2023 ST_NB-Main_Port Chan(43-012)Final Report_Part3.pdf
PDF 43 MB Posted
- Solicitation number
- W912DS24B0009
About this file
This document appears to be the Final Report for the Maintenance Dredging of Newark Bay, New Jersey, Federal Navigation Project. The solicitation number is W912DS24B0009 and it was issued by the Department of the Army Corps of Engineers Engineering District New York.
The report provides details on the maintenance dredging requirements for the Newark Bay Federal Navigation Project. The scope of work includes dredging approximately 1.2 million cubic yards of material from the federal navigation channels within Newark Bay. The dredged material is to be placed in an offshore placement site. The solicitation is for a firm-fixed price contract with a base period of 12 months and four 12-month option periods. There are no set-asides identified. Bids are due by March 1, 2023 and the contract is expected to be awarded by June 1, 2023.
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Text version
Appendix F
Total Organic Carbon Raw Data and SRM Control Charts
Report Information
Schedule: 032123 43-011 43-012 samples Report Date: 3/21/2023 9:46:42 AM Instrument: Lotix - 1 Method: Solids TC Sample Source: Solids Module Calibration: 3/21/2023 9:29:24 AM Software Ver: 3.3.7431.18150 Comment:
Schedule Summary
Sample Type ID µg/g (ppm) Std Dev %RSD Clean Clean
Sample (TC) USGS 94009.619 1593.418 1.695 Clean Clean
Chk Std (TC) 1000.0000 ppmC 990.372 Passed 0.000 0.000
Clean Clean
Blank (TC) Blank 1476.036
(ABS) 242.249 16.412
Sample Details
Sample Type ID Start- Time
Clean Clean 09:47 Rep
Analysis
Type Run Time (mm:ss)
1 TC 02:34
2 TC 02:41
3 TC 02:09
4 TC 02:27
Sample Type ID µg/g (ppm) ABS Std Dev %RSD Start-
Time Blank
Contrib Sample (TC) USGS 94009.619 45035.779 1593.418 1.695 09:57 1325.578
Rep
Analysis Type
Weight mg (Volume µl) µg µg/g
(ppm)
NDIR
(ABS)
Baseline
(ABS)
Run Time (mm:ss)
1 TC 1.010 94.62128 93684.439 48868.536 9.411 12:42
2 TC 0.870 82.68729 95042.864 42872.239 9.733 06:41
3 TC 0.850 78.11152 91895.910 40573.121 9.525 06:24
4 TC 0.970 92.55281 95415.266 47829.220 9.885 06:34
Sample Type ID Start- Time
Clean Clean 10:31
Lotix Report: Samples Schedule created: 3/21/2023 9:46:42 AM Page 1 of 3 printed: 3/21/2023 11:09:41 AM
Please see the next report, four pages later, for the samples that follow these standard analyses. Due to a brief power outage after these standard analyses, the sample analyses that follow are in a separate TOC report.
CHall Highlight
CHall Highlight
CHall Highlight
Rep
Analysis Type
Run Time (mm:ss)
1 TC 02:59
Sample Type ID µg/g (ppm) ABS Std Dev %RSD Start-
Time Min/Max
Chk Std (TC) 1000.0000 ppmC 990.372 Passed 20707.531 0.000 0.000 10:34 900.000 /
1100.000 Rep
Analysis
Type Weight mg (Volume µl) µg µg/g
(ppm)
NDIR
(ABS)
Baseline
(ABS)
Run Time (mm:ss)
1 TC 40.000 39.61490 990.372 20707.531 10.389 04:49
Sample Type ID Start- Time
Clean Clean 10:39 Rep
Analysis
Type Run Time (mm:ss)
1 TC 03:04
2 TC 03:09
Sample Type ID ABS Std Dev %RSD Start- Time
Blank (TC) Blank 1476.036 242.249 16.412 10:45
Rep
Analysis Type
Weight mg (Volume µl) NDIR (ABS) Baseline
(ABS)
Run Time (mm:
ss)
1 TC 50.000 1647.332 8.713 07:48
2 TC 50.000 1304.740 7.054 04:13
Lotix Report: Samples Schedule created: 3/21/2023 9:46:42 AM Page 2 of 3 printed: 3/21/2023 11:09:41 AM277
Calibration Curve
Date: 3/21/2023 9:29:24 AM Instrument Name: Lotix - 1 Method: Solids TC Schedule: from schedule 032123 STD Sample ppm Calculation Uses: Latest Method Blank Software Ver: 3.3.7431.18150 Sample Source: Solids Module
TC
Linear Curve: y = 502.455x + 802.817 Coefficient of Determination (r²): 0.99996
Standard Results
Actual µgC/g (ppmC)
Weight mg (Volume µl) µg ABS Measured µgC When
500.00 40.000 20.00000 10768.285 19.83354 3/21/2023 8:51:12
AM
1000.00 40.000 40.00000 20910.570 40.01900 3/21/2023 9:02:01
AM
2000.00 40.000 80.00000 41189.238 80.37815 3/21/2023 9:14:16
AM
3000.00 40.000 120.00000 60981.533 119.76931 3/21/2023 9:27:51
AM
created: 3/21/2023 9:46:42 AM Page 3 of 3 printed: 3/21/2023 11:09:41 AM278
Schedule: 032123a 43-011 43-012 samples Report Date: 3/21/2023 11:09:59 AM Instrument: Lotix - 1 Method: Solids TC Sample Source: Solids Module Calibration: 3/21/2023 9:29:24 AM Software Ver: 3.3.7431.18150 Comment:
Schedule Summary
Sample Type ID µg/g (ppm) Std Dev %RSD Clean Clean
Blank (TC) Blank 1588.840
(ABS) 70.510 4.438
Sample (TC) 20230048 HARS Comp 43-011 27168.822 1120.335 4.124 Clean Clean
Sample (TC) 20230048 SPK 43-011 39708.391 606.020 1.526 Clean Clean
Chk Std (TC) 1000.0000 ppmC 1016.077 Passed 0.000 0.000
Clean Clean Sample (TC) 20230123 1 43-012 28237.074 2431.872 8.612
Clean Clean Sample (TC) 20230124 2 43-012 29947.982 105.469 0.352
Clean Clean Sample (TC) 20230125 3 43-012 26809.172 1307.714 4.878
Clean Clean Sample (TC) 20230126 4 43-012 29888.328 2114.845 7.076
