Attachment D ENERGY E QAPs Portfolio_CF.pdf

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Attachment J – ENERGY E‐QAPs

NOTE: The E QAPs are attached to this PDF Portfolio

SPE605-23-R-0211

Source Selection Information –See FAR 2.101 and 3.104

STURGEON.STEVEN.A

LAN.JR.1009816565

Digitally signed by

STURGEON.STEVEN.ALAN.JR.1009816565

Date: 2022.03.28 15:50:06 -04'00'

MILLS.KEITH.10501831

MILLS.KEITH.1050183110

Date: 2022.03.28 15:34:49 -04'00'

HEIDBREDER.MICHAE

L.G.1139641082

HEIDBREDER.MICHAEL.G.1139641082

Date: 2022.03.28 15:27:41 -04'00'

(March 2022)

TABLE I, Sample Retention1

LOCATION MINIMUM QUANTITY RETENTION PERIOD 1

Bulk Tank Cars/Tank Truck/Intermodal Container

Additives 0.5-gallon (2 liters)2 Until receipt and quality verification of each lot/batch

Fuels 1 gallon (3 liters) 2 15 days for fuels/45 days for lubricating oils

Lubricating Oils 0.25 gallons (1 liter) 2

AVGAS Drums 0,25 gallons (1 liter) (multi-drum composite) 3 45 days

Shipping Tank(s)

2 gallons (8 liters) for Aviation Turbine Fuels 1 gallon (3 liters) for all other Fuels, Lubricating Oils, and Additives

45 days

Tanker/Barge/Pipeline (Composite Line at Custody Transfer Point)

2 gallon (8 liters) for Aviation Turbine

1 gallon (3 liters) for all other Fuels

Tanker/Barge (Composite)

F.O.B. Origin 2 gallons (8 liters) for Aviation Turbine

1 gallon (3 liters) for all other fuels

F.O.B. Destination 2 gallons (8 liters) Until shore tests on-specification Tanker/Barge (Each Compartment)

F.O.B. Origin 1 gallon (3 liters) 45 days F.O.B. Destination 1 gallon (3 liters) Until shore test on-specification

NOTES:

1. Unless otherwise noted in this document or applicable contract, the retention period shall be for the stated number of days after the sample has been taken from the location indicated.

2. If the conveyance is compartmentalized, a proportional sample shall be taken from each compartment such that a total of one liter is collected from the conveyance.

3. A one-liter composite sample of each product lot shall be taken from a predetermined number of randomly selected drums IAW Table III of API MPSM, Chapter 8.1 (ASTM D 4057).

TABLE II, Minimum Sampling and Testing Requirements for Petroleum Products Series 1, 1,13

ITEM WHEN TO SAMPLE LOCATION OF SAMPLE TYPE OF SAMPLE2 TEST REQUIRED3

1.a Prior to Loading

Before acceptance of new materiel and after establishment of new batch4

(Procurement) Each shore storage tank Single Tank Composite or All

Levels A

1.b Prior to loading (Government Stock) Each shore storage tank Single Tank Composites or All

Levels B-11, 5

1.c After line pack but prior to loading

(Procurement & Government Stock) As close to the custody transfer point as possible Line Sample C6,7 Dedicated System B-1 Non-Dedicated System

1.d In coordination with vessel crew (Procurement & Government Stock) Each vessel cargo compartment Manual method or onboard ship equipment Gauge or Ullage Report (Dry

Tanks) 1.e D uring Loading

After first in 9 (Procurement) Vessel cargo compartment(s) Spot C6,7,8 1.f After first in 9(Government Stock) Vessel cargo compartment(s) Spot Appearance and Density6,7,8

1.g After first in 9

(Replenishment at sea) Each vessel cargo compartment Spot C6,7,8

1.h During loading

As close to the custody transfer point as possible Line Sample Hourly Visual6,8, Retain10

Discard retain after passing 1.j tests

1.i

A fter Loading

After loading

Each vessel cargo compartment

All Level (Combine All Levels into one

Multiple Compartment Composite Sample)

C 6,11

Remainder of B-112

(Retain fuel for B-1 referee testing)

1. Additional requirements to include retain samples may be required. See Quality Assurance Provisions (C or E-QAP) for further details or DFSP QCP.

2. Refer to ASTM International D4057 for sampling procedures.

3. Test results shall be compared against the quality release certificate. Any discrepancies shall be identified, investigated, and resolved.

4. Upon procurement at refineries, blending installations, etc. and at main installations including national depots & ocean importing points on establishment of new batches.

5. Government-owned stocks previously tested at any type B level test within 90 days need only type C (test FSII & SDA if present).

6. Test for FSII and SDA only if line injected.

7. If sample fails appearance (see 5.11.4.3) perform particulate matter IAW 5.2.1.10.1. Maximum particulate IAW Table I.

8. Lubricity also required for F-76 only if line injected.

9. First in shall be done after one (1) meter or after line displacement whichever is the greater.

10. For all tanker, barge, and pipeline shipments, a flow-proportional sample taken in accordance with MPMS Chapter 8, Section 2, is preferred at the custody transfer point. However, manual samples taken in accordance with MPMS Chapter 8, Section 1 are acceptable if they are taken hourly throughout the shipment and that the quantity of the composite sample meets the requirements in QAP E-1. For Government Shipments, pull a 1-quart sample hourly and retain until passing of 1.j B-1 tests.

11. Vessel may sail after “C” Tests; Remainder of B-1 tests to be completed before arrival at next load or discharge port. Test report will be provided to designated discharge port.

12. Type A level testing required for FOB Destination Procurements (unless otherwise specified by contract).

13. If a YON is being used as a barge, the QA requirements for waterborne transfer of petroleum products must be observed.

