KSC-TA-13017_App_B.pdf

EXECUTIVE SUMMARY

The work to be performed under this project consists of providing the labor, equipment, and material to close/demolish selected facilities at Kennedy Space Center (KSC, including KSC’s Headquarters Building (M6-0399) and the KSC Central Instrumentation Facility (CIF, M6-0342). The scope of work also includes demolition of facilities ancillary to the CIF, consisting of the Toxic Hazards Lab (M6-0392A), Hazardous Waste Staging Shelter (M6-0342B) and Tank Containment (M6-342C).

Base bid work consists of demolishing and disposing of permanent facilities at KSC. Facility demolition consists of dismantling, scrapping internals, abating asbestos, segregating universal waste, taking toxic constituent precautions, decommissioning utilities, preparing for disposal, and disposing of materials. The ground will be sodded and match existing grade.

The Auditorium and Training Building (M7-0351) will remain in service; therefore, the work also consists of providing the labor, equipment, and materials to reroute all utilities serving this facility from Headquarters.

The work also includes providing the labor, equipment, and materials to remove Headquarters from the central chilled-water system.

Removing the south parking lot circuitry from Headquarters is also part of this project. The parking lot will be relighted in the process using existing poles and providing new LED style luminaires.

This manual provides the standard NASA review of procedures for handling asbestos-containing material (ACM), construction and demolition debris (C&DD) including specific types of waste material expected and disposal options, and impacts to threatened and endangered (T&E) species.

This project also includes crushing and stockpiling unpainted concrete and hauling the material to the Diverted Aggregate Reclamation and Collection Yard (DARCY) at the KSC Class III Landfill.

The Contractor will perform the appropriate lock-out/tag-out procedures to ensure personnel safety in accordance with applicable Federal, State, and KSC requirements.

This project is within the boundaries of several identified solid waste management unit (SWMU) sites that are being investigated by the Remediation Group of NASA Environmental. A SWMU designation means that a site has had historical operations that may have had the potential to impact the environment. The requirements in this manual concerning management of soil and groundwater must be complied with during demolition activities.

KSC-TA-13017

CONTENTS

1. INTRODUCTION

2. APPLICABLE DOCUMENTS

3. DESIGN CONSIDERATIONS

3.1 ENVIRONMENTAL

3.1.1 Waste Generation

3.1.1.1 KSC Class III Landfill

3.1.1.2 Brevard County Landfill

3.1.2 Hazardous and Controlled Waste

3.1.2.1 Asbestos

3.1.2.1.1 Advantages and Disadvantages of Disposal of ACM at Schwartz Road

Landfill

3.1.2.2 Paint Coatings

3.1.2.2.1 Advantages and Disadvantages of Disposal of PCB Bulk Product Waste at

Schwartz Road Landfill

3.1.2.3 Equipment and Storage Tanks

3.1.3 Threatened and Endangered Species

3.1.4 Historic Property

3.1.5 Solid Waste Management Unit

3.1.6 Recycling

3.1.7 Water Resource Permitting

3.1.8 Erosion and Sediment Control and Excavation Permit

3.1.9 National Pollutant Discharge Elimination System Permit

3.1.10 Affirmative Procurement (AP)

3.2 ELECTRICAL

3.2.1 KSC Headquarters

3.2.2 Central Instrumentation Facility

3.2.2.1 Toxic Hazards Lab (M6-0392A)

3.2.2.2 Hazardous Waste Staging Shelter (M6-0342B)

3.3 MECHANICAL

3.3.1 KSC Headquarters

3.3.2 Central Instrumentation Facility

3.3.2.1 New Main Loop Return

3.3.2.2 OHF Branch Take-Off Modifications

APPENDIX A. CONTRACT DOCUMENTS

APPENDIX B. CIVIL/ENVIRONMENTAL DESIGN DATA

APPENDIX C. SITE INVESTIGATION

APPENDIX D. CONSTRUCTION SCHEDULES

APPENDIX E. TECHNICAL MEMORANDA

APPENDIX F. LESSONS LEARNED DATABASE CERTIFICATION

APPENDIX B

ANALYTICAL LABORATORY RESULTS

10775 Central Port Drive

Orlando FL, 32824

407.826.5314 407.850.6945Phone: FAX:

ENCO Workorder(s): A401309

Titusville, FL 32780

Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures.

Results for these procedures apply only to the samples as submitted.

The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative. This report shall not be reproduced except in full, without the written approval of the Laboratory.

This report contains only those analyses performed by Environmental Conservation

Laboratories. Unless otherwise noted, all analyses were performed at ENCO Orlando. Data from outside organizations will be reported under separate cover.

If you have any questions or require further information, please do not hesitate to contact me.

Sincerely, Enclosure(s)

Project Number: 14000-221-01, Project Name/Desc: Deconstruct Facilities, KSC HQ & CIF

Attn: Casey Coffey

Jones Edmunds & Associates (JO005)

3910 S. Washington Ave Suite 210

David Camacho

Project Manager

Tuesday, March 11, 2014

RE: Laboratory Results for

Dear Casey Coffey, Enclosed is a copy of your laboratory report for test samples received by our laboratory on

Friday, March 7, 2014.

Enclosure(s)

Page 1 of 13This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL www.encolabs.com

SAMPLE SUMMARY/LABORATORY CHRONICLE

HQ-Gray A401309-01 Sampled: 01/09/14 12:00 Received: 03/07/14 11:35Client ID: Lab ID:

Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)

EPA 8082A 01/09/15 03/09/14 07:30 03/10/14 11:0801/09/15

HQ-Black A401309-02 Sampled: 01/09/14 12:00 Received: 03/07/14 11:35Client ID: Lab ID:

Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)

EPA 8082A 01/09/15 03/09/14 07:30 03/10/14 11:2001/09/15

HQ-Black A401309-02RE1 Sampled: 01/09/14 12:00 Received: 03/07/14 11:35Client ID: Lab ID:

Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)

EPA 8082A 01/09/15 03/09/14 07:30 03/10/14 15:1201/09/15

HQ-Cream A401309-03 Sampled: 01/09/14 12:00 Received: 03/07/14 11:35Client ID: Lab ID:

Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)

EPA 8082A 01/09/15 03/09/14 07:30 03/10/14 11:3201/09/15

HQ-Cream A401309-03RE1 Sampled: 01/09/14 12:00 Received: 03/07/14 11:35Client ID: Lab ID:

Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)

EPA 8082A 01/09/15 03/09/14 07:30 03/10/14 15:2401/09/15

HQ-Green A401309-04 Sampled: 01/09/14 12:00 Received: 03/07/14 11:35Client ID: Lab ID:

Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)

EPA 8082A 01/09/15 03/09/14 07:30 03/10/14 11:4401/09/15

HQ-Green A401309-04RE1 Sampled: 01/09/14 12:00 Received: 03/07/14 11:35Client ID: Lab ID:

Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)

EPA 8082A 01/09/15 03/09/14 07:30 03/10/14 15:3601/09/15

HQ-White A401309-05 Sampled: 01/10/14 12:00 Received: 03/07/14 11:35Client ID: Lab ID:

Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)

EPA 8082A 01/10/15 03/09/14 07:30 03/10/14 11:5601/10/15

HQ-White A401309-05RE1 Sampled: 01/10/14 12:00 Received: 03/07/14 11:35Client ID: Lab ID:

Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)

EPA 8082A 01/10/15 03/09/14 07:30 03/10/14 15:4801/10/15

HQ-Black2 A401309-06 Sampled: 01/27/14 12:00 Received: 03/07/14 11:35Client ID: Lab ID:

Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)

EPA 8082A 01/27/15 03/09/14 07:30 03/10/14 12:0801/27/15

HQ-Black2 A401309-06RE1 Sampled: 01/27/14 12:00 Received: 03/07/14 11:35Client ID: Lab ID:

Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)

EPA 8082A 01/27/15 03/09/14 07:30 03/10/14 16:0001/27/15

HQ-Cream2 A401309-07 Sampled: 01/27/14 12:00 Received: 03/07/14 11:35Client ID: Lab ID:

Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)

EPA 8082A 01/27/15 03/09/14 07:30 03/10/14 12:2001/27/15

HQ-Cream2 A401309-07RE1 Sampled: 01/27/14 12:00 Received: 03/07/14 11:35Client ID: Lab ID:

Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)

