W912PL21B0002_Amendment0003.pdf
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- FY18 Ground Transport Equipment Facility Federal contract opportunity
- Solicitation number
- W912PL21B0002
About this file
This solicitation is for the construction of a Ground Transport Equipment Facility at Fort Huachuca, Arizona. Services required include the construction of a vehicle maintenance shop, organizational storage building, vehicle wash platform, vehicle loading dock, petroleum, oils and lubricants storage, hazardous waste storage, and demolition of three existing buildings totaling 10,072 square feet. The project is based on the medium-sized Tactical Equipment Maintenance Facility standard but customized for the customer's functions. Estimated costs range from $25-100 million. The NAICS code is 236220. The solicitation will be issued under full and open competition without exclusion of sources. The Department of the Army Corps of Engineers Engineering District Los Angeles is the issuing agency.
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Other files for this federal contract opportunity
| File | Type | Posted |
|---|---|---|
| Bid Abstract W912PL-20-B-0002.pdf | ||
| W912PL21B0002_Amendment0005.pdf | ||
| W912PL21B0002_Amendment0004.pdf | ||
| W912PL21B0002_Amendment0002.pdf | ||
| W912PL21B0002_Amendment0001.pdf | ||
| Site Visit Sign In.pdf | ||
| Plans_W912PL21B0002_Ft Huachuca.pdf | ||
| Spec_W912PL21B0002_Ft Huachuca_AZ.pdf | ||
| Plans_W912PL21B0002_Ft Huachuca.pdf |
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AMENDMENT OF SOLICITATION/MODIFICATION OF CONTRACT 1. CONTRACT ID CODE
2. AMENDMENT/MODIFICAITON NO. 3. EFFECTIVE DATE 4. REQUISITION/PURCHASE REQ. NO. 5. PROJECT NO. (If applicble)
7. ADMINISTERED BY (If other than Item 6) CODE
STANDARD FORM 30 (REV. 10-83)
Prescribed by GSA FAR (48 CFR) 53.243
FACILITY CODE
9A. AMENDMENT OF SOLICIATION NO.
9B. DATED (SEE ITEM 11)
10A. MODIFICATION OF CONTRACT/ORDER NO.
10B. DATED (SEE ITEM 13)
11. THIS ITEM ONLY APPLIES TO AMENDMENTS OF SOLICITATIONS
The above numbered solicitation is amended as set forth in Item 14. The hour and date specified for receipt of Offers is extended, is not extended.
Offers must acknowledge receipt of this amendment prior to the hour and date specified in the solicitation or as amended, by one of the following methods:
(a)By completing items 8 and 15, and returning copies of the amendment; (b) By acknowledging receipt of this amendment on each copy of the offer submitted;
or (c) By separate letter or telegram which includes a reference to the solicitation and amendment numbers. FAILURE OF YOUR ACKNOWLEDGMENT TO BE RECEIVED AT THE PLACE DESIGNATED FOR THE RECEIPT OF OFFERS PRIOR TO THE HOUR AND DATE SPECIFIED MAY RESULT IN REJECTION OF YOUR OFFER. If by virtue of this amendment your desire to change an offer already submitted, such change may be made by telegram or letter, provided each telegram or letter makes reference to the solicitation and this amendment, and is received prior to the opening hour and date specified.
12. ACCOUNTING AND APPROPIRATION DATA (If required)
13. THIS ITEM ONLY APPLIES TO MODIFICATION OF CONTRACTS/ORDERS.
IT MODIFIES THE CONTRACT/ORDER NO. AS DESCRIBED IN ITEM 14.
CHECK ONE A. THIS CHANGE ORDER IS ISSUED PURSUANT TO: (Specify authority) THE CHANGES SET FORTH IN ITEM 14 ARE MADE IN THE CONTRACT ORDER
NO. IN ITEM 10A.
B. THE ABOVE NUMBERED CONTRACT/ORDER IS MODIFIED TO REFLECT THE ADMINISTRATIVE CHANGES (such as changes in paying office, appropriation date, etc. ) SET FORTH IN ITEM 14, PURSUANT TO THE AUTHORITY OF FAR 43.103(b).
C. THIS SUPPLEMENTAL AGREEMENT IS ENTERED INTO PURSUANT TO AUTHORITY OF:
D. OTHER (Specify type of modification and authority)
E. IMPORTANT: Contractor is not, is required to sign this document and return copies to the issuing office.
Except as provided herein, all terms and conditions of the document referenced in Item 9A or 10A, as heretofore changed, remains unchanged and in full force and effect.
15C. DATE SIGNED
15A. NAME AND TITLE OF SIGNER (Type or print)
16C. DATE SIGNED
16A. NAME AND TITLE OF CONTRACTING OFFICER (Type or print)
14. DESCRIPTION OF AMENDMENT/MODIFICATION ( Organized by UCF section headings, including solicitation/contract subject matter where feasible.)
PAGE OF PAGES
6. ISSUED BY CODE
8. NAME AND ADDRESS OF CONTRACTOR (No., street, county, State and ZIP Code) (X)
CODE
15B. CONTRACTOR/OFFEROR
(Signature of person authorized to sign)
16B. UNITED STATES OF AMERICA
(Signature of Contracting Officer)
NSN 7540-01-152-8070
Previous edition unusable
0003 27 OCT 2020
W912PL
U.S Army Corps of Engineers,Los Angeles Dist CESPL-CT-E, East Region Branch 915 Wilshire Blvd.
Los Angeles, CA 90017
SEE ITEM 6
W912PL-21-B-0002
18 September2020
FY18 GROUND TRANSPORT EQUIPMENT FACILITY, FORT HUACHUCA, AZ
SEE CONTINUATION PAGE FOR AMENDMENT 0003 SUMMARY OF CHANGES.
PLEASE BE ADVISED THAT DOD SAFE DROP-OFF CODES EXPIRE IN 14 DAYS. ALL BIDDERS MUST REQUEST A
NEW CODE IF THEIR EXISTING CODE WILL EXPIRE BEFORE BID SUBMITTAL.
GROUND TRANSPORTATION EQUIPMENT BUILDING (GTEB) FORT HUACHUCA
AMENDMENT 0003 SUMMARY OF CHANGES
SPECIFICATIONS:
1. Revise Table of Contents Page 5 adding an Appendices Section and
a. Appendix 1. Hazardous Material Reports for Existing Motor Pool buildings to be demolished. NOTE: Contractor to bid based on info in that attached test results. If no results are available for a building, for bidding purposes, contractor shall assume no HAZMAT.