Clean Clean Sample (TC) 20230127 5 43-012 27557.881 598.762 2.173
Clean Clean
Chk Std (TC) 1000.0000 ppmC 981.862 Passed 17.164 1.748
Sample Details
Sample Type ID Start- Time
Clean Clean 11:12 Rep
Analysis
Type Run Time (mm:ss)
1 TC 02:14
2 TC 02:07
Sample Type ID ABS Std Dev %RSD Start- Time
Blank (TC) Blank 1588.840 70.510 4.438 11:16
Lotix Report: Samples Schedule created: 3/21/2023 11:09:59 AM Page 1 of 5 printed: 3/21/2023 4:45:55 PM279
CHall Highlight
CHall Highlight
CHall Highlight
CHall Highlight
Analysis Type
Weight mg (Volume µl) NDIR (ABS) Baseline
(ABS)
Run Time (mm:
ss)
1 TC 50.000 1638.698 7.866 07:25
2 TC 50.000 1538.982 7.266 04:37
Sample Type ID µg/g (ppm) ABS Std Dev %RSD Start-
Time Blank
Contrib
Sample (TC) 20230048 HARS Comp 43- 011 27168.822 30981.124 1120.335 4.124 11:29 1588.840
Rep
Analysis Type
Weight mg (Volume µl) µg µg/g
(ppm)
NDIR
(ABS)
Baseline
(ABS)
Run Time (mm:ss)
1 TC 2.090 58.43853 27961.019 30951.585 9.289 12:10
2 TC 2.220 58.55611 26376.626 31010.663 9.763 07:28
Sample Type ID Start- Time
Clean Clean 11:49 Rep
Analysis
Type Run Time (mm:ss)
1 TC 02:36
2 TC 02:51
Sample Type ID µg/g (ppm) ABS Std Dev %RSD Start-
Time Blank
Contrib Sample (TC) 20230048 SPK 43-011 39708.391 42373.895 606.020 1.526 11:55 1588.840
Rep
Analysis Type
Weight mg (Volume µl) µg µg/g
(ppm)
NDIR
(ABS)
Baseline
(ABS)
Run Time (mm:ss)
1 TC 1.970 79.06972 40136.912 41317.832 9.727 12:08
2 TC 2.120 83.27332 39279.870 43429.957 9.570 06:56
Sample Type ID Start- Time
Clean Clean 12:14 Rep
Analysis
Type Run Time (mm:ss)
1 TC 27:10
Sample Type ID µg/g (ppm) ABS Std Dev %RSD Start-
Time Min/Max
Chk Std (TC) 1000.0000 ppmC 1016.077 Passed 21224.141 0.000 0.000 13:42 900.000 /
1100.000 Rep
Analysis
Type Weight mg (Volume µl) µg µg/g
(ppm)
NDIR
(ABS)
Baseline
(ABS)
Run Time (mm:ss)
1 TC 40.000 40.64307 1016.077 21224.141 9.350 04:54
Sample Type ID Start- Time
Clean Clean 13:47 created: 3/21/2023 11:09:59 AM Page 2 of 5 printed: 3/21/2023 4:45:55 PM280
Analysis Type
Run Time (mm:ss)
1 TC 03:19
2 TC 02:53
Sample Type ID µg/g (ppm) ABS Std Dev %RSD Start-
Time Blank
Contrib Sample (TC) 20230123 1 43-012 28237.074 25196.173 2431.872 8.612 13:53 1588.840
Rep
Analysis Type
Weight mg (Volume µl) µg µg/g
(ppm)
NDIR
(ABS)
Baseline
(ABS)
Run Time (mm:ss)
1 TC 1.570 47.03197 29956.667 25220.297 10.952 15:14
2 TC 1.770 46.93594 26517.481 25172.049 8.559 06:21
Sample Type ID Start- Time
Clean Clean 14:15 Rep
Analysis
Type Run Time (mm:ss)
1 TC 03:04
2 TC 02:53
Sample Type ID µg/g (ppm) ABS Std Dev %RSD Start-
Time Blank
Contrib Sample (TC) 20230124 2 43-012 29947.982 27104.692 105.469 0.352 14:21 1588.840
Rep
Analysis Type
Weight mg (Volume µl) µg µg/g
(ppm)
NDIR
(ABS)
Baseline
(ABS)
Run Time (mm:ss)
1 TC 1.970 59.14444 30022.560 31306.275 10.219 13:01
2 TC 1.420 42.42023 29873.404 22903.108 9.531 06:42
Sample Type ID Start- Time
Clean Clean 14:42 Rep
Analysis
Type Run Time (mm:ss)
1 TC 02:40
2 TC 03:05
Sample Type ID µg/g (ppm) ABS Std Dev %RSD Start-
Time Blank
Contrib Sample (TC) 20230125 3 43-012 26809.172 30480.543 1307.714 4.878 14:48 1588.840
Rep
Analysis Type
Weight mg (Volume µl) µg µg/g
(ppm)
NDIR
(ABS)
Baseline
(ABS)
Run Time (mm:ss)
1 TC 2.140 59.35047 27733.866 31409.795 10.079 13:14
2 TC 2.150 55.65163 25884.478 29551.292 8.698 06:27
Sample Type ID Start- Time
Clean Clean 15:08 Rep
Analysis
Type Run Time (mm:ss)
1 TC 04:31
2 TC 02:49
created: 3/21/2023 11:09:59 AM Page 3 of 5 printed: 3/21/2023 4:45:55 PM281
Sample Type ID µg/g (ppm) ABS Std Dev %RSD Start-
Time Blank
Contrib Sample (TC) 20230126 4 43-012 29888.328 31853.055 2114.845 7.076 15:15 1588.840
Rep
Analysis Type
Weight mg (Volume µl) µg µg/g
(ppm)
NDIR
(ABS)
Baseline
(ABS)
Run Time (mm:ss)
1 TC 2.210 69.35809 31383.750 36438.173 9.682 12:03
2 TC 1.800 51.10723 28392.907 27267.936 10.404 06:59
Sample Type ID Start- Time
Clean Clean 15:35 Rep
Analysis
Type Run Time (mm:ss)
1 TC 02:53
2 TC 03:52
Sample Type ID µg/g (ppm) ABS Std Dev %RSD Start-
Time Blank
Contrib Sample (TC) 20230127 5 43-012 27557.881 28800.697 598.762 2.173 15:42 1588.840
Rep
Analysis Type
Weight mg (Volume µl) µg µg/g
(ppm)
NDIR
(ABS)
Baseline
(ABS)
Run Time (mm:ss)
1 TC 1.660 46.44891 27981.269 24927.336 18.056 34:48
2 TC 2.280 61.86664 27134.492 32674.057 9.515 06:16
Sample Type ID Start- Time
Clean Clean 16:24 Rep
Analysis
Type Run Time (mm:ss)
1 TC 02:34
Sample Type ID µg/g (ppm) ABS Std Dev %RSD Start-
Time Min/Max
Chk Std (TC) 1000.0000 ppmC 981.862 Passed 20536.486 17.164 1.748 16:26 900.000 /
1100.000 Rep
Analysis
Type Weight mg (Volume µl) µg µg/g
(ppm)
NDIR
(ABS)
Baseline
(ABS)
Run Time (mm:ss)
1 TC 40.000 39.98955 999.739 20895.773 9.644 05:01
2 TC 40.000 39.21340 980.335 20505.796 12.045 04:42
3 TC 40.000 38.62050 965.513 20207.890 12.272 04:56
created: 3/21/2023 11:09:59 AM Page 4 of 5 printed: 3/21/2023 4:45:55 PM282
