H2O Analysis 16678 08012018.pdf

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NIST Center for Neutron Research Cooling Tower Maintenance and Repair Services
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1333ND20QNB610625
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This document outlines requirements for cooling tower maintenance and repair services at the National Institute of Standards and Technology Center for Neutron Research facility. The scope of work includes inspecting, cleaning, performing routine maintenance, and completing any necessary repairs on the main heavy water-moderated nuclear reactor's secondary cooling water cooling towers and associated subsystems over the next year. The cooling towers are located behind Building 235 and consist of a three-cell 2002 Balcke-Durr primary tower and a two-cell 2011 BAC modular secondary tower, with all cells containing aged Amarillo right-angle gear drives requiring special attention. Additional systems integrated with the cooling towers, such as a deicing mechanism, fire protection, and plume abatement equipment, are also included.

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QualiChem, Inc.

P.O. Box 926 • Salem, Virginia 24153

Phone: (540) 375-6700 • Fax: (540) 375-3880 www.qualichem.com

Customer No. Coastline Date Received: 07/25/18

Date Completed: 08/01/18

Company NIST

Location Gaithersburg, MD

System

Sample Name Makeup Cooling

Recirc

Sample Number #16678A #16678B

P-Alkalinity as CaCO3 0 ppm 20 ppm

M-Alkalinity as CaCO3 41 ppm 272 ppm

Total Phosphate as PO4 N/A ppm N/A ppm pH 6.5 8.6

Conductivity, Un-neutralized 230.7 uMS 1,271.0 uMS

Conductivity, neutralized N/A uMS N/A uMS

TDS (calculated) 173.0 ppm 953.3 ppm

Triazole N/A ppm 0.0 ppm

Glycol Type N/A N/A

Glycol Concentration N/A % v/v N/A % v/v

Reserve Alkalinity N/A mL N/A mL

PTSA N/A ppb 155.7 ppb

MP-AES Results

Calcium as Ca +2

16.3 ppm 160.5 ppm

Magnesium as Mg +2

4.1 ppm 27.5 ppm

Calcium Hardness as CaCO3 40.8 ppm 401.1 ppm

Magnesium Hardness as CaCO3 16.9 ppm 113.3 ppm

Total Hardness as CaCO3 57.7 ppm 514.4 ppm

Silica as SiO2 4.9 ppm 16.4 ppm

Total Iron as Fe 0.02 ppm 0.05 ppm

Copper as Cu <0.01 ppm 0.03 ppm

Molybdenum as Mo N/A ppm <0.02 ppm

IC Results

Chloride 37.7 ppm 164.0 ppm

Nitrite N/A ppm N/A ppm

Nitrate N/A ppm N/A ppm

Phosphate (as PO4) 0.8 ppm 1.2 ppm

Sulfate 7.6 ppm 173.3 ppm

ND = Not Detected

Detection Limit 0.1 ppm 0.1 ppm

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