HOWEVER, contractor is responsible for performing HAZMAT testing on all buildings to be demo’ed. Any discrepancies resulting from contractor testing will be addressed via Changes clause.
b. Appendix 2. Fort Huachuca Fire Department requirements. Note; these items are required for work under this contract.
2. Revise Section 01 57 20 Paragraph 3.18 regarding UXO monitors.
3. Revise CD-101 with FH Fire Department Requirements note.
4. Revise Drawing CD-104 adding Notes 5-9.
5. Revise Drawing C-510 showing fence fabric at 8 feet high.
6. Revise Drawing A-102 and add Drawing A-102a.
7. Revise Drawing A-620; A-640 and A-641.
8. Revise Drawing M-602 clarifying "Option" requirements.
9. Revise E-601 Note for wire size form DP-1 to XP-1.
10. Revise Drawing FA-601 adding Note 6 on Fire Alarm Panel requirement (Monaco).
11. Revise a series of Electrical drawings; E-001; EP-102; EG-102; E-401; E-402; E-504; 101;
T-102; T-103; T-501; T-502; T-601.
12. SF-1442. Change Bid due date from 30 October 2020 to 6 November 2020 12PM PST.
SOLICITATION, OFFER,
AND AWARD
(Construction, Alteration, or Repair)
1. SOLICITATION NUMBER 2. TYPE OF SOLICITATION
SEALED BID (IFB)
NEGOTIATED (RFP)
3. DATE ISSUED PAGE OF PAGES
IMPORTANT - The "offer" section on the reverse must be fully completed by the offeror.
4. CONTRACT NUMBER 5. REQUISITION/PURCHASE REQUEST NUMBER 6. PROJECT NUMBER
7. ISSUED BY CODE 8. ADDRESS OFFER TO
9. FOR INFORMATION CALL
A. NAME B. TELEPHONE NUMBER (Include area code) (NO COLLECT CALLS)
SOLICITATION
NOTE: In sealed bid solicitations "offer" and "offeror" mean "bid" and "bidder".
10. THE GOVERNMENT REQUIRES PERFORMANCE OF THE WORK DESCRIBED IN THESE DOCUMENTS (Title, identifying number, date):
11. The Contractor shall begin performance within calendar days and complete it within calendar days after receiving award, notice to proceed. This performance period is mandatory, negotiable. (See .)
12A. THE CONTRACTOR MUST FURNISH ANY REQUIRED PERFORMANCE PAYMENT BONDS?
(If "YES," indicate within how many calendar days after award in Item 12B.)
12B. CALENDAR DAYS
YES NO
13. ADDITIONAL SOLICITATION REQUIREMENTS:
A. Sealed offers in original and copies to perform the work required are due at the place specified in Item 8 by (hour) local time (date). If this is a sealed bid solicitation, offers will be publicly opened at that time. Sealed envelopes containing offers shall be marked to show the offeror’s name and address, the solicitation number, and the date and time offers are due.
B. An offer guarantee is, is not required.
C. All offers are subject to the (1) work requirements, and (2) other provisions and clauses incorporated in the solicitation in full text or by reference.
D. Offers providing less than calendar days for Government acceptance after the date offers are due will not be considered and will be rejected.
NSN 7540-01-155-3212
Designed using Perform Pro, WHS/DIOR, Oct 96
1442-103 STANDARD FORM 1442 (REV. 4-85) (EG)
Prescribed by GSA - FAR (48 CFR) 53.236-1(d)
W912PL21B0002 X 18 SEP 2020 1 OF
USACE, Los Angeles District Contracting Division, West Region Branch 915 Wilshire Blvd Los Angeles, CA 90017
DoD Secure Access File Exchange (DoD Safe) at https://safe.apps.mil/
See Section 00 22 13, Special Instructions Pertaining to Submission of Electronic Bids
JIMMY L. BARTON 213.452.3251
FY18 GROUND TRANSPORT EQUIPMENT FACILITY, FORT HUACHUCA, AZ
This a fully designed project (Design Bid Build). Construct a Ground Transport Equipment Building Complex. Project includes a vehicle maintenance shop (ground transport equipment building), organizational storage building, organizational vehicle parking, vehicle wash platform, vehicle loading dock, petroleum, oils and lubricants (POL) storage, and other hazardous waste/material storage. The vehicle maintenance facility will include mechanical and electrical rooms, telecommunications, HVAC, fire detection and sprinkler suppression systems, building information systems, intrusion detection system (IDS) installation, integrated energy, monitoring and control system (EMCS) connected to the base monitoring systems, and the installation of fire alarm systems. Supporting facilities will include connection to all utilities, lighting, paving, parking areas, sidewalks, curbs and gutters, rainwater harvesting systems, and signage. Heating and air conditioning will be provided by self-contained systems.
The estimated magnitude of project is between $25,000,000 and $100,000,000. This solicitation is UNRESTRICTED and all responsive and responsible parties are invited to submit a bid. The North American Industry Classification System (NAICS) code is 236220 Commercial and Institutional Building
BIDDERS PLEASE NOTE: “This project may be delayed, canceled or revised at any time prior to award.”
10 * 00 73 00
X X *Section 00 73 00
X 10
0 12PM
06 NOV 2020
X
OFFER (Must be fully completed by offeror)
STANDARD FORM 1442 BACK (REV. 4-85)
14. NAME AND ADDRESS OF OFFEROR (Include ZIP Code) 15. TELEPHONE NUMBER (Include area code)
16. REMITTANCE ADDRESS (Include only if different than Item 14)
CODE FACILITY CODE
17. The offeror agrees to perform the work required at the prices specified below in strict accordance with the terms of this solicitation, if this offer is accepted by the Government in writing within calendar days after the date offers are due. (Insert any number equal or greater than the minimum requirement stated in 13D. Failure to insert any number means the offeror accepts the minimum in Item 13D.)
AMOUNTS
18. The offeror agrees to furnish any required performance and payment bonds.
19. ACKNOWLEDGEMENT OF AMENDMENTS
(The offeror acknowledges receipt of amendments to the solicitation - give number and date of each)
AMENDMENT NO.
DATE
20A. NAME AND TITLE OF PERSON AUTHORIZED TO SIGN OFFER (Type or print) 20B. SIGNATURE 20C. OFFER DATE
AWARD (To be completed by Government)
21. ITEMS ACCEPTED
22. AMOUNT 23. ACCOUNTING AND APPROPRIATION DATA
24.SUBMIT INVOICES TO ADDRESS SHOWN IN
(4 copies unless otherwise specified)
ITEM 25. OTHER THAN FULL AND OPEN COMPETITION PURSUANT TO
10 U.S.C. 2304(c) ( ) 41 U.S.C. 253(c) ( )
26. ADMINISTERED BY 27. PAYMENT WILL BE MADE BYCODE
CONTRACTING OFFICER WILL COMPLETE ITEM 28 OR 29 AS APPLICABLE
28. NEGOTIATED AGREEMENT (Contractor is required to sign this document and return copies to the issuing office.) Contractor agrees to furnish and deliver all items or perform all work requirements identified on this form and any continuation sheets for the consideration stated in this contract. The rights and obligations of the parties to this contract shall be governed by (a) this contract award, (b) the solicitation, and
(c) the clauses, representations, certifications, and specifications incorporated by reference in or attached to this contract.