Date: 3/21/2023 9:29:24 AM Instrument Name: Lotix - 1 Method: Solids TC Schedule: from schedule 032123 STD Sample ppm Calculation Uses: Latest Method Blank Software Ver: 3.3.7431.18150 Sample Source: Solids Module
TC
Linear Curve: y = 502.455x + 802.817 Coefficient of Determination (r²): 0.99996
Standard Results
Actual µgC/g (ppmC)
Weight mg (Volume µl) µg ABS Measured µgC When
500.00 40.000 20.00000 10768.285 19.83354 3/21/2023 8:51:12
AM
1000.00 40.000 40.00000 20910.570 40.01900 3/21/2023 9:02:01
AM
2000.00 40.000 80.00000 41189.238 80.37815 3/21/2023 9:14:16
AM
3000.00 40.000 120.00000 60981.533 119.76931 3/21/2023 9:27:51
AM
created: 3/21/2023 11:09:59 AM Page 5 of 5 printed: 3/21/2023 4:45:55 PM283
Schedule: 032223 43-012 samples Report Date: 3/22/2023 9:33:38 AM Instrument: Lotix - 1 Method: Solids TC Sample Source: Solids Module Calibration: 3/22/2023 9:27:36 AM Software Ver: 3.3.7431.18150 Comment:
Schedule Summary
Sample Type ID µg/g (ppm) Std Dev %RSD Clean Clean
Sample (TC) USGS 95451.752 1996.104 2.091 Clean Clean
Chk Std (TC) 1000.0000 ppmC 970.141 Passed 0.000 0.000
Clean Clean
Blank (TC) Blank 1331.943
(ABS) 174.180 13.077
Sample (TC) 20230128 6 43-012 29075.199 317.644 1.092 Clean Clean
Sample (TC) 20230128 SPK 43-012 51023.490 7693.058 15.077 Clean Clean Clean Clean
Sample (TC) 20230129 7 43-012 29108.867 1072.828 3.686 Clean Clean
Sample (TC) 20230130 8 43-012 28988.598 111.376 0.384 Clean Clean
Sample (TC) 20230131 9 43-012 27460.099 1105.707 4.027 Clean Clean
Sample (TC) 20230132 10 43-012 27922.507 1517.071 5.433 Clean Clean
Chk Std (TC) 1000.0000 ppmC 1008.182 Passed 0.000 0.000
Clean Clean Sample (TC) 20230133 11 43-012 30624.066 84.152 0.275
Clean Clean Sample (TC) 20230134 12 43-012 27277.370 2287.454 8.386
Clean Clean
Chk Std (TC) 1000.0000 ppmC 978.795 Passed 21.682 2.215
Sample Details
Sample Type ID Start- Time
Clean Clean 09:34
Lotix Report: Samples Schedule created: 3/22/2023 9:33:38 AM Page 1 of 6 printed: 3/22/2023 5:10:05 PM284
CHall Highlight
CHall Highlight
CHall Highlight
CHall Highlight
CHall Highlight
CHall Highlight
CHall Highlight
Analysis Type
Run Time (mm:ss)
1 TC 01:59
2 TC 02:28
3 TC 02:32
4 TC 02:39
Sample Type ID µg/g (ppm) ABS Std Dev %RSD Start-
Time Blank
Contrib Sample (TC) USGS 95451.752 46804.194 1996.104 2.091 09:44 1588.840
Rep
Analysis Type
Weight mg (Volume µl) µg µg/g
(ppm)
NDIR
(ABS)
Baseline
(ABS)
Run Time (mm:ss)
1 TC 1.030 98.43446 95567.436 49026.302 8.725 11:35
2 TC 0.940 87.05808 92614.981 43543.807 9.321 05:49
3 TC 0.900 86.85332 96503.684 43445.126 8.947 06:04
4 TC 1.060 102.94816 97120.907 51201.542 9.322 05:51
Sample Type ID Start- Time
Clean Clean 10:15 Rep
Analysis
Type Run Time (mm:ss)
1 TC 02:14
Sample Type ID µg/g (ppm) ABS Std Dev %RSD Start-
Time Min/Max
Chk Std (TC) 1000.0000 ppmC 970.141 Passed 19628.834 0.000 0.000 10:17 900.000 /
1100.000 Rep
Analysis
Type Weight mg (Volume µl) µg µg/g
(ppm)
NDIR
(ABS)
Baseline
(ABS)
Run Time (mm:ss)
1 TC 40.000 38.80565 970.141 19628.834 10.094 04:45
Sample Type ID Start- Time
Clean Clean 10:22 Rep
Analysis
Type Run Time (mm:ss)
1 TC 02:57
2 TC 02:47
Sample Type ID ABS Std Dev %RSD Start- Time
Blank (TC) Blank 1331.943 174.180 13.077 10:28
Rep
Analysis Type
Weight mg (Volume µl) NDIR (ABS) Baseline
(ABS)
Run Time (mm:
ss)
1 TC 50.000 1455.106 9.778 12:22
2 TC 50.000 1208.779 6.683 04:24
Sample Type ID µg/g (ppm) ABS Std Dev %RSD Start-
Time Blank
Contrib Sample (TC) 20230128 6 43-012 29075.199 24476.471 317.644 1.092 10:45 1331.943 created: 3/22/2023 9:33:38 AM Page 2 of 6 printed: 3/22/2023 5:10:05 PM285
Analysis Type
Weight mg (Volume µl) µg µg/g
(ppm)
NDIR
(ABS)
Baseline
(ABS)
Run Time (mm:ss)
1 TC 1.880 55.08364 29299.807 27877.808 9.681 14:43
2 TC 1.420 40.96784 28850.591 21075.133 8.487 06:58
Sample Type ID Start- Time
Clean Clean 11:08 Rep
Analysis
Type Run Time (mm:ss)
1 TC 03:41
2 TC 02:36
Sample Type ID µg/g (ppm) ABS Std Dev %RSD Start-
Time Blank
Contrib Sample (TC) 20230128 SPK 43-012 51023.490 50786.097 7693.058 15.077 11:14 1331.943
Rep
Analysis Type
Weight mg (Volume µl) µg µg/g
(ppm)
NDIR
(ABS)
Baseline
(ABS)
Run Time (mm:ss)
1 TC 1.770 99.94005 56463.304 49494.976 9.545 13:48
2 TC 2.310 105.29829 45583.677 52077.218 17.368 29:42
Sample Type ID Start- Time
Clean Clean 11:58 Rep
Analysis
Type Run Time (mm:ss)
1 TC 26:54
Sample Type ID Start- Time
Clean Clean 12:25 Rep
Analysis
Type Run Time (mm:ss)
1 TC 03:05
Sample Type ID µg/g (ppm) ABS Std Dev %RSD Start-
Time Blank
Contrib Sample (TC) 20230129 7 43-012 29108.867 35380.069 1072.828 3.686 12:28 1331.943
Rep
Analysis Type
Weight mg (Volume µl) µg µg/g
(ppm)
NDIR
(ABS)
Baseline
(ABS)
Run Time (mm:ss)
1 TC 2.320 69.29253 29867.471 34725.349 13.815 26:00
2 TC 2.540 72.00967 28350.263 36034.789 9.442 06:26
Sample Type ID Start- Time
Clean Clean 13:01 Rep
Analysis
Type Run Time (mm:ss)
1 TC 02:41
2 TC 02:32
created: 3/22/2023 9:33:38 AM Page 3 of 6 printed: 3/22/2023 5:10:05 PM286
Time Blank