Series 2, 1,8

ITEM WHEN TO SAMPLE LOCATION OF SAMPLE TYPE OF SAMPLE 2 TEST REQUIRED3

2.a

Prior to Shipm ent

Before acceptance of new materiel and after establishment of new batch4

(Procurement) Each Shipment Storage Tank Single Tank Composite or All Levels A10

2.b Prior to shipment (Government Stock) Each Shipment Storage Tank Single Tank Composite or All Levels B-15

2.c After line pack but prior to loading/shipment

As close to the custody transfer point as possible Line Sample C6,7 Dedicated System

B-1 Non-Dedicated System

2.d

D uring Shipm ent

Immediately after start of loading/shipment

Downstream of the filter separator (if equipped) or closest to the custody transfer point as possible Line Sample C6

2.e Hourly after start of loading or shipment

Pipeline Only point as possible Line Sample

Apperance6

(Retain fuel for B-1 referee testing)

2.f

Daily on first fill and anytime a new tank is placed on issue (after line displacement) TT, TC, ISO, Refuelers or other over the road transportation modes only point as possible (Loading Rack or Fill Point)

Line Sample Color (by visual method) and Appearance6.

If visual fails perform C7

2.g fter Loading

Daily for each conveyance mode *Not required for pipeline operations

Each Cargo Compartment or another point that provides a representative sample All Level

Appearance on each compartment

C on composite 6,7,9

1. Additional contractual requirements to include retain samples may be required. See Contract Quality Assurance Plans (C or E-QAPs) for further details

2. Refer to ASTM International D4057 for sampling procedures.

3. Test results shall be compared against the quality release certificate. Any discrepancies shall be identified, investigated, and resolved.

4. Upon procurement at refineries, blending installations, etc., and at main installations including national depots & ocean importing points on establishment of new batches.

5. Government-owned stocks that have been tested previously at any type B level test within 90 days need only type C (test FSII & SDA if present. Test for lubricity for F-76 when LIA is injected outbound only).

6. Test for FSII and SDA only if line injected.

7. If sample fails appearance (see 5.11.4.3), perform particulate matter IAW ¶ 5.2.1.10.1. Maximum particulate IAW IGRL

8. Type A level testing required for FOB Destination Procurements (unless otherwise specified by contract).

9. Road tank truck vehicles with multiple compartments shall have a 1-quart representative sample obtained from each compartment.

10. Filtration time testing is required for JP-4, JP-5 & JP-8 and shall meet MIL-STD-3004-1 Table I or contract requirement, whichever is more stringent.

Series 3, product receipt and discharges for tankers and barges6, 7, 8, 10

ITEM WHEN TO SAMPLE LOCATION OF SAMPLE TYPE OF SAMPLE TEST REQUIRED

3.a

Prior to D ischarge

Prior to discharge (Multi Product Cargo)

From each vessel cargo compartment All Level Appearance and Density1,2

3.b From each vessel cargo compartment

(Combine All Levels into one

B-13

3.c (Single Product Cargo) (Procurement & Government Stock) From each vessel cargo compartment

(Combine All Levels into one

C4,5

3.d D uring

Within 30 minutes after start and each hour after until completion

Dock/Discharge Manifold Header Line Sample / Retain

Perform Appearance test5,9 and then retain fuel for

Referee testing

3.e At 1 hour after start, Midpoint and 1 hour prior to completion

Dock/Discharge Manifold Header Line Sample Particulate (if applicable)

3.f A fter

After receipt by waterborne vessel (Procurement & Government Stock) Receipt tank All Level B-1

3.g If remainder of fuel will be shipped to another DFSP

Each vessel compartment with fuel remaining on board All Level Retain until discharged at next destination

1. Test for flash point on high flash cargo tanks if low and high flash cargoes are carried together aboard the same vessel without segregated venting systems

2. If on-spec, discharge is authorized.

3. It is preferred that B-1 testing is completed before discharge. In the event capabilities do not exist or time does not allow, the vessel can be discharged once appearance and density testing is completed on each compartment per Table IX 3.a, and C5 testing on the volumetric composite in 3.b. If B-1 testing is not completed prior to discharge, volumetric composite for 3b. shall be retained until receiving tank testing passes. Once discharging is completed, a B-1 test will be performed on the receiving tanks per Table IX 3.i. If receiving tank fails, a B-1 will be performed on retained fuel.

4. Discharge is authorized after conformance with type C tests, and the provisions of Section 5.1.3.1 are met. Retain composite sample until the receiving tank analysis is complete. If product fails, perform B-1 tests on retain composite to help determine the cause of the off-specification problem.

5. For aviation fuel delivery, FSII and SDA shall be tested only if line injected. This requires an additional quart sample.

6. Refer to ASTM International D4057 for sampling procedures.

7. Flash Point at the receiving point is not required for product used by the U.S. Army. This fuel is tested IAW Petroleum Laboratory Operations (TM 4-43.31)

8. Type A level testing required for FOB Destination Procurements (unless otherwise specified by contract).

9. Test for additives if line injected downstream of the injector. (If line injecting LIA into F-76, test for lubricity.)

10. If a YON is being used as a barge, the QA requirements for waterborne transfer of petroleum products must be observed.

TABLE III, Tests required aviation gasoline3

PROPERTIES B-1 TEST B-2 TEST B-3 TEST C TEST

Appearance 1,2 X X X X

Color (Visual) X X X X Density or API gravity X X X X Distillation X X X Copper strip corrosion X X X Existent gum X X Vapor pressure X X Free water determination2 X X X Lead content X X Potential gum X Color (Saybolt)

Freeze Point

Knock Value Total Sulfur Oxidation Stability

1. Obtain sample in a clear round 1 quart glass bottle, swirl the bottle vigorously so a vortex is formed. Visually check for sediment at the point of the vortex. If sediment is visible, an investigation is necessary in order to determine the source of the contaminant (a spot larger than 3 mm diameter indicates corrective action may be required to prevent the delivery of contaminated fuel).

2. AVGAS samples shall be checked for particulate and water. Particulate shall be determined visually upstream of filter separators and/or by the particle assessment method downstream of the filter separator. Free water shall be determined downstream of filter separator using a water detector (AEL Aqua-Glo test method or Hydro-Light).