29. AWARD. (Contractor is not required to sign this document.) Your offer on this solicitation is hereby accepted as to the items listed. This award consummates the contract, which consists of (a) the Government solicitation and your offer, and (b) this contract award. No further contractual document is necessary.
30A. NAME AND TITLE OF CONTRACTOR OR PERSON AUTHORIZED TO SIGN
(Type or print)
30B. SIGNATURE 30C. DATE
31A. NAME OF CONTRACTING OFFICER (Type or print)
31B. UNITED STATES OF AMERICA 31C. AWARD DATE
BY
DUNS NO.: TAX ID NO.:
CAGE CODE NO.:
( ) - ; FAX ( ) -
USACE, Finance Center
ATTN: CEFCO-AO-D
5722 Integrity Drive Millington, TN 38054-5005
FY18 Ground Transport Facility W912PL21B0002 Ft Huachuca, AZ
TABLE OF CONTENTS - 5
DIVISION 27 - COMMUNICATIONS
27 05 14.00 10 CABLE TELEVISION PREMISES DISTRIBUTION SYSTEM
27 05 28.36 CABLE TRAYS FOR COMMUNICATIONS SYSTEMS
27 10 00 BUILDING TELECOMMUNICATIONS CABLING SYSTEM
27 13 23 COMMUNICATIONS OPTICAL BACKBONE CABLING
27 51 16 RADIO AND PUBLIC ADDRESS SYSTEMS
DIVISION 28 - ELECTRONIC SAFETY AND SECURITY
28 08 10 ELECTRONIC SECURITY SYSTEM ACCEPTANCE TESTING
28 10 05 ELECTRONIC SECURITY SYSTEMS (ESS)
28 31 49 CARBON MONOXIDE DETECTORS
28 31 76 INTERIOR FIRE ALARM AND MASS NOTIFICATION SYSTEM
DIVISION 31 - EARTHWORK
31 00 00 EARTHWORK
31 11 00 CLEARING AND GRUBBING
DIVISION 32 - EXTERIOR IMPROVEMENTS
32 11 20 SUBBASES FOR FLEXIBLE PAVING
32 11 23 AGGREGATE BASE COURSES
32 12 10 BITUMINOUS TACK COAT
32 12 17 HOT MIX BITUMINOUS PAVEMENT
32 12 18 RESIN MODIFIED PAVEMENT SURFACING MATERIAL
32 16 13 CONCRETE SIDEWALKS AND CURBS AND GUTTERS
32 17 23 PAVEMENT MARKINGS
32 31 13.53 HIGH-SECURITY CHAIN LINK FENCES AND GATES
DIVISION 33 - UTILITIES
33 08 55 COMMISSIONING OF FUEL FACILITY SYSTEMS
33 11 00 WATER UTILITY DISTRIBUTION PIPING
33 30 00 SANITARY SEWERS
33 40 00 STORM DRAINAGE UTILITIES
33 51 13 NATURAL-GAS METERING
33 51 15 NATURAL-GAS DISTRIBUTION
33 56 10 FACTORY-FABRICATED FUEL STORAGE TANKS
33 58 00 LEAK DETECTION FOR FUELING SYSTEMS
33 71 02 UNDERGROUND ELECTRICAL DISTRIBUTION
33 82 00 TELECOMMUNICATIONS OUTSIDE PLANT (OSP)
DIVISION 41 - MATERIAL PROCESSING AND HANDLING EQUIPMENT
41 22 13.13 BRIDGE CRANES
-- End of Table of Contents --
APPENDICES
APPENDIX 1
APPENDIX 2
HAZARDOUS MATERIAL REPORTS
FORT HUACHUCA FIRE DEPARTMENT REQUIRMENTS
AMENDMENT 3
Client Job: 1-1580911 PO Number:68056
JobNumber: 201300606
Routing Number: -
# Samples: 1
PLMn
PLM The "New" Method; see below
Client:
Polarized Light Microscope (PLM) Analysis for Asbestos in Bulk Sample
Method and Analysis Information:
Each bulk sample is first dissected under a 7-30x magnification stereo-microscope. This examination is used to determine the general type of sample, how many and what type of layers it has, and initial estimates of fiber types and quantities. Second, liquid media mounts are made of each layer - such mounts may be of selected fibers (used solely for identification purposes) or may be representative of the layer as a whole (used for quantitation purposes). The mounts may be made in a synthetic Canadian balsam, one of several solvents, or in refractive index oils (media of known refractive index). Generally, a variety of different mounts are made: some optimized for fiber visibility, some optimized for fiber identification, and some optimized for fiber quantitation. The mounted slides are then examined at 50-400x magnification on a Nikon Labphot-pol microscope. Optical characteristics are used to identify each observed fiber type; the optical data are contained for each sample on its detail analysis sheet, attached.
Current EPA and NESHAP regulations designate a result of <=1 % asbestos as "negative" and >1 % asbestos as "positive". Samples containing layers that have been determined to be "positive" may have to be handled differently during a renovation or demolition than samples whose layers have been determined to be "negative."