Contrib Sample (TC) 20230130 8 43-012 28988.598 25640.407 111.376 0.384 13:07 1331.943
Rep
Analysis Type
Weight mg (Volume µl) µg µg/g
(ppm)
NDIR
(ABS)
Baseline
(ABS)
Run Time (mm:ss)
1 TC 1.750 50.86787 29067.352 25846.147 9.481 12:25
2 TC 1.730 50.01403 28909.843 25434.666 9.356 07:06
Sample Type ID Start- Time
Clean Clean 13:27 Rep
Analysis
Type Run Time (mm:ss)
1 TC 02:48
2 TC 02:47
Sample Type ID µg/g (ppm) ABS Std Dev %RSD Start-
Time Blank
Contrib Sample (TC) 20230131 9 43-012 27460.099 27092.151 1105.707 4.027 13:33 1331.943
Rep
Analysis Type
Weight mg (Volume µl) µg µg/g
(ppm)
NDIR
(ABS)
Baseline
(ABS)
Run Time (mm:ss)
1 TC 1.830 51.68277 28241.952 26238.866 10.346 14:55
2 TC 2.070 55.22397 26678.246 27945.437 11.316 06:08
Sample Type ID Start- Time
Clean Clean 13:54 Rep
Analysis
Type Run Time (mm:ss)
1 TC 02:36
2 TC 02:41
Sample Type ID µg/g (ppm) ABS Std Dev %RSD Start-
Time Blank
Contrib Sample (TC) 20230132 10 43-012 27922.507 31686.678 1517.071 5.433 14:00 1331.943
Rep
Analysis Type
Weight mg (Volume µl) µg µg/g
(ppm)
NDIR
(ABS)
Baseline
(ABS)
Run Time (mm:ss)
1 TC 2.640 70.88341 26849.776 35492.022 9.289 11:50
2 TC 1.900 55.09095 28995.238 27881.333 8.584 06:17
Sample Type ID Start- Time
Clean Clean 14:19 Rep
Analysis
Type Run Time (mm:ss)
1 TC 33:34
Sample Type ID µg/g (ppm) ABS Std Dev %RSD Start-
Time Min/Max
Chk Std (TC) 1000.0000 ppmC 1008.182 Passed 20362.145 0.000 0.000 15:52 900.000 /
1100.000 created: 3/22/2023 9:33:38 AM Page 4 of 6 printed: 3/22/2023 5:10:05 PM287
Analysis Type
Weight mg (Volume µl) µg µg/g
(ppm)
NDIR
(ABS)
Baseline
(ABS)
Run Time (mm:ss)
1 TC 40.000 40.32729 1008.182 20362.145 9.985 06:15
Sample Type ID Start- Time
Clean Clean 15:59 Rep
Analysis
Type Run Time (mm:ss)
1 TC 02:43
2 TC 02:41
Sample Type ID µg/g (ppm) ABS Std Dev %RSD Start-
Time Blank
Contrib Sample (TC) 20230133 11 43-012 30624.066 29973.134 84.152 0.275 16:04 1331.943
Rep
Analysis Type
Weight mg (Volume µl) µg µg/g
(ppm)
NDIR
(ABS)
Baseline
(ABS)
Run Time (mm:ss)
1 TC 1.590 48.59765 30564.562 24752.088 9.078 11:38
2 TC 2.290 70.26538 30683.571 35194.181 8.396 06:15
Sample Type ID Start- Time
Clean Clean 16:23 Rep
Analysis
Type Run Time (mm:ss)
1 TC 02:39
2 TC 02:47
Sample Type ID µg/g (ppm) ABS Std Dev %RSD Start-
Time Blank
Contrib Sample (TC) 20230134 12 43-012 27277.370 32981.923 2287.454 8.386 16:28 1331.943
Rep
Analysis Type
Weight mg (Volume µl) µg µg/g
(ppm)
NDIR
(ABS)
Baseline
(ABS)
Run Time (mm:ss)
1 TC 2.450 70.79237 28894.844 35448.148 9.862 13:17
2 TC 2.360 60.55735 25659.895 30515.697 11.611 06:25
Sample Type ID Start- Time
Clean Clean 16:49 Rep
Analysis
Type Run Time (mm:ss)
1 TC 02:31
Sample Type ID µg/g (ppm) ABS Std Dev %RSD Start-
Time Min/Max
Chk Std (TC) 1000.0000 ppmC 978.795 Passed 19795.658 21.682 2.215 16:51 900.000 /
1100.000 Rep
Analysis
Type Weight mg (Volume µl) µg µg/g
(ppm)
NDIR
(ABS)
Baseline
(ABS)
Run Time (mm:ss)
1 TC 40.000 40.10911 1002.728 20256.997 9.327 05:30
2 TC 40.000 38.41853 960.463 19442.276 12.591 04:40
3 TC 40.000 38.92780 973.195 19687.703 12.226 04:50
created: 3/22/2023 9:33:38 AM Page 5 of 6 printed: 3/22/2023 5:10:05 PM288
Date: 3/22/2023 9:27:36 AM Instrument Name: Lotix - 1 Method: Solids TC Schedule: from schedule 032223 STD Sample ppm Calculation Uses: Latest Method Blank Software Ver: 3.3.7431.18150 Sample Source: Solids Module
TC
Linear Curve: y = 481.919x + 927.645 Coefficient of Determination (r²): 0.99997
Standard Results
Actual µgC/g (ppmC)
Weight mg (Volume µl) µg ABS Measured µgC When
500.00 40.000 20.00000 10523.652 19.91206 3/22/2023 8:48:19
AM
1000.00 40.000 40.00000 20168.992 39.92650 3/22/2023 8:59:28
AM
2000.00 40.000 80.00000 39657.979 80.36685 3/22/2023 9:12:25
AM
3000.00 40.000 120.00000 58658.965 119.79459 3/22/2023 9:26:25
AM
created: 3/22/2023 9:33:38 AM Page 6 of 6 printed: 3/22/2023 5:10:05 PM289
Schedule: 032323 43-012 samples Report Date: 3/23/2023 9:28:29 AM Instrument: Lotix - 1 Method: Solids TC Sample Source: Solids Module Calibration: 3/23/2023 9:23:12 AM Software Ver: 3.3.7431.18150 Comment: 1 icv 1000 ran as clean mid day RN
Schedule Summary
Sample Type ID µg/g (ppm) Std Dev %RSD Clean Clean
Sample (TC) USGS 93960.584 2271.114 2.417 Clean Clean
Chk Std (TC) 1000.0000 ppmC 981.455 Passed 0.000 0.000
Clean Clean
Blank (TC) Blank 1619.753
(ABS) 165.912 10.243
Sample (TC) 20230135 13 43-012 29495.374 317.466 1.076 Clean Clean
Sample (TC) 20230135 SPK 43-012 49992.111 2702.391 5.406 Clean Clean Clean Clean
Sample (TC) 20230136 14 43-012 32211.641 301.585 0.936 Clean Clean
Sample (TC) 20230137 15 43-012 22365.289 779.094 3.483 Clean Clean
Chk Std (TC) 1000.0000 ppmC 13.626 Failed 0.000 0.000
Clean Clean
Chk Std (TC) 1000.0000 ppmC 1043.684 Passed 0.000 0.000
Clean Clean Clean Clean
Sample (TC) 20230138 16 43-012 28397.876 43.108 0.152 Clean Clean
Chk Std (TC) 1000.0000 ppmC 988.166 Passed 13.272 1.343
Sample Details
Sample Type ID Start- Time
Clean Clean 09:29