3. For determining correct testing results (rounding protocol) see 4.2.2.2.1 Testing Rounding Protocol

TABLE IV, Tests required for aviation turbine 7

Appearance 1 X X X X Color (visual) X X X X Density or API gravity X X X X Particulate matter X X X Distillation X X X Copper strip corrosion X X X Freezing point X X X Existent gum X X X Vapor pressure (JP-4 only) X X X Flash point (except JP-4) 11 X X X X Water reaction2 Lead content (If contaminated with leaded fuels suspected)

X X X

Fuel system icing inhibitor 3 X X X Filtration time X X X

MSEP (JP-4, JP-8, F-24, F-27, Jet A & Jet A-1) 4,5

Conductivity (JP-4 and JP-8, F-24, F-27 & Jet A-1) 6

Thermal stability (B-1 requirement applies only to JPTS and marine/multi-product mode receipt tank sample)10

X X

Color (Saybolt) X

Acid number X

Peroxide Number 8 X

Fatty Acid Methyl Ester (FAME) 9 X X X

1. Obtain sample in a clear round 1 quart glass bottle, swirl the bottle vigorously so a vortex is formed. Visually check for sediment at the point of the vortex. If sediment is visible, an investigation is necessary to determine the source of the contaminant (a spot larger than 3 mm diameter indicates corrective action may be required to prevent the delivery of contaminated fuel).

2. Optional or at the request of Service Control Point.

3. If product contains FSII, product shall be checked on delivery into a bulk storage tank and every month thereafter.

4. If the capability does not exist to perform this test at the terminal, send sample to the nearest Service laboratory that has capability. In the event operational necessity dictates issue of product before results are obtained from the Service laboratory, shipments may be made, however, when laboratory results indicate failure, notify DLA Energy Quality Operations Division.

5. In all cases where MSEP is measured, conductivity will also be measured using ASTM D2624. For unadditized Jet A that is injected outbound of a facility an MSEP shall be performed using either D7224 or D8073 where possible. If either method is not available testing may be conducted with D3948. Passing results for D3948 will be considered acceptable. Failing fuels shall be retested using D7224 or D8073. If the fuel passes D7224 with a minimum limit of 85 or D8073 with a limit of 88 the fuel is considered to be acceptable with no further action. If the fuel fails D7224 or D8073, an investigation shall be performed.

6. If fuel contains conductivity additive, wait approximately 2 minutes after obtaining sample for charges in the fuel to dissipate before performing CU testing.

7. For determining correct reporting of test results (rounding protocol) see 4.2.2.2.1 Testing Rounding Protocol

8. Only applicable to Jet A use by the Navy.

9. Only for product transported through multi-product systems, including marine transport.

10. For JPTS: Ellipsometer (ETR) or Interferometer (ITR) IAW QAP C16.08-13. ETR is the referee. For all other fuels, follow specification requirements (excluding MSC chartered/contracted tankers and barges in dedicated/long term service).

11. Flash Point at the receiving point is not required for product used by the U.S. Army. This fuel is tested in accordance with Petroleum Laboratory Operations (TM 4-43.31).

TABLE V, Support for secure fuel 4

JP-5 Jet A Jet A-1 7 JP-8 F-24 Min. Max. Min. Max. Min. Max. Min. Max. Min. Max.

Appearance 2 C&B C&B C&B C&B C&B C&B C&B C&B C&B C&B

Gravity, API @ 60 °F D1298/D4052 36.0 48.0 37.0 51.0 37.0 51.0 37.0 51.0 37.0 51.0

Density at 15°C (kg/m3) 788 845 775 840 775 840 775 840 775 840 Weight: lb/USG Calculated 6.6 7.0 6.5 7.0 6.5 7.0 6.5 7.0 6.5 7.0 Distillation (°C) D86 3

10% Recovered 205 205 205 205 205 20% Recovered Report Report 50% Recovered Report Report Report Report Report 90% Recovered Report Report Report Report Report Final Boiling Point 300 300 300 300 300 Freezing point, °C D5972/D2386

-46

-40

-47

-47

-40

Flash point, °C D93/D56 60 38 38 38 38

Particulate Matter (mg/L) D2276, D5452, MIL- DTL- 83133

0.5

Conductivity (pS/m) D2624 Report Report 50 700 50 700 Copper strip corrosion D130 No.1 No.1 No.1 No.1 No.1 Existent gum (mg/100 mL) D381 7 7 7 7 7 FSII, (vol %) D5006 1 0.07 0.20 0.04 0.15 0.04 0.15 Thermal Stability D3241

Change in pressure drop, mm Hg 25 25 25 25 25 One of the tube deposit rating methods shall be run:

(1) Ellipsometer (ETR) 6 (nm) or Interferometer (ITR) (nm)

(2) Heater tube deposit, Visual Tube Rating

(VTR)

< 3

< 3 < 3 < 3 < 3

Fatty Acid Methyl Ester (FAME) 5

1. Only use FSII meeting specification MIL-DTL-85470, Inhibitor, Icing, Fuel System, High Flash, NATO Code S-1745.

2. Fuel shall be clear, bright, and free of water and sediment on visual examination. Sample will be taken downstream of final filtration on refueler or hydrant servicing equipment.

3. Distillation property criteria are specified in ASTM D86 scale units. ASTM D2887 results shall be converted to estimated D86 results by application of the correlation in Appendix X4, “Correlation for Jet and Diesel Fuel (Procedures A and B)” of D2887 for comparison with the specified property criteria. Distillation residue and loss limits provide control of the distillation process during the D86 test method and do not apply to D2887.

4. Alternate test methods may be performed provided they are authorized by the specification of the product being tested. Referee test methods are preferred.

5. Only for product transported through multi-product systems. FAME (fatty acid methyl esters) is defined as material meeting the limits of EN14214 or ASTM D6751. FAME that fails to meet the biodiesel quality standards are not permitted in aviation turbine fuel.

