert-Butyl alcohol 16 Methyl acetate 9.564 -4.4 17 lodomethane 10.219 2.2

10 18 AcetonItrile 19 Methylene chloride

20 Carbon gisulfide 21 AcrylonItrile 22 tert-Butyl methyl ether (MTBE) 23 trans-1,2-Dichloroethene 24 Isopropyl ether (DIPE) 25 1.1-Dichloroethane 26 VInyl acetate

25 27 2-Butanol 28 tert-Butyl ethyl ether (ETBE)

5 29 2-Butanone 30 2.2-Dichloropropane 31 cls-1,2-Dichloroethene 32 Chloroform

33 Bromochloromethane 34 tert-Amyl alcohol 35 Dibromofluoromethane 36 Tetrahydrofuran 37 1, '(1-Trichloroethane 38 Cyc ohexane 39 2,2,4-Trimethylpentane 401,1-Dichloropropene 41 Carbon tetrachloride 42 tert-Am~l meth~l ether (TAME) 43 1,2-Dic loroet ane-d4 44 1,2-Dic loroet ane 45 Benzene 46 Trichloroethene 47 Methylcyclohexane 48 1,2-Dichloropropane 49 Bromodlchloromethane

20 50 1.4-Dioxane 51 Dlbromomethane 52 2-Chloroethyl vinyl ether

5 53 4-Methyl-?-pentanone 54 cis-1

3-Dlchloropropene

55 CHLOR BENZENE-D5

56 Toluene-dB 57 Toluene 58 Ethyl methacrylate 59 trans-1,~-Dichloropropene 60 1,1,2-Trlchloroethane

5 61 2-Hex{lnone 62 1,3-Dlchloropropane 63 Tetrachloroethene 64 Dibromochloromethane 65 1,2-Dibromoethane 66 1-Chlorohexane 67 Chlorobenzene

L 1,1

2-Tetrachloroethane

69 E,hyl enzene 2 70 m-Xylene & p-Xylene

71 o-Xylene 72 Styrene 73 Isopropylbenzene

74 1,2-DICHLOROBENZENE-D4

75 Bromoform 76 1,1,2,2-Tetrachloroethane 77 4-BrQmofluorobenzene 78 1,2,3-Trjchloropropane 79 trans-1{4-Dichloro-2-butene 80 n-Propy benzene 81 Bromobenzene 82 1,3g5-TrimethYlbenzene 83 2-C lorotoluene 84 4-C lorotoluene 85 tert-Butylbenz~ne 86 1,2,4-Trlmethylbenzene 87 sec-Butyl benzene 88 p-Isop'ropyltoluene 89 1,3-Dichlorobenzene 90 1,4-Dichlorobenzene 91 n-Butylb~nzene 92 1,2-Dlchlorobenzene 93 1,2-DibrQmo-3-chloropropane 94 1,2,4-Trlchlorobenzehe 95 Hexachlorobutadiene 96 NaPhthalene 97 1,2,3-Trichlorobenzene ~ I\mount = Nom1nat "mount • ~

8.940 -10.6

9.608 -3.9

47.828 -4.3

9.555 -4.5

9.575 -4.2

10.133 1.3

9.661 -3.4

26~j~~ -1~j

9.358 -6.4

48.529 -2.9

9.497 -5.0

9.780 -2.2

10.002 0.0

9.788 -2.1

47.907 -4.2

10.135 1.1 9.388 -6.

9.674 -3.

1~:~3~ 1~J

9.974 -0.3

9.529 -4.7

10.085 0.9

9.999 -O.~ 9.960 -0.

10.357 3.

9.561 -4.4

10.937 9.4

198:iU :2:~

9.671 -3.3

9.662 -3.4

18J~~ -t:~

10.330 3.3

9.950 -0.5

10.109 1. 1 10.53i 5.~ 9.55 -4.

48.26 -3.

9.939 -0.6

9.836 -1.6

9.981 -0.2 9.7~2 -3.0 9.2 7 -7.5

9.8 8 -!.1 9.893 -.1

9.739 -.6

19.585 -2.1

9.933 -0.7

10.241 2.4 18:683 1.8

10.329 3.3

9.802 -2.0

10.37:t 3.7

9.913 -0.9

9.976 -0.2

10.400 4.0

10.032 0.3

9.933 -0.7

10.457 4.6

9.694 -3.1

10.267 2.7

10.108 1. 1

10.030 0.3 10.1861.9

10.167 1. 7

10.125 1.3 19.J90 1.~ 1O:2*~ -t4

10.641 6.4

10.557 5.! 9.619 -3.