The method of fiber identification and quantitation is the “Standard Operating Procedures for the Analysis of Asbestos in Bulk Samples using Polarized Light Microscopy”, Chapter 7 of the Quality Assurance and Management Manual. This SOP and its associated reporting have been designed to satisfy all requirements in both EPA Method 600/M4-82-020 (The Interim Method) and EPA Method 600/R-93/116 (The New Method). The Interim Method is the required method for AHERA (US EPA 40 CFR Pt. 763), but this method calls for the reporting of composited results of multi-layered samples that is no longer an acceptable reporting practice in most circumstances. Current EPA rules, such as NESHAP (US EPA 40CFT Pt. 61), as well as NVLAP accreditation policies, call for separate reporting for each layer of multi-layered samples. The New Method contains the same procedures for identification and quantification of asbestos as does the Interim Method, except that multi-layered samples are reported to comply with the latest US
EPA rule. Fiberquant not only reports the asbestos content of each layer of multi-layered samples separately (satisfying current EPA and NVLAP reporting requirements), but Fiberquant also reports what percentage of the sample each layer comprises. Therefore, the results may be arithmetically composited to satisfy the reporting requirements of the Interim Method. The method of fiber quantitation is an estimation technique in which the analysts quantitation is routinely calibrated by reference quantitation standards, and which has been shown to be equivalent in precision and accuracy to point counting. Friability is estimated for the purposes of deciding when to point count. Friabilities determined in the field take precedence over those determined in the laboratory. Those sample layers which are friable and estimated by the analyst to contain <= 1% asbestos are point counted using 400 points. Such point counting is required by NESHAP (National Emission Standards for Hazardous Air Polutants, Nov. 1990) in order to rely on analytical results that are <= 1%. The coefficient of variation for the estimation quantitation technique is 100% in the range 0- 5%. This means that PLM analysis is not capable of conclusively determining whether a layer containing close to 1% asbestos is actually "positive" or
"negative". For this reason, Fiberquant refers to results where asbestos was detected but <= 1% as "borderline negative", and results where asbestos was >1 % but <= 2% as "borderline positive" to indicate the uncertainty in assigning a "positive" or "negative" label. In the sample summary, "ND" means that no asbestos was detected during the analysis. A "Tr" or "Trace" of asbestos reported is defined for our purposes as the detection of several asbestos fibers during the analysis; this level would be right at the limit of detection for the method. Trace is only reported on the analysis detail - in the summary a trace would be reported as <=1%. The limit of detection (the smallest % of asbestos that can be detected) varies greatly depending on the matrix in which the asbestos is found. As little as 0.001% asbestos can be detected in favorable samples, while detection in unfavorable samples may approach the detection limit of 1% stated in the method. During the analysis, the analyst, for Fiberquant identification purposes only, determines the "apparent sample type" and "apparent layer types." It must be emphasized that these types are only what is apparent. Often, different materials appear similar or identical after sampling, so the analyst may assign a type other than what was sampled.
Floor tiles present a special problem for PLM asbestos analysis. Floor tile can contain chrysotile fibers so thin that they cannot be resolved by optical methods. In such a case, we may observe a percentage of asbestos which is lower than the actual percentage, or not observe asbestos at all when some is present. For this reason, floor tiles reported as negative should be confirmed to be negative using transmission electron microscope
(TEM) analysis. Likewise, vermiculite insulation materials containing traces of asbestiform asbestos present a problem for routine PLM analysis - the amphiboles are sometimes present in trace amounts inhomogeneously distributed. For this reason, loose vermiculite samples reported as negative should be confirmed to contain no amphibole using hydroseparation techniques.
The samples were analyzed under the following ongoing quality assurance program: Blank samples are routinely analyzed to maintain contamination-free materials. Each analyst has at least a bachelor's degree in physical science, and has also completed extensive training specific to asbestos analysis for 1-3 months before being allowed to analyze client samples. Qualitative reference samples are routinely analyzed to assure that analysts can identify asbestos and asbestos-look-alike fibers. Quantitative reference samples are routinely analyzed to calibrate and characterize the
Method: EPA 600/R-93/116Rec: 1/17/2013
Report Date: 1/23/2013 Date Analyzed: 1/23/2013
Fiberquant Internal SOP:
EMCOR GOVERNMENT SVCS
CLARKSTON RD BLDG 30033
FT HUACHUCA, AZ
Office Phone: (520) 533-5906
FAX: (520) 533-3699
85613-0000
5025 S. 33rd Street Phoenix, Arizona 85040-2816 Phone: 602-276-6139 1-800-743-2687 FAX: 602-276-4558
Fiberquant, Inc. Page 1 of 3
PLM Analysis Summary: Job Number: 201300606 1-1580911 estimation procedure. Microscope alignment is checked each day. Refractive index oils are calibrated at least quarterly. At least 10% of client samples are re-analyzed from scratch by a different analyst than the original, and any discrepancies are resolved for the sample and similar sample types before the results are reported. All quality checks performed for these samples were in control except as detailed in the "Analytical Notes" below. All analysts participate in interlab round robins and proficiency testing to assure competence. Fiberquant is accredited by NVLAP (Lab #101031) for the analysis of bulk samples for asbestos using PLM. Accreditation does not imply endorsement by the EPA, any other United States governmental agency or any private agency or association. Each lab analysis refers only to the sample tested, and may not, due to the sampling process, be representative of the material sampled. This report may not be reproduced except in full, without the approval of Fiberquant Analytical
Services.
Job Analysis Notes:
Some results may have been calculated using client supplied data, such as volume or area sampled, for which Fiberquant assumes no liability for accuracy.
Sample Number Lab Number Apparent Sample Type * Positive Layer Yes or No
Layer Color Apparent Layer Type * Asbestos Results
Roofing2013-00606- 168056-01 Positive Layer? YesSample # no asbestos detectedroofing roll/shingleblackLayer # 1 no asbestos detectedroofing roll/shingleblackLayer # 2
20-30% chrysotile asbestosroofing roll/shingleblackLayer # 3
20-30% chrysotile asbestosroofing roll/shingleblackLayer # 4
20-30% chrysotile asbestosroofing roll/shingleblackLayer # 5 no asbestos detectedroofing roll/shingleblackLayer # 6 no asbestos detectedroofing roll/shingleblackLayer # 7 no asbestos detectedroofing roll/shingleblackLayer # 8
30-40% chrysotile asbestosroof plyblackLayer # 9 no asbestos detectedroof plyblackLayer # 10
* Apparent Sample Types and Apparent Layer Types are as they appeared to the analyst. Since many types of materials appear similar after sampling damage, the apparent type of material may not be the actual type of material.
5025 S. 33rd Street Phoenix, Arizona 85040-2816 Phone: 602-276-6139 1-800-743-2687 FAX: 602-276-4558
Fiberquant, Inc. Page 2 of 3
PLM Analysis Details Job Number: 201300606 1-1580911
2013-00606- 168056-01 Lab Number Sample Sampled:
DMSAnalyzed By 1/23/2013
Homogeneous
Roofing
No
Fibrous SolidOKAn?
10# Layers YesPos Layer?
Apparent Smp Type cellulose fiber chrysotile asbestosFiber Identification:
Sample Analytical Note
Procedure: tweased apart using forceps. Procedure: dissolution of matrix using solvent. Note: there appears to be more than one sample layer sequence in the bag (e.g., samples from more than one location); therefore, the reported layer sequence has been estimated/composited.
