Attachment 1 - SOW.pdf

Solicitation SPE603-25-R-0520

Attachment 1 - Statement of Work US Territory of Guam Lab, South Pacific Region

Statement of Work for

Contracted Laboratory Services

Guam March 2024

Contents C-1.0 General Description:

C-1.0.1 Service Locations:

When ordered, the Contractor shall be able to provide services required in this SOW to DLA Energy in the location listed below.

Contractor testing facility shall be located within Guam and shall meet the required turn-around times listed in paragraph C-5.5. 1

C-1.1 Specifications, Standards and Handbooks:

C-1.2 Facilities:

C-1.3 Scheduling of Services:

C-2.0 Contractor Detailed Plans:

C-2.1 Contract Compliance Plan:

C-2.2 Contract Contingency Plan:

C-2.3 Contract Training Plan:

C-2.4 Laboratory Testing Plan:

C-2.5 Safety Plan:

C-2.6 Transportation Plan:

C-2.7 Laboratory Equipment Plan:

C-2.8 Monthly Reporting:

C-3.0 Laboratory Requirements:

C-3.1 Operating Hours:

C-3.2 Staffing:

C-3.3 Knowledge and Skills:

C-3.4 Access:

C-3.5 Epoxy Lined Sample Cans:

C-3.6 Thermal Oxidation Stability Failures:

C-3.7 Ellipsometric Tube Deposit Rater (ETR):

C-3.8 Sample Testing Turnaround Times:

C-3.9 Retain samples:

C-4.0 Transportation Performance Requirements:

C-5.0 Secured Fuels Performance Requirements:

C-5.1 Secured Fuels Logistics:

C-6.0 Sample Shipment to External Laboratories:

Attachment 1: Products to be Tested Attachment 2: Series Testing Requirements Attachment 3: Approved Testing Methods Attachment 4: Annual Estimates by Location:

Attachment 5: Sample Shipment

Page | 1

C-1.0 General Description:

This Statement of Work (SOW) is established to identify the Contractor responsibilities for the period of performance identified in the solicitation and resultatnt contract(s). The Contractor will be responsible for the laboratory testing of Defense Working Capital Product (DWCF) owned petroleum products in accordance with the specifications as described herein, and transportation of samples from contracted location in C-1.0.1 to the contractor’s laboratory.

C-1.0.1 Service Locations:

When ordered, the Contractor shall be able to provide services required in this SOW to DLA Energy in the location listed below. Contractor testing facility shall be located within Guam and shall meet the required turn-around times listed in paragraph C-5.5.

Guam Anderson AFB DFSP Guam DFSP Guam II

C-1.1 Specifications, Standards and Handbooks:

The Contractor shall maintain all of the required specifications, standards, test methods, handbooks, etc., per this SOW and perform services in accordance with testing requirements. Military Specifications referenced in Attachment 1 for petroleum product types can be obtained at http://quicksearch.dla.mil or https://assist.dla.mil but can also be supplied by the Contracting Officer (CO) or Contracting Officer’s Representative (COR) if requested in writing.

C-1.2 Facilities:

The Contractor shall have facilities in accordance with paragraph C-1.0.1 to meet the required turn-around times in section C-5.5, provide the location(s) of the facility where the product shall be tested, facility testing capabilities and contact information. If testing of products requirements cannot be accomplished locally, i.e., in the same location or origin, the Contractor shall submit an exemption request with a detailed plan on where the samples shall be tested and how the location shall meet coordinated turn-around times.

C-1.3 Scheduling of Services:

All plans shall be submitted to the CO for review and acceptance as a part of the technical proposal as documented in the solicitation. Plans shall be kept current for the life of the contract. The government reserves the right to request changes or modifications to any detailed plans at any time throughout the contract performance period. Plans shall be made available for government review upon request at any time during the contract performance period.

C-2.0 Contractor Detailed Plans:

All plans shall be submitted to the CO for review and acceptance as a part of the technical proposal as documented in the solicitation. Plans shall be kept current for the life of the contract. The Government reserves the right to request changes or modifications to any detailed plans at any time throughout the contract performance period. Plans shall be made available for Government review upon request at any time during the contract performance period.

C-2.1 Contract Compliance Plan:

The Contractor is responsible for compliance with all contract performance requirements. The Contractor is responsible for all actions taken by any sub-contractor utilized under this contract. The Contractor shall be ISO 9001 or ISO/IEC 17025 certified. Contractors which have to sub-contract certain test methods or tasks out, due to whatever circumstances, must inform the CO during the offer period, request for an exception, deviation or waiver (EDW) for that particular task.

