B919 OWS Liquid and Sludge Analytical Report Feb 2024.pdf

PDF 412 KB Posted May 30, 2024

Attached to: OWS STI-SP001 Inspection
Solicitation number: FA667024Q0004
Issued by: Department of the Air Force Reserve Command

About this file

Written by GovTribe AI · May 30, 2024

This document is a combined synopsis/solicitation for a commercial services contract issued by the Department of the Air Force Reserve Command. The requirement is for a one-time inspection of an underground storage tank at the Niagara Falls Air Reserve Station. The work includes removing water/sludge from the tank and conducting an STI-SP001 out of service inspection. The solicitation is a 100% small business set-aside with a NAICS code of 541380. The agency is seeking firm-fixed price quotes from small businesses by June 7, 2024 at 1:00 PM EDT. Award will be made to the responsive, responsible offeror with the lowest price whose technical capability is determined to be acceptable. No incumbent contractor is identified.

View the file

Other files

File	Type	Posted
OWS location.pdf	PDF	Jun 3, 2024
Amendment 3 - Questions and Answers.pdf	PDF	Jun 3, 2024
Questions and Answers 2.pdf	PDF	Jun 3, 2024
Amendment 2 - Questions and Answers.pdf	PDF	May 30, 2024
Questions and Answers 1.pdf	PDF	May 30, 2024
OWS As Built.pdf	PDF	May 30, 2024
Amendment 1 - Wage Determination.pdf	PDF	May 30, 2024
Amendment 1 - Wage Determation 2015-4147 - 29 Apr 24.pdf	PDF	May 30, 2024
Attachment 0 - Combined Synopsis Solicitation RFQ.pdf	PDF	May 23, 2024
Attachment 1 - OWS STI Inspection - 21 Jan 24.pdf	PDF	May 23, 2024

On GovTribe

Work with this file

Download the original file
Contacts named in this file
Similar government files
Ask GovTribe AI about this file

Try for free Login

Text version

The file's text, extracted by GovTribe without its formatting.

L2409617

AFI Environmental

NFAB MM

NFAB MM 20240222

Client:

Project Name:

Project Number:

02/29/24

Eight Walkup Drive, Westborough, MA 01581-1019

Lab Number:

Report Date:

508-898-9220 (Fax) 508-898-9193 800-624-9220 - www.alphalab.com

8644 Buffalo Avenue

PO Box 4049

Joshua HeitzenraterATTN:

ANALYTICAL REPORT

Certifications & Approvals: MA (M-MA086), NH NELAP (2064), CT (PH-0826), IL (200077), IN (C-MA-03), KY (KY98045), ME (MA00086), MD (348), NJ (MA935), NY (11148), NC (25700/666), OH (CL108), OR (MA-1316), PA (68-03671), RI (LAO00065), TX (T104704476), VT (VT-0935), VA (460195), USDA (Permit #525-23-122-91930).

Niagara Falls, NY 14304

(716) 940-2725Phone:

The original project report/data package is held by Alpha Analytical. This report/data package is paginated and should be reproduced only in its entirety. Alpha Analytical holds no responsibility for results and/or data that are not consistent with the original.

Serial_No:02292415:55

ORGANICS

VOLATILES

Methylene chloride

1,1-Dichloroethane

Chloroform

Carbon tetrachloride

1,2-Dichloropropane

Dibromochloromethane

1,1,2-Trichloroethane

Tetrachloroethene

Chlorobenzene

Trichlorofluoromethane

1,2-Dichloroethane

1,1,1-Trichloroethane

Bromodichloromethane trans-1,3-Dichloropropene cis-1,3-Dichloropropene

Bromoform

1,1,2,2-Tetrachloroethane

Benzene

Toluene

Ethylbenzene

Chloromethane

Bromomethane

Vinyl chloride

Chloroethane

1,1-Dichloroethene trans-1,2-Dichloroethene

Trichloroethene

1,2-Dichlorobenzene

Parameter Result Dilution Factor

ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg

Qualifier Units RL

Volatile Organics by GC/MS - Westborough Lab

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFAB MM 20240222

NFAB MM

L2409617

02/29/24

B-919 OWS 20240222 1155Client ID:

02/22/24 11:55Date Collected:

02/22/24Date Received:

NFABSample Location:

L2409617-01Lab ID:

Field Prep: Not Specified

Matrix: Oil Analytical Method:

Analytical Date:

Analyst:

1,8260D 02/29/24 13:34

LAC

Percent Solids: Results reported on an 'AS RECEIVED' basis.