Fibers
Color Mrph Iso Pleo Bi Elg Ext Oil Col Par Col Per RI Par RI Per
Refractive Index Determinations cellulose fiber chrysotile asbestos 1.556 1.5491.550 vb/g pb/r
W F N N H + U
W A N N L + P
Non-Fibrous Components (in approx. decreasing order): bitumen, rock, 30# Sub-Samples
Condition:acceptable
Layers
# Layer Type % Color Friability
Percents of Each Fiber
Fib 1 Fib 2 Fib 3 Fib 4 Fib 5 Fib 6
1 11 30-40% n.d. - - - -roofing roll/shingle black 1
2 11 30-40% n.d. - - - -roofing roll/shingle black 1
3 11 2-5% 20-30% - - - -roofing roll/shingle black 1
4 11 2-5% 20-30% - - - -roofing roll/shingle black 1
5 11 2-5% 20-30% - - - -roofing roll/shingle black 1
6 11 30-40% n.d. - - - -roofing roll/shingle black 1
7 11 30-40% n.d. - - - -roofing roll/shingle black 1
8 11 30-40% n.d. - - - -roofing roll/shingle black 1
9 6 5-10% 30-40% - - - -roof ply black 1
10 6 60-70% n.d. - - - -roof ply black 1
100Total % 20-30% 10-20% - - - -Overall %
Fr=Friability: 1=very non-friable; 2= non-friable; 3=friable; 4=highly friable Colors: B=black;BL=blue;BR=brown;CL=clear;G=Green;GY=gray;OR=orange;OW=off-white;PN=pink;PU=purple;R=red;TN=tan;W=white;Y=yellow;V=various Fiber Morphology: A=fine fibers/bundles, white, sinewy, flexible; B=fine fibers/bundles, w-br, straight, broomed ends; C=fine fibers/bundles, blue, straight, broomed ends;
D=fine to coarse fibers, CL-B, brittle; E=coarse fibers,CL or dyed, striated; F=coarse fibers or splinters, W-BR, ribbon-like; G=lath-like or shards, low aspect ratio, may taper Iso=isotropism - may be yes or no; Pleo=pleochroism - may be yes or no; Bi=birefringence - may be None, Low, Medium or High Elg=sign of elongation - may be +, - or B (both); Ext=extinction - may be Parallel, Oblique, None or Undulating; Oil=medium used to for dispersion staining Col Par=dispersion staining colors parallel to the fiber (fiber/halo): b/w=black/white; dg/py=dark gray/pale yellow; vg/y=violet gray/yellow; db/ly=dark blue/lemon yellow; vb/g= vivid blue/gold; sb/o=sky blue/orange; pb/r=pale blue/red; gb/dr=gray blue/dark red; w/b=white/black. Col Perp=same only perpendicular to fiber.
RI Par=refractive index parallel to fiber; RI Perp=refractive index perpendicular to fiber
23-Jan-13Analyst: DAVID M. SCHALLER
Larry S. Pierce, Approved Accreditation Signatory
Printed:
23-Jan-13Original Print Date:
5025 S. 33rd Street Phoenix, Arizona 85040-2816 Phone: 602-276-6139 1-800-743-2687 FAX: 602-276-4558
Fiberquant, Inc. Page 3 of 3
Client Job: 1-1610512 PO Number: 68056
JobNumber: 201301115
Routing Number: -
# Samples: 1
PLMn
PLM The "New" Method; see below
Client:
Polarized Light Microscope (PLM) Analysis for Asbestos in Bulk Sample
Method and Analysis Information:
Each bulk sample is first dissected under a 7-30x magnification stereo-microscope. This examination is used to determine the general type of sample, how many and what type of layers it has, and initial estimates of fiber types and quantities. Second, liquid media mounts are made of each layer - such mounts may be of selected fibers (used solely for identification purposes) or may be representative of the layer as a whole (used for quantitation purposes). The mounts may be made in a synthetic Canadian balsam, one of several solvents, or in refractive index oils (media of known refractive index). Generally, a variety of different mounts are made: some optimized for fiber visibility, some optimized for fiber identification, and some optimized for fiber quantitation. The mounted slides are then examined at 50-400x magnification on a Nikon Labphot-pol microscope. Optical characteristics are used to identify each observed fiber type; the optical data are contained for each sample on its detail analysis sheet, attached.
Current EPA and NESHAP regulations designate a result of <=1 % asbestos as "negative" and >1 % asbestos as "positive". Samples containing layers that have been determined to be "positive" may have to be handled differently during a renovation or demolition than samples whose layers have been determined to be "negative."
The method of fiber identification and quantitation is the “Standard Operating Procedures for the Analysis of Asbestos in Bulk Samples using Polarized Light Microscopy”, Chapter 7 of the Quality Assurance and Management Manual. This SOP and its associated reporting have been designed to satisfy all requirements in both EPA Method 600/M4-82-020 (The Interim Method) and EPA Method 600/R-93/116 (The New Method). The Interim Method is the required method for AHERA (US EPA 40 CFR Pt. 763), but this method calls for the reporting of composited results of multi-layered samples that is no longer an acceptable reporting practice in most circumstances. Current EPA rules, such as NESHAP (US EPA 40CFT Pt. 61), as well as NVLAP accreditation policies, call for separate reporting for each layer of multi-layered samples. The New Method contains the same procedures for identification and quantification of asbestos as does the Interim Method, except that multi-layered samples are reported to comply with the latest US
EPA rule. Fiberquant not only reports the asbestos content of each layer of multi-layered samples separately (satisfying current EPA and NVLAP reporting requirements), but Fiberquant also reports what percentage of the sample each layer comprises. Therefore, the results may be arithmetically composited to satisfy the reporting requirements of the Interim Method. The method of fiber quantitation is an estimation technique in which the analysts quantitation is routinely calibrated by reference quantitation standards, and which has been shown to be equivalent in precision and accuracy to point counting. Friability is estimated for the purposes of deciding when to point count. Friabilities determined in the field take precedence over those determined in the laboratory. Those sample layers which are friable and estimated by the analyst to contain <= 1% asbestos are point counted using 400 points. Such point counting is required by NESHAP (National Emission Standards for Hazardous Air Polutants, Nov. 1990) in order to rely on analytical results that are <= 1%. The coefficient of variation for the estimation quantitation technique is 100% in the range 0- 5%. This means that PLM analysis is not capable of conclusively determining whether a layer containing close to 1% asbestos is actually "positive" or
"negative". For this reason, Fiberquant refers to results where asbestos was detected but <= 1% as "borderline negative", and results where asbestos was >1 % but <= 2% as "borderline positive" to indicate the uncertainty in assigning a "positive" or "negative" label. In the sample summary, "ND" means that no asbestos was detected during the analysis. A "Tr" or "Trace" of asbestos reported is defined for our purposes as the detection of several asbestos fibers during the analysis; this level would be right at the limit of detection for the method. Trace is only reported on the analysis detail - in the summary a trace would be reported as <=1%. The limit of detection (the smallest % of asbestos that can be detected) varies greatly depending on the matrix in which the asbestos is found. As little as 0.001% asbestos can be detected in favorable samples, while detection in unfavorable samples may approach the detection limit of 1% stated in the method. During the analysis, the analyst, for Fiberquant identification purposes only, determines the "apparent sample type" and "apparent layer types." It must be emphasized that these types are only what is apparent. Often, different materials appear similar or identical after sampling, so the analyst may assign a type other than what was sampled.
