B.08.02_Attachment K_J157715-1 Std_Tal_L4 Final Report.pdf
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- Solicitation number
- W912DS24B0005
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This document appears to be the Final Report for Contract J157715-1 Standard Talus L4, which is related to the federal contract opportunity for the Maintenance Dredging of Mattituck Harbor, New York, Federal Navigation Channel.
The key details are as follows:
The federal contract opportunity is for the Maintenance Dredging of the Mattituck Harbor, New York Federal Navigation Project. It is a 100% Small Business Set-Aside with a NAICS code of 237990 and a size standard of $37,000,000.00. The project magnitude range is between $1,000,000 to $5,000,000.00. The Contract Specialist is Jo Ann McCue with the email jo.a.mccue@usace.army.mil. The solicitation number is W912DS24B0005 and the agency is the Department of the Army Corps of Engineers Engineering District New York.
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ANALYTICAL REPORT
PREPARED FOR
Attn: Carole Peven McCarthy
Battelle 141 Longwater Dr
Suite 202 Norwell MA 02061
Generated 6/29/2023 1:41 PM
JOB DESCRIPTION
Mattituck Harbor, NY
JOB NUMBER
180-157715-1
See page two for job notes and contact information.
Pittsburgh PA 15238 RIDC Park 301 Alpha Drive Eurofins Pittsburgh https://eol.et.eurofinsus.com/myEOL/ http://
Eurofins Pittsburgh
Eurofins Pittsburgh is a laboratory within Eurofins Environment Testing Northeast LLC, a company within Eurofins Environment Testing Group of Companies
Job Notes This report may not be reproduced except in full, and with written approval from the laboratory. The results relate only to the samples tested. For questions please contact the Project Manager at the e-mail address or telephone number listed on this page.
PA Lab ID: 02-00416
The test results in this report relate only to the samples as received by the laboratory and will meet all requirements of the methodology, with any exceptions noted. This report shall not be reproduced except in full, without the express written approval of the laboratory. All questions should be directed to the Eurofins Pittsburgh Project Manager.
Authorization
Generated
6/29/2023 1:41 PM
Authorized for release by Carrie L Gamber, Senior Project Manager Carrie.Gamber@et.eurofinsus.com 412 963-2428
Table of Contents Cover Title Page
Data Summaries
Definitions
Case Narrative
Detection Summary
Client Sample Results
Default Detection Limits
Surrogate Summary
QC Sample Results
QC Association
Chronicle
Certification Summary
Method Summary
Sample Summary
Manual Integration Summary
Reagent Traceability
COAs
Organic Sample Data
GC/MS VOA
8260D 8260D QC Summary 8260D Sample Data Standards Data
8260D ICAL Data 8260D CCAL Data
Raw QC Data
Table of Contents 8260D Tune Data 8260D Blank Data 8260D LCS/LCSD Data 8260D MS/MSD Data
8260D Run Logs 8260D Prep Data
Inorganic Sample Data
General Chemistry Data
Gen Chem Cover Page
Gen Chem MDL
Gen Chem Analysis Run Log
Gen Chem Prep Data
Gen Chem Raw Data
Shipping and Receiving Documents
Client Chain of Custody
Sample Receipt Checklist
Definitions/Glossary Job ID: 180-157715-1Client: Battelle
Project/Site: Mattituck Harbor, NY
Qualifiers
GC/MS VOA
Qualifier Description
F2 MS/MSD RPD exceeds control limits
Qualifier
U Indicates the analyte was analyzed for but not detected.
Glossary These commonly used abbreviations may or may not be present in this report.
¤ Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Level"
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative / Absent
POS Positive / Present
PQL Practical Quantitation Limit
PRES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
CASE NARRATIVE
Client: Battelle
Project: Mattituck Harbor, NY
Report Number: 180-157715-1
With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples, the reporting limits are adjusted relative to the dilution required.
Calculations are performed before rounding to avoid round-off errors in calculated results.
All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the individual sections below.
RECEIPT
The samples were received on 06/08/2023; the samples arrived in good condition, properly preserved and on ice. The temperature of the coolers at receipt was 3.4 C.
VOLATILES
Acetone exceeded the RPD limit for the MSD of sample #20230470A MC-8AMSD (180-157715-3) in batch 180-437636.
The continuing calibration verification (CCV) analyzed in batch 180-437636 was outside the method criteria for the following analyte(s):
Acrolein, Bromoform, 1,2-Dibromo-3-Chloropropane, Vinyl acetate and Bromomethane .(LOW). A CCV standard at or below the reporting limit (RL) was analyzed with the affected samples and found to be acceptable. As indicated in the reference method, sample analysis may proceed; however, any detection for the affected analyte(s) is considered estimated.
The continuing calibration verification (CCV) analyzed in batch 180-437636 was outside the method criteria for the following analyte(s):
1,4-Dioxane(RF). A CCV standard at or below the reporting limit (RL) was analyzed with the affected samples and found to be acceptable. As indicated in the reference method, sample analysis may proceed; however, any detection for the affected analyte(s) is considered estimated.
PERCENT SOLIDS
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Detection Summary
Project/Site: Mattituck Harbor, NY
Client Sample ID: #20230471A MC-9A Lab Sample ID: 180-157715-1
No Detections.
Client Sample ID: #20230471B MC-9B Lab Sample ID: 180-157715-2
No Detections.
Client Sample ID: #20230470A MC-8A Lab Sample ID: 180-157715-3
No Detections.
Client Sample ID: #20230470B MC-8B Lab Sample ID: 180-157715-4
No Detections.
Client Sample ID: #20230469A MC-7A Lab Sample ID: 180-157715-5
No Detections.
Client Sample ID: #20230469B MC-7B Lab Sample ID: 180-157715-6
No Detections.
Client Sample ID: #20230468A MC-6A Lab Sample ID: 180-157715-7
No Detections.
Client Sample ID: #20230468B MC-6B Lab Sample ID: 180-157715-8
No Detections.
Eurofins Pittsburgh