6. Tube deposit rating shall be measured by ASTM D3241 ETR Ellipsometer (ETR), when available: otherwise, use Interferometer (ITR) or visual (VTR). ETR shall be the referee procedure, otherwise ITR.

7. DEF STAN 91-091, ASTM D1655 and GOST R 52050 are acceptable.

TABLE VI, Tests required for automotive gasoline

Appearance X X X X Color (Visual) X X X X Water and Particulate (Visual Check) X X X X Density or API gravity X X X X Distillation X X X

Vapor pressure X X

Copper strip corrosion X X Unwashed gum/Solvent-washed gum X X 1 Knock rating (RON and MON) X 2 X 2 Oxidation stability X

1. Unwashed gum, without solvent wash, shall not increase by more than 2 mg as compared to the original product. In the event of gum increase exceeding 2 mg, run type A test as defined in the legend.

2. Perform only if Lead Content is performed and fails and/or contamination with another product is suspected. In the case of pipeline, this test shall be performed when considered necessary.

TABLE VII, Tests required for E85 (ASTM D5798) 1, 2

Appearance X X X X Water X X X Ethanol Volume X X X

Vapor Pressure X X X

Sulfur X X Acidity X Solvent Washed Gum X X pH X Unwashed Gum X Copper X X

1. For cleaning see 5.9.4.2

2. In accordance with DOE Handbook for Handling, Storing and Dispensing E85 and Other Ethanol- Gasoline Blends, it is recommended at a minimum to test the following every one to two months: electrical conductivity, particulate content, hydrocarbon content (D5501 with D5798), water content and RVP. The DOE Guidebook link is https://www.afdc.energy.gov/uploads/publication/ethanol_handbook.pdf (May need to save file vs open document) https://www.afdc.energy.gov/uploads/publication/ethanol_handbook.pdf

TABLE VIII, Tests required for diesel fuels and kerosene

Appearance 1 X X X X Color (Visual) X X X X Density X X X X Distillation X X

Flash point X X X X Carbon residue (F-76 only) X X Cloud point X Pour point (F-76 only) X Copper strip corrosion X

Cetane index 2 X Viscosity (F-76 only) X Water & sediment by centrifuge X

Particulate (F-76 only) X X Storage stability (F-76 only) X Sulfur 3, 4 X X

Fatty Acid Methyl Ester (FAME) (F-76 only) X X

Lubricity (F-76 only) X X

1. For NATO F-76, if the sample has no visible particulates, but is otherwise not clear and bright per ASTM D4176, procedure 1, then the product shall meet the requirements of ASTM D2709, 0.05 percent volume of water and sediment, maximum. The fuel is acceptable for appearance if the water and sediment content is

0.05 percent volume or less. If the sample fails ASTM D4176, procedure 1, because it contains visible sediment or particulate matter, but meets the requirement of 10 mg /L, maximum, in accordance with ASTM D5452 or ASTM D6217, then the fuel shall be considered acceptable provided all other requirements are met.

2. Cetane Index can only be run if no ignition improvers are present. Otherwise, Cetane number shall be given.

3. Kerosene. Grade No.-1K only, if intended for non-flue connected burner.

4. Sulfur testing is required for ULSD or LSD believed to be contaminated with a higher sulfur content fuel.

TABLE IX, Test required for BDI

Appearance 1 X X X X Distillation X X Flash Point X X X X Cloud Point or LTFT/CFPP X

Viscosity X

Copper Strip Corrosion X

Water and Sediment X

Sulfur X Ramsbottom Carbon Residue X X Particulate Content X X Acid Number X

Ash Content X

Biodiesel Content X X X Oxidation Stability X

NOTE:

1. Obtain a sample in a clear round 1 quart bottle, swirl the bottle vigorously so a vortex is formed. Visually check for sediment at the point of the vortex. If sediment is visible, an investigation is necessary in order to determine the source of contamination.

TABLE X, Tests required for burner fuel oils

BS&W 1 (centrifuge) X X X X Density/API Gravity X X X X Viscosity X X Ash X Carbon Residue X Sediment by extraction X Pour point X

NOTE:

1. Perform only if water is observed.

TABLE XI, Tests required for residual marine fuel (RME 180 grade)

Kinematic Viscosity X X X X Density at 15o C X X X X Flash Point X X X X

CCAI X

Hydrogen Sulfide X Acid Number X Total sediment aged X X Carbon Residue X X

Pour Point X

Water X X Ash X Sodium X

TABLE XII, Tests required for residual marine fuel (RMG 380 grade)

Kinematic Viscosity X X X X Density at 15o C X X X X Flash Point X X X X

CCAI X

Hydrogen Sulfide X

Total sediment aged X X

Water` X X

Ash X Sodium X

TABLE XIII, Test required for marine gas oil (DMA grade)

Kinematic Viscosity X

Density at 15 o C X X X Flash Point X X X X Cetane Index X Sulfur X Oxidation Stability X X

Carbon Residue X X

Appearance X X X X Fatty Acid Methyl Ester (FAME) X X

TABLE XIV, Tests required for bulk lubrication oils 1, 2

PROPERTIES B-1 TEST C TEST

Appearance (to include visual sediment & water) X X Emulsion test 3 X Density or API Gravity X X Viscosity 4 X Flash point X

Foam test X Water 3 X

Solid contaminants 3 X

1. For application of these tests see Table IX.

2. B-2 tests are listed in Table XXII.

3. Only if the specification has this requirement.

. For MIL-PRF-17331 and MIL-PRF-9000 viscosity is not required unless the tank has been in long term storage for 3 months.

