Analytical Final Report.pdf

ANALYTICAL REPORT

Job Number: 400-56023-1

Job Description: HAZ WASTE

For:

1SO CES

415 Independence Road Building 90053

Hurlburt Field, FL 32544

Attention: Mr. Randy Trent

Approved for release.

Cheyenne Whitmire Project Manager II

6/2/2011 3:24 PM

Cheyenne Whitmire Project Manager II cheyenne.whitmire@testamericainc.com 06/02/2011

The test results in this report meet all NELAP requirements for accredited parameters, unless otherwise noted, and relate only to the referenced samples. Pursuant to NELAP, this report may not be reproduced, except in full, without written approval from the laboratory. For questions please contact the Project Manager at the e-mail address listed on this page, or the telephone number at the bottom of the page. TestAmerica Pensacola Certifications and Approvals:

Alabama (40150), Arizona (AZ0710), Arkansas (88-0689), Florida (E81010), Illinois (200041), Iowa (367), Kansas (E- 10253), Kentucky UST (53), Louisiana (30748), Maryland (233), Massachusetts (M-FL094), Michigan (9912), New Hampshire (250510), New Jersey (FL006), North Carolina (314), Oklahoma (9810), Pennsylvania (68-00467), Rhode Island (LAO00307), South Carolina (96026), Tennessee (TN02907), Texas (T104704286-10-2), Virginia (00008), Washington (C2043), West Virginia (136), USDA Foreign Soil Permit (P330-08-00006).

TestAmerica Laboratories, Inc.

TestAmerica Pensacola 3355 McLemore Drive, Pensacola, FL 32514

Tel (850) 474-1001 Fax (850) 478-2671 www.testamericainc.com

06/02/2011Page 1 of 14 mailto:cheyenne.whitmire@testamericainc.com http://www.testamericainc.com http://

METHOD SUMMARY

Client: 1SO CES Job Number: 400-56023-1

Preparation MethodMethodLab LocationDescription

Matrix: Solid

Metals (ICP) TAL PEN SW846 6010B

TCLP Extraction TAL PEN SW846 1311

Preparation, Total Metals TAL PEN SW846 3010A

Mercury (CVAA) TAL PEN SW846 7470A

TCLP Extraction TAL PEN SW846 1311

Preparation, Mercury TAL PEN SW846 7470A

Lab References:

TAL PEN = TestAmerica Pensacola

Method References:

SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.

TestAmerica Pensacola 06/02/2011Page 2 of 14

METHOD / ANALYST SUMMARY

Method Analyst Analyst ID

St. Pere, Gary GSSW846 6010B

Cortez, Maria MCSW846 7470A

TestAmerica Pensacola

06/02/2011Page 3 of 14

SAMPLE SUMMARY

Client Sample IDLab Sample ID Client Matrix Sampled Received

Date/Time Date/Time

400-56023-1 441-11 PAINT CHIP PED

BRIDGE

Solid 05/11/2011 0730 05/18/2011 1238

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SAMPLE RESULTS

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Analytical Data

Client Sample ID:

Lab Sample ID:

441-11 PAINT CHIP PED BRIDGE

Client Matrix:

400-56023-1

Solid

Date Sampled: 05/11/2011 0730

Date Received: 05/18/2011 1238

6010B Metals (ICP)-TCLP

6010B Instrument ID:

Lab File ID: N/A

Dilution: 5.0 Initial Weight/Volume: 50 mL

05/25/2011 1509 Final Weight/Volume: 50 mL

05/24/2011 1639

3010A

6500 ICP Duo

Analysis Date:

Prep Date:

Analysis Batch: 400-131857

400-131742

400-131715

Prep Batch:

Analysis Method:

Prep Method:

Leach Batch:

05/23/2011 1605Leach Date:

Analyte DryWt Corrected: N Result (mg/L) Qualifier MDL PQL

0.010 U 0.0250.010Silver

0.020 U 0.0250.020Arsenic

0.050 U 5.00.050Barium

0.0050 U 0.0250.0050Cadmium

0.010 U 0.0250.010Chromium

0.010 U 0.0250.010Lead

0.020 U 0.0500.020Selenium

7470A Mercury (CVAA)-TCLP

7470A Instrument ID:

Lab File ID: HW131875.PRN

Dilution: 1.0 Initial Weight/Volume: 5 mL

05/26/2011 1352 Final Weight/Volume: 40 mL

05/26/2011 0820

7470A

HYDRA AA

Analysis Date:

Prep Date:

Analysis Batch: 400-131933

400-131880

400-131715

Prep Batch:

Analysis Method:

Prep Method:

Leach Batch:

05/23/2011 1605Leach Date:

Analyte DryWt Corrected: N Result (mg/L) Qualifier MDL PQL

0.00056 U 0.00160.00056Mercury

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DATA REPORTING QUALIFIERS

Lab Section Qualifier Description

Metals

Indicates that the compound was analyzed for but not detected.