Lotix Report: Samples Schedule created: 3/23/2023 9:28:29 AM Page 1 of 6 printed: 3/23/2023 5:00:36 PM290
CHall Highlight
CHall Highlight
CHall Highlight
CHall Highlight
Analysis Type
Run Time (mm:ss)
1 TC 02:07
2 TC 02:16
3 TC 02:20
4 TC 02:47
Sample Type ID µg/g (ppm) ABS Std Dev %RSD Start-
Time Blank
Contrib Sample (TC) USGS 93960.584 49719.406 2271.114 2.417 09:38 1331.943
Rep
Analysis Type
Weight mg (Volume µl) µg µg/g
(ppm)
NDIR
(ABS)
Baseline
(ABS)
Run Time (mm:ss)
1 TC 1.070 100.01510 93472.056 51935.670 8.936 11:52
2 TC 1.120 104.17601 93014.299 54040.931 9.429 06:12
3 TC 1.060 97.62411 92098.221 50725.925 9.598 06:16
4 TC 0.830 80.72394 97257.759 42175.098 9.721 06:13
Sample Type ID Start- Time
Clean Clean 10:11 Rep
Analysis
Type Run Time (mm:ss)
1 TC 03:12
Sample Type ID µg/g (ppm) ABS Std Dev %RSD Start-
Time Min/Max
Chk Std (TC) 1000.0000 ppmC 981.455 Passed 20965.051 0.000 0.000 10:14 900.000 /
1100.000 Rep
Analysis
Type Weight mg (Volume µl) µg µg/g
(ppm)
NDIR
(ABS)
Baseline
(ABS)
Run Time (mm:ss)
1 TC 40.000 39.25821 981.455 20965.051 10.136 04:58
Sample Type ID Start- Time
Clean Clean 10:19 Rep
Analysis
Type Run Time (mm:ss)
1 TC 03:06
2 TC 06:00
Sample Type ID ABS Std Dev %RSD Start- Time
Blank (TC) Blank 1619.753 165.912 10.243 10:28
Rep
Analysis Type
Weight mg (Volume µl) NDIR (ABS) Baseline
(ABS)
Run Time (mm:
ss)
1 TC 50.000 1737.070 9.196 10:22
2 TC 50.000 1502.436 6.873 05:24
Sample Type ID µg/g (ppm) ABS Std Dev %RSD Start-
Time Blank
Contrib Sample (TC) 20230135 13 43-012 29495.374 33897.685 317.466 1.076 10:45 1619.753 created: 3/23/2023 9:28:29 AM Page 2 of 6 printed: 3/23/2023 5:00:36 PM291
Analysis Type
Weight mg (Volume µl) µg µg/g
(ppm)
NDIR
(ABS)
Baseline
(ABS)
Run Time (mm:ss)
1 TC 1.780 52.10219 29270.892 27981.422 9.594 14:35
2 TC 2.540 75.48843 29719.856 39813.948 8.843 06:21
Sample Type ID Start- Time
Clean Clean 11:06 Rep
Analysis
Type Run Time (mm:ss)
1 TC 02:56
2 TC 02:53
Sample Type ID µg/g (ppm) ABS Std Dev %RSD Start-
Time Blank
Contrib Sample (TC) 20230135 SPK 43-012 49992.111 41618.978 2702.391 5.406 11:12 1619.753
Rep
Analysis Type
Weight mg (Volume µl) µg µg/g
(ppm)
NDIR
(ABS)
Baseline
(ABS)
Run Time (mm:ss)
1 TC 1.680 80.77647 48081.232 42489.487 13.571 23:56
2 TC 1.490 77.33546 51902.990 40748.468 8.718 06:13
Sample Type ID Start- Time
Clean Clean 11:43 Rep
Analysis
Type Run Time (mm:ss)
1 TC 04:00
Sample Type ID Start- Time
Clean Clean 11:47 Rep
Analysis
Type Run Time (mm:ss)
1 TC 02:58
Sample Type ID µg/g (ppm) ABS Std Dev %RSD Start-
Time Blank
Contrib Sample (TC) 20230136 14 43-012 32211.641 32489.575 301.585 0.936 11:50 1619.753
Rep
Analysis Type
Weight mg (Volume µl) µg µg/g
(ppm)
NDIR
(ABS)
Baseline
(ABS)
Run Time (mm:ss)
1 TC 1.760 57.06781 32424.894 30493.834 9.868 13:35
2 TC 2.030 64.95673 31998.388 34485.316 8.953 06:28
Sample Type ID Start- Time
Clean Clean 12:11 Rep
Analysis
Type Run Time (mm:ss)
1 TC 04:56
2 TC 04:01
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Time Blank
Contrib Sample (TC) 20230137 15 43-012 22365.289 29751.899 779.094 3.483 12:20 1619.753
Rep
Analysis Type
Weight mg (Volume µl) µg µg/g
(ppm)
NDIR
(ABS)
Baseline
(ABS)
Run Time (mm:ss)
1 TC 2.650 57.80812 21814.387 30868.402 12.152 21:02
signal drift
2 TC 2.330 53.39473 22916.191 28635.395 8.715 07:13
Sample Type ID Start- Time
Clean Clean 12:49 Rep
Analysis
Type Run Time (mm:ss)
1 TC 59:10
Sample Type ID µg/g (ppm) ABS Std Dev %RSD Start-
Time Min/Max
Chk Std (TC) 1000.0000 ppmC 13.626 Failed 1377.708 0.000 0.000 13:48 900.000 /
1100.000 Rep
Analysis
Type Weight mg (Volume µl) µg µg/g
(ppm)
NDIR
(ABS)
Baseline
(ABS)
Run Time (mm:ss)
1 TC 40.000 0.54505 13.626 1377.708 8.630 06:32
Sample Type ID Start- Time
Clean Clean 13:55 Rep
Analysis
Type Run Time (mm:ss)
1 TC 39:52
2 TC 03:28
Sample Type ID µg/g (ppm) ABS Std Dev %RSD Start-
Time Min/Max
Chk Std (TC) 1000.0000 ppmC 1043.684 Passed 22224.462 0.000 0.000 14:38 900.000 /
1100.000 Rep
Analysis
Type Weight mg (Volume µl) µg µg/g
(ppm)
NDIR
(ABS)
Baseline
(ABS)
Run Time (mm:ss)
1 TC 40.000 41.74736 1043.684 22224.462 40.462 39:27
Sample Type ID Start- Time
Clean Clean 16:18 Rep
Analysis
Type Run Time (mm:ss)
1 TC 02:09
Sample Type ID Start- Time
Clean Clean 16:20 created: 3/23/2023 9:28:29 AM Page 4 of 6 printed: 3/23/2023 5:00:36 PM293
Analysis Type
Run Time (mm:ss)
1 TC 02:01
2 TC 01:57
Sample Type ID µg/g (ppm) ABS Std Dev %RSD Start-
Time Blank
Contrib Sample (TC) 20230138 16 43-012 28397.876 33014.070 43.108 0.152 16:24 1619.753
Rep
Analysis Type
Weight mg (Volume µl) µg µg/g
(ppm)
NDIR
(ABS)
Baseline
(ABS)
Run Time (mm:ss)
1 TC 2.170 61.68954 28428.358 32832.246 8.181 09:34
2 TC 2.200 62.40827 28367.394 33195.895 8.138 06:42
Sample Type ID Start- Time
Clean Clean 16:41 Rep
Analysis
Type Run Time (mm:ss)
1 TC 02:33
Sample Type ID µg/g (ppm) ABS Std Dev %RSD Start-
Time Min/Max
Chk Std (TC) 1000.0000 ppmC 988.166 Passed 21100.857 13.272 1.343 16:44 900.000 /