This Detection Summary does not include radiochemical test results.
Client Sample Results
Project/Site: Mattituck Harbor, NY
Method: SW846 EPA 8260D - Volatile Organic Compounds by GC/MS
Lab Sample ID: 180-157715-1Client Sample ID: #20230471A MC-9A Matrix: SedimentDate Collected: 06/07/23 10:22
Percent Solids: 52.9Date Received: 06/08/23 09:15
RL MDL
8.9 U 8.9 3.0 ug/Kg ☼ 06/12/23 07:42 06/12/23 16:00 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1,1,1-Trichloroethane
8.9 2.8 ug/Kg 06/12/23 07:42 06/12/23 16:00 1☼8.9 U1,1-Dichloroethane
8.9 2.5 ug/Kg 06/12/23 07:42 06/12/23 16:00 1☼8.9 UBenzene
8.9 4.0 ug/Kg 06/12/23 07:42 06/12/23 16:00 1☼8.9 U1,1-Dichloroethene
8.9 3.1 ug/Kg 06/12/23 07:42 06/12/23 16:00 1☼8.9 U1,2,4-Trimethylbenzene
8.9 3.0 ug/Kg 06/12/23 07:42 06/12/23 16:00 1☼8.9 U1,2-Dichlorobenzene
8.9 2.6 ug/Kg 06/12/23 07:42 06/12/23 16:00 1☼8.9 UToluene
8.9 2.6 ug/Kg 06/12/23 07:42 06/12/23 16:00 1☼8.9 U1,2-Dichloroethane
18 13 ug/Kg 06/12/23 07:42 06/12/23 16:00 1☼18 UXylenes, Total
8.9 3.3 ug/Kg 06/12/23 07:42 06/12/23 16:00 1☼8.9 U1,3,5-Trimethylbenzene
8.9 5.5 ug/Kg 06/12/23 07:42 06/12/23 16:00 1☼8.9 U1,3-Dichlorobenzene
8.9 2.7 ug/Kg 06/12/23 07:42 06/12/23 16:00 1☼8.9 U1,4-Dichlorobenzene
1800 130 ug/Kg 06/12/23 07:42 06/12/23 16:00 1☼1800 U1,4-Dioxane
45 4.5 ug/Kg 06/12/23 07:42 06/12/23 16:00 1☼45 U2-Butanone (MEK)
45 6.9 ug/Kg 06/12/23 07:42 06/12/23 16:00 1☼45 UAcetone
8.9 3.6 ug/Kg 06/12/23 07:42 06/12/23 16:00 1☼8.9 UCarbon tetrachloride
8.9 2.3 ug/Kg 06/12/23 07:42 06/12/23 16:00 1☼8.9 UChlorobenzene
8.9 6.0 ug/Kg 06/12/23 07:42 06/12/23 16:00 1☼8.9 UChloroform
8.9 2.7 ug/Kg 06/12/23 07:42 06/12/23 16:00 1☼8.9 Ucis-1,2-Dichloroethene
8.9 3.3 ug/Kg 06/12/23 07:42 06/12/23 16:00 1☼8.9 UEthylbenzene
8.9 2.6 ug/Kg 06/12/23 07:42 06/12/23 16:00 1☼8.9 UMethyl tert-butyl ether
8.9 8.0 ug/Kg 06/12/23 07:42 06/12/23 16:00 1☼8.9 UMethylene Chloride
8.9 4.4 ug/Kg 06/12/23 07:42 06/12/23 16:00 1☼8.9 Un-Butylbenzene
8.9 3.2 ug/Kg 06/12/23 07:42 06/12/23 16:00 1☼8.9 UN-Propylbenzene
8.9 4.4 ug/Kg 06/12/23 07:42 06/12/23 16:00 1☼8.9 Usec-Butylbenzene
8.9 3.8 ug/Kg 06/12/23 07:42 06/12/23 16:00 1☼8.9 Utert-Butylbenzene
8.9 3.6 ug/Kg 06/12/23 07:42 06/12/23 16:00 1☼8.9 UTetrachloroethene
8.9 3.1 ug/Kg 06/12/23 07:42 06/12/23 16:00 1☼8.9 Utrans-1,2-Dichloroethene
8.9 2.8 ug/Kg 06/12/23 07:42 06/12/23 16:00 1☼8.9 UTrichloroethene
8.9 6.4 ug/Kg 06/12/23 07:42 06/12/23 16:00 1☼8.9 UVinyl chloride
1,2-Dichloroethane-d4 (Surr) 104 73 - 135 06/12/23 07:42 06/12/23 16:00 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
4-Bromofluorobenzene (Surr) 92 06/12/23 07:42 06/12/23 16:00 160 - 124
Dibromofluoromethane (Surr) 99 06/12/23 07:42 06/12/23 16:00 169 - 126
Toluene-d8 (Surr) 84 06/12/23 07:42 06/12/23 16:00 167 - 134
Project/Site: Mattituck Harbor, NY
Method: SW846 EPA 8260D - Volatile Organic Compounds by GC/MS
Lab Sample ID: 180-157715-2Client Sample ID: #20230471B MC-9B Matrix: SedimentDate Collected: 06/07/23 10:22
Percent Solids: 50.8Date Received: 06/08/23 09:15
RL MDL
9.4 U 9.4 3.1 ug/Kg ☼ 06/12/23 07:42 06/12/23 17:08 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1,1,1-Trichloroethane
9.4 3.0 ug/Kg 06/12/23 07:42 06/12/23 17:08 1☼9.4 U1,1-Dichloroethane
9.4 2.7 ug/Kg 06/12/23 07:42 06/12/23 17:08 1☼9.4 UBenzene
9.4 4.3 ug/Kg 06/12/23 07:42 06/12/23 17:08 1☼9.4 U1,1-Dichloroethene
9.4 3.2 ug/Kg 06/12/23 07:42 06/12/23 17:08 1☼9.4 U1,2,4-Trimethylbenzene
9.4 3.2 ug/Kg 06/12/23 07:42 06/12/23 17:08 1☼9.4 U1,2-Dichlorobenzene
9.4 2.7 ug/Kg 06/12/23 07:42 06/12/23 17:08 1☼9.4 UToluene
9.4 2.7 ug/Kg 06/12/23 07:42 06/12/23 17:08 1☼9.4 U1,2-Dichloroethane
19 14 ug/Kg 06/12/23 07:42 06/12/23 17:08 1☼19 UXylenes, Total
9.4 3.5 ug/Kg 06/12/23 07:42 06/12/23 17:08 1☼9.4 U1,3,5-Trimethylbenzene
9.4 5.8 ug/Kg 06/12/23 07:42 06/12/23 17:08 1☼9.4 U1,3-Dichlorobenzene
9.4 2.8 ug/Kg 06/12/23 07:42 06/12/23 17:08 1☼9.4 U1,4-Dichlorobenzene
1900 140 ug/Kg 06/12/23 07:42 06/12/23 17:08 1☼1900 U1,4-Dioxane
47 4.8 ug/Kg 06/12/23 07:42 06/12/23 17:08 1☼47 U2-Butanone (MEK)
47 7.3 ug/Kg 06/12/23 07:42 06/12/23 17:08 1☼47 UAcetone
9.4 3.8 ug/Kg 06/12/23 07:42 06/12/23 17:08 1☼9.4 UCarbon tetrachloride
9.4 2.4 ug/Kg 06/12/23 07:42 06/12/23 17:08 1☼9.4 UChlorobenzene
9.4 6.3 ug/Kg 06/12/23 07:42 06/12/23 17:08 1☼9.4 UChloroform
9.4 2.8 ug/Kg 06/12/23 07:42 06/12/23 17:08 1☼9.4 Ucis-1,2-Dichloroethene
9.4 3.5 ug/Kg 06/12/23 07:42 06/12/23 17:08 1☼9.4 UEthylbenzene
9.4 2.8 ug/Kg 06/12/23 07:42 06/12/23 17:08 1☼9.4 UMethyl tert-butyl ether
9.4 8.5 ug/Kg 06/12/23 07:42 06/12/23 17:08 1☼9.4 UMethylene Chloride
9.4 4.7 ug/Kg 06/12/23 07:42 06/12/23 17:08 1☼9.4 Un-Butylbenzene
9.4 3.4 ug/Kg 06/12/23 07:42 06/12/23 17:08 1☼9.4 UN-Propylbenzene
9.4 4.6 ug/Kg 06/12/23 07:42 06/12/23 17:08 1☼9.4 Usec-Butylbenzene
9.4 4.0 ug/Kg 06/12/23 07:42 06/12/23 17:08 1☼9.4 Utert-Butylbenzene
9.4 3.8 ug/Kg 06/12/23 07:42 06/12/23 17:08 1☼9.4 UTetrachloroethene
9.4 3.3 ug/Kg 06/12/23 07:42 06/12/23 17:08 1☼9.4 Utrans-1,2-Dichloroethene
9.4 3.0 ug/Kg 06/12/23 07:42 06/12/23 17:08 1☼9.4 UTrichloroethene
9.4 6.8 ug/Kg 06/12/23 07:42 06/12/23 17:08 1☼9.4 UVinyl chloride
1,2-Dichloroethane-d4 (Surr) 107 73 - 135 06/12/23 07:42 06/12/23 17:08 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
4-Bromofluorobenzene (Surr) 97 06/12/23 07:42 06/12/23 17:08 160 - 124
Dibromofluoromethane (Surr) 102 06/12/23 07:42 06/12/23 17:08 169 - 126
Toluene-d8 (Surr) 86 06/12/23 07:42 06/12/23 17:08 167 - 134
Project/Site: Mattituck Harbor, NY
Method: SW846 EPA 8260D - Volatile Organic Compounds by GC/MS
Lab Sample ID: 180-157715-3Client Sample ID: #20230470A MC-8A Matrix: SedimentDate Collected: 06/07/23 11:37
Percent Solids: 31.1Date Received: 06/08/23 09:15
RL MDL
15 U 15 5.0 ug/Kg ☼ 06/12/23 07:42 06/12/23 15:38 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1,1,1-Trichloroethane
15 4.8 ug/Kg 06/12/23 07:42 06/12/23 15:38 1☼15 U1,1-Dichloroethane
15 4.3 ug/Kg 06/12/23 07:42 06/12/23 15:38 1☼15 UBenzene
15 6.8 ug/Kg 06/12/23 07:42 06/12/23 15:38 1☼15 U1,1-Dichloroethene
15 5.2 ug/Kg 06/12/23 07:42 06/12/23 15:38 1☼15 U1,2,4-Trimethylbenzene