U

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QUALITY CONTROL RESULTS

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Quality Control Results

QC Association Summary

Lab Sample ID Client Sample ID Client Matrix Method Prep Batch

Report

Basis

Metals

Prep Batch: 400-131715

TCLP SPLPE Leachate Blank Solid 1311LB 400-131715/1-D P

TCLP SPLPE Leachate Blank Solid 1311LB 400-131715/1-F P

Solid441-11 PAINT CHIP PED BRIDGE 1311400-56023-1 P

Matrix Spike Solid 1311400-56023-1MS P

Matrix Spike Duplicate Solid 1311400-56023-1MSD P

Matrix Spike Solid 1311400-56150-A-1-D MS P

Matrix Spike Duplicate Solid 1311400-56150-A-1-E MSD P

Prep Batch: 400-131742

Lab Control Sample Water 3010ALCS 400-131742/17-A T

TCLP SPLPE Leachate Blank Solid 400-1317153010ALB 400-131715/1-D P

Solid 400-131715441-11 PAINT CHIP PED BRIDGE 3010A400-56023-1 P

Matrix Spike Solid 400-1317153010A400-56023-1MS P

Matrix Spike Duplicate Solid 400-1317153010A400-56023-1MSD P

Analysis Batch:400-131857

TCLP SPLPE Leachate Blank Solid 400-1317426010BLB 400-131715/1-D P

Lab Control Sample Water 400-1317426010BLCS 400-131742/17-A T

Solid 400-131742441-11 PAINT CHIP PED BRIDGE 6010B400-56023-1 P

Matrix Spike Solid 400-1317426010B400-56023-1MS P

Matrix Spike Duplicate Solid 400-1317426010B400-56023-1MSD P

Prep Batch: 400-131880

Lab Control Sample Water 7470ALCS 400-131880/15-A T

TCLP SPLPE Leachate Blank Solid 400-1317157470ALB 400-131715/1-F P

Solid 400-131715441-11 PAINT CHIP PED BRIDGE 7470A400-56023-1 P

Matrix Spike Solid 400-1317157470A400-56150-A-1-D MS P

Matrix Spike Duplicate Solid 400-1317157470A400-56150-A-1-E MSD P

Analysis Batch:400-131933

TCLP SPLPE Leachate Blank Solid 400-1318807470ALB 400-131715/1-F P

Lab Control Sample Water 400-1318807470ALCS 400-131880/15-A T

Solid 400-131880441-11 PAINT CHIP PED BRIDGE 7470A400-56023-1 P

Matrix Spike Solid 400-1318807470A400-56150-A-1-D MS P

Matrix Spike Duplicate Solid 400-1318807470A400-56150-A-1-E MSD P

Report Basis

P = TCLP

T = Total

06/02/2011Page 9 of 14

Job Number: 400-56023-1Client: 1SO CES

SolidClient Matrix:

5.0Dilution:

Lab Sample ID:

05/25/2011 1502

TCLP SPLPE Leachate Blank - Batch: 400-131742

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

05/24/2011 1639

05/23/2011 1605

50 mL

50 mLUnits: mg/L

Method: 6010B

Preparation: 3010A

TCLP

6500 ICP DuoLB 400-131715/1-D

Analysis Date:

Prep Date:

Leach Date:

Analysis Batch:

Prep Batch:

Leach Batch:

400-131857

400-131742

400-131715

N/A

Analyte Result Qual MDL PQL

0.010 U 0.0250.010Silver

0.020 U 0.0250.020Arsenic

0.050 U 5.00.050Barium

0.0050 U 0.0250.0050Cadmium

0.010 U 0.0250.010Chromium

0.010 U 0.0250.010Lead

0.020 U 0.0500.020Selenium

Water

5.0

Lab Control Sample - Batch: 400-131742

Client Matrix:

Lab Sample ID:

Dilution:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

50 mL

50 mLUnits: mg/L

Method: 6010B

Preparation: 3010A

6500 ICP DuoLCS 400-131742/17-A

Analysis Date: 05/25/2011 1506

Prep Date:

Leach Date:

05/24/2011 1639

Analysis Batch:

Prep Batch:

Leach Batch:

400-131857

400-131742 N/A

N/A

N/A

Analyte QualLimit% Rec.ResultSpike Amount

0.500 0.525 105 80 - 120Silver

1.00 1.03 103 80 - 120Arsenic

6.00 6.40 107 80 - 120Barium

0.500 0.526 105 80 - 120Cadmium

1.00 1.06 106 80 - 120Chromium

1.00 1.01 101 80 - 120Lead

1.00 1.04 104 80 - 120Selenium

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Dilution:

Dilution:

05/25/2011 1525

05/25/2011 1529

Solid

Matrix Spike/

Matrix Spike Duplicate Recovery Report - Batch: 400-131742

5.0

5.0

Client Matrix:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Client Matrix: Solid

05/24/2011 1639

05/24/2011 1639

05/23/2011 1605

05/23/2011 1605

50 mL

50 mL

50 mL

50 mL

Method: 6010B

Preparation: 3010A

TCLP

N/A

N/A

6500 ICP Duo

6500 ICP Duo

400-56023-1

400-56023-1

MS Lab Sample ID:

MSD Lab Sample ID:

Analysis Date:

Prep Date:

Leach Date:

Analysis Date:

Prep Date:

Leach Date:

Analysis Batch:

Prep Batch:

Leach Batch:

400-131857

400-131742

400-131715

Analysis Batch:

Prep Batch:

Leach Batch:

400-131857

400-131742

400-131715

Analyte RPD LimitRPDLimit

% Rec.