TABLE XV, Type B-2 tests for bulk lubricating oils 2

CHARACTERISTICS

SPECIFICATION

MIL-PRF-6081

(LA6)

MIL-PRF-9000

(LO6)

MIL-PRF-17331

(LTL)

MIL-PRF-32644

(CLB)

Appearance / workmanship X X X X Color X

Viscosity @ 100°C X X X Viscosity @ 54°C

Viscosity @ 40°C X 1 X X X Viscosity @ -40°C X

Viscosity @ -54°C X

Relative density X

Pour point X X X Acid number X X X Total Base number X Copper strip corrosion X X X Corrosion & oxidation stability X

Evaporation loss

Precipitation number

Ash/Sulfated Ash X X Emulsion X

Foam test X X1 X Water content X

Particulate content / trace sediment X X X Trace metals

Hydrolytic stability

Minimum retest frequency (months) 36 24 24 36 Visual check frequency (months) 12

Military symbol(s) None 9250 2190-TEP None

NATO Code Numbers O-133 O-278 O-250 None

1. Option A may be used for Government owned 2190 TEP if the conditions are met as required by ASTM D892.

2. For packaged product information refer to MIL-STD-3004-2. Only an approved laboratory under the DoD Shelf-Life Program can authorize a shelf-life extension of any item. For laboratories that cannot perform the full B-2 series tests, recommend the following statement be included in the remarks section of the lab report: "All required tests for shelf-life extension were not performed. This lab report does not give authorization to extend the shelf-life extension of this item."

TABLE XVI, Conversion chart for tank trucks (TT) tank cars (TC), tank wagons (TW), tank & trailer (TRR), and intermodal containers

(IMC)1, 2

Last Product Carried

PRODUCT TO BE LOADED5

Gasolines: MUR, MUM, MUP, EFM, E85, 100, 130, JP-4, JAB

Aviation Turbine Fuels: JAA/A1, JP-8, F-24, JP-5, TS1, KS1/R/N, Aviation Turbine

Fuel3: JPTS

RP1/RP2 JP-10/PF1 Diesel Fuel: F-76 FSII Lubricating Oils

Diesel Fuels:

DF1, DF2,

DS1, DS2,

DSS, DSW,

BDI, MGO

Gasolines4 MUR, MUM, MUP, EFM, E85, 100, 130, JP-4, JAB

Drain/Empty Steam/Dry Steam/Dry Steam/Dry Steam/Dry Steam/Dry Steam/Dry Steam/Dry Steam/Dry

Aviation Turbine Fuels4, 9

JAA/A1, JP-8, F-24,

JP-5, TS1, KS1/R/N,

Drain/Empty

Drain/Empty

Steam/Dry

Aviation Turbine Fuel3 JPTS Drain/Empty Drain/Empty Drain/Empty Drain/Empty Steam/Dry Steam/Dry Steam/Dry Steam Dry Steam/Dry

RP1/RP2 Steam/Dry Steam/Dry Steam/Dry Drain/Empty Steam/Dry Steam/Dry Steam/Dry Steam/Dry Steam/Dry J10/PF-1 Steam Dry Steam/Dry Steam/Dry Steam Dry Drain/Empty Steam/Dry Steam/Dry Steam/Dry Steam/Dry Petroleum Solvent or Paint Thinner Steam/Dry Steam/Dry Steam/Dry Steam/Dry Steam/Dry Steam/Dry Steam/Dry Steam/Dry Steam/Dry

Diesel Fuel: F-76 Steam/Dry Steam/Dry Steam/Dry Steam/Dry Steam/Dry Drain/Empty Steam/Dry Steam/Dry Drain/Empty Diesel Fuels4 DF1, DF2, DS1, DS2, DSS, DSW, MGO

Steam/Dry Steam/Dry7 Steam/Dry Steam/Dry Steam/Dry Steam/Dry Steam/Dry Steam/Dry Drain/Empty

FSII (SIH) Drain/Empty Drain/Empty Steam/Dry Steam/Dry Steam/Dry Steam/Dry Drain/Empty Steam/Dry Steam/Dry Lubricating Oils NO LOAD NO LOAD NO LOAD NO LOAD NO LOAD NO LOAD NO LOAD Steam/Dry6 Steam/Dry Biodiesel Blends(<B15)4

DF1, DF2, DS1, DS2, DSS,

DSW

Steam/Dry7

NO LOAD

Biodiesel Blends(>B15):

DF1, DF2, DS1, DS2,

BDI

Steam/Dry8

Heavy Fuel Oils, Distillate Fuels4 FS1, FS2, FS4, FS5, FS6

Residual Fuel Oils:

ISO 8217, class F (IFOs)

Naphtha Drain/Empty Steam/Dry Steam/Dry Steam/Dry Steam/Dry Steam/Dry Steam/Dry Steam/Dry Steam/Dry

TABLE XVI Continued, Conversion chart for tank trucks (TT) tank cars (TC), tank wagons (TW), tank & trailer (TRR), and intermodal containers (IMC)1, 2

1. For previous cargoes not listed, contact DLA Energy Product Technology and Standardization Division at DLAEnergyProductTechnology@dla.mil for acceptability/cleaning procedures.

2. General Instructions for Tank Cars and Trucks

a. Conveyances (all) shall be dry and free from loose rust, scale, and dirt

b. Saran lined equipment should not be steam cleaned; water wash should suffice.

c. Petroleum products shall not be loaded into the conveyances where the previous cargo was caustic, acid, or chlorinated solvents.

d. Tank trucks and cars in liquid fertilizer service shall not load aviation turbine fuels directly but shall carry out at least two loads of commercial gasoline prior to the aviation turbine fuel load.

e. Conversion of Government-owned tank cars from liquid fertilizer service to aviation turbine fuel service shall only be done when no other alternative exists. Tank cars being converted from liquid fertilizer service to a petroleum product shall be adequately cleaned to remove all traces of liquid fertilizer. At a minimum, the equipment must be steam cleaned; dried and must be free from loose rust, scale, and dirt. After cleaning, but before loading aviation turbine fuels, at least two loads of commercial gasoline shall be carried prior to loading aviation turbine fuel. Equipment with unlined compartments should have its compartments lined with an approved coating at this time. Conveyances carrying their initial load of aviation turbine fuel following conversion shall not be released from the loading until they have been sampled a minimum of 24 hours after loading. In accordance with MIL-STD-3004-1A, samples shall undergo type B-2 testing plus Thermal Stability Test (if required by the product specification). After type B-2 tests indicate compliance with specification requirements, the conveyance can be released pending results of the Thermal Stability tests. The conveyance shall not be unloaded until the loading point notifies the destination that the Thermal Stability test (when required) has passed. When the above condition applies, the DD-250, Wide Area Workflow (WAWF) Energy Receiving Report (ERR) or equivalent form shall be so noted.