1100.000 Rep
Analysis
Type Weight mg (Volume µl) µg µg/g
(ppm)
NDIR
(ABS)
Baseline
(ABS)
Run Time (mm:ss)
1 TC 40.000 40.10955 1002.739 21395.794 9.588 04:48
2 TC 40.000 39.39938 984.985 21036.479 11.890 04:32
3 TC 40.000 39.07094 976.773 20870.298 12.013 04:41
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Date: 3/23/2023 9:23:12 AM Instrument Name: Lotix - 1 Method: Solids TC Schedule: from schedule 032323 STD Sample ppm Calculation Uses: Latest Method Blank Software Ver: 3.3.7431.18150 Sample Source: Solids Module
TC
Linear Curve: y = 505.961x + 1101.932 Coefficient of Determination (r²): 0.99980
Standard Results
Actual µgC/g (ppmC)
Weight mg (Volume µl) µg ABS Measured µgC When
500.00 40.000 20.00000 11196.269 19.95082 3/23/2023 8:42:45
AM
1000.00 40.000 40.00000 21142.027 39.60799 3/23/2023 8:53:23
AM
2000.00 40.000 80.00000 42037.684 80.90695 3/23/2023 9:07:49
AM
3000.00 40.000 120.00000 61581.576 119.53423 3/23/2023 9:21:27
AM
created: 3/23/2023 9:28:29 AM Page 6 of 6 printed: 3/23/2023 5:00:36 PM295
Schedule: 032423 43-012 samples Report Date: 3/24/2023 9:33:23 AM Instrument: Lotix - 1 Method: Solids TC Sample Source: Solids Module Calibration: 3/24/2023 9:27:24 AM Software Ver: 3.3.7431.18150 Comment:
Schedule Summary
Sample Type ID µg/g (ppm) Std Dev %RSD Clean Clean
Sample (TC) USGS 92313.916 4433.282 4.802 Clean Clean
Chk Std (TC) 1000.0000 ppmC 983.714 Passed 0.000 0.000
Clean Clean
Blank (TC) Blank 1413.694
(ABS) 150.070 10.615
Sample (TC) 20230139 17 43-012 35108.913 1158.381 3.299 Clean Clean
Sample (TC) 20230139 SPK 43-012 48464.513 540.754 1.116 Clean Clean Clean Clean
Sample (TC) 20230140 18 43-012 32971.881 2015.098 6.112 Clean Clean
Chk Std (TC) 1000.0000 ppmC 983.381 Passed 0.000 0.000
Clean Clean Sample (TC) 20230141 19 43-012 34306.768 1432.960 4.177
Clean Clean Sample (TC) 20230142 20 43-012 31528.007 719.082 2.281
Clean Clean Sample (TC) 20230143 21 43-012 31133.229 1814.388 5.828
Clean Clean Sample (TC) 20230144 22 43-012 30956.811 2765.148 8.932
Clean Clean Sample (TC) 20230145 23 43-012 31153.522 1479.320 4.748
Clean Clean Sample (TC) 20230146 24 43-012 33297.144 2256.727 6.778
Clean Clean
Chk Std (TC) 1000.0000 ppmC 981.539 Passed 6.581 0.670
Sample Details
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Sample Type ID Start- Time
Clean Clean 09:34 Rep
Analysis
Type Run Time (mm:ss)
1 TC 07:08
2 TC 02:23
3 TC 02:22
4 TC 02:25
Sample Type ID µg/g (ppm) ABS Std Dev %RSD Start-
Time Blank
Contrib Sample (TC) USGS 92313.916 46821.438 4433.282 4.802 09:48 1619.753
Rep
Analysis Type
Weight mg (Volume µl) µg µg/g
(ppm)
NDIR
(ABS)
Baseline
(ABS)
Run Time (mm:ss)
1 TC 0.910 81.69670 89776.590 42907.951 9.269 14:26
2 TC 1.040 93.40247 89810.067 48823.861 8.938 06:18
3 TC 0.920 91.01570 98930.108 47617.626 10.011 08:24
4 TC 1.010 91.64629 90738.899 47936.315 9.629 07:03
Sample Type ID Start- Time
Clean Clean 10:26 Rep
Analysis
Type Run Time (mm:ss)
1 TC 03:07
Sample Type ID µg/g (ppm) ABS Std Dev %RSD Start-
Time Min/Max
Chk Std (TC) 1000.0000 ppmC 983.714 Passed 20806.342 0.000 0.000 10:29 900.000 /
1100.000 Rep
Analysis
Type Weight mg (Volume µl) µg µg/g
(ppm)
NDIR
(ABS)
Baseline
(ABS)
Run Time (mm:ss)
1 TC 40.000 39.34855 983.714 20806.342 10.367 04:59
Sample Type ID Start- Time
Clean Clean 10:34 Rep
Analysis
Type Run Time (mm:ss)
1 TC 02:56
2 TC 03:19
Sample Type ID ABS Std Dev %RSD Start- Time
Blank (TC) Blank 1413.694 150.070 10.615 10:41
Rep
Analysis Type
Weight mg (Volume µl) NDIR (ABS) Baseline
(ABS)
Run Time (mm:
ss)
1 TC 50.000 1519.810 8.989 08:41
2 TC 50.000 1307.579 6.604 04:20
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Time Blank
Contrib Sample (TC) 20230139 17 43-012 35108.913 38604.347 1158.381 3.299 10:54 1413.694
Rep
Analysis Type
Weight mg (Volume µl) µg µg/g
(ppm)
NDIR
(ABS)
Baseline
(ABS)
Run Time (mm:ss)
1 TC 1.720 61.79618 35928.012 32644.491 9.176 13:58
2 TC 2.490 85.38164 34289.814 44564.202 8.405 07:00
Sample Type ID Start- Time
Clean Clean 11:16 Rep
Analysis
Type Run Time (mm:ss)
1 TC 04:16
2 TC 03:21
Sample Type ID µg/g (ppm) ABS Std Dev %RSD Start-
Time Blank
Contrib Sample (TC) 20230139 SPK 43-012 48464.513 33511.363 540.754 1.116 11:24 1413.694
Rep
Analysis Type
Weight mg (Volume µl) µg µg/g
(ppm)
NDIR
(ABS)
Baseline
(ABS)
Run Time (mm:ss)
1 TC 1.370 66.92023 48846.884 35234.104 9.693 13:51
2 TC 1.250 60.10268 48082.142 31788.622 10.001 07:59
Sample Type ID Start- Time
Clean Clean 11:46 Rep
Analysis
Type Run Time (mm:ss)
1 TC 03:50
Sample Type ID Start- Time
Clean Clean 11:50 Rep
Analysis
Type Run Time (mm:ss)
1 TC 02:46
Sample Type ID µg/g (ppm) ABS Std Dev %RSD Start-
Time Blank
Contrib Sample (TC) 20230140 18 43-012 32971.881 35240.517 2015.098 6.112 11:53 1413.694
Rep
Analysis Type
Weight mg (Volume µl) µg µg/g
(ppm)
NDIR
(ABS)
Baseline
(ABS)
Run Time (mm:ss)
1 TC 2.030 69.82544 34396.771 36702.353 18.722 40:49