MDL

72.

69.

62.

69.

97.

63.

83.

54.

78.

82.

70.

68.

71.

Sample Depth:

1,3-Dichlorobenzene

1,4-Dichlorobenzene

Methyl tert butyl ether p/m-Xylene o-Xylene cis-1,2-Dichloroethene

Styrene

Dichlorodifluoromethane

Acetone

Carbon disulfide

2-Butanone

4-Methyl-2-pentanone

2-Hexanone

Bromochloromethane

1,2-Dibromoethane

1,2-Dibromo-3-chloropropane

Isopropylbenzene

1,2,3-Trichlorobenzene

1,2,4-Trichlorobenzene

Methyl Acetate

Cyclohexane

1,4-Dioxane

Freon-113

Methyl cyclohexane

Parameter Result

Dilution Factor

ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg

Qualifier Units RL

Volatile Organics by GC/MS - Westborough Lab

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFAB MM 20240222

NFAB MM

L2409617

40000

1,2-Dichloroethane-d4

Toluene-d8

4-Bromofluorobenzene

Dibromofluoromethane

70-130

Acceptance Criteria

Surrogate % Recovery Qualifier

02/29/24

B-919 OWS 20240222 1155Client ID:

02/22/24 11:55Date Collected:

02/22/24Date Received:

NFABSample Location:

L2409617-01Lab ID:

Field Prep: Not Specified

MDL

73.

85.

87.

97.

54.

17000

Sample Depth:

1,1-Dichloroethane

Chloroform

Carbon tetrachloride

1,2-Dichloropropane

Dibromochloromethane

1,1,2-Trichloroethane

Tetrachloroethene

Chlorobenzene

Trichlorofluoromethane

1,2-Dichloroethane

1,1,1-Trichloroethane

Bromodichloromethane trans-1,3-Dichloropropene cis-1,3-Dichloropropene

Bromoform

1,1,2,2-Tetrachloroethane

Benzene

Toluene

Ethylbenzene

Chloromethane

Bromomethane

Vinyl chloride

Chloroethane

1,1-Dichloroethene trans-1,2-Dichloroethene

Trichloroethene

1,2-Dichlorobenzene

Parameter Result Dilution Factor

ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg

Qualifier Units RL

Volatile Organics by GC/MS - Westborough Lab

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFAB MM 20240222

NFAB MM

L2409617

02/29/24

B-919 OWS 20240222 1200Client ID:

02/22/24 12:00Date Collected:

02/22/24Date Received:

NFABSample Location:

L2409617-02Lab ID:

Field Prep: Not Specified

Matrix: Oil Analytical Method:

Analytical Date:

Analyst:

1,8260D 02/29/24 13:55

LAC

Percent Solids: Results reported on an 'AS RECEIVED' basis.

MDL

70.

67.

60.

67.

94.

61.

80.

52.

76.

80.

68.

66.

69.

Sample Depth:

Methyl tert butyl ether p/m-Xylene o-Xylene cis-1,2-Dichloroethene

Styrene

Dichlorodifluoromethane

Acetone

Carbon disulfide

2-Butanone

4-Methyl-2-pentanone

2-Hexanone

Bromochloromethane

1,2-Dibromoethane

1,2-Dibromo-3-chloropropane

Isopropylbenzene

1,2,3-Trichlorobenzene

1,2,4-Trichlorobenzene

Methyl Acetate

Cyclohexane

1,4-Dioxane

Freon-113

Methyl cyclohexane

Parameter Result

Dilution Factor

ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg

Qualifier Units RL

Volatile Organics by GC/MS - Westborough Lab

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFAB MM 20240222

NFAB MM

L2409617

38000

1,2-Dichloroethane-d4

Toluene-d8

4-Bromofluorobenzene

Dibromofluoromethane

70-130

Acceptance Criteria

Surrogate % Recovery Qualifier

02/29/24

B-919 OWS 20240222 1200Client ID:

02/22/24 12:00Date Collected:

02/22/24Date Received:

NFABSample Location:

L2409617-02Lab ID:

Field Prep: Not Specified

MDL

71.

82.

97.

84.

94.

98.

52.