EPA 8082A 01/27/15 03/09/14 07:30 03/10/14 16:1201/27/15

HQ-Gray2 A401309-08 Sampled: 01/27/14 12:00 Received: 03/07/14 11:35Client ID: Lab ID:

Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)

EPA 8082A 01/27/15 03/09/14 07:30 03/10/14 12:3201/27/15

HQ-Gray2 A401309-08RE1 Sampled: 01/27/14 12:00 Received: 03/07/14 11:35Client ID: Lab ID:

Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)

EPA 8082A 01/27/15 03/09/14 07:30 03/10/14 16:2401/27/15

Page 2 of 13This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL

HQ-Gray3 A401309-09 Sampled: 02/18/14 12:00 Received: 03/07/14 11:35Client ID: Lab ID:

Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)

EPA 8082A 02/18/15 03/09/14 07:30 03/10/14 12:4402/18/15

HQ-Brown A401309-10 Sampled: 02/18/14 12:00 Received: 03/07/14 11:35Client ID: Lab ID:

Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)

EPA 8082A 02/18/15 03/09/14 07:30 03/10/14 12:5602/18/15

HQ-White2 A401309-11 Sampled: 02/18/14 12:00 Received: 03/07/14 11:35Client ID: Lab ID:

Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)

EPA 8082A 02/18/15 03/09/14 07:30 03/10/14 13:3502/18/15

HQ-Yellow A401309-12 Sampled: 02/18/14 12:00 Received: 03/07/14 11:35Client ID: Lab ID:

Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)

EPA 8082A 02/18/15 03/09/14 07:30 03/10/14 13:4702/18/15

HQ-LT Gray A401309-13 Sampled: 02/20/14 12:00 Received: 03/07/14 11:35Client ID: Lab ID:

Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)

EPA 8082A 02/20/15 03/09/14 07:30 03/10/14 14:0002/20/15

HQ-LT Gray A401309-13RE1 Sampled: 02/20/14 12:00 Received: 03/07/14 11:35Client ID: Lab ID:

Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)

EPA 8082A 02/20/15 03/09/14 07:30 03/10/14 14:3202/20/15

Page 3 of 13This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL

SAMPLE DETECTION SUMMARY

Lab ID:Client ID: HQ-Gray A401309-01

Analyte MethodUnitsPQLResults Flag NotesMDL

1.7 0.51 mg/kg wet EPA 8082A GC-07PCB-1016/1242 0.42

38 0.51 mg/kg wet EPA 8082A PCB-1254 0.48

8.3 0.51 mg/kg wet EPA 8082A PCB-1260 0.33

Lab ID:Client ID: HQ-Black A401309-02

Analyte MethodUnitsPQLResults Flag NotesMDL

7.0 0.46 mg/kg wet EPA 8082A GC-07PCB-1016/1242 0.38

16 0.46 mg/kg wet EPA 8082A PCB-1260 0.30

Lab ID:Client ID: HQ-Black A401309-02RE1

Analyte MethodUnitsPQLResults Flag NotesMDL

100 2.3 mg/kg wet EPA 8082A PCB-1254 2.2

Lab ID:Client ID: HQ-Cream A401309-03

Analyte MethodUnitsPQLResults Flag NotesMDL

8.0 0.51 mg/kg wet EPA 8082A GC-07PCB-1016/1242 0.42

28 0.51 mg/kg wet EPA 8082A PCB-1260 0.33

Lab ID:Client ID: HQ-Cream A401309-03RE1

Analyte MethodUnitsPQLResults Flag NotesMDL

97 2.6 mg/kg wet EPA 8082A PCB-1254 2.4

Lab ID:Client ID: HQ-Green A401309-04

Analyte MethodUnitsPQLResults Flag NotesMDL

6.1 0.51 mg/kg wet EPA 8082A GC-07PCB-1016/1242 0.42

16 0.51 mg/kg wet EPA 8082A PCB-1260 0.33

Lab ID:Client ID: HQ-Green A401309-04RE1

Analyte MethodUnitsPQLResults Flag NotesMDL

76 2.6 mg/kg wet EPA 8082A PCB-1254 2.4

Lab ID:Client ID: HQ-White A401309-05

Analyte MethodUnitsPQLResults Flag NotesMDL

5.0 0.46 mg/kg wet EPA 8082A GC-07PCB-1016/1242 0.38

7.5 0.46 mg/kg wet EPA 8082A PCB-1260 0.30

Lab ID:Client ID: HQ-White A401309-05RE1

Analyte MethodUnitsPQLResults Flag NotesMDL

45 0.93 mg/kg wet EPA 8082A PCB-1254 0.87

Lab ID:Client ID: HQ-Black2 A401309-06

Analyte MethodUnitsPQLResults Flag NotesMDL

3.7 0.51 mg/kg wet EPA 8082A GC-07PCB-1016/1242 0.42

16 0.51 mg/kg wet EPA 8082A PCB-1260 0.33

Lab ID:Client ID: HQ-Black2 A401309-06RE1

Analyte MethodUnitsPQLResults Flag NotesMDL

92 2.6 mg/kg wet EPA 8082A PCB-1254 2.4

Lab ID:Client ID: HQ-Cream2 A401309-07

Analyte MethodUnitsPQLResults Flag NotesMDL

4.0 0.51 mg/kg wet EPA 8082A GC-07PCB-1016/1242 0.42

12 0.51 mg/kg wet EPA 8082A PCB-1260 0.33

Lab ID:Client ID: HQ-Cream2 A401309-07RE1

Analyte MethodUnitsPQLResults Flag NotesMDL

58 1.0 mg/kg wet EPA 8082A PCB-1254 0.96

Lab ID:Client ID: HQ-Gray2 A401309-08

Analyte MethodUnitsPQLResults Flag NotesMDL

5.6 0.51 mg/kg wet EPA 8082A GC-07PCB-1016/1242 0.42

16 0.51 mg/kg wet EPA 8082A PCB-1260 0.33

Lab ID:Client ID: HQ-Gray2 A401309-08RE1

Analyte MethodUnitsPQLResults Flag NotesMDL

88 2.6 mg/kg wet EPA 8082A PCB-1254 2.4

Page 4 of 13This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL

Lab ID:Client ID: HQ-Gray3 A401309-09

Analyte MethodUnitsPQLResults Flag NotesMDL

0.54 0.51 mg/kg wet EPA 8082A PCB-1254 0.48

Lab ID:Client ID: HQ-White2 A401309-11

Analyte MethodUnitsPQLResults Flag NotesMDL

3.6 0.51 mg/kg wet EPA 8082A PCB-1254 0.48

Lab ID:Client ID: HQ-Yellow A401309-12

Analyte MethodUnitsPQLResults Flag NotesMDL

2.7 0.46 mg/kg wet EPA 8082A PCB-1254 0.44

Lab ID:Client ID: HQ-LT Gray A401309-13

Analyte MethodUnitsPQLResults Flag NotesMDL

5.3 0.51 mg/kg wet EPA 8082A GC-07PCB-1016/1242 0.42

25 0.51 mg/kg wet EPA 8082A PCB-1260 0.33

Lab ID:Client ID: HQ-LT Gray A401309-13RE1

Analyte MethodUnitsPQLResults Flag NotesMDL

120 5.1 mg/kg wet EPA 8082A PCB-1254 4.8

Page 5 of 13This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL

ANALYTICAL RESULTS

HQ-GrayDescription: Lab Sample ID:A401309-01 03/07/14 11:35Received:

A401309Work Order:01/09/14 12:00Sampled:SolidMatrix:

% Solids:casey CoffeySampled By:Project: Deconstruct Facilities, KSC HQ & CIF

Polychlorinated Biphenyls by GC

^ - ENCO Orlando certified analyte [NELAC E83182]

NotesFlag PQL Batch ByAnalyzedMethodMDLResults Units DFAnalyte [CAS Number] mg/kg wet EPA 8082A 03/10/14 11:08PCB-1016/1242

[12674-11-2/53469-21-9]^

1 0.42 RC4C090030.511.7 GC-07

mg/kg wet EPA 8082A 03/10/14 11:08PCB-1221 [11104-28-2]^ 1 0.42 RC4C090030.510.42 U mg/kg wet EPA 8082A 03/10/14 11:08PCB-1232 [11141-16-5]^ 1 0.42 RC4C090030.510.42 U mg/kg wet EPA 8082A 03/10/14 11:08PCB-1248 [12672-29-6]^ 1 0.19 RC4C090030.510.19 U mg/kg wet EPA 8082A 03/10/14 11:08PCB-1254 [11097-69-1]^ 1 0.48 RC4C090030.5138 mg/kg wet EPA 8082A 03/10/14 11:08PCB-1260 [11096-82-5]^ 1 0.33 RC4C090030.518.3

Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF

2,4,5,6-TCMX 20-13778 % RCEPA 8082A 03/10/14 11:084C090030.78 1.00 1

Decachlorobiphenyl 13-183110 % RCEPA 8082A 03/10/14 11:084C090031.1 1.00 1

HQ-BlackDescription: Lab Sample ID:A401309-02 03/07/14 11:35Received:

A401309Work Order:01/09/14 12:00Sampled:SolidMatrix:

% Solids:casey CoffeySampled By:Project: Deconstruct Facilities, KSC HQ & CIF

Polychlorinated Biphenyls by GC

^ - ENCO Orlando certified analyte [NELAC E83182]

NotesFlag PQL Batch ByAnalyzedMethodMDLResults Units DFAnalyte [CAS Number] mg/kg wet EPA 8082A 03/10/14 11:20PCB-1016/1242

[12674-11-2/53469-21-9]^

1 0.38 RC4C090030.467.0 GC-07

mg/kg wet EPA 8082A 03/10/14 11:20PCB-1221 [11104-28-2]^ 1 0.38 RC4C090030.460.38 U mg/kg wet EPA 8082A 03/10/14 11:20PCB-1232 [11141-16-5]^ 1 0.38 RC4C090030.460.38 U mg/kg wet EPA 8082A 03/10/14 11:20PCB-1248 [12672-29-6]^ 1 0.17 RC4C090030.460.17 U mg/kg wet EPA 8082A 03/10/14 15:12PCB-1254 [11097-69-1]^ 5 2.2 RC4C090032.3100 mg/kg wet EPA 8082A 03/10/14 11:20PCB-1260 [11096-82-5]^ 1 0.30 RC4C090030.4616

Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF

2,4,5,6-TCMX 20-13793 % RCEPA 8082A 03/10/14 11:204C090030.84 0.909 1

Decachlorobiphenyl 13-183121 % RCEPA 8082A 03/10/14 11:204C090031.1 0.909 1

HQ-CreamDescription: Lab Sample ID:A401309-03 03/07/14 11:35Received:

A401309Work Order:01/09/14 12:00Sampled:SolidMatrix:

% Solids:casey CoffeySampled By:Project: Deconstruct Facilities, KSC HQ & CIF

Polychlorinated Biphenyls by GC

^ - ENCO Orlando certified analyte [NELAC E83182]

NotesFlag PQL Batch ByAnalyzedMethodMDLResults Units DFAnalyte [CAS Number] mg/kg wet EPA 8082A 03/10/14 11:32PCB-1016/1242

[12674-11-2/53469-21-9]^

1 0.42 RC4C090030.518.0 GC-07

mg/kg wet EPA 8082A 03/10/14 11:32PCB-1221 [11104-28-2]^ 1 0.42 RC4C090030.510.42 U mg/kg wet EPA 8082A 03/10/14 11:32PCB-1232 [11141-16-5]^ 1 0.42 RC4C090030.510.42 U mg/kg wet EPA 8082A 03/10/14 11:32PCB-1248 [12672-29-6]^ 1 0.19 RC4C090030.510.19 U mg/kg wet EPA 8082A 03/10/14 15:24PCB-1254 [11097-69-1]^ 5 2.4 RC4C090032.697 mg/kg wet EPA 8082A 03/10/14 11:32PCB-1260 [11096-82-5]^ 1 0.33 RC4C090030.5128

Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF

2,4,5,6-TCMX 20-137107 % RCEPA 8082A 03/10/14 11:324C090031.1 1.00 1

Decachlorobiphenyl 13-183133 % RCEPA 8082A 03/10/14 11:324C090031.3 1.00 1

Page 6 of 13This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL

HQ-GreenDescription: Lab Sample ID:A401309-04 03/07/14 11:35Received:

A401309Work Order:01/09/14 12:00Sampled:SolidMatrix:

% Solids:casey CoffeySampled By:Project: Deconstruct Facilities, KSC HQ & CIF

Polychlorinated Biphenyls by GC

^ - ENCO Orlando certified analyte [NELAC E83182]

NotesFlag PQL Batch ByAnalyzedMethodMDLResults Units DFAnalyte [CAS Number] mg/kg wet EPA 8082A 03/10/14 11:44PCB-1016/1242

[12674-11-2/53469-21-9]^

1 0.42 RC4C090030.516.1 GC-07

mg/kg wet EPA 8082A 03/10/14 11:44PCB-1221 [11104-28-2]^ 1 0.42 RC4C090030.510.42 U mg/kg wet EPA 8082A 03/10/14 11:44PCB-1232 [11141-16-5]^ 1 0.42 RC4C090030.510.42 U mg/kg wet EPA 8082A 03/10/14 11:44PCB-1248 [12672-29-6]^ 1 0.19 RC4C090030.510.19 U mg/kg wet EPA 8082A 03/10/14 15:36PCB-1254 [11097-69-1]^ 5 2.4 RC4C090032.676 mg/kg wet EPA 8082A 03/10/14 11:44PCB-1260 [11096-82-5]^ 1 0.33 RC4C090030.5116

Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF

2,4,5,6-TCMX 20-13788 % RCEPA 8082A 03/10/14 11:444C090030.88 1.00 1

Decachlorobiphenyl 13-183117 % RCEPA 8082A 03/10/14 11:444C090031.2 1.00 1

HQ-WhiteDescription: Lab Sample ID:A401309-05 03/07/14 11:35Received:

A401309Work Order:01/10/14 12:00Sampled:SolidMatrix:

% Solids:casey CoffeySampled By:Project: Deconstruct Facilities, KSC HQ & CIF

Polychlorinated Biphenyls by GC

^ - ENCO Orlando certified analyte [NELAC E83182]

NotesFlag PQL Batch ByAnalyzedMethodMDLResults Units DFAnalyte [CAS Number] mg/kg wet EPA 8082A 03/10/14 11:56PCB-1016/1242

[12674-11-2/53469-21-9]^

1 0.38 RC4C090030.465.0 GC-07

mg/kg wet EPA 8082A 03/10/14 11:56PCB-1221 [11104-28-2]^ 1 0.38 RC4C090030.460.38 U mg/kg wet EPA 8082A 03/10/14 11:56PCB-1232 [11141-16-5]^ 1 0.38 RC4C090030.460.38 U mg/kg wet EPA 8082A 03/10/14 11:56PCB-1248 [12672-29-6]^ 1 0.17 RC4C090030.460.17 U mg/kg wet EPA 8082A 03/10/14 15:48PCB-1254 [11097-69-1]^ 2 0.87 RC4C090030.9345 mg/kg wet EPA 8082A 03/10/14 11:56PCB-1260 [11096-82-5]^ 1 0.30 RC4C090030.467.5

Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF

2,4,5,6-TCMX 20-13788 % RCEPA 8082A 03/10/14 11:564C090030.80 0.909 1

Decachlorobiphenyl 13-183109 % RCEPA 8082A 03/10/14 11:564C090030.99 0.909 1

HQ-Black2Description: Lab Sample ID:A401309-06 03/07/14 11:35Received:

A401309Work Order:01/27/14 12:00Sampled:SolidMatrix:

% Solids:casey CoffeySampled By:Project: Deconstruct Facilities, KSC HQ & CIF

Polychlorinated Biphenyls by GC

^ - ENCO Orlando certified analyte [NELAC E83182]

NotesFlag PQL Batch ByAnalyzedMethodMDLResults Units DFAnalyte [CAS Number] mg/kg wet EPA 8082A 03/10/14 12:08PCB-1016/1242

[12674-11-2/53469-21-9]^

1 0.42 RC4C090030.513.7 GC-07

mg/kg wet EPA 8082A 03/10/14 12:08PCB-1221 [11104-28-2]^ 1 0.42 RC4C090030.510.42 U mg/kg wet EPA 8082A 03/10/14 12:08PCB-1232 [11141-16-5]^ 1 0.42 RC4C090030.510.42 U mg/kg wet EPA 8082A 03/10/14 12:08PCB-1248 [12672-29-6]^ 1 0.19 RC4C090030.510.19 U mg/kg wet EPA 8082A 03/10/14 16:00PCB-1254 [11097-69-1]^ 5 2.4 RC4C090032.692 mg/kg wet EPA 8082A 03/10/14 12:08PCB-1260 [11096-82-5]^ 1 0.33 RC4C090030.5116

Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF

2,4,5,6-TCMX 20-13770 % RCEPA 8082A 03/10/14 12:084C090030.70 1.00 1

Decachlorobiphenyl 13-183121 % RCEPA 8082A 03/10/14 12:084C090031.2 1.00 1

Page 7 of 13This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL

HQ-Cream2Description: Lab Sample ID:A401309-07 03/07/14 11:35Received:

A401309Work Order:01/27/14 12:00Sampled:SolidMatrix:

% Solids:casey CoffeySampled By:Project: Deconstruct Facilities, KSC HQ & CIF

Polychlorinated Biphenyls by GC

^ - ENCO Orlando certified analyte [NELAC E83182]

NotesFlag PQL Batch ByAnalyzedMethodMDLResults Units DFAnalyte [CAS Number] mg/kg wet EPA 8082A 03/10/14 12:20PCB-1016/1242

[12674-11-2/53469-21-9]^

1 0.42 RC4C090030.514.0 GC-07

mg/kg wet EPA 8082A 03/10/14 12:20PCB-1221 [11104-28-2]^ 1 0.42 RC4C090030.510.42 U mg/kg wet EPA 8082A 03/10/14 12:20PCB-1232 [11141-16-5]^ 1 0.42 RC4C090030.510.42 U mg/kg wet EPA 8082A 03/10/14 12:20PCB-1248 [12672-29-6]^ 1 0.19 RC4C090030.510.19 U mg/kg wet EPA 8082A 03/10/14 16:12PCB-1254 [11097-69-1]^ 2 0.96 RC4C090031.058 mg/kg wet EPA 8082A 03/10/14 12:20PCB-1260 [11096-82-5]^ 1 0.33 RC4C090030.5112

Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF

2,4,5,6-TCMX 20-13793 % RCEPA 8082A 03/10/14 12:204C090030.93 1.00 1

Decachlorobiphenyl 13-183115 % RCEPA 8082A 03/10/14 12:204C090031.1 1.00 1

HQ-Gray2Description: Lab Sample ID:A401309-08 03/07/14 11:35Received:

A401309Work Order:01/27/14 12:00Sampled:SolidMatrix:

% Solids:casey CoffeySampled By:Project: Deconstruct Facilities, KSC HQ & CIF

Polychlorinated Biphenyls by GC

^ - ENCO Orlando certified analyte [NELAC E83182]

NotesFlag PQL Batch ByAnalyzedMethodMDLResults Units DFAnalyte [CAS Number] mg/kg wet EPA 8082A 03/10/14 12:32PCB-1016/1242

[12674-11-2/53469-21-9]^

1 0.42 RC4C090030.515.6 GC-07

mg/kg wet EPA 8082A 03/10/14 12:32PCB-1221 [11104-28-2]^ 1 0.42 RC4C090030.510.42 U mg/kg wet EPA 8082A 03/10/14 12:32PCB-1232 [11141-16-5]^ 1 0.42 RC4C090030.510.42 U mg/kg wet EPA 8082A 03/10/14 12:32PCB-1248 [12672-29-6]^ 1 0.19 RC4C090030.510.19 U mg/kg wet EPA 8082A 03/10/14 16:24PCB-1254 [11097-69-1]^ 5 2.4 RC4C090032.688 mg/kg wet EPA 8082A 03/10/14 12:32PCB-1260 [11096-82-5]^ 1 0.33 RC4C090030.5116

Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF

2,4,5,6-TCMX 20-13787 % RCEPA 8082A 03/10/14 12:324C090030.87 1.00 1

Decachlorobiphenyl 13-18398 % RCEPA 8082A 03/10/14 12:324C090030.98 1.00 1

HQ-Gray3Description: Lab Sample ID:A401309-09 03/07/14 11:35Received:

A401309Work Order:02/18/14 12:00Sampled:SolidMatrix:

% Solids:casey CoffeySampled By:Project: Deconstruct Facilities, KSC HQ & CIF

Polychlorinated Biphenyls by GC

^ - ENCO Orlando certified analyte [NELAC E83182]

NotesFlag PQL Batch ByAnalyzedMethodMDLResults Units DFAnalyte [CAS Number] mg/kg wet EPA 8082A 03/10/14 12:44PCB-1016/1242 [12674-11-2/53469-21-9]^ 1 0.42 RC4C090030.510.42 U mg/kg wet EPA 8082A 03/10/14 12:44PCB-1221 [11104-28-2]^ 1 0.42 RC4C090030.510.42 U mg/kg wet EPA 8082A 03/10/14 12:44PCB-1232 [11141-16-5]^ 1 0.42 RC4C090030.510.42 U mg/kg wet EPA 8082A 03/10/14 12:44PCB-1248 [12672-29-6]^ 1 0.19 RC4C090030.510.19 U mg/kg wet EPA 8082A 03/10/14 12:44PCB-1254 [11097-69-1]^ 1 0.48 RC4C090030.510.54 mg/kg wet EPA 8082A 03/10/14 12:44PCB-1260 [11096-82-5]^ 1 0.33 RC4C090030.510.33 U

Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF

2,4,5,6-TCMX 20-13744 % RCEPA 8082A 03/10/14 12:444C090030.44 1.00 1

Decachlorobiphenyl 13-18359 % RCEPA 8082A 03/10/14 12:444C090030.59 1.00 1

Page 8 of 13This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL

HQ-BrownDescription: Lab Sample ID:A401309-10 03/07/14 11:35Received:

A401309Work Order:02/18/14 12:00Sampled:SolidMatrix:

% Solids:casey CoffeySampled By:Project: Deconstruct Facilities, KSC HQ & CIF

Polychlorinated Biphenyls by GC

^ - ENCO Orlando certified analyte [NELAC E83182]

NotesFlag PQL Batch ByAnalyzedMethodMDLResults Units DFAnalyte [CAS Number] mg/kg wet EPA 8082A 03/10/14 12:56PCB-1016/1242 [12674-11-2/53469-21-9]^ 1 0.42 RC4C090030.510.42 U mg/kg wet EPA 8082A 03/10/14 12:56PCB-1221 [11104-28-2]^ 1 0.42 RC4C090030.510.42 U mg/kg wet EPA 8082A 03/10/14 12:56PCB-1232 [11141-16-5]^ 1 0.42 RC4C090030.510.42 U mg/kg wet EPA 8082A 03/10/14 12:56PCB-1248 [12672-29-6]^ 1 0.19 RC4C090030.510.19 U mg/kg wet EPA 8082A 03/10/14 12:56PCB-1254 [11097-69-1]^ 1 0.48 RC4C090030.510.48 U mg/kg wet EPA 8082A 03/10/14 12:56PCB-1260 [11096-82-5]^ 1 0.33 RC4C090030.510.33 U

Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF

2,4,5,6-TCMX 20-13726 % RCEPA 8082A 03/10/14 12:564C090030.26 1.00 1

Decachlorobiphenyl 13-18348 % RCEPA 8082A 03/10/14 12:564C090030.48 1.00 1

HQ-White2Description: Lab Sample ID:A401309-11 03/07/14 11:35Received:

A401309Work Order:02/18/14 12:00Sampled:SolidMatrix:

% Solids:casey CoffeySampled By:Project: Deconstruct Facilities, KSC HQ & CIF

Polychlorinated Biphenyls by GC

^ - ENCO Orlando certified analyte [NELAC E83182]

NotesFlag PQL Batch ByAnalyzedMethodMDLResults Units DFAnalyte [CAS Number] mg/kg wet EPA 8082A 03/10/14 13:35PCB-1016/1242 [12674-11-2/53469-21-9]^ 1 0.42 RC4C090030.510.42 U mg/kg wet EPA 8082A 03/10/14 13:35PCB-1221 [11104-28-2]^ 1 0.42 RC4C090030.510.42 U mg/kg wet EPA 8082A 03/10/14 13:35PCB-1232 [11141-16-5]^ 1 0.42 RC4C090030.510.42 U mg/kg wet EPA 8082A 03/10/14 13:35PCB-1248 [12672-29-6]^ 1 0.19 RC4C090030.510.19 U mg/kg wet EPA 8082A 03/10/14 13:35PCB-1254 [11097-69-1]^ 1 0.48 RC4C090030.513.6 mg/kg wet EPA 8082A 03/10/14 13:35PCB-1260 [11096-82-5]^ 1 0.33 RC4C090030.510.33 U

Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF

2,4,5,6-TCMX 20-13751 % RCEPA 8082A 03/10/14 13:354C090030.51 1.00 1

Decachlorobiphenyl 13-18383 % RCEPA 8082A 03/10/14 13:354C090030.83 1.00 1

HQ-YellowDescription: Lab Sample ID:A401309-12 03/07/14 11:35Received:

A401309Work Order:02/18/14 12:00Sampled:SolidMatrix:

% Solids:casey CoffeySampled By:Project: Deconstruct Facilities, KSC HQ & CIF

Polychlorinated Biphenyls by GC

^ - ENCO Orlando certified analyte [NELAC E83182]

NotesFlag PQL Batch ByAnalyzedMethodMDLResults Units DFAnalyte [CAS Number] mg/kg wet EPA 8082A 03/10/14 13:47PCB-1016/1242 [12674-11-2/53469-21-9]^ 1 0.38 RC4C090030.460.38 U mg/kg wet EPA 8082A 03/10/14 13:47PCB-1221 [11104-28-2]^ 1 0.38 RC4C090030.460.38 U mg/kg wet EPA 8082A 03/10/14 13:47PCB-1232 [11141-16-5]^ 1 0.38 RC4C090030.460.38 U mg/kg wet EPA 8082A 03/10/14 13:47PCB-1248 [12672-29-6]^ 1 0.17 RC4C090030.460.17 U mg/kg wet EPA 8082A 03/10/14 13:47PCB-1254 [11097-69-1]^ 1 0.44 RC4C090030.462.7 mg/kg wet EPA 8082A 03/10/14 13:47PCB-1260 [11096-82-5]^ 1 0.30 RC4C090030.460.30 U

Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF

2,4,5,6-TCMX 20-13764 % RCEPA 8082A 03/10/14 13:474C090030.58 0.909 1

Decachlorobiphenyl 13-18387 % RCEPA 8082A 03/10/14 13:474C090030.79 0.909 1

Page 9 of 13This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL

HQ-LT GrayDescription: Lab Sample ID:A401309-13 03/07/14 11:35Received:

A401309Work Order:02/20/14 12:00Sampled:SolidMatrix:

% Solids:casey CoffeySampled By:Project: Deconstruct Facilities, KSC HQ & CIF

Polychlorinated Biphenyls by GC

^ - ENCO Orlando certified analyte [NELAC E83182]

NotesFlag PQL Batch ByAnalyzedMethodMDLResults Units DFAnalyte [CAS Number] mg/kg wet EPA 8082A 03/10/14 14:00PCB-1016/1242

[12674-11-2/53469-21-9]^

1 0.42 RC4C090030.515.3 GC-07

mg/kg wet EPA 8082A 03/10/14 14:00PCB-1221 [11104-28-2]^ 1 0.42 RC4C090030.510.42 U mg/kg wet EPA 8082A 03/10/14 14:00PCB-1232 [11141-16-5]^ 1 0.42 RC4C090030.510.42 U mg/kg wet EPA 8082A 03/10/14 14:00PCB-1248 [12672-29-6]^ 1 0.19 RC4C090030.510.19 U mg/kg wet EPA 8082A 03/10/14 14:32PCB-1254 [11097-69-1]^ 10 4.8 RC4C090035.1120 mg/kg wet EPA 8082A 03/10/14 14:00PCB-1260 [11096-82-5]^ 1 0.33 RC4C090030.5125

Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF

2,4,5,6-TCMX 20-13782 % RCEPA 8082A 03/10/14 14:004C090030.82 1.00 1

Decachlorobiphenyl 13-183114 % RCEPA 8082A 03/10/14 14:004C090031.1 1.00 1

Page 10 of 13This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL

QUALITY CONTROL DATA

Polychlorinated Biphenyls by GC - Quality Control

Batch 4C09003 - EPA 3550C

Prepared: 03/09/2014 07:30 Analyzed: 03/10/2014 08:43Blank (4C09003-BLK1)

FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL

Spike Source %REC RPD mg/kg wet0.0170.014 U PCB-1016/1242 mg/kg wet0.0170.014 U PCB-1221 mg/kg wet0.0170.014 U PCB-1232 mg/kg wet0.0170.0063 U PCB-1248 mg/kg wet0.0170.016 U PCB-1254 mg/kg wet0.0170.011 U PCB-1260 mg/kg wet 0.0333 20-1372,4,5,6-TCMX 880.029 mg/kg wet 0.0333 13-183Decachlorobiphenyl [2C] 980.032

Prepared: 03/09/2014 07:30 Analyzed: 03/10/2014 08:55LCS (4C09003-BS1)

FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL

Spike Source %REC RPD mg/kg wet0.017 0.333 29-185850.28 PCB-1016/1242 mg/kg wet0.017 0.333 66-171910.30 PCB-1260 mg/kg wet 0.0333 20-1372,4,5,6-TCMX 920.031 mg/kg wet 0.0333 13-183Decachlorobiphenyl [2C] 1120.038

Prepared: 03/09/2014 07:30 Analyzed: 03/10/2014 09:07LCS Dup (4C09003-BSD1)

FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL

Spike Source %REC RPD mg/kg wet0.017 0.333 2129-18590 50.30 PCB-1016/1242 mg/kg wet0.017 0.333 1766-17196 50.32 PCB-1260 mg/kg wet 0.0333 20-1372,4,5,6-TCMX 890.030 mg/kg wet 0.0333 13-183Decachlorobiphenyl [2C] 1160.039

Page 11 of 13This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL

FLAGS/NOTES AND DEFINITIONS

PQL: Practical Quantitation Limit.PQL

B Results are based upon membrane filter colony counts that are outside the method indicated ideal range.

I The reported value is between the laboratory method detection limit (MDL) and the practical quantitation limit (PQL).

J Estimated value.

K Off-scale low; Actual value is known to be less than the value given.

L Off-scale high; Actual value is known to be greater than value given.

M Presence of analyte is verified but not quantified; the actual value is less than the MRL but greater than the

MDL.

N Presumptive evidence of presence of material.

O Sampled, but analysis lost or not performed.

Q Sample exceeded the accepted holding time.

T Value reported is less than the laboratory method detection limit. The value is reported for informational purposes only and shall not be used in statistical analysis.

U Indicates that the compound was analyzed for but not detected.

V Indicates that the analyte was detected in both the sample and the associated method blank.

Y The laboratory analysis was from an improperly preserved sample. The data may not be accurate.

Z Too many colonies were present (TNTC); the numeric value represents the filtration volume.

? Data are rejected and should not be used. Some or all of the quality control data for the analyte were outside criteria, and the presence or absence of the analyte cannot be determined from the data.

* Not reported due to interference.

Confirmation result exceeds 40% RPD, lower result reported due to interference.GC-07

Page 12 of 13This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL

407.826.5314 407.850.6945Phone: FAX:

ENCO Workorder(s): A401401

Titusville, FL 32780

Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures.

Results for these procedures apply only to the samples as submitted.

The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative. This report shall not be reproduced except in full, without the written approval of the Laboratory.

This report contains only those analyses performed by Environmental Conservation

Laboratories. Unless otherwise noted, all analyses were performed at ENCO Orlando. Data from outside organizations will be reported under separate cover.

If you have any questions or require further information, please do not hesitate to contact me.

Sincerely, Enclosure(s)

Project Number: 14000-221-01, Project Name/Desc: Deconstruct Facilities, KSC HQ & CIF

Attn: Casey Coffey

Jones Edmunds & Associates (JO005)

3910 S. Washington Ave Suite 210

David Camacho

Project Manager

Tuesday, March 18, 2014

RE: Laboratory Results for

Dear Casey Coffey, Enclosed is a copy of your laboratory report for test samples received by our laboratory on

Thursday, March 13, 2014.