2 TC 2.030 64.04039 31546.992 33778.681 10.558 05:59
Sample Type ID Start- Time
Clean Clean 12:41 Rep
Analysis
Type Run Time (mm:ss)
1 TC 10:53
2 TC 02:25
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Time Min/Max
Chk Std (TC) 1000.0000 ppmC 983.381 Passed 20799.622 0.000 0.000 13:54 900.000 /
1100.000 Rep
Analysis
Type Weight mg (Volume µl) µg µg/g
(ppm)
NDIR
(ABS)
Baseline
(ABS)
Run Time (mm:ss)
1 TC 40.000 39.33525 983.381 20799.622 7.780 04:56
Sample Type ID Start- Time
Clean Clean 13:59 Rep
Analysis
Type Run Time (mm:ss)
1 TC 02:49
2 TC 02:43
Sample Type ID µg/g (ppm) ABS Std Dev %RSD Start-
Time Blank
Contrib Sample (TC) 20230141 19 43-012 34306.768 26423.706 1432.960 4.177 14:05 1413.694
Rep
Analysis Type
Weight mg (Volume µl) µg µg/g
(ppm)
NDIR
(ABS)
Baseline
(ABS)
Run Time (mm:ss)
1 TC 1.360 48.03523 35320.023 25689.929 9.208 12:15
2 TC 1.530 50.93907 33293.512 27157.484 13.396 07:35
Sample Type ID Start- Time
Clean Clean 14:25 Rep
Analysis
Type Run Time (mm:ss)
1 TC 03:10
2 TC 03:51
Sample Type ID µg/g (ppm) ABS Std Dev %RSD Start-
Time Blank
Contrib Sample (TC) 20230142 20 43-012 31528.007 30596.858 719.082 2.281 14:32 1413.694
Rep
Analysis Type
Weight mg (Volume µl) µg µg/g
(ppm)
NDIR
(ABS)
Baseline
(ABS)
Run Time (mm:ss)
1 TC 1.420 44.04775 31019.539 23674.717 9.365 13:13
2 TC 2.230 71.44134 32036.475 37519.000 8.484 06:58
Sample Type ID Start- Time
Clean Clean 14:53 Rep
Analysis
Type Run Time (mm:ss)
1 TC 02:50
2 TC 02:52
Sample Type ID µg/g (ppm) ABS Std Dev %RSD Start-
Time Blank
Contrib Sample (TC) 20230143 21 43-012 31133.229 30692.337 1814.388 5.828 14:59 1413.694 created: 3/24/2023 9:33:23 AM Page 4 of 7 printed: 3/24/2023 4:53:49 PM299
Analysis Type
Weight mg (Volume µl) µg µg/g
(ppm)
NDIR
(ABS)
Baseline
(ABS)
Run Time (mm:ss)
1 TC 1.880 60.94245 32416.195 32213.028 9.637 14:08
2 TC 1.840 54.92448 29850.263 29171.646 8.482 07:13
Sample Type ID Start- Time
Clean Clean 15:21 Rep
Analysis
Type Run Time (mm:ss)
1 TC 02:58
2 TC 02:26
Sample Type ID µg/g (ppm) ABS Std Dev %RSD Start-
Time Blank
Contrib Sample (TC) 20230144 22 43-012 30956.811 36272.567 2765.148 8.932 15:27 1413.694
Rep
Analysis Type
Weight mg (Volume µl) µg µg/g
(ppm)
NDIR
(ABS)
Baseline
(ABS)
Run Time (mm:ss)
1 TC 2.200 72.40655 32912.066 38006.799 9.297 11:53
2 TC 2.260 65.54352 29001.556 34538.335 9.284 06:42
Sample Type ID Start- Time
Clean Clean 15:46 Rep
Analysis
Type Run Time (mm:ss)
1 TC 03:31
2 TC 02:35
Sample Type ID µg/g (ppm) ABS Std Dev %RSD Start-
Time Blank
Contrib Sample (TC) 20230145 23 43-012 31153.522 38617.118 1479.320 4.748 15:52 1413.694
Rep
Analysis Type
Weight mg (Volume µl) µg µg/g
(ppm)
NDIR
(ABS)
Baseline
(ABS)
Run Time (mm:ss)
1 TC 2.160 69.55105 32199.559 36563.677 9.208 10:49
2 TC 2.580 77.67731 30107.484 40670.559 8.239 06:50
Sample Type ID Start- Time
Clean Clean 16:10 Rep
Analysis
Type Run Time (mm:ss)
1 TC 02:52
2 TC 02:45
Sample Type ID µg/g (ppm) ABS Std Dev %RSD Start-
Time Blank
Contrib Sample (TC) 20230146 24 43-012 33297.144 24354.932 2256.727 6.778 16:16 1413.694
Rep
Analysis Type
Weight mg (Volume µl) µg µg/g
(ppm)
NDIR
(ABS)
Baseline
(ABS)
Run Time (mm:ss)
1 TC 1.230 42.91825 34892.890 23103.891 8.829 10:17
2 TC 1.510 47.86911 31701.397 25605.973 7.801 06:08
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Clean Clean 16:33 Rep
Analysis
Type Run Time (mm:ss)
1 TC 02:14
Sample Type ID µg/g (ppm) ABS Std Dev %RSD Start-
Time Min/Max
Chk Std (TC) 1000.0000 ppmC 981.539 Passed 20762.384 6.581 0.670 16:36 900.000 /
1100.000 Rep
Analysis
Type Weight mg (Volume µl) µg µg/g
(ppm)
NDIR
(ABS)
Baseline
(ABS)
Run Time (mm:ss)
1 TC 40.000 39.43334 985.834 20849.195 8.842 04:28
2 TC 40.000 39.39287 984.822 20828.740 11.083 04:41
3 TC 40.000 38.95850 973.962 20609.217 11.128 04:58
created: 3/24/2023 9:33:23 AM Page 6 of 7 printed: 3/24/2023 4:53:49 PM301
Date: 3/24/2023 9:27:24 AM Instrument Name: Lotix - 1 Method: Solids TC Schedule: from schedule 032423 STD Sample ppm Calculation Uses: Latest Method Blank Software Ver: 3.3.7431.18150 Sample Source: Solids Module
TC
Linear Curve: y = 505.384x + 920.218 Coefficient of Determination (r²): 0.99999
Standard Results
Actual µgC/g (ppmC)
Weight mg (Volume µl) µg ABS Measured µgC When
500.00 40.000 20.00000 10964.247 19.87406 3/24/2023 8:43:53
AM
1000.00 40.000 40.00000 21168.132 40.06442 3/24/2023 8:55:34
AM
2000.00 40.000 80.00000 41444.945 80.18602 3/24/2023 9:08:15
AM
3000.00 40.000 120.00000 61503.372 119.87550 3/24/2023 9:25:05
AM
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80000
85000
90000
95000
100000
105000
1 3 5 7 9 11 13 15 17 19
T O
C V al u e p p m
C ar b o n
(Updated: 03/27/23)
Control Chart of TOC Values for USGS Standards
TOC Value Mean TOC Value Lower 95% CL (-2 SD)
Upper 95% CL (+2 SD) Lower 99.7% CL (-3 SD) Upper 99.7% CL (+3 SD)
Known Value of Standard -10% Known Value of Standard +10%