3. To be loaded only in aluminum or stainless-steel conveyance, or other conveyance lined with an approved epoxy coating. If equipment is coated, clean with hot fresh water not exceeding58°C (136°F) and dry thoroughly.

4. If previous cargo contained dye marker, all traces of color must be removed.

5. If product to be loaded does not contain dye, then the vehicle shall not contain any traces of dye prior to loading.

6. Drain/empty only when same specification product is being loaded.

7. Prior to loading the aviation fuels listed, the conveyance must have carried a previous non-FAME cargo and then be steam cleaned and dried. Trucks that have previously carried biodiesel create a risk of cross-contamination of aviation turbine fuel with residual biodiesel components. Diesel fuel may contain up to 5% FAME without reporting it as biodiesel.

Because of the difficulties in making a load-rack of the presence of FAME in the previous load, the more stringent “Steam/Dry is required.

8. Drain and empty if loading biodiesel blend.

9. Cargos carrying dyed kerosene shall use the steam/dry cleaning procedure.

mailto:DLAEnergyProductTechnology@dla.mil

TABLE XVII, Minimum Requirements for the Preparation of Barge and Tanker Cargo Tanks 1, 2

LAST PRODUCT CARRIED

(For information regarding 2nd and 3rd to last cargoes see note 8.)

PRODUCT TO BE LOADED

Gasolines4,5:

MUR, MUM,

MUP, EFM, E85,

100, 130, JP4, JAB

Jet Fuels:

JAA/A1, JP8,

F24, TS1,

KS1/R/N

Jet Fuel:

JP5

Jet Fuel:

JPTS

Diesel Fuel: F76 Sulfur greater than 15 ppm and less than or equal to

15ppm

Diesel Fuels with B5 or less5: DF1, DF2, DS1, DS2, DSS, DSW, MGO

Biodiesel Blends greater than B55:

DF1, DF2, DS1,

DS2, DSS, DSW

Heavy Fuel Oils:

ASTM D396 (FS4,

FS5, FS6)

ASTM D975 (No. 4D)

ISO 8217, Class F

(IFOs)

Gasolines5:: MUR, MUM, MUP, EFM, E85, 100, 130, JP4, JAB, Naphtha, Reformate and Alkylate

A, B

F

Jet Fuels:

JAA/A1, JP8, F24, TS1, KS1/R/N9

Jet Fuel: JP5 A A A F A, B A A A

Jet Fuel: JPTS A A A, B A A A A A Diesel Fuel (ULSD): F76 Sulfur less than or equal to 15 ppm

A, C

Diesel Fuel: F76 Sulfur greater than15 ppm A, C A, C A, C NO LOAD A A A A, C

Diesel Fuels with B5 or less5: DF1, DF2, DS1, DS2, DSS, DSW, MGO

Biodiesel Blends greater than B55: DF1, DF2, DS1, DS2, DSS, DSW

E

Heavy Fuel Oils: ASTM D396 (FS4, FS5, FS6) ASTM D975 (No. 4D)

ISO 8217, class F (IFOs)

A,D

Crude3 NO LOAD NO LOAD NO LOAD NO LOAD NO LOAD NO LOAD NO LOAD NO LOAD Lube Oils NO LOAD NO LOAD NO LOAD NO LOAD A, D A, D A, D A Water soluble chemicals6 A,C A,C A,C F A,C A,C A,C A,C

Table XVII Continued, Water Soluble and/or Water Miscible Chemicals

Product Name Minimum Required

Cleaning Procedures

Product Name Minimum Required Cleaning Procedures

2-Butanone A,C Isopropanol, 91 % A,C 1,4 butanediol A,C Isopropanol, Anhydrous A,C 15W-50 (syn.hydrocarbons & additives) A,C Malaic Anhydride A,C 2-Butanol A,C Maquat A,C 2-Hydroxyethly Methacrylate (HEMA) A,C Methanol A,C Butendiol A,C Methyl Amyl ketone A,C CHRYSO A,C Methyl Pyrrolidone A,C Coralube 737 RB (= hexylene glycol) A,C Methyl Salicylate C8H8O3 A,C Diethanolamine, IMO 9/ UN 3082/PG III A,C Monoethanolamine A,C Diethylene Trianine A,C Mpdiol Glycol A,C Diethylketone A,C MS (mineral sprint) rule 66 A,C Dimethylacetamide (DML) A,C MTBE A,C Dipropylene Glycol A,C Eastman EB Solvent, A,C dipropylene glycol methyl ether (DPM) A,C Neodol 23-6.5 A,C Diquat concentrate A,C N-Methyl-2-Pyrrolidone, Non Haz. A,C DOW 200 A,C n-Propanol A,C DOW Froth 250 A,C Petresul 550 A,C Eastman Glacial Acetic Acid A,C Propyl Alcohol Sasol A,C Ethanol, Anhydrous A,C Propylene Carbonate, Non Haz. A,C Ethoxylated Sorbitan Laurate A,C Propylene Glycol Ethyl Ether (EPG) A,C Ethylene Carbonate, Non Haz. A,C Propylene glycol methyl ether (PM) A,C Ethylenediamine (EDA) A,C Terathane 2900 polyether glycol A,C Floquat (FL 4620 PWG) A,C Tetrahydrofuran (THF) A,C furfural alcohol A,C Triehtylene Glycol Ethyl Ether (ETG) A,C Furfurayl alcohol A,C triethanolamine 99 A,C Gamma Butyrolactone A,C Triethylene Glycol A,C Glycerol A,C Tripropylene Glycol A,C Glycol Ether DB Acetate A,C UAN (Urea Ammonia Nitrate) A,C Glycol Ether PNP A,C Hitec 614 (benzene sulfonic acid -calcium salt) A,C

TABLE XVII Continued, Vessel Cleaning Requirements Legend and Notes

A All cargo lines shall be dropped, tanks stripped, ballast residue removed.