10.339 3.

1--- -- ---- -- -- --- --- -- --- --- --- ---

REPORT ID: 20A093 Page 30 of 253

Evaluate Continuing Calibration Report

Data File D:\HPCHEM\1\DATA\20A16\RAC316.D Acq On 16 Jan 2020 12:50 pm Sample IV067A1502 Misc 10ppb 8260/50ppb KET-AA/250ppb TBA MS Integration Params: RTE.P

Vial: 2 Operator: RMinam Inst 67 Multiplr: 1.00

Method Title

D:\HPCHEM\1\METHODS\V067A15.M (RTE Integrator)

METHOD 8260B

Last Update Response via

Thu Jan 16 17:14:48 2020 Multiple Level Calibration

Min. RRF Max. RRF Dev

0.000 Min. ReI. Area

20% Max. ReI. Area

50% Max. R.T. Dev 0.16min 200%

Compound

1 I 1,4-DIFLUOROBENZENE

2 T,M Dichlorodifluoromethane 3 T,M Dichlorotetrafluoroethane 4 P,T,M Chloromethane 5 C,T,M Vinyl chloride 6 T,M Bromomethane 7 T,M Chloroethane 8 T,M Dichlorofluoromethane 9 T,M Trichlorofluoromethane

10 T,M sec-Propyl alcohol 11 T,M Acrolein 12 T,M 1,l,2-Trichloro-l,2,2-trifl 13 T,M Acetone 14 C,T,M l,l-Dichloroethene 15 T,M tert-Butyl alcohol 16 T,M Methyl acetate 17 T,M Iodomethane 18 T,M Acetonitrile 19 T,M Methylene chloride 20 T,M Carbon disulfide 21 T,M Acrylonitrile 22 T,M tert-Butyl methyl ether (MT 23 T,M trans-l,2-Dichloroethene 24 T,M Isopropyl ether (DIPE) 25 P,T,M l,l-Dichloroethane 26 TiM Vinyl acetate 27 T,M 2-Butanol 28 T,M tert-Butyl ethyl ether (ETB 29 T,M 2-Butanone 30 T,M 2,2-Dichloropropane 31 T,M cis-1,2-Dichloroethene 32 C,T,M Chloroform 33 T,M Bromochloromethane 34 T,M tert-Amyl alcohol 35 S Dibromofluorornethane 36 T,M Tetrahydrofuran 37 T,M l,l,l-Trichloroethane 38 T,M Cyclohexane 39 T,M 2,2,4-Trimethylpentane 40 T,M l,l-Dichloropropene 41 T,M Carbon tetrachloride

Amount Calc.

10.000 10.000

10.000 10.415 -1.000 0.000

10.000 9.915

10.000 9.360

10.000 9.039

10.000 9.406

10.000 10.247

10.000 10.205 -1.000 0.000

50.000 43.559

10.000 9.118

50.000 45.999

10.000 9.160

250.000 223.909

10.000 9.564

10.000 10.219

100.000 0.000

10.000 8.940

10.000 9.608

50.000 47.828

10.000 9.555

10.000 9.575

10.000 10.133

10.000 9.661

10.000 10.238

250.000 202.513

10.000 9.358

50.000 48.529

10.000 9.497

10.000 9.780

10.000 10.002

10.000 9.788

50.000 47.907

10.000 10.135

10.000 9.388

10.000 9.673

10.000 10.256

10.000 11.533

10.000 9.974

10.000 9.529

(#) = Out of Range RAC316.D V067A15.M Thu Jan 16 18:13:31 2020

%Dev Area% Dev(min)