Enclosure(s)

Page 1 of 9This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL

CIF-BLACK A401401-01 Sampled: 02/24/14 12:00 Received: 03/13/14 11:25Client ID: Lab ID:

Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)

EPA 8082A 02/24/15 03/17/14 10:19 03/17/14 17:2002/24/15

CIF-BLACK A401401-01RE1 Sampled: 02/24/14 12:00 Received: 03/13/14 11:25Client ID: Lab ID:

Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)

EPA 8082A 02/24/15 03/17/14 10:19 03/18/14 10:2402/24/15

CIF-Gray A401401-02 Sampled: 02/24/14 12:00 Received: 03/13/14 11:25Client ID: Lab ID:

Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)

EPA 8082A 02/24/15 03/17/14 10:19 03/17/14 17:3202/24/15

CIF-Gray A401401-02RE1 Sampled: 02/24/14 12:00 Received: 03/13/14 11:25Client ID: Lab ID:

Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)

EPA 8082A 02/24/15 03/17/14 10:19 03/18/14 10:3702/24/15

CIF-White A401401-03 Sampled: 02/25/14 12:00 Received: 03/13/14 11:25Client ID: Lab ID:

Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)

EPA 8082A 02/25/15 03/17/14 10:19 03/17/14 17:4402/25/15

CIF-White A401401-03RE1 Sampled: 02/25/14 12:00 Received: 03/13/14 11:25Client ID: Lab ID:

Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)

EPA 8082A 02/25/15 03/17/14 10:19 03/18/14 10:4902/25/15

CIF-Cream A401401-04 Sampled: 02/25/14 12:00 Received: 03/13/14 11:25Client ID: Lab ID:

Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)

EPA 8082A 02/25/15 03/17/14 10:19 03/17/14 17:5602/25/15

CIF-Cream A401401-04RE1 Sampled: 02/25/14 12:00 Received: 03/13/14 11:25Client ID: Lab ID:

Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)

EPA 8082A 02/25/15 03/17/14 10:19 03/18/14 11:0102/25/15

THL-Cream A401401-05 Sampled: 03/10/14 12:00 Received: 03/13/14 11:25Client ID: Lab ID:

Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)

EPA 8082A 03/10/15 03/17/14 10:19 03/17/14 18:3303/10/15

THL-White A401401-06 Sampled: 03/10/14 12:00 Received: 03/13/14 11:25Client ID: Lab ID:

Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)

EPA 8082A 03/10/15 03/17/14 10:19 03/17/14 18:4503/10/15

THL-Gray A401401-07 Sampled: 03/10/14 12:00 Received: 03/13/14 11:25Client ID: Lab ID:

Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)

EPA 8082A 03/10/15 03/17/14 10:19 03/17/14 18:5703/10/15

CIF-White2 A401401-08 Sampled: 03/11/14 12:00 Received: 03/13/14 11:25Client ID: Lab ID:

Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)

EPA 8082A 03/11/15 03/17/14 10:19 03/17/14 19:0903/11/15

CIF-Black2 A401401-09 Sampled: 03/11/14 12:00 Received: 03/13/14 11:25Client ID: Lab ID:

Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)

EPA 8082A 03/11/15 03/17/14 10:19 03/17/14 19:2103/11/15

CIF-Black2 A401401-09RE1 Sampled: 03/11/14 12:00 Received: 03/13/14 11:25Client ID: Lab ID:

Prep Date/Time(s)Hold Date/Time(s)Parameter Analysis Date/Time(s)

EPA 8082A 03/11/15 03/17/14 10:19 03/18/14 11:1303/11/15

Page 2 of 9This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL

Lab ID:Client ID: CIF-BLACK A401401-01

Analyte MethodUnitsPQLResults Flag NotesMDL

21 0.51 mg/kg wet EPA 8082A GC-07PCB-1016/1242 0.42

Lab ID:Client ID: CIF-BLACK A401401-01RE1

Analyte MethodUnitsPQLResults Flag NotesMDL

690 10 mg/kg wet EPA 8082A PCB-1254 9.6

340 10 mg/kg wet EPA 8082A PCB-1260 6.6

Lab ID:Client ID: CIF-Gray A401401-02

Analyte MethodUnitsPQLResults Flag NotesMDL

16 0.51 mg/kg wet EPA 8082A GC-07PCB-1016/1242 0.42

18 0.51 mg/kg wet EPA 8082A PCB-1260 0.33

Lab ID:Client ID: CIF-Gray A401401-02RE1

Analyte MethodUnitsPQLResults Flag NotesMDL

130 2.6 mg/kg wet EPA 8082A PCB-1254 2.4

Lab ID:Client ID: CIF-White A401401-03

Analyte MethodUnitsPQLResults Flag NotesMDL

9.0 0.51 mg/kg wet EPA 8082A GC-07PCB-1016/1242 0.42

16 0.51 mg/kg wet EPA 8082A PCB-1260 0.33

Lab ID:Client ID: CIF-White A401401-03RE1

Analyte MethodUnitsPQLResults Flag NotesMDL

94 2.6 mg/kg wet EPA 8082A PCB-1254 2.4

92 2.6 mg/kg wet EPA 8082A PCB-1254 2.4

Lab ID:Client ID: CIF-Cream A401401-04

Analyte MethodUnitsPQLResults Flag NotesMDL

13 0.51 mg/kg wet EPA 8082A GC-07PCB-1016/1242 0.42

21 0.51 mg/kg wet EPA 8082A PCB-1260 0.33

Lab ID:Client ID: CIF-Cream A401401-04RE1

Analyte MethodUnitsPQLResults Flag NotesMDL

84 2.6 mg/kg wet EPA 8082A PCB-1254 2.4

86 2.6 mg/kg wet EPA 8082A PCB-1254 2.4

Lab ID:Client ID: THL-Cream A401401-05

Analyte MethodUnitsPQLResults Flag NotesMDL

2.7 0.51 mg/kg wet EPA 8082A PCB-1254 0.48

1.9 0.51 mg/kg wet EPA 8082A PCB-1260 0.33

Lab ID:Client ID: THL-White A401401-06

Analyte MethodUnitsPQLResults Flag NotesMDL

2.4 0.51 mg/kg wet EPA 8082A PCB-1254 0.48

0.62 0.51 mg/kg wet EPA 8082A PCB-1260 0.33

Lab ID:Client ID: CIF-White2 A401401-08

Analyte MethodUnitsPQLResults Flag NotesMDL

1.1 0.51 mg/kg wet EPA 8082A PCB-1254 0.48

Lab ID:Client ID: CIF-Black2 A401401-09

Analyte MethodUnitsPQLResults Flag NotesMDL

11 0.51 mg/kg wet EPA 8082A GC-07PCB-1016/1242 0.42

Lab ID:Client ID: CIF-Black2 A401401-09RE1

Analyte MethodUnitsPQLResults Flag NotesMDL

310 5.1 mg/kg wet EPA 8082A PCB-1254 4.8

110 5.1 mg/kg wet EPA 8082A PCB-1260 3.3

Page 3 of 9This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL

CIF-BLACKDescription: Lab Sample ID:A401401-01 03/13/14 11:25Received:

A401401Work Order:02/24/14 12:00Sampled:SolidMatrix:

% Solids:Casey CoffeySampled By:Project: Deconstruct Facilities, KSC HQ & CIF

Polychlorinated Biphenyls by GC

^ - ENCO Orlando certified analyte [NELAC E83182]

NotesFlag PQL Batch ByAnalyzedMethodMDLResults Units DFAnalyte [CAS Number] mg/kg wet EPA 8082A 03/17/14 17:20PCB-1016/1242

[12674-11-2/53469-21-9]^

1 0.42 RC4C170030.5121 GC-07

mg/kg wet EPA 8082A 03/17/14 17:20PCB-1221 [11104-28-2]^ 1 0.42 RC4C170030.510.42 U mg/kg wet EPA 8082A 03/17/14 17:20PCB-1232 [11141-16-5]^ 1 0.42 RC4C170030.510.42 U mg/kg wet EPA 8082A 03/17/14 17:20PCB-1248 [12672-29-6]^ 1 0.19 RC4C170030.510.19 U mg/kg wet EPA 8082A 03/18/14 10:24PCB-1254 [11097-69-1]^ 20 9.6 RC4C1700310690 mg/kg wet EPA 8082A 03/18/14 10:24PCB-1260 [11096-82-5]^ 20 6.6 RC4C1700310340

Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF

2,4,5,6-TCMX 20-137119 % RCEPA 8082A 03/17/14 17:204C170031.2 1.00 1

Decachlorobiphenyl 13-183109 % RCEPA 8082A 03/17/14 17:204C170031.1 1.00 1

CIF-GrayDescription: Lab Sample ID:A401401-02 03/13/14 11:25Received:

A401401Work Order:02/24/14 12:00Sampled:SolidMatrix:

% Solids:Casey CoffeySampled By:Project: Deconstruct Facilities, KSC HQ & CIF

Polychlorinated Biphenyls by GC

^ - ENCO Orlando certified analyte [NELAC E83182]

NotesFlag PQL Batch ByAnalyzedMethodMDLResults Units DFAnalyte [CAS Number] mg/kg wet EPA 8082A 03/17/14 17:32PCB-1016/1242

[12674-11-2/53469-21-9]^

1 0.42 RC4C170030.5116 GC-07

mg/kg wet EPA 8082A 03/17/14 17:32PCB-1221 [11104-28-2]^ 1 0.42 RC4C170030.510.42 U mg/kg wet EPA 8082A 03/17/14 17:32PCB-1232 [11141-16-5]^ 1 0.42 RC4C170030.510.42 U mg/kg wet EPA 8082A 03/17/14 17:32PCB-1248 [12672-29-6]^ 1 0.19 RC4C170030.510.19 U mg/kg wet EPA 8082A 03/18/14 10:37PCB-1254 [11097-69-1]^ 5 2.4 RC4C170032.6130 mg/kg wet EPA 8082A 03/17/14 17:32PCB-1260 [11096-82-5]^ 1 0.33 RC4C170030.5118

Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF

2,4,5,6-TCMX 20-13795 % RCEPA 8082A 03/17/14 17:324C170030.95 1.00 1

Decachlorobiphenyl 13-183104 % RCEPA 8082A 03/17/14 17:324C170031.0 1.00 1

CIF-WhiteDescription: Lab Sample ID:A401401-03 03/13/14 11:25Received:

A401401Work Order:02/25/14 12:00Sampled:SolidMatrix:

% Solids:Casey CoffeySampled By:Project: Deconstruct Facilities, KSC HQ & CIF

Polychlorinated Biphenyls by GC

^ - ENCO Orlando certified analyte [NELAC E83182]

NotesFlag PQL Batch ByAnalyzedMethodMDLResults Units DFAnalyte [CAS Number] mg/kg wet EPA 8082A 03/17/14 17:44PCB-1016/1242

[12674-11-2/53469-21-9]^

1 0.42 RC4C170030.519.0 GC-07

mg/kg wet EPA 8082A 03/17/14 17:44PCB-1221 [11104-28-2]^ 1 0.42 RC4C170030.510.42 U mg/kg wet EPA 8082A 03/17/14 17:44PCB-1232 [11141-16-5]^ 1 0.42 RC4C170030.510.42 U mg/kg wet EPA 8082A 03/17/14 17:44PCB-1248 [12672-29-6]^ 1 0.19 RC4C170030.510.19 U mg/kg wet EPA 8082A 03/18/14 10:49PCB-1254 [11097-69-1]^ 5 2.4 RC4C170032.694 mg/kg wet EPA 8082A 03/18/14 10:49PCB-1254 [11097-69-1]^ 5 2.4 RC4C170032.692 mg/kg wet EPA 8082A 03/17/14 17:44PCB-1260 [11096-82-5]^ 1 0.33 RC4C170030.5116

Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF

2,4,5,6-TCMX 20-13799 % RCEPA 8082A 03/17/14 17:444C170030.99 1.00 1

Decachlorobiphenyl 13-183101 % RCEPA 8082A 03/17/14 17:444C170031.0 1.00 1

Page 4 of 9This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL

CIF-CreamDescription: Lab Sample ID:A401401-04 03/13/14 11:25Received:

A401401Work Order:02/25/14 12:00Sampled:SolidMatrix:

% Solids:Casey CoffeySampled By:Project: Deconstruct Facilities, KSC HQ & CIF

Polychlorinated Biphenyls by GC

^ - ENCO Orlando certified analyte [NELAC E83182]

NotesFlag PQL Batch ByAnalyzedMethodMDLResults Units DFAnalyte [CAS Number] mg/kg wet EPA 8082A 03/17/14 17:56PCB-1016/1242

[12674-11-2/53469-21-9]^

1 0.42 RC4C170030.5113 GC-07

mg/kg wet EPA 8082A 03/17/14 17:56PCB-1221 [11104-28-2]^ 1 0.42 RC4C170030.510.42 U mg/kg wet EPA 8082A 03/17/14 17:56PCB-1232 [11141-16-5]^ 1 0.42 RC4C170030.510.42 U mg/kg wet EPA 8082A 03/17/14 17:56PCB-1248 [12672-29-6]^ 1 0.19 RC4C170030.510.19 U mg/kg wet EPA 8082A 03/18/14 11:01PCB-1254 [11097-69-1]^ 5 2.4 RC4C170032.684 mg/kg wet EPA 8082A 03/18/14 11:01PCB-1254 [11097-69-1]^ 5 2.4 RC4C170032.686 mg/kg wet EPA 8082A 03/17/14 17:56PCB-1260 [11096-82-5]^ 1 0.33 RC4C170030.5121

Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF

2,4,5,6-TCMX 20-13794 % RCEPA 8082A 03/17/14 17:564C170030.94 1.00 1

Decachlorobiphenyl 13-18391 % RCEPA 8082A 03/17/14 17:564C170030.91 1.00 1

THL-CreamDescription: Lab Sample ID:A401401-05 03/13/14 11:25Received:

A401401Work Order:03/10/14 12:00Sampled:SolidMatrix:

% Solids:Casey CoffeySampled By:Project: Deconstruct Facilities, KSC HQ & CIF

Polychlorinated Biphenyls by GC

^ - ENCO Orlando certified analyte [NELAC E83182]

NotesFlag PQL Batch ByAnalyzedMethodMDLResults Units DFAnalyte [CAS Number] mg/kg wet EPA 8082A 03/17/14 18:33PCB-1016/1242 [12674-11-2/53469-21-9]^ 1 0.42 RC4C170030.510.42 U GC-07 mg/kg wet EPA 8082A 03/17/14 18:33PCB-1221 [11104-28-2]^ 1 0.42 RC4C170030.510.42 U mg/kg wet EPA 8082A 03/17/14 18:33PCB-1232 [11141-16-5]^ 1 0.42 RC4C170030.510.42 U mg/kg wet EPA 8082A 03/17/14 18:33PCB-1248 [12672-29-6]^ 1 0.19 RC4C170030.510.19 U mg/kg wet EPA 8082A 03/17/14 18:33PCB-1254 [11097-69-1]^ 1 0.48 RC4C170030.512.7 mg/kg wet EPA 8082A 03/17/14 18:33PCB-1260 [11096-82-5]^ 1 0.33 RC4C170030.511.9

Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF

2,4,5,6-TCMX 20-137102 % RCEPA 8082A 03/17/14 18:334C170031.0 1.00 1

Decachlorobiphenyl 13-183112 % RCEPA 8082A 03/17/14 18:334C170031.1 1.00 1

THL-WhiteDescription: Lab Sample ID:A401401-06 03/13/14 11:25Received:

A401401Work Order:03/10/14 12:00Sampled:SolidMatrix:

% Solids:Casey CoffeySampled By:Project: Deconstruct Facilities, KSC HQ & CIF

Polychlorinated Biphenyls by GC

^ - ENCO Orlando certified analyte [NELAC E83182]

NotesFlag PQL Batch ByAnalyzedMethodMDLResults Units DFAnalyte [CAS Number] mg/kg wet EPA 8082A 03/17/14 18:45PCB-1016/1242 [12674-11-2/53469-21-9]^ 1 0.42 RC4C170030.510.42 U mg/kg wet EPA 8082A 03/17/14 18:45PCB-1221 [11104-28-2]^ 1 0.42 RC4C170030.510.42 U mg/kg wet EPA 8082A 03/17/14 18:45PCB-1232 [11141-16-5]^ 1 0.42 RC4C170030.510.42 U mg/kg wet EPA 8082A 03/17/14 18:45PCB-1248 [12672-29-6]^ 1 0.19 RC4C170030.510.19 U mg/kg wet EPA 8082A 03/17/14 18:45PCB-1254 [11097-69-1]^ 1 0.48 RC4C170030.512.4 mg/kg wet EPA 8082A 03/17/14 18:45PCB-1260 [11096-82-5]^ 1 0.33 RC4C170030.510.62

Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF

2,4,5,6-TCMX 20-137101 % RCEPA 8082A 03/17/14 18:454C170031.0 1.00 1

Decachlorobiphenyl 13-183111 % RCEPA 8082A 03/17/14 18:454C170031.1 1.00 1

Page 5 of 9This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL

THL-GrayDescription: Lab Sample ID:A401401-07 03/13/14 11:25Received:

A401401Work Order:03/10/14 12:00Sampled:SolidMatrix:

% Solids:Casey CoffeySampled By:Project: Deconstruct Facilities, KSC HQ & CIF

Polychlorinated Biphenyls by GC

^ - ENCO Orlando certified analyte [NELAC E83182]

NotesFlag PQL Batch ByAnalyzedMethodMDLResults Units DFAnalyte [CAS Number] mg/kg wet EPA 8082A 03/17/14 18:57PCB-1016/1242 [12674-11-2/53469-21-9]^ 1 0.42 RC4C170030.510.42 U mg/kg wet EPA 8082A 03/17/14 18:57PCB-1221 [11104-28-2]^ 1 0.42 RC4C170030.510.42 U mg/kg wet EPA 8082A 03/17/14 18:57PCB-1232 [11141-16-5]^ 1 0.42 RC4C170030.510.42 U mg/kg wet EPA 8082A 03/17/14 18:57PCB-1248 [12672-29-6]^ 1 0.19 RC4C170030.510.19 U mg/kg wet EPA 8082A 03/17/14 18:57PCB-1254 [11097-69-1]^ 1 0.48 RC4C170030.510.48 U mg/kg wet EPA 8082A 03/17/14 18:57PCB-1260 [11096-82-5]^ 1 0.33 RC4C170030.510.33 U

Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF

2,4,5,6-TCMX 20-137105 % RCEPA 8082A 03/17/14 18:574C170031.0 1.00 1

Decachlorobiphenyl 13-183104 % RCEPA 8082A 03/17/14 18:574C170031.0 1.00 1

CIF-White2Description: Lab Sample ID:A401401-08 03/13/14 11:25Received:

A401401Work Order:03/11/14 12:00Sampled:SolidMatrix:

% Solids:Casey CoffeySampled By:Project: Deconstruct Facilities, KSC HQ & CIF

Polychlorinated Biphenyls by GC

^ - ENCO Orlando certified analyte [NELAC E83182]

NotesFlag PQL Batch ByAnalyzedMethodMDLResults Units DFAnalyte [CAS Number] mg/kg wet EPA 8082A 03/17/14 19:09PCB-1016/1242 [12674-11-2/53469-21-9]^ 1 0.42 RC4C170030.510.42 U mg/kg wet EPA 8082A 03/17/14 19:09PCB-1221 [11104-28-2]^ 1 0.42 RC4C170030.510.42 U mg/kg wet EPA 8082A 03/17/14 19:09PCB-1232 [11141-16-5]^ 1 0.42 RC4C170030.510.42 U mg/kg wet EPA 8082A 03/17/14 19:09PCB-1248 [12672-29-6]^ 1 0.19 RC4C170030.510.19 U mg/kg wet EPA 8082A 03/17/14 19:09PCB-1254 [11097-69-1]^ 1 0.48 RC4C170030.511.1 mg/kg wet EPA 8082A 03/17/14 19:09PCB-1260 [11096-82-5]^ 1 0.33 RC4C170030.510.33 U

Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF

2,4,5,6-TCMX 20-137118 % RCEPA 8082A 03/17/14 19:094C170031.2 1.00 1

Decachlorobiphenyl 13-183132 % RCEPA 8082A 03/17/14 19:094C170031.3 1.00 1

CIF-Black2Description: Lab Sample ID:A401401-09 03/13/14 11:25Received:

A401401Work Order:03/11/14 12:00Sampled:SolidMatrix:

% Solids:Casey CoffeySampled By:Project: Deconstruct Facilities, KSC HQ & CIF

Polychlorinated Biphenyls by GC

^ - ENCO Orlando certified analyte [NELAC E83182]

NotesFlag PQL Batch ByAnalyzedMethodMDLResults Units DFAnalyte [CAS Number] mg/kg wet EPA 8082A 03/17/14 19:21PCB-1016/1242

[12674-11-2/53469-21-9]^

1 0.42 RC4C170030.5111 GC-07

mg/kg wet EPA 8082A 03/17/14 19:21PCB-1221 [11104-28-2]^ 1 0.42 RC4C170030.510.42 U mg/kg wet EPA 8082A 03/17/14 19:21PCB-1232 [11141-16-5]^ 1 0.42 RC4C170030.510.42 U mg/kg wet EPA 8082A 03/17/14 19:21PCB-1248 [12672-29-6]^ 1 0.19 RC4C170030.510.19 U mg/kg wet EPA 8082A 03/18/14 11:13PCB-1254 [11097-69-1]^ 10 4.8 RC4C170035.1310 mg/kg wet EPA 8082A 03/18/14 11:13PCB-1260 [11096-82-5]^ 10 3.3 RC4C170035.1110

Surrogates Results Spike Lvl % Rec Batch Method Analyzed By% Rec Limits NotesDF

2,4,5,6-TCMX 20-137114 % RCEPA 8082A 03/17/14 19:214C170032.3 2.00 1

Decachlorobiphenyl 13-183129 % RCEPA 8082A 03/17/14 19:214C170032.6 2.00 1

Page 6 of 9This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL

Batch 4C17003 - EPA 3550C

Prepared: 03/17/2014 10:19 Analyzed: 03/17/2014 16:07Blank (4C17003-BLK1)

FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL

Spike Source %REC RPD mg/kg wet0.0170.014 U PCB-1016/1242 mg/kg wet0.0170.014 U PCB-1221 mg/kg wet0.0170.014 U PCB-1232 mg/kg wet0.0170.0063 U PCB-1248 mg/kg wet0.0170.016 U PCB-1254 mg/kg wet0.0170.011 U PCB-1260 mg/kg wet 0.0333 20-1372,4,5,6-TCMX 1260.042 mg/kg wet 0.0333 13-183Decachlorobiphenyl 1700.057

Prepared: 03/17/2014 10:19 Analyzed: 03/17/2014 16:19LCS (4C17003-BS1)

FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL

Spike Source %REC RPD mg/kg wet0.017 0.333 29-1851100.37 PCB-1016/1242 mg/kg wet0.017 0.333 66-1711200.40 PCB-1260 mg/kg wet 0.0333 20-1372,4,5,6-TCMX 1280.043 mg/kg wet 0.0333 13-183Decachlorobiphenyl 1770.059

Prepared: 03/17/2014 10:19 Analyzed: 03/17/2014 16:32Matrix Spike (4C17003-MS1)

Source: A401454-28

FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL

Spike Source %REC RPD mg/kg wet0.017 0.334 29-1855000.014 U1.7 L E, QM-05PCB-1016/1242 mg/kg wet0.017 0.334 66-171780.011 U0.26 PCB-1260 mg/kg wet 0.0334 20-1372,4,5,6-TCMX 940.031 mg/kg wet 0.0334 13-183Decachlorobiphenyl 920.031

Prepared: 03/17/2014 10:19 Analyzed: 03/17/2014 16:44Matrix Spike Dup (4C17003-MSD1)

Source: A401454-28

FlagResult Units Level Result %REC Limits RPD Limit Notes Analyte PQL

Spike Source %REC RPD mg/kg wet0.017 0.337 2129-185520 50.014 U1.7 L E, QM-05PCB-1016/1242 mg/kg wet0.017 0.337 1766-17181 40.011 U0.27 PCB-1260 mg/kg wet 0.0337 20-1372,4,5,6-TCMX 1000.034 mg/kg wet 0.0337 13-183Decachlorobiphenyl 1010.034

Page 7 of 9This report relates only to the sample as received by the laboratory, and may only be reproduced in full.FINAL

B Results are based upon membrane filter colony counts that are outside the method indicated ideal range.

I The reported value is between the laboratory method detection limit (MDL) and the practical quantitation limit (PQL).

J Estimated value.

K Off-scale low; Actual value is known to be less than the value given.

L Off-scale high; Actual value is…