B All cargo and vent lines shall be drained of previous product and flushed with cold water. Cargo tanks must be thoroughly machine washed using cold water. Cargo tanks must be free of water, loose rust, sludge, mud, silt, etc.

C The same as for “B,” except that hot water shall be used instead of cold. If tank interiors are coated, water temperature should not exceed 58°C (136°F).

D Cargo tanks and systems shall be processed in accordance with the instructions contained in EI HM 50 Guidelines for the cleaning of tanks and lines for marine tank vessels carrying petroleum and refined products.

E Not to be loaded without special cleaning instructions. Three clean product/zero biological content intermediate cargoes required. (See Note 5 below) F Special tank preparations and cargo handling is required for JPTS, to prevent contamination. Tanks used for loading must be stainless steel or coated with an approved epoxy. Coating must be adherent: no flaking, peeling, or blistering. Prior to loading JPTS, tank cleaning requirements are: tanks must be machine washed with hot water, if cleaning chemical and/or salt water is used, the final wash must be with fresh water.

Tank bottoms, interior bulk heads, and internals must be completely free of sediment, scale, and other contaminants. Tanks must be dry and all liquids completely removed from the tank’s lines after cleaning, must be flushed with fresh water, drained and free of all water. Loading and unloading system must be completely isolated. This will be accomplished by completely separate piping systems or by use of blinds. Valves will not be depended on to effect isolation. Cargo tank valves will not be considered as part of the “double block” requirement for cargo system segregation. No common lines will be used. Steam smothering lines should have at least two valves that can be sealed from the main line to the tanks, or a blind installed that can be readily removed. Each tank will have its own individual vent. If ship has a common vent system, tanks used for JPTS must be isolated from balance of the vent system.

1. See Vessel Cleaning Requirements Legend for cleaning type code (A, B, C, D, E, F) details.

2. This table is included as a guide only. Requirements for tanker cleaning are determined by MSC vessel cleaning policy. Contact DLA Energy Quality Operations Division for tank cleaning requirements for any product not listed in the Table. If tank contains ballast water or water used for tank cleaning/washing, every effort shall be made to remove this free water to the minimum level possible by draining or by use of a pump.

3. There are no circumstances where a crude carrier is capable of cleaning tanks, pumps and lines sufficiently to load an aviation fuel immediately after a crude cargo. Crude carriers converted to a distillate diesel, aviation fuel or naphtha-based fuel must carry three cargoes of a commercial like product without a quality incident.

4. Gas free, lift scale and mop. Consideration may be given to substituting mopping by enhanced stripping and drying per EI (Energy Institute) HM 50 Guide.

5. FAME (Fatty Acid Methyl Ester) Contamination:

Aviation Gasoline or Aviation Kerosene/Turbine Fuel (Aviation Fuel Products)

- To avoid contamination from FAME in Aviation Gasoline, Aviation Kerosene/Turbine Fuel cargoes. See below instructions.

-- Following cargoes with pure biodiesel (B100) or any cargo with FAME content greater than 5 vol % (B5): Prior to loading Aviation Fuel Product cargoes requires three intermediate cargoes of a compatible fuel product. The three intermediate cargoes SHALL NOT contain FAME content greater than 5 vol % (B5). When any of the last three cargoes have consisted of diesel or heating oil products, FAME testing shall be conducted for each cargo; attestation as described in the RFP is not sufficient for these products. Examples of diesel or heating oil products include, but are not limited to, F-76, DF1, DF2, DS1, DS2, DSS, DSW, MGO, Gasoil, FS1, FS2, FS4, FS5, FS6, and IFO. Evidence by presentation of CoQs representing the last three cargoes with FAME testing (EN 14078 and ASTM D7371) demonstrating B5 or less shall be provided as proof. In scenarios where FAME testing (EN 14078 and ASTM D7371) was not conducted for a diesel or heating oil product, or such data is unable to be provided for all three of the last cargoes, the vessel shall be assumed to contain FAME greater than 5 vol %. The vessel tanks shall be evaluated and cleaned under the Minimum Requirements for Preparation of Tanker Cargo Tanks table above under procedures for Biodiesel Blends greater than B5 procedures. Alternatively, another vessel with FAME testing for the last three cargoes conducted may be nominated instead.

-- Tanks shall be in good condition and washing shall be particularly stringent, including flushing of pumps and lines, followed by drain and mop, at a minimum. A fresh- water rinse is required if sea water is used. Uncoated tanks shall be hot water washed and have loose bottom scale removed prior to loading an aviation fuel product cargo load.

-- Following cargoes with a FAME content of 5 vol % or less (B5 or below): Prior to loading Aviation Fuel Product cargoes, recommend a hot water wash, including flushing of the pumps and lines, followed by draining, at a minimum. A fresh-water rinse is required if sea water is used.

Special note:

Specifications for sensitive grades will require extreme care during sampling to avoid contamination from previous cargoes or buildup of residues. To reduce the possibility of drawing unrepresentative samples, cleaning of sampling equipment, vapor locks, standpipes and stilling wells is recommended as part of cleaning when tanks have previously held cargoes containing FAME.

6. Water soluble chemicals: include Ethanol, Mono Ethylene Glycol, Di Ethylene Glycol. See page four (4) for additional water soluble/miscible chemicals.

7. Previous automotive and aviation gasoline cargoes for loading JPTS are unacceptable unless the concentration of lead is verified to be less than 13ppm.