C-2.2 Contract Contingency Plan:

The contract contingency plan shall outline contractor actions to ensure there is no significant interruption of services resulting from labor disputes, catastrophic failure of equipment, or the effects of natural disasters/emergencies to include ensuring the facility is operational or has a sub-contracting plan incase of power outage for more than 48 hours.

C-2.3 Contract Training Plan:

The Contractor shall provide a detailed plan that identifies employee training requirements and procedures necessary to maintain proficiency. The plan shall identify length of training, training sources, and a brief description of courses such as

Page | 2 safety, environmental protection, and job qualification training. The Contractor is responsible for ensuring all individual training requirements are accomplished. The Contractor must demonstrate current participation, in a proficiency program or suitable means to verify laboratory performance.

C-2.4 Laboratory Testing Plan:

The Contractor shall maintain detailed plans regarding the required characteristic tests as presented in Attachments 2 and 3.

Contractor shall maintain all of the necessary testing standards and specifications, as noted in paragraph C-1.1 above. If the Contractor is unable to provide certain specification tests, as listed in the maintained standards and specifications, the Contractor must request an exception, deviation or waiver (EDW) during the solicitation process and after award if any changes have occurred. EDW request must be detailed with the cause of such request and the Contractor’s means of correcting the deficiency. If the Contractor plans on using a subcontractor to perform certain tests and/or functions, the Contractor must provide that information in their plan.. The Contractor must also ensure they either possess or have access to all referee methods described in the various specifications. If the Contractor plans on using another laboratory for either normal sample testing as described in this SOW or for referee method support, the Contractor must be able to adhere to the turnaround times listed in C-3.8 below.

C-2.5 Safety Plan:

The Contractor shall provide a detailed plan outlining the policy, procedures and actions necessary to maintain a safe working environment for employees and visitors. The plan shall cover the products stored, handled, Safety Data Sheets (SDS) and guidelines regarding the safe handling of such products and shall be maintained and updated over the course of the contract.

C-2.6 Transportation Plan:

The Contractor is required to submit a plan for review to transport the petroleum samples to an approved laboratory for testing or shipping (Contractor supplied transport, third party delivery service, etc.) and how they plan on tracking the chain of custody to the Contractor’s facility. Product quality must be preserved and not altered by shipment. DLA Energy or its storage terminal contractor(s) do not have the ability or certification to ship or package fuel samples.

C-2.7 Laboratory Equipment Plan:

The Contractor will furnish annually to the CO directly the status by name, model and serviceability of all equipment used in laboratory testing. Equipment that malfunctions or is non-serviceable will be reported to the CO within 48 hours with miagration plan to provide testing capability.

C-2.8 Monthly Reporting: The Contractor shall provide a monthly written report to the CO and contract officer representative (COR) with the number of laboratory tests performed, what testing was included during reporting month, and the location of performance.

C-3.0 Laboratory Requirements: The below are general requirements for all contractor laboratories. Laboratories are required to have the listed referee test methods, which is referenced in the product specifications and international test methods (ASTM, EI, etc.).

C-3.1 Operating Hours: The Contractor shall be responsible for adjusting hours of operation to meet workload demands and turn-around times in section C-3.8.

C-3.2 Staffing: The Contractor shall provide sufficient staff to accomplish all functions and tasks, to include simultaneous operations of performing multiple tests at a time and provide the contact information for laboratory manager or assistant laboratory manager, if the laboratory is not manned 24 hours, seven days a week.

C-3.3 Knowledge and Skills: The Contractor shall ensure that personnel assigned to tasks have the requisite knowledge and skills to meet the performance standards and comply with all applicable country laws, state laws, regulations, and codes.

All contractor supervisors and contractor key employees shall be able to read and understand English so they can understand and follow oral or written instructions, directions, directives, regulations, and operating procedures. All contractor supervisors and contractor key employees shall be capable of writing in English to compose the required detailed reports.

C-3.4 Access: The Contractor shall allow DLA Energy representatives to witness testing or sampling. The Contractor

Page | 3 shall provide the applicable information for access and provide follow-up to obtain access (for personnel and vehicles) to all facilities that product is tested or sampled. For areas that require special admission, the Contractor will assist, DLA Energy representatives, in gaining access.

C-3.5 Epoxy Lined Sample Cans: The Contractor shall maintain a supply of ten, unused, epoxy lined fuel sample shipping containers, to be provided to DLA Energy personnel, per request. Sample containers shall be stored to ensure they are clean and free from all substances that might contaminate the product being sampled. Containers must meet the following specifics: Complies with ASTM D-4306, height not to exceed 9 inches, diameter not to exceed 7 inches, capacity 1 USG, Bung Plug ¾ inch with lock-wire hole, carrying handle able to be shipped as hazardous material.