15 5.1 ug/Kg 06/12/23 07:42 06/12/23 15:38 1☼15 U1,2-Dichlorobenzene
15 4.3 ug/Kg 06/12/23 07:42 06/12/23 15:38 1☼15 UToluene
15 4.3 ug/Kg 06/12/23 07:42 06/12/23 15:38 1☼15 U1,2-Dichloroethane
30 22 ug/Kg 06/12/23 07:42 06/12/23 15:38 1☼30 UXylenes, Total
15 5.6 ug/Kg 06/12/23 07:42 06/12/23 15:38 1☼15 U1,3,5-Trimethylbenzene
15 9.3 ug/Kg 06/12/23 07:42 06/12/23 15:38 1☼15 U1,3-Dichlorobenzene
15 4.5 ug/Kg 06/12/23 07:42 06/12/23 15:38 1☼15 U1,4-Dichlorobenzene
3000 230 ug/Kg 06/12/23 07:42 06/12/23 15:38 1☼3000 U1,4-Dioxane
75 7.7 ug/Kg 06/12/23 07:42 06/12/23 15:38 1☼75 U2-Butanone (MEK)
75 12 ug/Kg 06/12/23 07:42 06/12/23 15:38 1☼75 U F2Acetone
15 6.1 ug/Kg 06/12/23 07:42 06/12/23 15:38 1☼15 UCarbon tetrachloride
15 3.9 ug/Kg 06/12/23 07:42 06/12/23 15:38 1☼15 UChlorobenzene
15 10 ug/Kg 06/12/23 07:42 06/12/23 15:38 1☼15 UChloroform
15 4.6 ug/Kg 06/12/23 07:42 06/12/23 15:38 1☼15 Ucis-1,2-Dichloroethene
15 5.6 ug/Kg 06/12/23 07:42 06/12/23 15:38 1☼15 UEthylbenzene
15 4.4 ug/Kg 06/12/23 07:42 06/12/23 15:38 1☼15 UMethyl tert-butyl ether
15 14 ug/Kg 06/12/23 07:42 06/12/23 15:38 1☼15 UMethylene Chloride
15 7.5 ug/Kg 06/12/23 07:42 06/12/23 15:38 1☼15 Un-Butylbenzene
15 5.4 ug/Kg 06/12/23 07:42 06/12/23 15:38 1☼15 UN-Propylbenzene
15 7.4 ug/Kg 06/12/23 07:42 06/12/23 15:38 1☼15 Usec-Butylbenzene
15 6.4 ug/Kg 06/12/23 07:42 06/12/23 15:38 1☼15 Utert-Butylbenzene
15 6.1 ug/Kg 06/12/23 07:42 06/12/23 15:38 1☼15 UTetrachloroethene
15 5.3 ug/Kg 06/12/23 07:42 06/12/23 15:38 1☼15 Utrans-1,2-Dichloroethene
15 4.7 ug/Kg 06/12/23 07:42 06/12/23 15:38 1☼15 UTrichloroethene
15 11 ug/Kg 06/12/23 07:42 06/12/23 15:38 1☼15 UVinyl chloride
1,2-Dichloroethane-d4 (Surr) 90 73 - 135 06/12/23 07:42 06/12/23 15:38 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
4-Bromofluorobenzene (Surr) 72 06/12/23 07:42 06/12/23 15:38 160 - 124
Dibromofluoromethane (Surr) 85 06/12/23 07:42 06/12/23 15:38 169 - 126
Toluene-d8 (Surr) 77 06/12/23 07:42 06/12/23 15:38 167 - 134
Project/Site: Mattituck Harbor, NY
Method: SW846 EPA 8260D - Volatile Organic Compounds by GC/MS
Lab Sample ID: 180-157715-4Client Sample ID: #20230470B MC-8B Matrix: SedimentDate Collected: 06/07/23 11:37
Percent Solids: 38.0Date Received: 06/08/23 09:15
RL MDL
13 U 13 4.4 ug/Kg ☼ 06/12/23 07:42 06/12/23 17:32 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1,1,1-Trichloroethane
13 4.2 ug/Kg 06/12/23 07:42 06/12/23 17:32 1☼13 U1,1-Dichloroethane
13 3.7 ug/Kg 06/12/23 07:42 06/12/23 17:32 1☼13 UBenzene
13 5.9 ug/Kg 06/12/23 07:42 06/12/23 17:32 1☼13 U1,1-Dichloroethene
13 4.5 ug/Kg 06/12/23 07:42 06/12/23 17:32 1☼13 U1,2,4-Trimethylbenzene
13 4.4 ug/Kg 06/12/23 07:42 06/12/23 17:32 1☼13 U1,2-Dichlorobenzene
13 3.8 ug/Kg 06/12/23 07:42 06/12/23 17:32 1☼13 UToluene
13 3.8 ug/Kg 06/12/23 07:42 06/12/23 17:32 1☼13 U1,2-Dichloroethane
26 19 ug/Kg 06/12/23 07:42 06/12/23 17:32 1☼26 UXylenes, Total
13 4.9 ug/Kg 06/12/23 07:42 06/12/23 17:32 1☼13 U1,3,5-Trimethylbenzene
13 8.0 ug/Kg 06/12/23 07:42 06/12/23 17:32 1☼13 U1,3-Dichlorobenzene
13 3.9 ug/Kg 06/12/23 07:42 06/12/23 17:32 1☼13 U1,4-Dichlorobenzene
2600 200 ug/Kg 06/12/23 07:42 06/12/23 17:32 1☼2600 U1,4-Dioxane
65 6.6 ug/Kg 06/12/23 07:42 06/12/23 17:32 1☼65 U2-Butanone (MEK)
65 10 ug/Kg 06/12/23 07:42 06/12/23 17:32 1☼65 UAcetone
13 5.3 ug/Kg 06/12/23 07:42 06/12/23 17:32 1☼13 UCarbon tetrachloride
13 3.4 ug/Kg 06/12/23 07:42 06/12/23 17:32 1☼13 UChlorobenzene
13 8.7 ug/Kg 06/12/23 07:42 06/12/23 17:32 1☼13 UChloroform
13 3.9 ug/Kg 06/12/23 07:42 06/12/23 17:32 1☼13 Ucis-1,2-Dichloroethene
13 4.8 ug/Kg 06/12/23 07:42 06/12/23 17:32 1☼13 UEthylbenzene
13 3.8 ug/Kg 06/12/23 07:42 06/12/23 17:32 1☼13 UMethyl tert-butyl ether
13 12 ug/Kg 06/12/23 07:42 06/12/23 17:32 1☼13 UMethylene Chloride
13 6.5 ug/Kg 06/12/23 07:42 06/12/23 17:32 1☼13 Un-Butylbenzene
13 4.6 ug/Kg 06/12/23 07:42 06/12/23 17:32 1☼13 UN-Propylbenzene
13 6.4 ug/Kg 06/12/23 07:42 06/12/23 17:32 1☼13 Usec-Butylbenzene
13 5.5 ug/Kg 06/12/23 07:42 06/12/23 17:32 1☼13 Utert-Butylbenzene
13 5.2 ug/Kg 06/12/23 07:42 06/12/23 17:32 1☼13 UTetrachloroethene
13 4.6 ug/Kg 06/12/23 07:42 06/12/23 17:32 1☼13 Utrans-1,2-Dichloroethene
13 4.1 ug/Kg 06/12/23 07:42 06/12/23 17:32 1☼13 UTrichloroethene
13 9.4 ug/Kg 06/12/23 07:42 06/12/23 17:32 1☼13 UVinyl chloride
1,2-Dichloroethane-d4 (Surr) 96 73 - 135 06/12/23 07:42 06/12/23 17:32 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
4-Bromofluorobenzene (Surr) 93 06/12/23 07:42 06/12/23 17:32 160 - 124
Dibromofluoromethane (Surr) 98 06/12/23 07:42 06/12/23 17:32 169 - 126
Toluene-d8 (Surr) 88 06/12/23 07:42 06/12/23 17:32 167 - 134
Project/Site: Mattituck Harbor, NY
Method: SW846 EPA 8260D - Volatile Organic Compounds by GC/MS
Lab Sample ID: 180-157715-5Client Sample ID: #20230469A MC-7A Matrix: SedimentDate Collected: 06/07/23 12:55
Percent Solids: 44.9Date Received: 06/08/23 09:15
RL MDL
11 U 11 3.6 ug/Kg ☼ 06/12/23 07:42 06/12/23 17:54 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1,1,1-Trichloroethane
11 3.5 ug/Kg 06/12/23 07:42 06/12/23 17:54 1☼11 U1,1-Dichloroethane
11 3.1 ug/Kg 06/12/23 07:42 06/12/23 17:54 1☼11 UBenzene
11 4.9 ug/Kg 06/12/23 07:42 06/12/23 17:54 1☼11 U1,1-Dichloroethene
11 3.7 ug/Kg 06/12/23 07:42 06/12/23 17:54 1☼11 U1,2,4-Trimethylbenzene
11 3.6 ug/Kg 06/12/23 07:42 06/12/23 17:54 1☼11 U1,2-Dichlorobenzene
11 3.1 ug/Kg 06/12/23 07:42 06/12/23 17:54 1☼11 UToluene
11 3.1 ug/Kg 06/12/23 07:42 06/12/23 17:54 1☼11 U1,2-Dichloroethane
22 16 ug/Kg 06/12/23 07:42 06/12/23 17:54 1☼22 UXylenes, Total
11 4.0 ug/Kg 06/12/23 07:42 06/12/23 17:54 1☼11 U1,3,5-Trimethylbenzene
11 6.7 ug/Kg 06/12/23 07:42 06/12/23 17:54 1☼11 U1,3-Dichlorobenzene
11 3.3 ug/Kg 06/12/23 07:42 06/12/23 17:54 1☼11 U1,4-Dichlorobenzene
2200 160 ug/Kg 06/12/23 07:42 06/12/23 17:54 1☼2200 U1,4-Dioxane
54 5.5 ug/Kg 06/12/23 07:42 06/12/23 17:54 1☼54 U2-Butanone (MEK)
54 8.5 ug/Kg 06/12/23 07:42 06/12/23 17:54 1☼54 UAcetone
11 4.4 ug/Kg 06/12/23 07:42 06/12/23 17:54 1☼11 UCarbon tetrachloride
11 2.8 ug/Kg 06/12/23 07:42 06/12/23 17:54 1☼11 UChlorobenzene
11 7.3 ug/Kg 06/12/23 07:42 06/12/23 17:54 1☼11 UChloroform