Floor tiles present a special problem for PLM asbestos analysis. Floor tile can contain chrysotile fibers so thin that they cannot be resolved by optical methods. In such a case, we may observe a percentage of asbestos which is lower than the actual percentage, or not observe asbestos at all when some is present. For this reason, floor tiles reported as negative should be confirmed to be negative using transmission electron microscope (TEM) analysis. Likewise, vermiculite insulation materials containing traces of asbestiform asbestos present a problem for routine PLM analysis - the amphiboles are sometimes present in trace amounts inhomogeneously distributed. For this reason, loose vermiculite samples reported as negative should be confirmed to contain no amphibole using hydroseparation techniques.
The samples were analyzed under the following ongoing quality assurance program: Blank samples are routinely analyzed to maintain contamination-free materials. Each analyst has at least a bachelor's degree in physical science, and has also completed extensive training specific to asbestos analysis for 1-3 months before being allowed to analyze client samples. Qualitative reference samples are routinely analyzed to assure that
Method: EPA 600/R-93/116Rec: 1/31/2013
Report Date: 2/5/2013 Date Analyzed: 2/5/2013
Fiberquant Internal SOP:
EMCOR GOVERNMENT SVCS
CLARKSTON RD BLDG 30033
FT HUACHUCA, AZ
Office Phone: (520) 533-5906
5025 S. 33rd Street Phoenix, Arizona 85040-2816 Phone: 602-276-6139 1-800-743-2687 FAX: 602-276-4558
PLM Analysis Summary: Job Number: 201301115 1-1610512 analysts can identify asbestos and asbestos-look-alike fibers. Quantitative reference samples are routinely analyzed to calibrate and characterize the estimation procedure. Microscope alignment is checked each day. Refractive index oils are calibrated at least quarterly. At least 10% of client samples are re-analyzed from scratch by a different analyst than the original, and any discrepancies are resolved for the sample and similar sample types before the results are reported. All quality checks performed for these samples were in control except as detailed in the "Analytical Notes" below. All analysts participate in interlab round robins and proficiency testing to assure competence. Fiberquant is accredited by NVLAP (Lab
#101031) for the analysis of bulk samples for asbestos using PLM. Accreditation does not imply endorsement by the EPA, any other United States governmental agency or any private agency or association. Each lab analysis refers only to the sample tested, and may not, due to the sampling process, be representative of the material sampled. This report may not be reproduced except in full, without the approval of Fiberquant Analytical Services.
Job Analysis Notes:
Some results may have been calculated using client supplied data, such as volume or area sampled, for which Fiberquant assumes no liability for accuracy.
Sample Number Lab Number Apparent Sample Type * Positive Layer Yes or No
Layer Color Apparent Layer Type * Asbestos Results
Wall System2013-01115- 168056-01 Positive Layer? NoSample # no asbestos detectedpaintblackLayer # 1 no asbestos detectedpaper/cardboardtanLayer # 2 no asbestos detecteddrywall corewhiteLayer # 3
* Apparent Sample Types and Apparent Layer Types are as they appeared to the analyst. Since many types of materials appear similar after sampling damage, the
5025 S. 33rd Street Phoenix, Arizona 85040-2816 Phone: 602-276-6139 1-800-743-2687 FAX: 602-276-4558
PLM Analysis Details Job Number: 201301115 1-1610512
2013-01115- 168056-01 Lab Number Sample Sampled:
MACAnalyzed By 2/5/2013
Homogeneous
Wall System
No
Fibrous SolidOKAn?
3# Layers NoPos Layer?
Apparent Smp Type cellulose fiber Fiber Identification:
Sample Analytical Note
Procedure: tweased apart using forceps. Procedure: dissolution of matrix using solvent. Note: no texture layer observed.
Fibers
Color Mrph Iso Pleo Bi Elg Ext Oil Col Par Col Per RI Par RI Per
Refractive Index Determinations cellulose fiber
W F N N H + U
Non-Fibrous Components (in approx. decreasing order): powder, polymer, 8# Sub-Samples
Condition: acceptable
Layers
# Layer Type % Color Friability
Percents of Each Fiber
Fib 1 Fib 2 Fib 3 Fib 4 Fib 5 Fib 6
1 2 n.d. - - - - -paint black 1
2 4 90-100% - - - - -paper/cardboard tan 2
3 94 <=1% - - - - -drywall core white 3
100Total % 2-5% - - - - -Overall %
Fr=Friability: 1=very non-friable; 2= non-friable; 3=friable; 4=highly friable
Colors: B=black;BL=blue;BR=brown;CL=clear;G=Green;GY=gray;OR=orange;OW=off-white;PN=pink;PU=purple;R=red;TN=tan;W=white;Y=yellow;V=various
Fiber Morphology: A=fine fibers/bundles, white, sinewy, flexible; B=fine fibers/bundles, w-br, straight, broomed ends; C=fine fibers/bundles, blue, straight, broomed ends;
D=fine to coarse fibers, CL-B, brittle; E=coarse fibers,CL or dyed, striated; F=coarse fibers or splinters, W-BR, ribbon-like; G=lath-like or shards, low aspect ratio, may taper
Iso=isotropism - may be yes or no; Pleo=pleochroism - may be yes or no; Bi=birefringence - may be None, Low, Medium or High
Elg=sign of elongation - may be +, - or B (both); Ext=extinction - may be Parallel, Oblique, None or Undulating; Oil=medium used to for dispersion staining
Col Par=dispersion staining colors parallel to the fiber (fiber/halo): b/w=black/white; dg/py=dark gray/pale yellow; vg/y=violet gray/yellow; db/ly=dark blue/lemon yellow;
vb/g= vivid blue/gold; sb/o=sky blue/orange; pb/r=pale blue/red; gb/dr=gray blue/dark red; w/b=white/black. Col Perp=same only perpendicular to fiber.