C-3.6 Thermal Oxidation Stability Failures: If a failure occurs using an ALCOR (PAC) Mark IV, the retest shall not be conducted on any ALCOR (PAC) Mark IV model.

C-3.7 Ellipsometric Tube Deposit Rater (ETR): The Contractor shall perform ASTM D3241 Annex 3 ETR within the testing turn-around times in section C-3.8. Sample Testing Turnaround Times. ETR is the preferred method and shall be treated as the referee method.

C-3.8 Sample Testing Turnaround Times: Turn-around time starts when the Contractor is notified that the sample is prepared for transportation from sample location to the servicing laboratory. The Contractor shall be responsible for transportation of the sample from the location in paragraph C-1.0.1 to contractor’s laboratory (see C-4.0 for sample transportation requirements). Turn-around time ends when fuel sample reaches the laboratory. DLA Energy will give the Contractor at least 12 hours of advance notice of the sample being prepared for transportation (prime contractor is responsible for any sub-contractor actions).

Maximum Turn-around Hours Chart A level/Full spec testing 24 hours B-1, B-2, B-3 Testing 18 hours C-level Testing 6 hours Individual Tests 4 hours Secured Fuels Testing 6 hours Expedite Request 4 hours

Note: The 12 hours of advance notice is not included in the turn-around time.

C-3.9 Retain samples: After analysis, the Contractor shall retain samples for a minimum of 45 days. In the event of a suspected quality issue or dispute, a longer sample retention period may be requested by DLA Energy and, upon receipt of such notification, The Contractor is obligated to retain the sample until notified that disposal is permitted. The Contractor shall be responsible for disposal of excess fuel samples and sample containers in accordance with applicable laws and regulations.

C-4.0 Transportation Performance Requirements: The Contractor shall be responsible for packing and transporting all petroleum samples from a job site to the laboratory in accordance with applicable laws and regulations. When requested, by DLA Energy personnel, the Contractor shall be able to provide an epoxy line sample can, detailed in C-3.6 for replacement. When sample transportation is not required of the contractor, they shall be notified in advance.

C-5.0 Secured Fuels Performance Requirements: Due to mission demands, DLA Energy may request petroleum testing services under Attachment 2: Series Testing Requirements and Test Methods from MIL-STD-3004-1 table XII.

Samples will be transported directly to the Contractor testing facility by a DLA Energy QAR that shall provide the Contractor with as much advance notice as possible. The turn-around time shall not exceed six (6) hours once the laboratory is in receipt of the sample(s). After a task order is issued, the QAR will coordinate the specifics/logistics required for the secured fuels testing services.

C-5.1 Secured Fuels Logistics: In the event that the contractor’s available testing location(s) and capabilities creates a logistical concern, which is likely to unduly delay secured fuel testing and adversely impact mission requirements; DLA

Page | 4

Energy reserves the right to use, at its sole discretion, and as it deems necessary, a third-party service provider of its choosing.

Note: In the event that the contractor’s available testing location(s) creates a logistical concern which is likely to unduly delay secured fuel testing and adversely impact mission requirements, DLA Energy reserves the right to use at its sole discretion and as it deems necessary, a third-party service provider of its choosing.

C-6.0 Sample Shipment to External Laboratories: The Contractor shall, upon request and proper task order, be responsible for shipping fuel samples from locations in C-1.0.1 to the laboratories in the chart below. Fuel samples shall be shipped within 48 hours of sample receipt and arrive to the identified laboratory within five calendar days. Estimated shipping volume is based on one-gallon shipments.

Naval Air Systems Command HAZMART Bldg. 2385 22680 Hammond Road Patuxent River, MD 20670

US ARMY TARDEC

Petroleum Laboratory Bldg. 5085 U Avenue, Bldg 85 New Cumberland, PA 17070-

Aerospace Fuels Laboratory AFPA/PTPLA 2430 C Street, Bldg 70, Area B Wright Patterson AFB OH 45433-

Naval Research Laboratory 4555 Overlook Avenue, SW Washington, DC 20375

Southwest Research Institute 6220 Culebra Rd San Antonio, TX 78238-5166

Air Force Research Laboratory AFRL 2977 Hobson Way

WPAFB, OH 45433

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Attachment 1: Products to be Tested

The following are products, which are utilized by DLA Energy and its customers that may require testing at the Contractor’s facility(ies) per the requirements set forth in this SOW. The Contractor must be familiar with all of the product specifications listed below and develop operating procedures and/or checklists to allow their technicians to perform the proper tests and complete the tasks as requested per the task order and in a timely manner. All referenced material can be obtained at http://quicksearch.dla.mil/ or https://assist.dla.mil/ or by contacting the CO or the COR.