MS MSD MS Qual MSD Qual

106 107 75 - 125 1 20Silver

104 104 75 - 125 0 20Arsenic

104 105 75 - 125 1 20Barium

105 105 75 - 125 0 20Cadmium

104 104 75 - 125 0 20Chromium

103 104 75 - 125 1 20Lead

103 103 75 - 125 0 20Selenium

TestAmerica Pensacola 06/02/2011Page 11 of 14

SolidClient Matrix:

1.0Dilution:

Lab Sample ID:

05/26/2011 1314

TCLP SPLPE Leachate Blank - Batch: 400-131880

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

05/26/2011 0820

05/23/2011 1605

HW131875.PRN

5 mL

40 mLUnits: mg/L

Method: 7470A

Preparation: 7470A

TCLP

HYDRA AALB 400-131715/1-F

Analysis Date:

Prep Date:

Leach Date:

Analysis Batch:

Prep Batch:

Leach Batch:

400-131933

400-131880

400-131715

Analyte Result Qual MDL PQL

0.00056 U 0.00160.00056Mercury

Water

1.0

Lab Control Sample - Batch: 400-131880

Client Matrix:

Lab Sample ID:

Dilution:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

HW131875.PRN

5 mL

40 mLUnits: mg/L

Method: 7470A

Preparation: 7470A

HYDRA AALCS 400-131880/15-A

Analysis Date: 05/26/2011 1316

Prep Date:

Leach Date:

05/26/2011 0820

Analysis Batch:

Prep Batch:

Leach Batch:

400-131933

400-131880

N/A

N/A

Analyte QualLimit% Rec.ResultSpike Amount

0.00800 0.00904 113 80 - 120Mercury

Dilution:

Dilution:

05/26/2011 1332

05/26/2011 1334

Solid

Matrix Spike/

Matrix Spike Duplicate Recovery Report - Batch: 400-131880

1.0

1.0

Client Matrix:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Client Matrix: Solid

05/26/2011 0820

05/26/2011 0820

05/23/2011 1605

05/23/2011 1605

HW131875.PRN

5 mL

40 mL

HW131875.PRN

5 mL

40 mL

Method: 7470A

Preparation: 7470A

TCLP

HYDRA AA

HYDRA AA

400-56150-A-1-D MS

400-56150-A-1-E MSD

MS Lab Sample ID:

MSD Lab Sample ID:

Analysis Date:

Prep Date:

Leach Date:

Analysis Date:

Prep Date:

Leach Date:

Analysis Batch:

Prep Batch:

Leach Batch:

400-131933

400-131880

400-131715

Analysis Batch:

Prep Batch:

Leach Batch:

400-131933

400-131880

400-131715

Analyte RPD LimitRPDLimit

% Rec.

MS MSD MS Qual MSD Qual

95 97 85 - 115 2 20Mercury

TestAmerica Pensacola 06/02/2011Page 12 of 14

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Login Sample Receipt Checklist

Login Number: 56023

Question Answer Comment

Creator: Hor, Koma

List Source: TestAmerica Pensacola

List Number: 1

N/ARadioactivity either was not measured or, if measured, is at or below background

N/AThe cooler's custody seal, if present, is intact.

TrueThe cooler or samples do not appear to have been compromised or tampered with.

N/ASamples were received on ice.

TrueCooler Temperature is acceptable.

N/ACooler Temperature is recorded.

TrueCOC is present.

TrueCOC is filled out in ink and legible.

TrueCOC is filled out with all pertinent information.

TrueIs the Field Sampler's name present on COC?

TrueThere are no discrepancies between the sample IDs on the containers and the COC.

TrueSamples are received within Holding Time.

TrueSample containers have legible labels.

TrueContainers are not broken or leaking.

TrueSample collection date/times are provided.

TrueAppropriate sample containers are used.

TrueSample bottles are completely filled.

TrueSample Preservation Verified.

TrueThere is sufficient vol. for all requested analyses, incl. any requested

MS/MSDs

N/AVOA sample vials do not have headspace or bubble is <6mm (1/4") in diameter.

TrueMultiphasic samples are not present.

TrueSamples do not require splitting or compositing.

TrueResidual Chlorine Checked.

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