RI Par=refractive index parallel to fiber; RI Perp=refractive index perpendicular to fiber
05-Feb-13Analyst: MICHAEL A. COOK
Larry S. Pierce, Approved Accreditation Signatory
05-Feb-13Original Print Date:
5025 S. 33rd Street Phoenix, Arizona 85040-2816 Phone: 602-276-6139 1-800-743-2687 FAX: 602-276-4558
Client Job: 1-1580912 PO Number:68057
JobNumber: 201300604
Routing Number: -
# Samples: 1
PLMn
PLM The "New" Method; see below
Client:
Polarized Light Microscope (PLM) Analysis for Asbestos in Bulk Sample
Method and Analysis Information:
Each bulk sample is first dissected under a 7-30x magnification stereo-microscope. This examination is used to determine the general type of sample, how many and what type of layers it has, and initial estimates of fiber types and quantities. Second, liquid media mounts are made of each layer - such mounts may be of selected fibers (used solely for identification purposes) or may be representative of the layer as a whole (used for quantitation purposes). The mounts may be made in a synthetic Canadian balsam, one of several solvents, or in refractive index oils (media of known refractive index). Generally, a variety of different mounts are made: some optimized for fiber visibility, some optimized for fiber identification, and some optimized for fiber quantitation. The mounted slides are then examined at 50-400x magnification on a Nikon Labphot-pol microscope. Optical characteristics are used to identify each observed fiber type; the optical data are contained for each sample on its detail analysis sheet, attached.
Current EPA and NESHAP regulations designate a result of <=1 % asbestos as "negative" and >1 % asbestos as "positive". Samples containing layers that have been determined to be "positive" may have to be handled differently during a renovation or demolition than samples whose layers have been determined to be "negative."
The method of fiber identification and quantitation is the “Standard Operating Procedures for the Analysis of Asbestos in Bulk Samples using Polarized Light Microscopy”, Chapter 7 of the Quality Assurance and Management Manual. This SOP and its associated reporting have been designed to satisfy all requirements in both EPA Method 600/M4-82-020 (The Interim Method) and EPA Method 600/R-93/116 (The New Method). The Interim Method is the required method for AHERA (US EPA 40 CFR Pt. 763), but this method calls for the reporting of composited results of multi-layered samples that is no longer an acceptable reporting practice in most circumstances. Current EPA rules, such as NESHAP (US EPA 40CFT Pt. 61), as well as NVLAP accreditation policies, call for separate reporting for each layer of multi-layered samples. The New Method contains the same procedures for identification and quantification of asbestos as does the Interim Method, except that multi-layered samples are reported to comply with the latest US
EPA rule. Fiberquant not only reports the asbestos content of each layer of multi-layered samples separately (satisfying current EPA and NVLAP reporting requirements), but Fiberquant also reports what percentage of the sample each layer comprises. Therefore, the results may be arithmetically composited to satisfy the reporting requirements of the Interim Method. The method of fiber quantitation is an estimation technique in which the analysts quantitation is routinely calibrated by reference quantitation standards, and which has been shown to be equivalent in precision and accuracy to point counting. Friability is estimated for the purposes of deciding when to point count. Friabilities determined in the field take precedence over those determined in the laboratory. Those sample layers which are friable and estimated by the analyst to contain <= 1% asbestos are point counted using 400 points. Such point counting is required by NESHAP (National Emission Standards for Hazardous Air Polutants, Nov. 1990) in order to rely on analytical results that are <= 1%. The coefficient of variation for the estimation quantitation technique is 100% in the range 0- 5%. This means that PLM analysis is not capable of conclusively determining whether a layer containing close to 1% asbestos is actually "positive" or
"negative". For this reason, Fiberquant refers to results where asbestos was detected but <= 1% as "borderline negative", and results where asbestos was >1 % but <= 2% as "borderline positive" to indicate the uncertainty in assigning a "positive" or "negative" label. In the sample summary, "ND" means that no asbestos was detected during the analysis. A "Tr" or "Trace" of asbestos reported is defined for our purposes as the detection of several asbestos fibers during the analysis; this level would be right at the limit of detection for the method. Trace is only reported on the analysis detail - in the summary a trace would be reported as <=1%. The limit of detection (the smallest % of asbestos that can be detected) varies greatly depending on the matrix in which the asbestos is found. As little as 0.001% asbestos can be detected in favorable samples, while detection in unfavorable samples may approach the detection limit of 1% stated in the method. During the analysis, the analyst, for Fiberquant identification purposes only, determines the "apparent sample type" and "apparent layer types." It must be emphasized that these types are only what is apparent. Often, different materials appear similar or identical after sampling, so the analyst may assign a type other than what was sampled.
Floor tiles present a special problem for PLM asbestos analysis. Floor tile can contain chrysotile fibers so thin that they cannot be resolved by optical methods. In such a case, we may observe a percentage of asbestos which is lower than the actual percentage, or not observe asbestos at all when some is present. For this reason, floor tiles reported as negative should be confirmed to be negative using transmission electron microscope
(TEM) analysis. Likewise, vermiculite insulation materials containing traces of asbestiform asbestos present a problem for routine PLM analysis - the amphiboles are sometimes present in trace amounts inhomogeneously distributed. For this reason, loose vermiculite samples reported as negative should be confirmed to contain no amphibole using hydroseparation techniques.
The samples were analyzed under the following ongoing quality assurance program: Blank samples are routinely analyzed to maintain contamination-free materials. Each analyst has at least a bachelor's degree in physical science, and has also completed extensive training specific to asbestos analysis for 1-3 months before being allowed to analyze client samples. Qualitative reference samples are routinely analyzed to assure that analysts can identify asbestos and asbestos-look-alike fibers. Quantitative reference samples are routinely analyzed to calibrate and characterize the
Method: EPA 600/R-93/116Rec: 1/17/2013
Report Date: 1/23/2013 Date Analyzed: 1/23/2013
Fiberquant Internal SOP:
EMCOR GOVERNMENT SVCS
CLARKSTON RD BLDG 30033
FT HUACHUCA, AZ
Office Phone: (520) 533-5906
5025 S. 33rd Street Phoenix, Arizona 85040-2816 Phone: 602-276-6139 1-800-743-2687 FAX: 602-276-4558
PLM Analysis Summary: Job Number: 201300604 1-1580912 estimation procedure. Microscope alignment is checked each day. Refractive index oils are calibrated at least quarterly. At least 10% of client samples are re-analyzed from scratch by a different analyst than the original, and any discrepancies are resolved for the sample and similar sample types before the results are reported. All quality checks performed for these samples were in control except as detailed in the "Analytical Notes" below. All analysts participate in interlab round robins and proficiency testing to assure competence. Fiberquant is accredited by NVLAP (Lab #101031) for the analysis of bulk samples for asbestos using PLM. Accreditation does not imply endorsement by the EPA, any other United States governmental agency or any private agency or association. Each lab analysis refers only to the sample tested, and may not, due to the sampling process, be representative of the material sampled. This report may not be reproduced except in full, without the approval of Fiberquant Analytical
Services.