1) Aviation Turbine Fuel, Grade JET A (Specification: ASTM D1655 latest version) and JET A-1, NATO F-35 (DEF

Stan 91-091 latest version)

2) Turbine Fuel, Aviation, Kerosene Types, NATO F-34 (JP8) (Specification: MIL-DTL-83133 latest version)

3) Turbine Fuel, Aviation, Grade JP5 NATO F-44 (Specification: MIL-DTL-5624 latest version)

4) Fuel, Navy Distillate NATO F-76 (Specification: MIL-DTL-16884 latest version)

5) Inhibitor, Fuel System Icing, High Flash (FSII) (Specification: MIL-DTL-85470 latest version)

6) Marine Residual Fuel Oil Grade (RME-180/380) (Specification: ISO 8217 latest version)

7) Lubrication Oil, Steam Turbine and Gear (LTL) MIL Symbol 2190 (Specification: MIL-PRF-17331 latest version)

8) Lubrication Oil, (LO6), MIL Symbol 9250, Shipboard Internal Combustion, High Output Diesel

(Specification: MIL-PRF-9000 latest version)

9) Diesel Fuel Oil (NATO F54) Series Testing Requirements for Specifications ASTM D975, EN 590, latest version

Page | 6

Attachment 2: Series Testing Requirements

1. Secured Fuel Series Testing Requirements for Aviation Fuel

Page | 7

2. Jet A & Jet A-1 (NATO F35) Series Testing Requirements for Specifications ASTM D1655 and Def Stan 91-

A Series Characteristics ASTM

D1655 Def Stan 91-091

B-1 Series

B-2 Series

B-3 Series

C-Series

Appearance/Workmanship X X X X X X Color (Visual) X X X X X X Particulate Contamination/Particulate Matter

X X X X X

Particle Count (Particulate) X Total Acidity X X X Aromatics X X Total Sulfur X X Mercaptan Sulfur X X Doctor Test X X Distillation X X X X X Flash Point X X X X X X API Gravity or Density at 15°C

X X X X X X

Freezing Point X X X X X Viscosity at minus 20°C X X Smoke Point X X Naphthalenes X X Specific Energy (Net Heat of Cumbusiton)

X X

Copper Strip X X X X X Thermal Stability X X X X Existent Gum X X X X X Microseparometer X X X X X Electrical Conductivity X X X X X Lubricity X Color, Saybolt X X Particulate Contamination/Particulate Matter with Filtration Time

X X X X X

Fuel System Icing Inhibitor X X X X X

FAME X X X X X

Page | 8

3. JP8 (NATO F34) Series Testing Requirements for Specifications MIL DTL 83133

Characteristics MIL DTL 83133

B-1 Series

B-2 Series

B-3

Appearance/Workmanship X X X X X Color (Visual) X X X X X Particulate Contamination/Particulate Matter

X X X X

Particle Count X Total Acidity X X Aromatics X Total Sulfur X Mercaptan Sulfur X Doctor Test X Distillation X X X X Flash Point X X X X X API Gravity or Density at 15°C

X X X X X

Freezing Point X X X X Viscosity at minus 20°C X Smoke Point X Naphthalenes X Specific Energy (Net Heat of Combustion)

X

Copper Strip X X X X Thermal Stability X X X Existent Gum X X X X Microseparometer X X X X Electrical Conductivity X X X X Lubricity Colour, Saybolt X X Particulate Contamination/Particulate Matter with Filtration Time

X X X X

Fuel System Icing Inhibitor X X X X

FAME X X X X

Hydrogen Content X Cetane Index, Calculated X

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4. JP5 (NATO F44) Series Testing Requirements for Specifications MIL DTL 5624

Characteristics MIL DTL 5624 B-1

Series B-2

Series B-3

C- Series

Appearance/Workmanship X X X X X Color (Visual) X X X X X Particulate Contamination/ Particulate Matter

X X X X

Particle Count X Total Acidity X X Aromatics X Total Sulfur X Mercaptan Sulfur X Doctor Test X Distillation X X X X Flash Point X X X X X API or Density at 15 deg. C X X X X X Vapor Pressure X Freezing Point X X X X Viscosity at minus 20°C X Smoke Point X Specific Energy (Net Heat of Combustion)