11 3.3 ug/Kg 06/12/23 07:42 06/12/23 17:54 1☼11 Ucis-1,2-Dichloroethene
11 4.0 ug/Kg 06/12/23 07:42 06/12/23 17:54 1☼11 UEthylbenzene
11 3.2 ug/Kg 06/12/23 07:42 06/12/23 17:54 1☼11 UMethyl tert-butyl ether
11 9.8 ug/Kg 06/12/23 07:42 06/12/23 17:54 1☼11 UMethylene Chloride
11 5.4 ug/Kg 06/12/23 07:42 06/12/23 17:54 1☼11 Un-Butylbenzene
11 3.9 ug/Kg 06/12/23 07:42 06/12/23 17:54 1☼11 UN-Propylbenzene
11 5.3 ug/Kg 06/12/23 07:42 06/12/23 17:54 1☼11 Usec-Butylbenzene
11 4.6 ug/Kg 06/12/23 07:42 06/12/23 17:54 1☼11 Utert-Butylbenzene
11 4.4 ug/Kg 06/12/23 07:42 06/12/23 17:54 1☼11 UTetrachloroethene
11 3.8 ug/Kg 06/12/23 07:42 06/12/23 17:54 1☼11 Utrans-1,2-Dichloroethene
11 3.4 ug/Kg 06/12/23 07:42 06/12/23 17:54 1☼11 UTrichloroethene
11 7.8 ug/Kg 06/12/23 07:42 06/12/23 17:54 1☼11 UVinyl chloride
1,2-Dichloroethane-d4 (Surr) 99 73 - 135 06/12/23 07:42 06/12/23 17:54 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
4-Bromofluorobenzene (Surr) 95 06/12/23 07:42 06/12/23 17:54 160 - 124
Dibromofluoromethane (Surr) 100 06/12/23 07:42 06/12/23 17:54 169 - 126
Toluene-d8 (Surr) 90 06/12/23 07:42 06/12/23 17:54 167 - 134
Project/Site: Mattituck Harbor, NY
Method: SW846 EPA 8260D - Volatile Organic Compounds by GC/MS
Lab Sample ID: 180-157715-6Client Sample ID: #20230469B MC-7B Matrix: SedimentDate Collected: 06/07/23 12:55
Percent Solids: 50.8Date Received: 06/08/23 09:15
RL MDL
9.2 U 9.2 3.1 ug/Kg ☼ 06/12/23 07:42 06/12/23 18:17 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1,1,1-Trichloroethane
9.2 3.0 ug/Kg 06/12/23 07:42 06/12/23 18:17 1☼9.2 U1,1-Dichloroethane
9.2 2.6 ug/Kg 06/12/23 07:42 06/12/23 18:17 1☼9.2 UBenzene
9.2 4.2 ug/Kg 06/12/23 07:42 06/12/23 18:17 1☼9.2 U1,1-Dichloroethene
9.2 3.2 ug/Kg 06/12/23 07:42 06/12/23 18:17 1☼9.2 U1,2,4-Trimethylbenzene
9.2 3.1 ug/Kg 06/12/23 07:42 06/12/23 18:17 1☼9.2 U1,2-Dichlorobenzene
9.2 2.7 ug/Kg 06/12/23 07:42 06/12/23 18:17 1☼9.2 UToluene
9.2 2.7 ug/Kg 06/12/23 07:42 06/12/23 18:17 1☼9.2 U1,2-Dichloroethane
18 13 ug/Kg 06/12/23 07:42 06/12/23 18:17 1☼18 UXylenes, Total
9.2 3.4 ug/Kg 06/12/23 07:42 06/12/23 18:17 1☼9.2 U1,3,5-Trimethylbenzene
9.2 5.7 ug/Kg 06/12/23 07:42 06/12/23 18:17 1☼9.2 U1,3-Dichlorobenzene
9.2 2.8 ug/Kg 06/12/23 07:42 06/12/23 18:17 1☼9.2 U1,4-Dichlorobenzene
1800 140 ug/Kg 06/12/23 07:42 06/12/23 18:17 1☼1800 U1,4-Dioxane
46 4.7 ug/Kg 06/12/23 07:42 06/12/23 18:17 1☼46 U2-Butanone (MEK)
46 7.2 ug/Kg 06/12/23 07:42 06/12/23 18:17 1☼46 UAcetone
9.2 3.8 ug/Kg 06/12/23 07:42 06/12/23 18:17 1☼9.2 UCarbon tetrachloride
9.2 2.4 ug/Kg 06/12/23 07:42 06/12/23 18:17 1☼9.2 UChlorobenzene
9.2 6.2 ug/Kg 06/12/23 07:42 06/12/23 18:17 1☼9.2 UChloroform
9.2 2.8 ug/Kg 06/12/23 07:42 06/12/23 18:17 1☼9.2 Ucis-1,2-Dichloroethene
9.2 3.4 ug/Kg 06/12/23 07:42 06/12/23 18:17 1☼9.2 UEthylbenzene
9.2 2.7 ug/Kg 06/12/23 07:42 06/12/23 18:17 1☼9.2 UMethyl tert-butyl ether
9.2 8.3 ug/Kg 06/12/23 07:42 06/12/23 18:17 1☼9.2 UMethylene Chloride
9.2 4.6 ug/Kg 06/12/23 07:42 06/12/23 18:17 1☼9.2 Un-Butylbenzene
9.2 3.3 ug/Kg 06/12/23 07:42 06/12/23 18:17 1☼9.2 UN-Propylbenzene
9.2 4.5 ug/Kg 06/12/23 07:42 06/12/23 18:17 1☼9.2 Usec-Butylbenzene
9.2 3.9 ug/Kg 06/12/23 07:42 06/12/23 18:17 1☼9.2 Utert-Butylbenzene
9.2 3.7 ug/Kg 06/12/23 07:42 06/12/23 18:17 1☼9.2 UTetrachloroethene
9.2 3.2 ug/Kg 06/12/23 07:42 06/12/23 18:17 1☼9.2 Utrans-1,2-Dichloroethene
9.2 2.9 ug/Kg 06/12/23 07:42 06/12/23 18:17 1☼9.2 UTrichloroethene
9.2 6.7 ug/Kg 06/12/23 07:42 06/12/23 18:17 1☼9.2 UVinyl chloride
1,2-Dichloroethane-d4 (Surr) 120 73 - 135 06/12/23 07:42 06/12/23 18:17 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
4-Bromofluorobenzene (Surr) 108 06/12/23 07:42 06/12/23 18:17 160 - 124
Dibromofluoromethane (Surr) 116 06/12/23 07:42 06/12/23 18:17 169 - 126
Toluene-d8 (Surr) 99 06/12/23 07:42 06/12/23 18:17 167 - 134
Project/Site: Mattituck Harbor, NY
Method: SW846 EPA 8260D - Volatile Organic Compounds by GC/MS
Lab Sample ID: 180-157715-7Client Sample ID: #20230468A MC-6A Matrix: SedimentDate Collected: 06/07/23 13:47
Percent Solids: 36.5Date Received: 06/08/23 09:15
RL MDL
13 U 13 4.5 ug/Kg ☼ 06/12/23 07:42 06/12/23 18:39 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1,1,1-Trichloroethane
13 4.3 ug/Kg 06/12/23 07:42 06/12/23 18:39 1☼13 U1,1-Dichloroethane
13 3.8 ug/Kg 06/12/23 07:42 06/12/23 18:39 1☼13 UBenzene
13 6.1 ug/Kg 06/12/23 07:42 06/12/23 18:39 1☼13 U1,1-Dichloroethene
13 4.6 ug/Kg 06/12/23 07:42 06/12/23 18:39 1☼13 U1,2,4-Trimethylbenzene
13 4.5 ug/Kg 06/12/23 07:42 06/12/23 18:39 1☼13 U1,2-Dichlorobenzene
13 3.9 ug/Kg 06/12/23 07:42 06/12/23 18:39 1☼13 UToluene
13 3.9 ug/Kg 06/12/23 07:42 06/12/23 18:39 1☼13 U1,2-Dichloroethane
27 19 ug/Kg 06/12/23 07:42 06/12/23 18:39 1☼27 UXylenes, Total
13 5.0 ug/Kg 06/12/23 07:42 06/12/23 18:39 1☼13 U1,3,5-Trimethylbenzene
13 8.3 ug/Kg 06/12/23 07:42 06/12/23 18:39 1☼13 U1,3-Dichlorobenzene
13 4.0 ug/Kg 06/12/23 07:42 06/12/23 18:39 1☼13 U1,4-Dichlorobenzene
2700 200 ug/Kg 06/12/23 07:42 06/12/23 18:39 1☼2700 U1,4-Dioxane
67 6.9 ug/Kg 06/12/23 07:42 06/12/23 18:39 1☼67 U2-Butanone (MEK)
67 11 ug/Kg 06/12/23 07:42 06/12/23 18:39 1☼67 UAcetone
13 5.5 ug/Kg 06/12/23 07:42 06/12/23 18:39 1☼13 UCarbon tetrachloride
13 3.5 ug/Kg 06/12/23 07:42 06/12/23 18:39 1☼13 UChlorobenzene
13 9.0 ug/Kg 06/12/23 07:42 06/12/23 18:39 1☼13 UChloroform
13 4.1 ug/Kg 06/12/23 07:42 06/12/23 18:39 1☼13 Ucis-1,2-Dichloroethene
13 5.0 ug/Kg 06/12/23 07:42 06/12/23 18:39 1☼13 UEthylbenzene
13 4.0 ug/Kg 06/12/23 07:42 06/12/23 18:39 1☼13 UMethyl tert-butyl ether
13 12 ug/Kg 06/12/23 07:42 06/12/23 18:39 1☼13 UMethylene Chloride
13 6.7 ug/Kg 06/12/23 07:42 06/12/23 18:39 1☼13 Un-Butylbenzene
13 4.8 ug/Kg 06/12/23 07:42 06/12/23 18:39 1☼13 UN-Propylbenzene
13 6.6 ug/Kg 06/12/23 07:42 06/12/23 18:39 1☼13 Usec-Butylbenzene
13 5.7 ug/Kg 06/12/23 07:42 06/12/23 18:39 1☼13 Utert-Butylbenzene
13 5.4 ug/Kg 06/12/23 07:42 06/12/23 18:39 1☼13 UTetrachloroethene
13 4.7 ug/Kg 06/12/23 07:42 06/12/23 18:39 1☼13 Utrans-1,2-Dichloroethene
13 4.2 ug/Kg 06/12/23 07:42 06/12/23 18:39 1☼13 UTrichloroethene
13 9.7 ug/Kg 06/12/23 07:42 06/12/23 18:39 1☼13 UVinyl chloride