0.0 -4.1 0.0 0.9 6.4

9.6 5.9

-2.5 -2.1 0.0

12.9 8.8 8.0 8.4

10.4 4.4

-2.2 100.0# 10.6 3.9 4.3 4.5 4.3

-1.3 3.4

-2.4 19.0 6.4 2.9 5.0 2.2 -0.0 2.1 4.2

-1.3 6.1 3.3

-2.6 -15.3

0.3 4.7 o o o

-0.01 0.00 0.00 0.00 0.00

0.00 0.00 0.00

-0.02 0.00 0.00 0.00 0.00

0.00 0.00 0.00

-0.01 0.00 0.00

-0.01 0.00 0.00

-0.01 -0.01

0.00 0.00 0.00 0.00

-0.01 0.00 0.00

0.00 0.00 0.00

-0.01 -0.01

0.00 0.00

-0.01 -0.01 -0.01

REPORT ID: 20A093 Page 31 of 253

Data File D:\HPCHEM\1\DATA\20A16\RAC316.D Acq On 16 Jan 2020 12:50 pm Sample IV067A1502 Misc 10ppb 8260/50ppb KET-AA/250ppb TBA MS Integration Params: RTE.P

Vial: 2 Operator: RMinam Inst 67 Multiplr: 1.00

Method Title

D:\HPCHEM\1\METHODS\V067A15.M (RTE Integrator)

METHOD 8260B

Last Update Response via

Thu Jan 16 17:14:48 2020 Multiple Level Calibration

Min. RRF Max. RRF Dev

0.000 Min. ReI. Area

20% Max. ReI. Area

50% Max. R.T. Dev 0.16min 200%

Compound

T,M tert-Amyl methyl ether (TAM S l,2-Dichloroethane-d4 T,M l,2-Dichloroethane T,M Benzene T,M Trichloroethene T,M Methylcyclohexane C,T,M l,2-Dichloropropane T,M Bromodichloromethane T,M l,4-Dioxane T,M Dibromomethane T,M 2-Chloroethyl vinyl ether T,M 4-Methyl-2-pentanone T,M cis-1,3-Dichloropropene

55 I CHLOROBENZENE-D5

56 S Toluene-d8 57 C,T,M Toluene 58 T,M Ethyl methacrylate 59 T,M trans-1,3-Dichloropropene 60 T,M 1,1,2-Trichloroethane 61 T,M 2-Hexanone 62 T,M 1,3-Dichloropropane 63 T,M Tetrachloroethene 64 T,M Dibromochloromethane 65 T,M l,2-Dibromoethane 66 T,M 1-Chlorohexane 67 P,M Chlorobenzene 68 T,M 1,1,1,2-Tetrachloroethane 69 C,T,M Ethylbenzene 70 T,M m-Xylene & p-Xylene 71 T,M o-Xylene 72 T,M Styrene 73 T,M Isopropylbenzene

74 I l,2-DICHLOROBENZENE-D4 75 P,T,M Bromoform 76 P,T,M 1, 1, 2, 2-Tetrachloroethane 77 S 4-Bromofluorobenzene 78 T,M l,2,3-Trichloropropane 79 T,M trans-1,4-Dichloro-2-butene 80 T,M n-Propylbenzene

Amount Calc.

10.000 10.000 10.000 10.000 10.000 10.000

10.000 10.000

200.000 10.000 10.000 50.000 10.000

10.000 10.000

10.000 10.000 10.000 10.000 50.000 10.000 10.000 10.000 10.000 10.000 10.000 10.000

10.000 20.000 10.000 10.000 10.000

10.000 10.000 10.000

10.000 10.000 10.000 10.000

10.085 9.999 9.960

10.357 9.561

10.937 9.851

9.932 190.422

9.671 9.662

47.668 10.121

10.000 10.330

9.950 10.109 10.532

9.551 48.266

9.939 9.836 9.981 9.702 9.247 9.888 9.893

9.739 19.585

9.933 10.241 10.164

10.000 10.329

9.802 10.374

9.913 9.976

10.400

(#) = Out of Range RAC316.D V067A15.M Thu Jan 16 18:13:32 2020

%Dev Area% Dev(min)

-0.9 0.0 0.4

-3.6 4.4

-9.4 1.5

0.7 4.8 3.3 3.4 4.7

-1. 2

0.0 -3.3

0.5 -1.1 -5.3 4.5 3.5 0.6 1.6 0.2 3.0 7.5 1.1 1.1 2.6

2.1 0.7

-2.4 -1. 6

0.0 -3.3 2.0

-3.7 0.9 0.2

-4.0

-0.01 0.00

-0.01 -0.01 0.00

-0.01 -0.01

-0.01 -0.01 0.00

-0.01 -0.01 -0.01

0.00 -0.01

0.00 -0.01 0.00

-0.01 -0.01 0.00

-0.01 0.00

-0.01 0.00

-0.01…