X

Copper Strip X X X X Thermal Stability X X X Existent Gum X X X X Microseparometer X Electrical Conductivity X Colour, Saybolt X X Particulate Contamination/Particulate Matter with Filtration Time

X X X X

Fuel System Icing Inhibitor X X X X

FAME X X X X

Hydrogen Content X Cetane Index, Calculated X

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5. F-76 Series Testing Requirements for Specifications MIL-DTL-16884

Characteristics MIL F 16884 B-1

Series B-2

Series B-3

Series C-

Series

Appearance/Workmanship X X X X X Demulsification X API Gravity or Density at 15°C X X X X X Distillation X X X Cloud Point X X Color X X X X X Flashpoint X X X X X Particulate Contamination X X X Pour Point X X Viscosity at 40°C X X Acid Number X Ash X Aromatics X Carbon Residue X X X Copper Strip Corrosion X X Hydrogen Content X Ignition Quality (Cetane Number, Cetane Index, or Derived Cetane Number)

X X

Storage Stability X X Sulfur Content X X X Trace Metals (Ca, Pb, Na, K and V) X Lubricity X X X Water and Sediment X X X X

FAME X X X X

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6. Fuel System Icing Inhibitor (FSII) (NATO S-1745) Series Testing Requirements for Specifications MIL-

DTL-85470

7. Marine Residual Fuel Oil (RME 180/380) Series Testing Requirements for Specification ISO 8217

Characteristics MIL DTL 85470 B-1

Series B-2

B-3 Series C-Series

Acid Number X X Color, Platinum Cobalt X Distillation X X Ethylene Glycol X X pH of 25 % solution in water X X Relative density X X X Water (mass %) X X Flash point X X Appearance/Workmanship X X X

A Series Characteristics ISO 8217 B-1

Series B-2

Series B-3

Kinematic Viscosity at 50°C X X X X X

Density at 15°C X X X X X Calculated Carbon Aromaticity

Index X X

Sulfur X X Flash point X X X X X

Hydrogen sulfide X X Acid Number X X

Total Sediment aged X X X Carbon Residue X X X

Pour Point X X Water X X X Ash X X

Vanadium X Sodium X X

Aluminum plus silicon X Used lubricating oils X

Page | 12

8. Lubrication Oil (LTL) (NATO O-250) Series Testing Requirements for Specification MIL PRF 17331

Characteristics MIL PRF

17331 B-1

Series B-2

Series B-3

Sulfur X n/a Acid Number X n/a Corrosion X X n/a Corrosion, Copper Strip X n/a Water content, mass% X X X n/a X Gravity X X n/a X Flash point X X X n/a Pour Point X X n/a Viscosity (per MIL PRF 17331) X X n/a Viscosity @100°C X X X n/a Viscosity @ 40°C X X X n/a X Emulsion test X X X n/a Foam Test X n/a Cleanliness (Solid Particle Contamination)

X X X n/a X

Neutralization number (acid/base) X n/a Appearance (to include visual sediment & water)

X X n/a

Solid contaminants X X n/a X X X X n/a

9. Lubrication Oil (LO6) (NATO O-278) Series Testing Requirements for Specification MIL PRF 9000

Characteristics MIL PRF 9000 B-1

Series B-2

Series B-3

Series C-Series n/a X Appearance/Workmanship X X X X Flash point X X X n/a Foam (stability only) X X X n/a Gravity X X n/a X Metals/Elements:Calcium, Magnesium, Zinc, Phosphorus

X n/a

Pour Point X X n/a Sulfur X n/a Total base number X n/a Viscosity index X n/a Viscosity at 100°C X X X n/a Viscosity at 40°C X n/a Neutralization number (acid/base) X X n/a Solid contaminants X X n/a Emulsion test X X n/a Water (by centrifuge) X X n/a X Ash, sulfated X X X

Page | 13

10. Diesel Fuel Oil (NATO F54) Series Testing Requirements for Specifications ASTM D975, EN 590

Characteristics ASTM

D975

EN 590 B-1

Series B-2

Series B-3

Flash point X X X X X X Water and Sediment X X Distillation X X X X Kinematic Viscosity X X Ash X X Sulfur X X X X Copper strip corrosion X X X Cetane number X X Cetane index X X X Aromaticity X Cloud Point X X X

LTFT/CFPP X X

Ramsbottom Carbon Residue

X X

Lubricity X Conductivity X API Gravity or Density at 15°C

X X X X X X

Polycyclic aromatic hydrocarbons

X X

Manganese content X X Water Content X X X X Total Contamination X X

FAME X X X X

Oxidation stability X X Appearance/Workmanship X X X X X X Pour Point X X X

Page | 14

Attachment 3: Approved Testing Methods

Table 1: Aviation Turbine Fuels

Def Stan 91-

Jet A/A-1

(ASTM

D1655)