1,2-Dichloroethane-d4 (Surr) 116 73 - 135 06/12/23 07:42 06/12/23 18:39 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
4-Bromofluorobenzene (Surr) 99 06/12/23 07:42 06/12/23 18:39 160 - 124
Dibromofluoromethane (Surr) 107 06/12/23 07:42 06/12/23 18:39 169 - 126
Toluene-d8 (Surr) 91 06/12/23 07:42 06/12/23 18:39 167 - 134
Project/Site: Mattituck Harbor, NY
Method: SW846 EPA 8260D - Volatile Organic Compounds by GC/MS
Lab Sample ID: 180-157715-8Client Sample ID: #20230468B MC-6B Matrix: SedimentDate Collected: 06/07/23 13:47
Percent Solids: 45.1Date Received: 06/08/23 09:15
RL MDL
10 U 10 3.5 ug/Kg ☼ 06/12/23 07:42 06/12/23 19:02 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
1,1,1-Trichloroethane
10 3.3 ug/Kg 06/12/23 07:42 06/12/23 19:02 1☼10 U1,1-Dichloroethane
10 2.9 ug/Kg 06/12/23 07:42 06/12/23 19:02 1☼10 UBenzene
10 4.7 ug/Kg 06/12/23 07:42 06/12/23 19:02 1☼10 U1,1-Dichloroethene
10 3.6 ug/Kg 06/12/23 07:42 06/12/23 19:02 1☼10 U1,2,4-Trimethylbenzene
10 3.5 ug/Kg 06/12/23 07:42 06/12/23 19:02 1☼10 U1,2-Dichlorobenzene
10 3.0 ug/Kg 06/12/23 07:42 06/12/23 19:02 1☼10 UToluene
10 3.0 ug/Kg 06/12/23 07:42 06/12/23 19:02 1☼10 U1,2-Dichloroethane
21 15 ug/Kg 06/12/23 07:42 06/12/23 19:02 1☼21 UXylenes, Total
10 3.9 ug/Kg 06/12/23 07:42 06/12/23 19:02 1☼10 U1,3,5-Trimethylbenzene
10 6.4 ug/Kg 06/12/23 07:42 06/12/23 19:02 1☼10 U1,3-Dichlorobenzene
10 3.1 ug/Kg 06/12/23 07:42 06/12/23 19:02 1☼10 U1,4-Dichlorobenzene
2100 160 ug/Kg 06/12/23 07:42 06/12/23 19:02 1☼2100 U1,4-Dioxane
52 5.3 ug/Kg 06/12/23 07:42 06/12/23 19:02 1☼52 U2-Butanone (MEK)
52 8.2 ug/Kg 06/12/23 07:42 06/12/23 19:02 1☼52 UAcetone
10 4.2 ug/Kg 06/12/23 07:42 06/12/23 19:02 1☼10 UCarbon tetrachloride
10 2.7 ug/Kg 06/12/23 07:42 06/12/23 19:02 1☼10 UChlorobenzene
10 7.0 ug/Kg 06/12/23 07:42 06/12/23 19:02 1☼10 UChloroform
10 3.2 ug/Kg 06/12/23 07:42 06/12/23 19:02 1☼10 Ucis-1,2-Dichloroethene
10 3.9 ug/Kg 06/12/23 07:42 06/12/23 19:02 1☼10 UEthylbenzene
10 3.1 ug/Kg 06/12/23 07:42 06/12/23 19:02 1☼10 UMethyl tert-butyl ether
10 9.4 ug/Kg 06/12/23 07:42 06/12/23 19:02 1☼10 UMethylene Chloride
10 5.2 ug/Kg 06/12/23 07:42 06/12/23 19:02 1☼10 Un-Butylbenzene
10 3.7 ug/Kg 06/12/23 07:42 06/12/23 19:02 1☼10 UN-Propylbenzene
10 5.1 ug/Kg 06/12/23 07:42 06/12/23 19:02 1☼10 Usec-Butylbenzene
10 4.4 ug/Kg 06/12/23 07:42 06/12/23 19:02 1☼10 Utert-Butylbenzene
10 4.2 ug/Kg 06/12/23 07:42 06/12/23 19:02 1☼10 UTetrachloroethene
10 3.7 ug/Kg 06/12/23 07:42 06/12/23 19:02 1☼10 Utrans-1,2-Dichloroethene
10 3.3 ug/Kg 06/12/23 07:42 06/12/23 19:02 1☼10 UTrichloroethene
10 7.5 ug/Kg 06/12/23 07:42 06/12/23 19:02 1☼10 UVinyl chloride
1,2-Dichloroethane-d4 (Surr) 117 73 - 135 06/12/23 07:42 06/12/23 19:02 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
4-Bromofluorobenzene (Surr) 104 06/12/23 07:42 06/12/23 19:02 160 - 124
Dibromofluoromethane (Surr) 114 06/12/23 07:42 06/12/23 19:02 169 - 126
Toluene-d8 (Surr) 97 06/12/23 07:42 06/12/23 19:02 167 - 134
Project/Site: Mattituck Harbor, NY
General Chemistry
Lab Sample ID: 180-157715-1Client Sample ID: #20230471A MC-9A Matrix: SedimentDate Collected: 06/07/23 10:22
Date Received: 06/08/23 09:15
RL MDL
52.9 0.1 0.1 % 06/15/23 10:46 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Percent Solids (SM22 2540G)
Project/Site: Mattituck Harbor, NY
General Chemistry
Lab Sample ID: 180-157715-2Client Sample ID: #20230471B MC-9B Matrix: SedimentDate Collected: 06/07/23 10:22
Date Received: 06/08/23 09:15
RL MDL
50.8 0.1 0.1 % 06/15/23 10:46 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Percent Solids (SM22 2540G)
Project/Site: Mattituck Harbor, NY
General Chemistry
Lab Sample ID: 180-157715-3Client Sample ID: #20230470A MC-8A Matrix: SedimentDate Collected: 06/07/23 11:37
Date Received: 06/08/23 09:15
RL MDL
31.1 0.1 0.1 % 06/15/23 10:46 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Percent Solids (SM22 2540G)
Project/Site: Mattituck Harbor, NY
General Chemistry
Lab Sample ID: 180-157715-4Client Sample ID: #20230470B MC-8B Matrix: SedimentDate Collected: 06/07/23 11:37
Date Received: 06/08/23 09:15
RL MDL
38.0 0.1 0.1 % 06/15/23 10:46 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Percent Solids (SM22 2540G)
Project/Site: Mattituck Harbor, NY
General Chemistry
Lab Sample ID: 180-157715-5Client Sample ID: #20230469A MC-7A Matrix: SedimentDate Collected: 06/07/23 12:55
Date Received: 06/08/23 09:15
RL MDL
44.9 0.1 0.1 % 06/15/23 10:46 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Percent Solids (SM22 2540G)
Project/Site: Mattituck Harbor, NY
General Chemistry
Lab Sample ID: 180-157715-6Client Sample ID: #20230469B MC-7B Matrix: SedimentDate Collected: 06/07/23 12:55
Date Received: 06/08/23 09:15
RL MDL
50.8 0.1 0.1 % 06/15/23 10:46 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Percent Solids (SM22 2540G)
Project/Site: Mattituck Harbor, NY
General Chemistry
Lab Sample ID: 180-157715-7Client Sample ID: #20230468A MC-6A Matrix: SedimentDate Collected: 06/07/23 13:47
Date Received: 06/08/23 09:15
RL MDL
36.5 0.1 0.1 % 06/15/23 10:46 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Percent Solids (SM22 2540G)
Project/Site: Mattituck Harbor, NY
General Chemistry
Lab Sample ID: 180-157715-8Client Sample ID: #20230468B MC-6B Matrix: SedimentDate Collected: 06/07/23 13:47
Date Received: 06/08/23 09:15
RL MDL
45.1 0.1 0.1 % 06/15/23 10:46 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Percent Solids (SM22 2540G)
Default Detection Limits Client: Battelle Job ID: 180-157715-1 Project/Site: Mattituck Harbor, NY
Method: EPA 8260D - Volatile Organic Compounds by GC/MS Prep: 5030C
5.01,1,1-Trichloroethane ug/Kg
Analyte UnitsMDLRL
1.7
5.01,1-Dichloroethane ug/Kg1.6
5.01,1-Dichloroethene ug/Kg2.3
5.01,2,4-Trimethylbenzene ug/Kg1.7
5.01,2-Dichlorobenzene ug/Kg1.7
5.01,2-Dichloroethane ug/Kg1.4
5.01,3,5-Trimethylbenzene ug/Kg1.9
5.01,3-Dichlorobenzene ug/Kg3.1
5.01,4-Dichlorobenzene ug/Kg1.5
10001,4-Dioxane ug/Kg76
252-Butanone (MEK) ug/Kg2.5
25Acetone ug/Kg3.9
5.0Benzene ug/Kg1.4
5.0Carbon tetrachloride ug/Kg2.0
5.0Chlorobenzene ug/Kg1.3