17000

Sample Depth:

L2408454

AFI Environmental

NFAB MM

NFAB MM 20240215

Client:

Project Name:

Project Number:

03/19/24

Eight Walkup Drive, Westborough, MA 01581-1019

Lab Number:

Report Date:

508-898-9220 (Fax) 508-898-9193 800-624-9220 - www.alphalab.com

8644 Buffalo Avenue

PO Box 4049

Joshua HeitzenraterATTN:

ANALYTICAL REPORT

Niagara Falls, NY 14304

(716) 940-2725Phone:

Serial_No:03192416:36

L2408454-01

L2408454-02

L2408454-03

L2408454-04

L2408454-05

Alpha Sample ID

B-919 OWS 20240215

B-919 OWS 20240215 1004

B-915 PWT 20240215

B-851 SM 20240215 0850

Client ID

NFAB

Sample Location

NFAB MM 20240215

NFAB MM

Project Name:

Project Number:

Lab Number:

Report Date:

L2408454 03/19/24

02/15/24 10:00

02/15/24 10:14

02/15/24 10:04

02/15/24 09:32

02/15/24 08:50

Collection Date/TimeMatrix Receive Date

SOLID

OIL

LIQUID

OIL

LIQUID

02/15/24

NFAB MM 20240215

NFAB MM

Project Name:

Project Number:

Lab Number:

Report Date:

L2408454

03/19/24

Case Narrative

The samples were received in accordance with the Chain of Custody and no significant deviations were encountered during the preparation or analysis unless otherwise noted. Sample Receipt, Container Information, and the Chain of Custody are located at the back of the report.

Results contained within this report relate only to the samples submitted under this Alpha Lab Number and meet NELAP requirements for all

NELAP accredited parameters unless otherwise noted in the following narrative. The data presented in this report is organized by parameter

(i.e. VOC, SVOC, etc.). Sample specific Quality Control data (i.e. Surrogate Spike Recovery) is reported at the end of the target analyte list for each individual sample, followed by the Laboratory Batch Quality Control at the end of each parameter. Tentatively Identified

Compounds (TICs), if requested, are reported for compounds identified to be present and are not part of the method/program Target

Compound List, even if only a subset of the TCL are being reported. If a sample was re-analyzed or re-extracted due to a required quality control corrective action and if both sets of data are reported, the Laboratory ID of the re-analysis or re-extraction is designated with an "R" or "RE", respectively.

When multiple Batch Quality Control elements are reported (e.g. more than one LCS), the associated samples for each element are noted in the grey shaded header line of each data table. Any Laboratory Batch, Sample Specific % recovery or RPD value that is outside the listed

Acceptance Criteria is bolded in the report. In reference to questions H (CAM) or 4 (RCP) when "NO" is checked, the performance criteria for CAM and RCP methods allow for some quality control failures to occur and still be within method compliance. In these instances, the specific failure is not narrated but noted in the associated QC Outlier Summary Report, located directly after the Case Narrative. QC information is also incorporated in the Data Usability Assessment table (Format 11) of our Data Merger tool, where it can be reviewed in conjunction with the sample result, associated regulatory criteria and any associated data usability implications.

Soil/sediments, solids and tissues are reported on a dry weight basis unless otherwise noted. Definitions of all data qualifiers and acronyms used in this report are provided in the Glossary located at the back of the report.

HOLD POLICY - For samples submitted on hold, Alpha's policy is to hold samples (with the exception of Air canisters) free of charge for 21 calendar days from the date the project is completed. After 21 calendar days, we will dispose of all samples submitted including those put on hold unless you have contacted your Alpha Project Manager and made arrangements for Alpha to continue to hold the samples. Air canisters will be disposed after 3 business days from the date the project is completed.

Please contact Project Management at 800-624-9220 with any questions.

Case Narrative (continued)

NFAB MM

Project Name:

Project Number:

Lab Number:

Report Date:

L2408454

03/19/24

Report Revision

March 19, 2024: This report includes the results of the following analyses:

L2408454-01: Semivolatile Organics

Report Submission

All non-detect (ND) or estimated concentrations (J-qualified) have been quantitated to the limit noted in the

MDL column.

The analyses of Extractable Organic Halides and Total Halogens were subcontracted. A copy of the laboratory report is included as an addendum. Please note: This data is only available in PDF format and is not available on Data Merger.

Sample Receipt

L2408454-04: The sample was received above the appropriate pH for the Total Metals analysis. The laboratory added additional HNO3; however, the pH would not adjust into the proper range.

L2408454-03: Headspace was noted in the sample containers submitted for Volatile Organics. The analysis was cancelled at the client's request.

Volatile Organics

L2408454-01: Any reported concentrations that are below 200 ug/kg may be biased low due to the sample not being collected according to 5035-L/5035A-L low-level specifications.