JP-8 (MIL-DTL-

83133)

JP-5 (MIL-

DTL-

5624)

Appearance Visual Visual Visual

ASTM D6986

Visual

Color (Visual) Visual Visual Visual Visual Density or API

Gravity

IP365,

D4052

D1298, IP 160,

D4052, IP

D1298, IP160, D4052

(referee), IP 365, D7777

D1298, D4052, D7777

Particulate Matter

IP 423,

D5452, IP 216, D2276,

IP 423, D5452

(referee)

D2276, D5452 (referee), IP 423

D2276, D5452 (referee)

Particle Count

IP 564, IP 565,

IP 577

IP 564, IP 565, IP

577, D7619

D8166, IP 564, IP 565,

IP 577

D7619 (referee)

D8166, IP 564, IP

565, IP 577

D7619 (referee)

Total Acidity IP 354, D3242 IP 354, D3242 IP 354, D3242 D3242

Aromatics IP 156, D1319, IP 436, D6379

IP 156, D1319, IP

436, D6379

IP 156, D1319 (referee), IP 436, D6379

D1319 (referee), D6379

Total Sulfur IP 336 D1266 D2622, D4294, D5453, IP

D129, D1266, D2622, D3120, D4294 (referee) , D5453, or IP

D129, D1266, D2622, D3120, D4264 (referee), D5453

Mercaptan Sulfur

IP 342, D3227 IP 342, D3227 IP 342, D3227 (referee) D3227

Doctor Test IP 30 D4952 D4952 D4952

Distillation IP 123, D86 D86, D2887, IP 406, D7344, D7345, IP

D86 (referee), D2887, IP 406, IP 123, D7345

D86 (referee) , D7345, D2887

Viscosity IP 71, D445 IP 71 Section 1, D445, D7042, D7945

IP 71 Section 1, D445 (referee), D7042, D7945

D445

Smoke Point IP 598, D1322 IP 598, D1322 IP 598, D1322 IP 598, D1322

Naphthalenes D1840 D1840 D1840 D1840

Specific Energy

D3338, D4809 (referee), IP 12, IP 355

D3338, D4529, D4809 (referee), IP

D3338, D4529, D4809 (referee), IP 12

D3338, D3338M, D4529, D4809 (referee)

Hydrogen Content

N/A

D3343, D3701, D3343, D3701, D5291, D7171 (referee)

D3701, D5291, D7171 (referee)

Calculated Cetane Index

D976, D4737 D976, D4737 D976, D4737

Copper Strip Corrosion

IP 154, D130 D130 D130, IP 154 D130

Freezing Point IP 16, D2386 D5972, IP 435, D7153, IP 529, D7154, IP

528, D2386, IP 16

D2386 (referee), IP 16, D5972, IP

435, D7153, IP

529, D7154, IP

D2386 (referee), D5972, D7153, D7154

Existent Gum IP 540 D381, IP 540 D381(referee), IP540 D381(referee), IP

Flash Point IP 170 D56, D93, D3828, IP 170, IP 523

D56, D93(referee), D3828, IP 170

D56, D93 (referee), Page | 15

D3828

Lead Content N/A N/A N/A N/A FSII IP 424, D5006 D5006 D5006 (referee), IP 424 D5006

Filtration Time N/A N/A D2276, D5452 (referee)

D2276, D5452( referee)

MSEP D3948 D3948 D3948,

D7224 (referee)

D3948, D7224 (referee)

Electrical Conductivity

IP 274,

D2624

D2624 D2624, IP 274 D2624

Thermal Stability

IP 323. D3241 D3241 (Annex A3 is referee) See C- 5.4.1

D3241 (Annex A3 is considered referee) See C-5.4.1;

IP 323

D3241 (Annex A3 is referee) See C-5.4.1

Color (Saybolt) D156, D6045 D156 D156 (referee) , D6045

D156 (referee), D6045

Peroxide Number

D3703 N/A N/A

FAME IP 585, IP 590 D7797, IP 583,

IP 585 (referee), IP

590, IP 599

D7797, IP 583,

IP 585 (referee), IP 590, IP 599

D7797, IP 583, IP

(referee), IP 590, IP 599

Lubricity D5001 D5001 N/A N/A

Table 2: Marine Diesel

F-76 (MIL-DTL-16884)

Appearance D4176

Color (Visual) D1500 (referee), D6045 Density or API Gravity D1298 (referee), D4052, D287, D7777