5.0Chloroform ug/Kg3.4
5.0cis-1,2-Dichloroethene ug/Kg1.5
5.0Ethylbenzene ug/Kg1.9
5.0Methyl tert-butyl ether ug/Kg1.5
5.0Methylene Chloride ug/Kg4.5
5.0n-Butylbenzene ug/Kg2.5
5.0N-Propylbenzene ug/Kg1.8
5.0sec-Butylbenzene ug/Kg2.5
5.0tert-Butylbenzene ug/Kg2.1
5.0Tetrachloroethene ug/Kg2.0
5.0Toluene ug/Kg1.4
5.0trans-1,2-Dichloroethene ug/Kg1.8
5.0Trichloroethene ug/Kg1.6
5.0Vinyl chloride ug/Kg3.6
10Xylenes, Total ug/Kg7.2
General Chemistry
0.1Percent Solids %
Analyte UnitsMDLRL
0.1
Surrogate Summary
Project/Site: Mattituck Harbor, NY
Method: EPA 8260D - Volatile Organic Compounds by GC/MS Prep Type: Total/NAMatrix: Sediment
Lab Sample ID Client Sample ID (73-135) (60-124) (69-126) (67-134)
DCA BFB DBFM TOL
104 92 99 84180-157715-1
Percent Surrogate Recovery (Acceptance Limits)
#20230471A MC-9A
107 97 102 86180-157715-2 #20230471B MC-9B
90 72 85 77180-157715-3 #20230470A MC-8A
95 95 94 89180-157715-3 MS #20230470A MC-8A
94 97 96 92180-157715-3 MSD #20230470A MC-8A
96 93 98 88180-157715-4 #20230470B MC-8B
99 95 100 90180-157715-5 #20230469A MC-7A
120 108 116 99180-157715-6 #20230469B MC-7B
116 99 107 91180-157715-7 #20230468A MC-6A
117 104 114 97180-157715-8 #20230468B MC-6B
86 95 92 94LCS 180-437636/4 Lab Control Sample
106 94 100 86MB 180-437636/8 Method Blank
Surrogate Legend
DCA = 1,2-Dichloroethane-d4 (Surr)
BFB = 4-Bromofluorobenzene (Surr)
DBFM = Dibromofluoromethane (Surr)
TOL = Toluene-d8 (Surr)
QC Sample Results
Project/Site: Mattituck Harbor, NY
Method: EPA 8260D - Volatile Organic Compounds by GC/MS
Client Sample ID: Method BlankLab Sample ID: MB 180-437636/8 Matrix: Sediment Prep Type: Total/NA Analysis Batch: 437636
RL MDL
1,1,1-Trichloroethane 5.0 U 5.0 1.7 ug/Kg 06/12/23 12:36 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
5.0 U 1.65.0 ug/Kg 06/12/23 12:36 11,1-Dichloroethane
5.0 U 1.45.0 ug/Kg 06/12/23 12:36 1Benzene
5.0 U 2.35.0 ug/Kg 06/12/23 12:36 11,1-Dichloroethene
5.0 U 1.75.0 ug/Kg 06/12/23 12:36 11,2,4-Trimethylbenzene
5.0 U 1.75.0 ug/Kg 06/12/23 12:36 11,2-Dichlorobenzene
5.0 U 1.45.0 ug/Kg 06/12/23 12:36 1Toluene
5.0 U 1.45.0 ug/Kg 06/12/23 12:36 11,2-Dichloroethane
10 U 7.210 ug/Kg 06/12/23 12:36 1Xylenes, Total
5.0 U 1.95.0 ug/Kg 06/12/23 12:36 11,3,5-Trimethylbenzene
5.0 U 3.15.0 ug/Kg 06/12/23 12:36 11,3-Dichlorobenzene
5.0 U 1.55.0 ug/Kg 06/12/23 12:36 11,4-Dichlorobenzene
1000 U 761000 ug/Kg 06/12/23 12:36 11,4-Dioxane
25 U 2.525 ug/Kg 06/12/23 12:36 12-Butanone (MEK)
25 U 3.925 ug/Kg 06/12/23 12:36 1Acetone
5.0 U 2.05.0 ug/Kg 06/12/23 12:36 1Carbon tetrachloride
5.0 U 1.35.0 ug/Kg 06/12/23 12:36 1Chlorobenzene
5.0 U 3.45.0 ug/Kg 06/12/23 12:36 1Chloroform
5.0 U 1.55.0 ug/Kg 06/12/23 12:36 1cis-1,2-Dichloroethene
5.0 U 1.95.0 ug/Kg 06/12/23 12:36 1Ethylbenzene
5.0 U 1.55.0 ug/Kg 06/12/23 12:36 1Methyl tert-butyl ether
5.0 U 4.55.0 ug/Kg 06/12/23 12:36 1Methylene Chloride
5.0 U 2.55.0 ug/Kg 06/12/23 12:36 1n-Butylbenzene
5.0 U 1.85.0 ug/Kg 06/12/23 12:36 1N-Propylbenzene
5.0 U 2.55.0 ug/Kg 06/12/23 12:36 1sec-Butylbenzene
5.0 U 2.15.0 ug/Kg 06/12/23 12:36 1tert-Butylbenzene
5.0 U 2.05.0 ug/Kg 06/12/23 12:36 1Tetrachloroethene
5.0 U 1.85.0 ug/Kg 06/12/23 12:36 1trans-1,2-Dichloroethene
5.0 U 1.65.0 ug/Kg 06/12/23 12:36 1Trichloroethene
5.0 U 3.65.0 ug/Kg 06/12/23 12:36 1Vinyl chloride
1,2-Dichloroethane-d4 (Surr) 106 73 - 135 06/12/23 12:36 1
MB MB
Surrogate Dil FacPrepared AnalyzedQualifier Limits%Recovery
94 06/12/23 12:36 14-Bromofluorobenzene (Surr) 60 - 124
100 06/12/23 12:36 1Dibromofluoromethane (Surr) 69 - 126
86 06/12/23 12:36 1Toluene-d8 (Surr) 67 - 134
Client Sample ID: Lab Control SampleLab Sample ID: LCS 180-437636/4 Matrix: Sediment Prep Type: Total/NA Analysis Batch: 437636
1,1,1-Trichloroethane 40.0 38.5 ug/Kg 96 72 - 134
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits
1,1-Dichloroethane 40.0 38.4 ug/Kg 96 73 - 124
Benzene 40.0 39.5 ug/Kg 99 77 - 120
1,1-Dichloroethene 40.0 40.3 ug/Kg 101 55 - 136
1,2,4-Trimethylbenzene 40.0 39.4 ug/Kg 99 74 - 127
1,2-Dichlorobenzene 40.0 36.4 ug/Kg 91 76 - 120
Project/Site: Mattituck Harbor, NY
Method: EPA 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 180-437636/4 Matrix: Sediment Prep Type: Total/NA Analysis Batch: 437636
Toluene 40.0 37.8 ug/Kg 95 76 - 120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits
1,2-Dichloroethane 40.0 35.1 ug/Kg 88 64 - 140
Xylenes, Total 80.0 75.0 ug/Kg 94 78 - 118
1,3,5-Trimethylbenzene 40.0 39.8 ug/Kg 99 69 - 131
1,3-Dichlorobenzene 40.0 37.5 ug/Kg 94 77 - 121
1,4-Dichlorobenzene 40.0 37.1 ug/Kg 93 79 - 120
2-Butanone (MEK) 40.0 32.9 ug/Kg 82 39 - 157
Acetone 40.0 44.7 ug/Kg 112 23 - 170
Carbon tetrachloride 40.0 36.2 ug/Kg 91 73 - 130
Chlorobenzene 40.0 36.9 ug/Kg 92 79 - 122
Chloroform 40.0 39.2 ug/Kg 98 73 - 126 cis-1,2-Dichloroethene 40.0 39.4 ug/Kg 98 77 - 118
Ethylbenzene 40.0 37.6 ug/Kg 94 79 - 119
Methyl tert-butyl ether 40.0 32.9 ug/Kg 82 58 - 132
Methylene Chloride 40.0 41.8 ug/Kg 104 67 - 131 n-Butylbenzene 40.0 40.1 ug/Kg 100 64 - 136
N-Propylbenzene 40.0 39.0 ug/Kg 97 71 - 127 sec-Butylbenzene 40.0 39.7 ug/Kg 99 65 - 130 tert-Butylbenzene 40.0 38.3 ug/Kg 96 69 - 133
Tetrachloroethene 40.0 37.6 ug/Kg 94 71 - 121 trans-1,2-Dichloroethene 40.0 39.7 ug/Kg 99 75 - 122
Trichloroethene 40.0 38.2 ug/Kg 95 69 - 118
Vinyl chloride 40.0 43.5 ug/Kg 109 64 - 134
1,2-Dichloroethane-d4 (Surr) 73 - 135
Surrogate
LCS LCS
Qualifier Limits%Recovery
954-Bromofluorobenzene (Surr) 60 - 124
92Dibromofluoromethane (Surr) 69 - 126
94Toluene-d8 (Surr) 67 - 134
Client Sample ID: #20230470A MC-8ALab Sample ID: 180-157715-3 MS Matrix: Sediment Prep Type: Total/NA Analysis Batch: 437636 Prep Batch: 437679
1,1,1-Trichloroethane 15 U 121 112 ug/Kg 92 72 - 134☼
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
1,1-Dichloroethane 15 U 121 112 ug/Kg 92 73 - 124☼
Benzene 15 U 121 116 ug/Kg 96 77 - 120☼
1,1-Dichloroethene 15 U 121 116 ug/Kg 96 55 - 136☼
1,2,4-Trimethylbenzene 15 U 121 108 ug/Kg 89 74 - 127☼
1,2-Dichlorobenzene 15 U 121 110 ug/Kg 91 76 - 120☼
Toluene 15 U 121 108 ug/Kg 89 76 - 120☼
1,2-Dichloroethane 15 U 121 116 ug/Kg 96 64 - 140☼