L2408454-01: The surrogate recoveries are outside the acceptance criteria for 4-bromofluorobenzene

(1334%) and dibromofluoromethane (139%); however, the sample was not re-analyzed due to coelution with an obvious interference. A copy of the chromatogram is included as an attachment to this report.

L2408454-04D: The sample has elevated detection limits due to the dilution required by the elevated concentrations of non-target compounds in the sample.

L2408454-04D: The surrogate recovery was below the acceptance criteria for 4-bromofluorobenzene (0%);

Case Narrative (continued)

NFAB MM

Project Name:

Project Number:

Lab Number:

Report Date:

L2408454

03/19/24 however, re-analysis achieved similar results: 4-bromofluorobenzene (37%). The results of both analyses are reported; however, all associated compounds are considered to have a potentially low bias.

Semivolatile Organics

L2408454-01D: The sample was extracted with the method required holding time exceeded. The sample has elevated detection limits due to the dilution required by the sample matrix.

The WG1897016-2/-3 LCS/LCSD recoveries, associated with L2408454-01D, are below the acceptance criteria for benzoic acid (0%/0%); however, it has been identified as a "difficult" analyte. The results of the associated sample are reported.

Total Metals

L2408454-05: The sample has elevated detection limits for all elements, with the exception of mercury, due to the dilution required by the sample matrix and due to the prep dilution required by the sample matrix.

L2408454-05: The sample has an elevated detection limit for mercury due to the prep dilution required by the sample matrix.

The WG1887743-1 Method Blank, associated with L2408454-02 and -04, has a concentration above the reporting limit for arsenic. Since the associated sample concentrations are non-detect to the RL for this target analyte, no corrective action is required.

Flash Point

WG1886668: A Laboratory Duplicate could not be performed due to insufficient sample volume available for analysis.

I, the undersigned, attest under the pains and penalties of perjury that, to the best of my knowledge and belief and based upon my personal inquiry of those responsible for providing the information contained in this analytical report, such information is accurate and complete. This certificate of analysis is not complete unless this page accompanies any and all pages of this report.

Authorized Signature:

Title: Technical Director/Representative Date: 03/19/24

ORGANICS

VOLATILES

1,1-Dichloroethane

Chloroform

Carbon tetrachloride

1,2-Dichloropropane

Dibromochloromethane

1,1,2-Trichloroethane

Tetrachloroethene

Chlorobenzene

Trichlorofluoromethane

1,2-Dichloroethane

1,1,1-Trichloroethane

Bromodichloromethane trans-1,3-Dichloropropene cis-1,3-Dichloropropene

Bromoform

1,1,2,2-Tetrachloroethane

Benzene

Toluene

Ethylbenzene

Chloromethane

Bromomethane

Vinyl chloride

Chloroethane

1,1-Dichloroethene trans-1,2-Dichloroethene

Trichloroethene

1,2-Dichlorobenzene

Parameter Result

Dilution Factor

3.4

ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg

Qualifier Units RL

Volatile Organics by GC/MS - Westborough Lab

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFAB MM 20240215

NFAB MM

L2408454

5.3

03/19/24

B-919 OWS 20240215Client ID:

02/15/24 10:00Date Collected:

02/15/24Date Received:

NFABSample Location:

L2408454-01Lab ID:

Field Prep: Not Specified

Matrix: Solid Analytical Method:

Analytical Date:

Analyst:

1,8260D 02/28/24 12:15

LAC

9%Percent Solids:

MDL

24.

1.5

2.4

1.3

1.5

2.8

2.1

1.3

7.4

2.7

1.8

1.2

2.9

1.7

2.6

1.8

5.8

1.5

9.9

6.2

3.6

4.8

2.5

1.4

1.5

Sample Depth:

Methyl tert butyl ether p/m-Xylene o-Xylene cis-1,2-Dichloroethene

Styrene

Dichlorodifluoromethane

Acetone

Carbon disulfide

2-Butanone

4-Methyl-2-pentanone

2-Hexanone

Bromochloromethane

1,2-Dibromoethane

1,2-Dibromo-3-chloropropane

Isopropylbenzene

1,2,3-Trichlorobenzene

1,2,4-Trichlorobenzene

Methyl Acetate

Cyclohexane

1,4-Dioxane

Freon-113

Methyl cyclohexane

Parameter Result

Dilution Factor

ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg

Qualifier Units RL

Volatile Organics by GC/MS - Westborough Lab

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFAB MM 20240215

NFAB MM

L2408454

1,2-Dichloroethane-d4

Toluene-d8

4-Bromofluorobenzene

Dibromofluoromethane

70-130

Acceptance Criteria

Surrogate % Recovery Qualifier

03/19/24

B-919 OWS 20240215Client ID:

02/15/24 10:00Date Collected:

02/15/24Date Received:

NFABSample Location:

L2408454-01Lab ID:

Field Prep: Not Specified

MDL

1.6

1.8

2.1

5.9

3.1

1.8

2.1

9.7

51.