Distillation D86 (referee), D2887 Flash Point D93(referee), D6450, D3828

Carbon Residue D524(referee), D189, D4530 Cloud Point D2500(referee), D5771, D5772, D5773 Pour point D97(referee), D5949, D5950, D5985

Copper Strip Corrosion D130 Viscosity D445, D7042

Water and Sediment D2709 Particulate D6217

Storage Stability D5304 (referee), D2274 Sulfur D5354(referee), D1266, D2622, D3120, D7039

Fatty Acid Methyl Ester (FAME) BS EN 14078, IP579, D7963 Lubricity D6079 (referee), D7688

Demulsification D1401 Particulate Contamination D6217 (referee), D5452

Acid Number D974 (referee), D664 Ash D482

Aromatics D6591 (referee), D2425 Hydrogen Content D7171 (referee), D4808, D5291

Ignition Quality (Cetane Number, Cetane Index or Derived Cetane

Number)

D613 (referee), D976, D6890, D7170

Trace Metals (Ca, Pb, Na, K and V) D7111 (referee), D3605

Page | 16

Table 3: Fuel System Icing Inhibitor

MIL-DTL-85470

Appearance Visual

Acid Number D1613 Color, Platinum Cobalt D1209 (referee), E450

Distillation D1078 Ethylene Glycol Per specification pH of 25% solution in water E70 Relative Density D891 (referee), D4052 Water (mass%) D1364 (referee), E1064, E203

Flash Point D93 (referee), D56, D3828

Table 4: Marine Residual Fuel Oil (RME180/380)

ISO 8217

Kinematic Viscosity ISO 3104 Density ISO 3675, ISO 12185

Calculated Carbon Aromaticity Index (CCAI)

Specification

Sulfur ISO 8754, ISO 14596, D4264 Flash Point ISO 2719

Hydrogen Sulfide IP570 Acid Number D664

Total Sediment, aged ISO 10307-2 Carbon Residue ISO 10370

Pour Point ISO 3016 Water ISO 3733

Ash ISO 6245 Vanadium IP 501 (referee), IP 470, ISO 14597

Sodium IP 501 (referee), IP 470 Aluminum plus silicon IP 501 (referee), IP 470, ISO 10478

Used lubricating Oil (ULO) IP 501 (referee), IP 470, IP 500 Cetane Index ISO 4264

Table 5: Lubrication Oil (LTL) (NATO O-250)

MIL-PRF-17331

Sulfur D129, D1552, D2622, D4927, D4951, D6443, D6481, D7751

Acid Number D974 (referee), ASTM D664

Corrosion D665, Procedure B Corrosion, Copper Strip D130

Water Content D6304 (referee), ASTM D7546 API Gravity D287, D1298 (referee), D4052 Flash Point D92, D93 (referee) Pour Point D97 (referee), D5950, D5949

Viscosity @ 4.4°C D445 (referee), D7042 Viscosity @100°C D445 (referee), D7042 Viscosity @40°C D445 (referee), D7042

Emulsion Test D1401 Total Sludge, iron and copper D4310

Foam test D892 Cleanliness (Solid Particle Contamination) D4898

Neutralization number (acid/base) D974 Solid contaminants (Coker Test Method) Specification, Appendix A Appearance (to include visual sediment & water) Visual

Page | 17

Table 6: Lubrication Oil (LO6) (NATO O-278)

MIL-PRF-9000

Appearance/Workmanship Visual Flash point D92

Foam (stability only) D892 Gravity D287, D1298, D4052 Calcium D4628, D4927, D4951, D6443, D6481

Magnesium D4628, D4927, D4951, D6443 Zinc D4638, D4927, D4951, D6443, D6481

Phosphorus D1091, D4047, D4927, D4951, D6443, D6481 Pour Point D97, D5949, D5950

Sulfur D129, D1552, D2622, D4927, D4951, D6443, D6481

Total base number D2896 Viscosity index D2270

Viscosity at 100°C D445 Viscosity at 40°C D445

Neutralization number (acid/base) D2896 Ash, sulfated D874

Corrosion, copper strip D130

Table 7: Diesel Fuel Oil

ASTM D975 EN 590

Flash point D93 EN ISO2719 Water and Sediment D2709, D1796 N/A

Distillation D86 EN ISO3405, EN ISO3924 Kinematic Viscosity D445 EN ISO3104

Ash D482 EN ISO6245 Sulfur D2622, D5453 EN ISO20846, EN ISO20884, EN

ISO13032

Copper strip corrosion D130 EN ISO2160

Cetane number D613 EN ISO5165, EN15195, EN16144 Cetane index D976 EN ISO4264 Aromaticity D1319 N/A Cloud Point D2500 EN23015