Xylenes, Total 30 U 242 212 ug/Kg 87 78 - 118☼
1,3,5-Trimethylbenzene 15 U 121 109 ug/Kg 90 69 - 131☼
1,3-Dichlorobenzene 15 U 121 108 ug/Kg 89 77 - 121☼
1,4-Dichlorobenzene 15 U 121 107 ug/Kg 88 79 - 120☼
2-Butanone (MEK) 75 U 121 137 ug/Kg 113 39 - 157☼
Project/Site: Mattituck Harbor, NY
Method: EPA 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: #20230470A MC-8ALab Sample ID: 180-157715-3 MS Matrix: Sediment Prep Type: Total/NA Analysis Batch: 437636 Prep Batch: 437679
Acetone 75 U F2 121 172 ug/Kg 142 23 - 170☼
Analyte
MS MS
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits
Carbon tetrachloride 15 U 121 106 ug/Kg 88 73 - 130☼
Chlorobenzene 15 U 121 107 ug/Kg 89 79 - 122☼
Chloroform 15 U 121 118 ug/Kg 97 73 - 126☼ cis-1,2-Dichloroethene 15 U 121 115 ug/Kg 95 77 - 118☼
Ethylbenzene 15 U 121 107 ug/Kg 88 79 - 119☼
Methyl tert-butyl ether 15 U 121 117 ug/Kg 96 58 - 132☼
Methylene Chloride 15 U 121 121 ug/Kg 100 67 - 131☼ n-Butylbenzene 15 U 121 110 ug/Kg 90 64 - 136☼
N-Propylbenzene 15 U 121 106 ug/Kg 87 71 - 127☼ sec-Butylbenzene 15 U 121 107 ug/Kg 88 65 - 130☼ tert-Butylbenzene 15 U 121 105 ug/Kg 87 69 - 133☼
Tetrachloroethene 15 U 121 105 ug/Kg 87 71 - 121☼ trans-1,2-Dichloroethene 15 U 121 115 ug/Kg 95 75 - 122☼
Trichloroethene 15 U 121 110 ug/Kg 91 69 - 118☼
Vinyl chloride 15 U 121 122 ug/Kg 101 64 - 134☼
1,2-Dichloroethane-d4 (Surr) 73 - 135
Surrogate
MS MS
Qualifier Limits%Recovery
954-Bromofluorobenzene (Surr) 60 - 124
94Dibromofluoromethane (Surr) 69 - 126
89Toluene-d8 (Surr) 67 - 134
Client Sample ID: #20230470A MC-8ALab Sample ID: 180-157715-3 MSD Matrix: Sediment Prep Type: Total/NA Analysis Batch: 437636 Prep Batch: 437679
1,1,1-Trichloroethane 15 U 118 111 ug/Kg 94 72 - 134 1 20☼
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits LimitRPD
RPD
1,1-Dichloroethane 15 U 118 111 ug/Kg 94 73 - 124 1 20☼
Benzene 15 U 118 114 ug/Kg 97 77 - 120 2 20☼
1,1-Dichloroethene 15 U 118 116 ug/Kg 98 55 - 136 0 21☼
1,2,4-Trimethylbenzene 15 U 118 108 ug/Kg 92 74 - 127 0 20☼
1,2-Dichlorobenzene 15 U 118 108 ug/Kg 92 76 - 120 1 20☼
Toluene 15 U 118 106 ug/Kg 90 76 - 120 2 20☼
1,2-Dichloroethane 15 U 118 111 ug/Kg 94 64 - 140 5 20☼
Xylenes, Total 30 U 235 213 ug/Kg 90 78 - 118 0 20☼
1,3,5-Trimethylbenzene 15 U 118 109 ug/Kg 92 69 - 131 0 20☼
1,3-Dichlorobenzene 15 U 118 107 ug/Kg 90 77 - 121 1 20☼
1,4-Dichlorobenzene 15 U 118 106 ug/Kg 90 79 - 120 1 20☼
2-Butanone (MEK) 75 U 118 111 ug/Kg 94 39 - 157 21 33☼
Acetone 75 U F2 118 120 F2 ug/Kg 102 23 - 170 36 35☼
Carbon tetrachloride 15 U 118 105 ug/Kg 90 73 - 130 1 21☼
Chlorobenzene 15 U 118 105 ug/Kg 89 79 - 122 2 20☼
Chloroform 15 U 118 115 ug/Kg 98 73 - 126 2 20☼ cis-1,2-Dichloroethene 15 U 118 115 ug/Kg 98 77 - 118 0 20☼
Ethylbenzene 15 U 118 106 ug/Kg 90 79 - 119 1 20☼
Methyl tert-butyl ether 15 U 118 111 ug/Kg 95 58 - 132 5 24☼
Project/Site: Mattituck Harbor, NY
Method: EPA 8260D - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: #20230470A MC-8ALab Sample ID: 180-157715-3 MSD Matrix: Sediment Prep Type: Total/NA Analysis Batch: 437636 Prep Batch: 437679
Methylene Chloride 15 U 118 118 ug/Kg 100 67 - 131 3 32☼
Analyte
MSD MSD
DUnitResult Qualifier %Rec
Spike
Added
Sample
Result
Sample
Qualifier
%Rec
Limits LimitRPD
RPD
n-Butylbenzene 15 U 118 110 ug/Kg 94 64 - 136 1 21☼
N-Propylbenzene 15 U 118 106 ug/Kg 90 71 - 127 0 20☼ sec-Butylbenzene 15 U 118 109 ug/Kg 92 65 - 130 2 20☼ tert-Butylbenzene 15 U 118 105 ug/Kg 89 69 - 133 0 23☼
Tetrachloroethene 15 U 118 104 ug/Kg 89 71 - 121 1 21☼ trans-1,2-Dichloroethene 15 U 118 115 ug/Kg 98 75 - 122 0 20☼
Trichloroethene 15 U 118 109 ug/Kg 92 69 - 118 1 20☼
Vinyl chloride 15 U 118 123 ug/Kg 104 64 - 134 0 23☼
1,2-Dichloroethane-d4 (Surr) 73 - 135
Surrogate
MSD MSD
Qualifier Limits%Recovery
974-Bromofluorobenzene (Surr) 60 - 124
96Dibromofluoromethane (Surr) 69 - 126
92Toluene-d8 (Surr) 67 - 134
QC Association Summary
Project/Site: Mattituck Harbor, NY
GC/MS VOA
Analysis Batch: 437636
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Sediment EPA 8260D 437679180-157715-1 #20230471A MC-9A Total/NA
Sediment EPA 8260D 437679180-157715-2 #20230471B MC-9B Total/NA
Sediment EPA 8260D 437679180-157715-3 #20230470A MC-8A Total/NA
Sediment EPA 8260D 437679180-157715-4 #20230470B MC-8B Total/NA
Sediment EPA 8260D 437679180-157715-5 #20230469A MC-7A Total/NA
Sediment EPA 8260D 437679180-157715-6 #20230469B MC-7B Total/NA
Sediment EPA 8260D 437679180-157715-7 #20230468A MC-6A Total/NA
Sediment EPA 8260D 437679180-157715-8 #20230468B MC-6B Total/NA
Sediment EPA 8260DMB 180-437636/8 Method Blank Total/NA
Sediment EPA 8260DLCS 180-437636/4 Lab Control Sample Total/NA
Sediment EPA 8260D 437679180-157715-3 MS #20230470A MC-8A Total/NA
Sediment EPA 8260D 437679180-157715-3 MSD #20230470A MC-8A Total/NA
Prep Batch: 437679
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Sediment 5030C180-157715-1 #20230471A MC-9A Total/NA
Sediment 5030C180-157715-2 #20230471B MC-9B Total/NA
Sediment 5030C180-157715-3 #20230470A MC-8A Total/NA
Sediment 5030C180-157715-4 #20230470B MC-8B Total/NA
Sediment 5030C180-157715-5 #20230469A MC-7A Total/NA
Sediment 5030C180-157715-6 #20230469B MC-7B Total/NA
Sediment 5030C180-157715-7 #20230468A MC-6A Total/NA
Sediment 5030C180-157715-8 #20230468B MC-6B Total/NA
Sediment 5030C180-157715-3 MS #20230470A MC-8A Total/NA
Sediment 5030C180-157715-3 MSD #20230470A MC-8A Total/NA
General Chemistry
Analysis Batch: 438071
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Sediment 2540G180-157715-1 #20230471A MC-9A Total/NA
Sediment 2540G180-157715-2 #20230471B MC-9B Total/NA
Sediment 2540G180-157715-3 #20230470A MC-8A Total/NA
Sediment 2540G180-157715-4 #20230470B MC-8B Total/NA
Sediment 2540G180-157715-5 #20230469A MC-7A Total/NA
Sediment 2540G180-157715-6 #20230469B MC-7B Total/NA
Sediment 2540G180-157715-7 #20230468A MC-6A Total/NA
Sediment 2540G180-157715-8 #20230468B MC-6B Total/NA
Lab Chronicle
Project/Site: Mattituck Harbor, NY
Client Sample ID: #20230471A MC-9A Lab Sample ID: 180-157715-1 Matrix: SedimentDate Collected: 06/07/23 10:22
Date Received: 06/08/23 09:15