48.

24.

14.

12.

2.2

3.0

10.

1.2

3.4

2.9

10.

5.8

7.4

6.4

Sample Depth:

SEMIVOLATILES

Acenaphthene

1,2,4-Trichlorobenzene

Hexachlorobenzene

Bis(2-chloroethyl)ether

2-Chloronaphthalene

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1,4-Dichlorobenzene

3,3'-Dichlorobenzidine

2,4-Dinitrotoluene

2,6-Dinitrotoluene

Fluoranthene

4-Chlorophenyl phenyl ether

4-Bromophenyl phenyl ether

Bis(2-chloroisopropyl)ether

Bis(2-chloroethoxy)methane

Hexachlorobutadiene

Hexachlorocyclopentadiene

Hexachloroethane

Isophorone

Naphthalene

Nitrobenzene

NDPA/DPA

n-Nitrosodi-n-propylamine

Bis(2-ethylhexyl)phthalate

Butyl benzyl phthalate

Di-n-butylphthalate

Di-n-octylphthalate

Parameter Result

Dilution Factor

35000

ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg

Qualifier Units RL

Semivolatile Organics by GC/MS - Westborough Lab

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFAB MM 20240215

NFAB MM

L2408454

15000

19000

11000

17000

19000

11000

19000

22000

20000

19000

54000

15000

17000

19000

17000

15000

19000

03/19/24

B-919 OWS 20240215Client ID:

02/15/24 10:00Date Collected:

02/15/24Date Received:

NFABSample Location:

L2408454-01Lab ID:

Field Prep: Not Specified

Matrix: Solid Extraction Method:

Analytical Method:

Analytical Date:

Analyst:

1,8270E 03/19/24 13:35

LJG

EPA 3540C

Extraction Date: 03/16/24 08:42

9%Percent Solids:

MDL

17000

Sample Depth:

Diethyl phthalate

Dimethyl phthalate

Benzo(a)anthracene

Benzo(a)pyrene

Benzo(b)fluoranthene

Benzo(k)fluoranthene

Chrysene

Acenaphthylene

Anthracene

Benzo(ghi)perylene

Fluorene

Phenanthrene

Dibenzo(a,h)anthracene

Indeno(1,2,3-cd)pyrene

Pyrene

Biphenyl

4-Chloroaniline

2-Nitroaniline

3-Nitroaniline

4-Nitroaniline

Dibenzofuran

2-Methylnaphthalene

1,2,4,5-Tetrachlorobenzene

Acetophenone

2,4,6-Trichlorophenol p-Chloro-m-cresol

2-Chlorophenol

2,4-Dichlorophenol

2,4-Dimethylphenol

2-Nitrophenol

4-Nitrophenol

2,4-Dinitrophenol

4,6-Dinitro-o-cresol

Pentachlorophenol

Phenol

2-Methylphenol

3-Methylphenol/4-Methylphenol

Parameter Result

Dilution Factor

ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg

Qualifier Units RL

Semivolatile Organics by GC/MS - Westborough Lab

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFAB MM 20240215

NFAB MM

L2408454

19000

11000

15000

11000

15000

11000

15000

19000

11000

15000

11000

43000

19000

22000

19000

11000

19000

17000

19000

40000

26000

90000

49000

15000

19000

27000

03/19/24

B-919 OWS 20240215Client ID:

02/15/24 10:00Date Collected:

02/15/24Date Received:

NFABSample Location:

L2408454-01Lab ID:

Field Prep: Not Specified

MDL

Sample Depth:

2,4,5-Trichlorophenol

Benzoic Acid

Benzyl Alcohol

Carbazole

1,4-Dioxane

Parameter Result Dilution Factor

ug/kg ug/kg ug/kg ug/kg ug/kg

Qualifier Units RL

Semivolatile Organics by GC/MS - Westborough Lab

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFAB MM 20240215

NFAB MM

L2408454

19000

61000

19000

2-Fluorophenol

Phenol-d6

Nitrobenzene-d5

2-Fluorobiphenyl

2,4,6-Tribromophenol

4-Terphenyl-d14

25-120

10-120

23-120

30-120

10-136

18-120

Acceptance Criteria

Surrogate % Recovery Qualifier

03/19/24

B-919 OWS 20240215Client ID:

02/15/24 10:00Date Collected:

02/15/24Date Received:

NFABSample Location:

L2408454-01Lab ID:

Field Prep: Not Specified

MDL

19000

Sample Depth:

Acenaphthene

Hexachlorobenzene

Bis(2-chloroethyl)ether

2-Chloronaphthalene

3,3'-Dichlorobenzidine

2,4-Dinitrotoluene

2,6-Dinitrotoluene

Fluoranthene

4-Chlorophenyl phenyl ether

4-Bromophenyl phenyl ether

Bis(2-chloroisopropyl)ether

Bis(2-chloroethoxy)methane

Hexachlorobutadiene

Hexachlorocyclopentadiene

Hexachloroethane

Isophorone

Naphthalene

Nitrobenzene

NDPA/DPA

n-Nitrosodi-n-propylamine

Bis(2-ethylhexyl)phthalate

Butyl benzyl phthalate

Di-n-butylphthalate

Di-n-octylphthalate

Diethyl phthalate

Dimethyl phthalate

Benzo(a)anthracene

Benzo(a)pyrene

Parameter Result Dilution Factor

ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg

Qualifier Units RL

Semivolatile Organics by GC/MS - Westborough Lab

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFAB MM 20240215

NFAB MM

L2408454

27000

20000

31000

34000

20000

34000

41000

37000

34000

98000

27000

31000

34000

31000

27000

34000

20000

27000

03/19/24

B-919 OWS 20240215Client ID:

02/15/24 10:14Date Collected:

02/15/24Date Received:

NFABSample Location:

L2408454-02Lab ID:

Field Prep: Not Specified

Matrix: Oil Extraction Method:

Analytical Method:

Analytical Date:

Analyst:

1,8270E 02/26/24 05:18

HNY

EPA 3580A

Extraction Date: 02/24/24 14:21

Percent Solids: Results reported on an 'AS RECEIVED' basis.

MDL

31000

12000

Sample Depth:

Benzo(b)fluoranthene

Benzo(k)fluoranthene

Chrysene

Acenaphthylene

Anthracene

Benzo(ghi)perylene

Fluorene

Phenanthrene

Dibenzo(a,h)anthracene

Indeno(1,2,3-cd)pyrene

Pyrene

Biphenyl

4-Chloroaniline

2-Nitroaniline

3-Nitroaniline

4-Nitroaniline

Dibenzofuran

2-Methylnaphthalene

1,2,4,5-Tetrachlorobenzene

Acetophenone

2,4,6-Trichlorophenol p-Chloro-m-cresol

2-Chlorophenol

2,4-Dichlorophenol

2,4-Dimethylphenol

2-Nitrophenol

4-Nitrophenol

2,4-Dinitrophenol

4,6-Dinitro-o-cresol

Pentachlorophenol

Phenol

2-Methylphenol

3-Methylphenol/4-Methylphenol

2,4,5-Trichlorophenol

Carbazole

Atrazine

Benzaldehyde

Parameter Result Dilution Factor

Qualifier Units RL

Semivolatile Organics by GC/MS - Westborough Lab

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFAB MM 20240215

NFAB MM

L2408454

20000

27000

20000

27000

34000

20000

27000

20000

78000

34000

41000

34000

20000

34000

31000

34000

74000

48000

160000

89000

27000

34000

49000

34000

27000

45000

03/19/24

B-919 OWS 20240215Client ID:

02/15/24 10:14Date Collected:

02/15/24Date Received:

NFABSample Location:

L2408454-02Lab ID:

Field Prep: Not Specified

MDL

14000

11000

13000

14000

16000

12000

Sample Depth:

Caprolactam

2,3,4,6-Tetrachlorophenol

Parameter Result Dilution Factor

ug/kg ug/kg

Qualifier Units RL

Semivolatile Organics by GC/MS - Westborough Lab

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFAB MM 20240215

NFAB MM

L2408454

34000

2-Fluorophenol

Phenol-d6

Nitrobenzene-d5

2-Fluorobiphenyl

2,4,6-Tribromophenol

4-Terphenyl-d14

25-120

10-120

23-120

30-120

10-136

18-120

Acceptance CriteriaSurrogate % Recovery Qualifier

03/19/24

B-919 OWS 20240215Client ID:

02/15/24 10:14Date Collected:

02/15/24Date Received:

NFABSample Location:

L2408454-02Lab ID:

Field Prep: Not Specified

MDL

10000

Sample Depth:

PCBS

Aroclor 1016

Aroclor 1221

Aroclor 1232

Aroclor 1242

Aroclor 1248

Aroclor 1254

Aroclor 1260

Aroclor 1262

Aroclor 1268

PCBs, Total

Parameter Result Dilution Factor

ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg

Qualifier Units RL

Polychlorinated Biphenyls by GC - Westborough Lab

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFAB MM 20240215

NFAB MM

L2408454

2,4,5,6-Tetrachloro-m-xylene

Decachlorobiphenyl

2,4,5,6-Tetrachloro-m-xylene

Decachlorobiphenyl

30-150

Acceptance Criteria

Surrogate % Recovery Qualifier Column

03/19/24

B-919 OWS 20240215Client ID:

02/15/24 10:00Date Collected:

02/15/24Date Received:

NFABSample Location:

L2408454-01Lab ID:

Field Prep: Not Specified

Matrix: Solid Extraction Method:

Cleanup Method:

Analytical Method:

Analytical Date:

Analyst:

1,8082A 02/21/24 14:24

RMP

EPA 3540C

EPA 3665A

Extraction Date: 02/18/24 10:40

Cleanup Date: 02/20/24 Cleanup Method: EPA 3660B Cleanup Date: 02/21/24

9%Percent Solids:

MDL

99.6

112.

238.

151.

168.

123.

207.

142.

116.

99.6

Column

Sample Depth:

Aroclor 1016

Aroclor 1221

Aroclor 1232

Aroclor 1242

Aroclor 1248

Aroclor 1254

Aroclor 1260

Aroclor 1262

Aroclor 1268

PCBs, Total

Parameter Result Dilution Factor

mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg

Qualifier Units RL

Polychlorinated Biphenyls by GC - Westborough Lab

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFAB MM 20240215

NFAB MM

L2408454

4.06

2,4,5,6-Tetrachloro-m-xylene

Decachlorobiphenyl

2,4,5,6-Tetrachloro-m-xylene

Decachlorobiphenyl

30-150

Acceptance Criteria

Surrogate % Recovery Qualifier Column

03/19/24

B-919 OWS 20240215Client ID:

02/15/24 10:14Date Collected:

02/15/24Date Received:

NFABSample Location:

L2408454-02Lab ID:

Field Prep: Not Specified

Matrix: Oil Extraction Method:

Cleanup Method:

Analytical Method:

Analytical Date:

Analyst:

1,8082A 02/18/24 18:54

MEO

EPA 3580A

EPA 3665A

Extraction Date: 02/18/24 08:04

Cleanup Date: 02/18/24 Cleanup Method: EPA 3660B Cleanup Date: 02/18/24

Percent Solids: Results reported on an 'AS RECEIVED' basis.

MDL

0.361

0.407

0.862

0.548

0.610

0.445

0.751

0.516

0.421

0.361

Column

Sample Depth:

METALS

Project Name:

Project Number:

Lab Number:

Report Date:

NFAB MM 20240215

NFAB MM

L2408454

03/19/24

SAMPLE RESULTS

B-919 OWS 20240215Client ID:

02/15/24 10:00Date Collected:

02/15/24Date Received:

Matrix: Solid

NFABSample Location:

L2408454-01Lab ID:

Field Prep: Not Specified

Parameter Result Dilution FactorQualifier Units RL

Date Analyzed

Analytical Method Analyst

Date Prepared

TCLP Metals by EPA 1311 - Mansfield Lab

Arsenic, TCLP

Barium, TCLP

Cadmium, TCLP

Chromium, TCLP

Lead, TCLP

Mercury, TCLP

Selenium, TCLP

Silver, TCLP

0.314

0.0165

0.0900

mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l

1.00

0.500

0.100

0.200

0.500

0.0010

0.500

0.100

02/21/24 20:55

02/21/24 21:04

02/21/24 20:55

1,6010D

1,7470A

1,6010D

JTS

GMG

JTS

02/21/24 15:30

02/21/24 12:50

02/21/24 15:30

EPA 3015

EPA 7470A

EPA 3015

Prep Method

02/17/24 04:24TCLP/SPLP Ext. Date:

Percent Solids: 9%

MDL

0.0190

0.0210

0.0100

0.0210

0.0270

0.0005

0.0350

0.0280

Sample Depth:

Project Name:

Project Number:

Lab Number:

Report Date:

NFAB MM 20240215

NFAB MM

L2408454

03/19/24

SAMPLE RESULTS

B-919 OWS 20240215Client ID:

02/15/24 10:14Date Collected:

02/15/24Date Received:

Matrix: Oil

NFABSample Location:

L2408454-02Lab ID:

Field Prep: Not Specified

Parameter Result Dilution FactorQualifier Units RL

Date Analyzed

Analytical Method Analyst

Date Prepared

Total Metals - Mansfield Lab

Arsenic, Total

Barium, Total

Cadmium, Total

Chromium, Total

Lead, Total

Mercury, Total

Selenium, Total

Silver, Total

mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg

1.34

6.72

0.073

2.69

0.672

02/23/24 20:35

02/26/24 12:51

02/23/24 20:35

1,6010D

1,7471B

1,6010D

DMC

MJR

DMC

02/22/24 22:20

02/26/24 11:02

02/22/24 22:20

EPA 3050B

EPA 7471B

EPA 3050B

Prep Method

Percent Solids: Results are reported on an 'AS RECEIVED' basis.

MDL

0.280

0.234

0.132

0.129

0.360

0.048

0.347

0.380

Sample Depth:

INORGANICS

MISCELLANEOUS

B-919 OWS 20240215Client ID:

02/15/24 10:00Date Collected:

02/15/24Date Received:

Parameter Result Dilution Factor

Matrix: Solid

NFABSample Location:

L2408454-01Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFAB MM 20240215

NFAB MM

L2408454

Field Prep:

Date Analyzed

Analytical Method Analyst

Not Specified

General Chemistry - Westborough Lab Solids, Total pH (H)

Flash Point

8.77

7.42

>150

deg F

0.100

02/16/24 12:05

02/17/24 05:10

02/19/24 09:45

121,2540G

1,9045D

1,1010A

ROI

CAR

MRS

Date Prepared

03/19/24

MDL

Sample Depth:

B-919 OWS 20240215Client ID:

02/15/24 10:14Date Collected:

02/15/24Date Received:

Parameter Result Dilution Factor

Matrix: Oil

NFABSample Location:

L2408454-02Lab ID:

Qualifier Units RL

SAMPLE RESULTS

Project Name:

Project Number:

Lab Number:

Report Date:

NFAB MM 20240215

NFAB MM

L2408454

Field Prep:

Date Analyzed

Analytical Method Analyst

Not Specified

General Chemistry - Westborough Lab pH (H)

Flash Point

6.41

>150

deg F

02/17/24 05:10

02/19/24 09:45

1,9045D

1,1010A

CAR

MRS

Date Prepared

03/19/24

MDL

Sample Depth:

Percent Solids: Results reported on an 'AS RECEIVED' basis.

Sterling Analytical, Inc.

15 Agawam Avenue West Springfield, MA 01089 Phone (413) 214-6541 Fax (413) 214-6842

February 27, 2024

C. Fox

Analysis of Solid & Oil Samples

Enclosed are Report No(s): 82384, 82385

Blank = <50mg/kg ICV 50 = 51.4mg/kg CCV 50 = 49.4mg/kg

Samples Analyzed

Customer

Sample Description

Laboratory Supervisor Dale Percoski customerservice@sterlinganalytical.com eMail

Report Date

Thank you for your business

Date

Alpha Analytical Lab

Contact

ALL the information contained in this report has been reviewed for accuracy and checked against all quality control requirements outlined in each applicable method.

This report may not be reproduced, except in full, without written approval from Sterling Analytical, Inc.

Visit our website: www.sterlinganalytical.com

2/27/2024 Dale Percoski, Laboratory Supervisor

24-1480Work OrderSample AnalysisVisit our website: www.sterlinganalytical.com

50.0Extractable Organic Halides Less Than mg/kg SW846 902350.00 02/21/24 sjr Parameter Results MethodRDL Analyzed/Time

82384 2/15/24L2408454-01 B-919 OWS Alpha Analytical Lab 2/20/24 Source Taken/Time ReceivedSample Description

10:00

Tech

50.0Total Halogens Less Than mg/kg SW846 9076(1)50.00 02/21/24 sjr Parameter Results MethodRDL Analyzed/Time

82385 2/15/24L2408454-02 B-919 OWS Alpha Analytical Lab 2/20/24 Source Taken/Time ReceivedSample Description

10:00

Tech

2Page of 2Sterling Analytical, Inc.(1) MA & CT do not certify this parameter

File details come from the government source that posted it. Updated May 30, 2024.