Job Analysis Notes:
Some results may have been calculated using client supplied data, such as volume or area sampled, for which Fiberquant assumes no liability for accuracy.
Sample Number Lab Number Apparent Sample Type * Positive Layer Yes or No
Layer Color Apparent Layer Type * Asbestos Results
Roofing2013-00604- 168057-01 Positive Layer? YesSample # no asbestos detectedroofing roll/shingleblackLayer # 1 no asbestos detectedroofing roll/shingleblackLayer # 2
20-30% chrysotile asbestosroofing roll/shingleblackLayer # 3
20-30% chrysotile asbestosroofing roll/shingleblackLayer # 4 no asbestos detectedroofing roll/shingleblackLayer # 5 no asbestos detectedroof plyblackLayer # 6 no asbestos detectedroof plyblackLayer # 7
* Apparent Sample Types and Apparent Layer Types are as they appeared to the analyst. Since many types of materials appear similar after sampling damage, the
5025 S. 33rd Street Phoenix, Arizona 85040-2816 Phone: 602-276-6139 1-800-743-2687 FAX: 602-276-4558
PLM Analysis Details Job Number: 201300604 1-1580912
2013-00604- 168057-01 Lab Number Sample Sampled:
DMSAnalyzed By 1/23/2013
Homogeneous
Roofing
No
Fibrous SolidOKAn?
7# Layers YesPos Layer?
Apparent Smp Type cellulose fiber synthetic fiber (extr chrysotile asbestosFiber Identification:
Sample Analytical Note
Procedure: tweased apart using forceps. Procedure: dissolution of matrix using solvent. Note: there appears to be more than one sample layer sequence in the bag (e.g., samples from more than one location); therefore, the reported layer sequence has been estimated/composited.
Fibers
Color Mrph Iso Pleo Bi Elg Ext Oil Col Par Col Per RI Par RI Per
Refractive Index Determinations cellulose fiber synthetic fiber (extruded) chrysotile asbestos 1.556 1.5491.550 vb/g pb/r
W F N N H + U
W E N N H + P
W A N N L + P
Non-Fibrous Components (in approx. decreasing order): bitumen, rock, 21# Sub-Samples
Condition:acceptable
Layers
# Layer Type % Color Friability
Percents of Each Fiber
Fib 1 Fib 2 Fib 3 Fib 4 Fib 5 Fib 6
1 17 30-40% 2-5% n.d. - - -roofing roll/shingle black 1
2 17 30-40% n.d. n.d. - - -roofing roll/shingle black 1
3 17 5-10% n.d. 20-30% - - -roofing roll/shingle black 1
4 17 5-10% n.d. 20-30% - - -roofing roll/shingle black 1
5 17 10-20% n.d. n.d. - - -roofing roll/shingle black 1
6 8 40-50% n.d. n.d. - - -roof ply black 1
7 7 60-70% n.d. n.d. - - -roof ply black 1
100Total % 20-30% <=1% 10-20% - - -Overall %
Fr=Friability: 1=very non-friable; 2= non-friable; 3=friable; 4=highly friable
Colors: B=black;BL=blue;BR=brown;CL=clear;G=Green;GY=gray;OR=orange;OW=off-white;PN=pink;PU=purple;R=red;TN=tan;W=white;Y=yellow;V=various
Fiber Morphology: A=fine fibers/bundles, white, sinewy, flexible; B=fine fibers/bundles, w-br, straight, broomed ends; C=fine fibers/bundles, blue, straight, broomed ends;
D=fine to coarse fibers, CL-B, brittle; E=coarse fibers,CL or dyed, striated; F=coarse fibers or splinters, W-BR, ribbon-like; G=lath-like or shards, low aspect ratio, may taper
Iso=isotropism - may be yes or no; Pleo=pleochroism - may be yes or no; Bi=birefringence - may be None, Low, Medium or High
Elg=sign of elongation - may be +, - or B (both); Ext=extinction - may be Parallel, Oblique, None or Undulating; Oil=medium used to for dispersion staining
Col Par=dispersion staining colors parallel to the fiber (fiber/halo): b/w=black/white; dg/py=dark gray/pale yellow; vg/y=violet gray/yellow; db/ly=dark blue/lemon yellow;
vb/g= vivid blue/gold; sb/o=sky blue/orange; pb/r=pale blue/red; gb/dr=gray blue/dark red; w/b=white/black. Col Perp=same only perpendicular to fiber.
RI Par=refractive index parallel to fiber; RI Perp=refractive index perpendicular to fiber
23-Jan-13Analyst: DAVID M. SCHALLER
Larry S. Pierce, Approved Accreditation Signatory
23-Jan-13Original Print Date:
5025 S. 33rd Street Phoenix, Arizona 85040-2816 Phone: 602-276-6139 1-800-743-2687 FAX: 602-276-4558
Client Job: 1-1610514 PO Number: 68057
JobNumber: 201301117
Routing Number: -
# Samples: 4
PLMn
PLM The "New" Method; see below
Client:
Polarized Light Microscope (PLM) Analysis for Asbestos in Bulk Sample
Method and Analysis Information:
Each bulk sample is first dissected under a 7-30x magnification stereo-microscope. This examination is used to determine the general type of sample, how many and what type of layers it has, and initial estimates of fiber types and quantities. Second, liquid media mounts are made of each layer - such mounts may be of selected fibers (used solely for identification purposes) or may be representative of the layer as a whole (used for quantitation purposes). The mounts may be made in a synthetic Canadian balsam, one of several solvents, or in refractive index oils (media of known refractive index). Generally, a variety of different mounts are made: some optimized for fiber visibility, some optimized for fiber identification, and some optimized for fiber quantitation. The mounted slides are then examined at 50-400x magnification on a Nikon Labphot-pol microscope. Optical characteristics are used to identify each observed fiber type; the optical data are contained for each sample on its detail analysis sheet, attached.
Current EPA and NESHAP regulations designate a result of <=1 % asbestos as "negative" and >1 % asbestos as "positive". Samples containing layers that have been determined to be "positive" may have to be handled differently during a renovation or demolition than samples whose layers have been determined to be "negative."
The method of fiber identification and quantitation is the “Standard Operating Procedures for the Analysis of Asbestos in Bulk Samples using Polarized Light Microscopy”, Chapter 7 of the Quality Assurance and Management Manual.
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