Analysis 2540G RSK06/15/23 10:461 EET PIT438071
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID: NOEQUIP
Client Sample ID: #20230471A MC-9A Lab Sample ID: 180-157715-1 Matrix: SedimentDate Collected: 06/07/23 10:22
Percent Solids: 52.9Date Received: 06/08/23 09:15
Prep 5030C PJJ06/12/23 07:42 EET PIT437679
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.3086 g 5 mL
Analysis EPA 8260D 1 437636 06/12/23 16:00 PJJ EET PITTotal/NA 5 mL 5 mL
CHHP3Instrument ID:
Client Sample ID: #20230471B MC-9B Lab Sample ID: 180-157715-2 Matrix: SedimentDate Collected: 06/07/23 10:22
Date Received: 06/08/23 09:15
Analysis 2540G RSK06/15/23 10:461 EET PIT438071
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID: NOEQUIP
Client Sample ID: #20230471B MC-9B Lab Sample ID: 180-157715-2 Matrix: SedimentDate Collected: 06/07/23 10:22
Percent Solids: 50.8Date Received: 06/08/23 09:15
Prep 5030C PJJ06/12/23 07:42 EET PIT437679
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.2236 g 5 mL
Analysis EPA 8260D 1 437636 06/12/23 17:08 PJJ EET PITTotal/NA 5 mL 5 mL
CHHP3Instrument ID:
Client Sample ID: #20230470A MC-8A Lab Sample ID: 180-157715-3 Matrix: SedimentDate Collected: 06/07/23 11:37
Date Received: 06/08/23 09:15
Analysis 2540G RSK06/15/23 10:461 EET PIT438071
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID: NOEQUIP
Client Sample ID: #20230470A MC-8A Lab Sample ID: 180-157715-3 Matrix: SedimentDate Collected: 06/07/23 11:37
Percent Solids: 31.1Date Received: 06/08/23 09:15
Prep 5030C PJJ06/12/23 07:42 EET PIT437679
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.3326 g 5 mL
Analysis EPA 8260D 1 437636 06/12/23 15:38 PJJ EET PITTotal/NA 5 mL 5 mL
CHHP3Instrument ID:
Project/Site: Mattituck Harbor, NY
Client Sample ID: #20230470B MC-8B Lab Sample ID: 180-157715-4 Matrix: SedimentDate Collected: 06/07/23 11:37
Date Received: 06/08/23 09:15
Analysis 2540G RSK06/15/23 10:461 EET PIT438071
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID: NOEQUIP
Client Sample ID: #20230470B MC-8B Lab Sample ID: 180-157715-4 Matrix: SedimentDate Collected: 06/07/23 11:37
Percent Solids: 38.0Date Received: 06/08/23 09:15
Prep 5030C PJJ06/12/23 07:42 EET PIT437679
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.0462 g 5 mL
Analysis EPA 8260D 1 437636 06/12/23 17:32 PJJ EET PITTotal/NA 5 mL 5 mL
CHHP3Instrument ID:
Client Sample ID: #20230469A MC-7A Lab Sample ID: 180-157715-5 Matrix: SedimentDate Collected: 06/07/23 12:55
Date Received: 06/08/23 09:15
Analysis 2540G RSK06/15/23 10:461 EET PIT438071
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID: NOEQUIP
Client Sample ID: #20230469A MC-7A Lab Sample ID: 180-157715-5 Matrix: SedimentDate Collected: 06/07/23 12:55
Percent Solids: 44.9Date Received: 06/08/23 09:15
Prep 5030C PJJ06/12/23 07:42 EET PIT437679
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.1349 g 5 mL
Analysis EPA 8260D 1 437636 06/12/23 17:54 PJJ EET PITTotal/NA 5 mL 5 mL
CHHP3Instrument ID:
Client Sample ID: #20230469B MC-7B Lab Sample ID: 180-157715-6 Matrix: SedimentDate Collected: 06/07/23 12:55
Date Received: 06/08/23 09:15
Analysis 2540G RSK06/15/23 10:461 EET PIT438071
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID: NOEQUIP
Client Sample ID: #20230469B MC-7B Lab Sample ID: 180-157715-6 Matrix: SedimentDate Collected: 06/07/23 12:55
Percent Solids: 50.8Date Received: 06/08/23 09:15
Prep 5030C PJJ06/12/23 07:42 EET PIT437679
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.3306 g 5 mL
Analysis EPA 8260D 1 437636 06/12/23 18:17 PJJ EET PITTotal/NA 5 mL 5 mL
CHHP3Instrument ID:
Project/Site: Mattituck Harbor, NY
Client Sample ID: #20230468A MC-6A Lab Sample ID: 180-157715-7 Matrix: SedimentDate Collected: 06/07/23 13:47
Date Received: 06/08/23 09:15
Analysis 2540G RSK06/15/23 10:461 EET PIT438071
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID: NOEQUIP
Client Sample ID: #20230468A MC-6A Lab Sample ID: 180-157715-7 Matrix: SedimentDate Collected: 06/07/23 13:47
Percent Solids: 36.5Date Received: 06/08/23 09:15
Prep 5030C PJJ06/12/23 07:42 EET PIT437679
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.0795 g 5 mL
Analysis EPA 8260D 1 437636 06/12/23 18:39 PJJ EET PITTotal/NA 5 mL 5 mL
CHHP3Instrument ID:
Client Sample ID: #20230468B MC-6B Lab Sample ID: 180-157715-8 Matrix: SedimentDate Collected: 06/07/23 13:47
Date Received: 06/08/23 09:15
Analysis 2540G RSK06/15/23 10:461 EET PIT438071
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Instrument ID: NOEQUIP
Client Sample ID: #20230468B MC-6B Lab Sample ID: 180-157715-8 Matrix: SedimentDate Collected: 06/07/23 13:47
Percent Solids: 45.1Date Received: 06/08/23 09:15
Prep 5030C PJJ06/12/23 07:42 EET PIT437679
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5.3043 g 5 mL
Analysis EPA 8260D 1 437636 06/12/23 19:02 PJJ EET PITTotal/NA 5 mL 5 mL
CHHP3Instrument ID:
Laboratory References:
EET PIT = Eurofins Pittsburgh, 301 Alpha Drive, RIDC Park, Pittsburgh, PA 15238, TEL (412)963-7058
Analyst References:
Lab: EET PIT
Batch Type: Prep
PJJ = Patrick Journet
Batch Type: Analysis
PJJ = Patrick Journet
RSK = Robert Kurtz
Accreditation/Certification Summary
Project/Site: Mattituck Harbor, NY
Laboratory: Eurofins Pittsburgh Unless otherwise noted, all analytes for this laboratory were covered under each accreditation/certification below.
Authority Program Identification Number Expiration Date
New Jersey NELAP PA005 06-25-23
The following analytes are included in this report, but the laboratory is not certified by the governing authority. This list may include analytes for which the agency does not offer certification.
Analysis Method Prep Method Matrix Analyte
2540G Sediment Percent Solids
New York NELAP 11182 06-25-23
The following analytes are included in this report, but the laboratory is not certified by the governing authority. This list may include analytes for which the agency does not offer certification.
Analysis Method Prep Method Matrix Analyte
2540G Sediment Percent Solids
Method Summary
Project/Site: Mattituck Harbor, NY
Method Method Description…
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