8. Certain products to be loaded on a tanker must not only consider the last cargo carried, but the 2nd and 3rd to last cargoes as well. These products include aviation turbine fuels and F-76 fuel oil, naval distillate. Previous cargoes of

Crude oil and products containing FAME are addressed in notes 3 and 5. Other 2nd and 3rd to last cargoes of concern include, but are not limited to, raw vegetable oil, lubricating oils, heavy fuel oils, and various chemicals.

Determinations for acceptability of 2nd and 3rd to last cargoes carried prior to loading aviation fuel and F-76 will be made on a case-by-case basis using applicable Certificates of Analysis, Certificates of Quality and other analytical data.

9. Cargos carrying dyed kerosene shall use the A/B cleaning procedure.

Table XVIII, Test Series Definition

TYPE DESCRIPTION

A Complete specification test as per specification detailed in the contract

B-1 A limited subset of principle characteristics of the type A full test specification requirement most likely to be affected by transportation of a product.

B-2 A more rigorous subset of the type A full test specification requirement than the type B-1 test schedule and aimed at those parameters susceptible to deterioration through aging, weathering, and long-term storage conditions.

B-3 Partial analysis for contamination; in particular, for controlling the re-injection of pipeline interface products.

Appearance To confirm that no free water and/or visual solid particulate are present in the fuel and that the fuel has a “clear & bright” appearance at ambient temperature.

C A limited number of tests performed to identify and compare product properties to ensure that no major changes have taken place during the fuel transfer process by any means of transport.

C+ (C-Plus) C-test plus additional tests. These tests are to be performed to ensure that critical properties are fulfilled and/or additives are present at the correct concentration.

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REVISIONS

REV DESCRIPTION DATE APPROVED

DLA ENERGY QAP E22 9 Feb 2022 9 Feb 2022

ENERGY QAP E22 LIST OF INSPECTION OFFICES FOR DLA ENERGY CONTRACTS (DLA ENERGY) (FEB 2022)

The following lists shall be used to identify the Government inspection office assigned inspection and/or acceptance responsibility for DLA Energy contracts in a particular geographic area. These contracts include, but are not limited to, those for bulk petroleum products and additives, into-plane refueling, petroleum storage and laboratory services, coal, aerospace energy (including compressed gases), and posts, camps, and stations. The area of inspection responsibility and corresponding office code are assigned in paragraphs (a) and (b). The address and phone number of each inspection office, by office code, is provided in paragraph (c). Unless a particular inspection office is identified in another part of the contract, the assignments in this QAP shall apply.

(a) AREAS OF RESPONSIBILITY AND OFFICE CODES WITHIN THE CONTINENTAL UNITED STATES

(CONUS):

Alabama 110 Maine 110 Oklahoma 110 Arizona 120 Maryland 110 Oregon 120 Arkansas 110 Massachusetts 110 Pennsylvania 110 California 120 Michigan 110 Rhode Island 110 Colorado 120 Minnesota 110 South Carolina 110 Connecticut 110 Mississippi 110 South Dakota 110 Delaware 110 Missouri 110 Tennessee 110 District of Columbia 110 Montana 120 Texas 110 I Florida 110 Nebraska 110 Utah 120 Georgia 110 Nevada 120 Vermont 110 Idaho 120 New Hampshire 110 Virginia 110 Illinois 110 New Jersey 110 Washington 120 Indiana 110 New Mexico 120 West Virginia 110 Iowa 110 New York 110 Wisconsin 110 Kansas 110 North Carolina 110 Wyoming 120 2

Kentucky 110 North Dakota 110 Louisiana 110 Ohio 110

EXCEPTIONS:

1 The El Paso, Texas, area is assigned to Code 120 (DLA Energy Americas West).

2 The Newcastle, Wyoming, area is assigned to Code 110 (DLA Energy Americas East).

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(b) AREAS OF RESPONSIBILITY AND OFFICE CODES OUTSIDE THE CONTINENTAL UNITED STATES (OCONUS) (INCLUDING ALASKA AND HAWAIi):

Afghanistan 400 Cyprus 200 Malaysia 300 Singapore 300 Africa 200 3 Egypt 400 3 Maldives 300 South America 110 Alaska 130 Europe (Continental) 200 Malta 200 South Korea 300 Antarctica 300 Georgia 200 Mauritius 200 Sri Lanka 300 Armenia 200 Greenland 200 Mexico 110 Syria 400 Ascension Island 110 Hawaiian Islands 300 Midway Island 300 Taiwan 300 Australia 300 Hong Kong 300 Mongolia 300 Tajikistan 400 Azerbaijan 200 Iceland 200 Myanmar 300 Thailand 300 Azores 200 India 300 Nepal 300 Turkey 200 Bahrain 400 Indonesia 300 New Zealand 300 Turkmenistan 400 Bangladesh 300 Ireland 200 North Korea 300 United Arab Bermuda 110 Iran 400 Oman 400 Emirates 400 Bhutan 300 Iraq 400 Pacific Islands United Kingdom 200 Brunei 300 Israel 200 (Central & South) 300 Uzbekistan 400 Cambodia 300 Japan 300 Pakistan 400 Vietnam 300 Canada 1104 Jordan 400 Papua New Guinea 300 Wake Island 300 Canary Island 200 Kazakhstan 400 Philippines 300 Yemen 400 Caribbean Islands 110 Kuwait 400 Qatar 400 Central America 110 Kyrgyzstan 400 Russia 200 Chagos Archipelago 300 Laos 300 Ryukus Islands, Japan 300 China 300 Lebanon 400 Saudi Arabia 400 Comoros 200 Madagascar 200 Seychelles Is. 200

EXCEPTIONS:

3 Except for Egypt, which is assigned to DLA Energy Middle East (Code 400), all other countries in Africa fall under DLA Energy Europe (Code 200).

4 For Canada locations, contact DLA Energy Americas East (Code 110) to confirm coverage.

(c) INSPECTION OFFICES AND CODES.

110. DLA Energy Americas East ATTN: Quality Manager 5

Federal Building, Suite 1005 2320 LaBranch Street Houston, TX 77004-1091 Phone: (713) 332-4113

FAX: (713) 718-3891

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