LTFT/CFPP D4539, D6371 EN116, EN16329

Carbon Residue D524 EN ISO10370 Lubricity D6079, D7688 EN ISO12156-1

Conductivity D2624 D4308 API Gravity or Density at 15°C

N/A EN ISO3675, EN ISO12185

Polycyclic aromatic hydrocarbons

N/A EN12916

Manganese content N/A prEN16576 Water Content N/A EN ISO12937

Total Contamination N/A EN12662

FAME N/A EN14078

Oxidation stability N/A EN ISO 12205, EN15751 Appearance/Workmansh ip Visual Visual

Page | 18

Table 8: Reclaimed Fuel Oil (FOR)

MIL-PRF-24951

Flashpoint D93 Explosiveness FED-STD-791 Test Method 1151.1

Water and Sediment D1796 Sediment D473

API Gravity or Density at 60°C D287 Viscosity at 40°C D445 Viscosity at 50°C D88

Pour Point D97 Neutrality FED-STD-791 Test Method 5101

Sulfur Content D129 Ash D482

Trace Metals: Arsenic, Cadmium, Chromium and Lead

EPA SW-846, Method 3040/3050 and proposed method for evaluating solid waste

Total Halogen D808-87

Page | 19

Attachment 4: Annual Estimates by Location:

Table listed below illustrates the annual estimated work by fuel grade to be performed. Attachment 2 defines the tests that makeup a series (slate) in accordance with specifications and/or MIL-STD-3004-1. Individual test shall be requested from any test in the A, B or C series but most common will be retests following a testing failure. Due to unpredictable situations unable to state the exact tests that will be requested but a historical series average.

Guam Jet A/A-1 JP-5 JP-8 F-76 FSII

A-Series 5 A-Series 5 A-Series 5 A-Series 5 A-Series 2

B-1 Series

30 B-1 Series 25 B-1

Series 5 B-1 Series 25 B-1 Series 0

B-2 Series

10 B-2 Series 10 B-2

Series 35 B-2 Series 5 B-2 Series 6

B-3 Series

0 B-3 Series 0 B-3

Series 0 B-3 Series 0 B-3 Series 0

C Series 30 C Series 5 C Series 25 C Series 39 C Series 0

Individual 10 Individual 10 Individual 25 Individual 15 Individual 1

RME LTL LO6 Diesel

A-Series 5 A-Series 3 A-Series 5 A-Series 1

B-1 Series 0 B-1

Series 0 B-1 Series 0 B-1 Series 1

B-2 Series 5 B-2

Series 3 B-2 Series 6 B-2 Series 5

B-3 Series 0 B-3

Series 0 B-3 Series 0 B-3 Series 0

C Series 5 C Series 1 C Series 0 C Series 6

Individual 1 Individual 1 Individual 12 Individual 5

Subic Bay Jet A/A-1 JP-5 JP-8 F-76

A-Series 5 A-Series 5 A-Series 0 A-Series 0

B-1 Series 0 B-1 Series 0 B-1 Series 0 B-1 Series 0

B-2 Series 10 B-2 Series 10 B-2 Series 10 B-2 Series 10

B-3 Series 0 B-3 Series 0 B-3 Series 0 B-3 Series 0

C Series 0 C Series 0 C Series 0 C Series 0

Individual 10 Individual 9 Individual 15 Individual 10

Page | 20

Attachment 5: Sample Shipment

1. Sample Shipment The Contractor shall upon request be responsible for shipping fuel samples from locations in C-1.0.1 to the laboratories in the chart below. Fuel samples shall be shipped within 48 hours of request and arrive to the below laboratory within five calendar days.

Naval Air Systems Command HAZMART Bldg. 2385 22680 Hammond Road Patuxent River, MD 20670

US ARMY TARDEC

Petroleum Laboratory Bldg. 5085 U Avenue, Bldg 85 New Cumberland, PA 17070-5083

Aerospace Fuels Laboratory AFPA/PTPLA 2430 C Street, Bldg 70, Area B Wright Patterson AFB OH 45433-7632

Naval Research Laboratory 4555 Overlook Avenue, SW Washington, DC 20375

Southwest Research Institute 6220 Culebra RD

San Antonio, TX 78238-5166

Air Force Research Laboratory AFRL 2977 Hobson Way

WPAFB, OH 45433

DLA Enery Okinawa Laboratory Okinawa Chibana Compound, RTE #74 Bldg. 53145

Chibana Okinawa City, Okinawa, Japan 904-2143

Intentionally Left Blank Intentionally Left Blank