Schedule: 032823 43-012 samples Report Date: 3/28/2023 9:24:57 AM Instrument: Lotix - 1 Method: Solids TC Sample Source: Solids Module Calibration: 3/28/2023 9:16:18 AM Software Ver: 3.3.7431.18150 Comment:
Schedule Summary
Sample Type ID µg/g (ppm) Std Dev %RSD Clean Clean
Sample (TC) USGS 98399.683 2201.889 2.238 Clean Clean
Chk Std (TC) 1000.0000 ppmC 956.781 Passed 0.000 0.000
Clean Clean
Blank (TC) Blank 1616.271
(ABS) 219.738 13.595
Sample (TC) 20230147 25 43-012 28622.519 781.246 2.729 Clean Clean
Sample (TC) 20230147 SPK 43-012 40917.306 1649.463 4.031 Clean Clean
Sample (TC) 20230148 26 43-012 31227.532 449.940 1.441 Clean Clean
Chk Std (TC) 1000.0000 ppmC 971.295 Passed 0.000 0.000
Clean Clean Sample (TC) 20230149 27 43-012 30001.313 1414.584 4.715
Clean Clean Sample (TC) 20230150 28 43-012 30354.498 262.868 0.866
Clean Clean Sample (TC) 20230151 29 43-012 33465.320 5928.033 17.714
Clean Clean Sample (TC) 20230152 30 43-012 39767.024 183.114 0.460
Clean Clean Sample (TC) 20230153 31 43-012 39193.340 1182.404 3.017
Clean Clean Sample (TC) 20230154 32 43-012 41768.624 829.072 1.985
Clean Clean Sample (TC) 20230169 Composite B 43-012 29112.819 333.279 1.145
Clean Clean Sample (TC) 20230170 Composite C 43-012 28067.854 1964.769 7.000
Clean Clean Sample (TC) 20230171 Composite D 43-012 25116.036 719.143 2.863
Clean Clean
Chk Std (TC) 1000.0000 ppmC 949.335 Passed 4.999 0.527
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Sample Details
Time
Clean Clean 09:25 Rep
Analysis
Type Run Time (mm:ss)
1 TC 02:28
2 TC 02:26
3 TC 06:38
4 TC 04:46
Sample Type ID µg/g (ppm) ABS Std Dev %RSD Start-
Time Blank
Contrib Sample (TC) USGS 98399.683 25256.327 2201.889 2.238 09:42 1413.694
Rep
Analysis Type
Weight mg (Volume µl) µg µg/g
(ppm)
NDIR
(ABS)
Baseline
(ABS)
Run Time (mm:ss)
1 TC 0.490 49.69160 101411.436 26434.632 5.530 06:51
2 TC 0.700 69.06122 98658.889 36187.709 6.519 05:25
3 TC 0.410 39.74285 96933.779 21425.191 7.124 05:23
4 TC 0.320 30.91028 96594.626 16977.777 6.606 05:13
Sample Type ID Start- Time
Clean Clean 10:06 Rep
Analysis
Type Run Time (mm:ss)
1 TC 08:06
Sample Type ID µg/g (ppm) ABS Std Dev %RSD Start-
Time Min/Max
Chk Std (TC) 1000.0000 ppmC 956.781 Passed 20534.887 0.000 0.000 10:14 900.000 /
1100.000 Rep
Analysis
Type Weight mg (Volume µl) µg µg/g
(ppm)
NDIR
(ABS)
Baseline
(ABS)
Run Time (mm:ss)
1 TC 40.000 38.27123 956.781 20534.887 8.260 04:51
Sample Type ID Start- Time
Clean Clean 10:19 Rep
Analysis
Type Run Time (mm:ss)
1 TC 03:10
2 TC 03:23
Sample Type ID ABS Std Dev %RSD Start- Time
Blank (TC) Blank 1616.271 219.738 13.595 10:26
Rep
Analysis Type
Weight mg (Volume µl) NDIR (ABS) Baseline
(ABS)
Run Time (mm:
ss)
1 TC 50.000 1771.650 5.534 05:09
2 TC 50.000 1460.893 5.066 04:22
created: 3/28/2023 9:24:57 AM Page 2 of 8 printed: 3/28/2023 5:03:18 PM305
Time Blank
Contrib Sample (TC) 20230147 25 43-012 28622.519 47983.807 781.246 2.729 10:36 1616.271
Rep
Analysis Type
Weight mg (Volume µl) µg µg/g
(ppm)
NDIR
(ABS)
Baseline
(ABS)
Run Time (mm:ss)
1 TC 3.840 112.03178 29174.944 58027.015 13.581 30:24
2 TC 2.570 72.14014 28070.094 37940.598 7.887 06:19
Sample Type ID Start- Time
Clean Clean 11:14 Rep
Analysis
Type Run Time (mm:ss)
1 TC 02:41
2 TC 02:40
Sample Type ID µg/g (ppm) ABS Std Dev %RSD Start-
Time Blank
Contrib Sample (TC) 20230147 SPK 43-012 40917.306 46159.330 1649.463 4.031 11:19 1616.271
Rep
Analysis Type
Weight mg (Volume µl) µg µg/g
(ppm)
NDIR
(ABS)
Baseline
(ABS)
Run Time (mm:ss)
1 TC 2.400 101.00077 42083.653 52472.628 7.417 10:42
2 TC 1.910 75.92433 39750.960 39846.031 7.392 06:06
Sample Type ID Start- Time
Clean Clean 11:37 Rep
Analysis
Type Run Time (mm:ss)
1 TC 03:00
2 TC 03:12
Sample Type ID µg/g (ppm) ABS Std Dev %RSD Start-
Time Blank
Contrib Sample (TC) 20230148 26 43-012 31227.532 39905.512 449.940 1.441 11:43 1616.271
Rep
Analysis Type
Weight mg (Volume µl) µg µg/g
(ppm)
NDIR
(ABS)
Baseline
(ABS)
Run Time (mm:ss)
1 TC 1.960 61.82955 31545.687 32748.961 7.230 10:48
2 TC 2.920 90.25538 30909.376 47062.062 7.544 06:19
Sample Type ID Start- Time
Clean Clean 12:01 Rep
Analysis
Type Run Time (mm:ss)
1 TC 03:38
Sample Type ID µg/g (ppm) ABS Std Dev %RSD Start-
Time Min/Max
Chk Std (TC) 1000.0000 ppmC 971.295 Passed 20827.211 0.000 0.000 13:04 900.000 /
1100.000 created: 3/28/2023 9:24:57 AM Page 3 of 8 printed: 3/28/2023 5:03:18 PM306
Analysis Type
Weight mg (Volume µl) µg µg/g
(ppm)
NDIR
(ABS)
Baseline
(ABS)
Run Time (mm:ss)
1 TC 40.000 38.85178 971.295 20827.211 7.536 04:48
Sample Type ID Start- Time
Clean Clean 13:10 Rep
Analysis
Type Run Time (mm:ss)
1 TC 03:18
2 TC 02:30
Sample Type ID µg/g (ppm) ABS Std Dev %RSD Start-
Time Blank
Contrib Sample (TC) 20230149 27 43-012 30001.313 31015.837 1414.584 4.715 13:15 1616.271
Rep
Analysis Type
Weight mg (Volume µl) µg µg/g
(ppm)
NDIR
(ABS)
Baseline
(ABS)
Run Time (mm:ss)
1 TC 1.980 61.38312 31001.575 32524.173 5.983 08:52
2 TC 1.910 55.39201 29001.051 29507.502 6.985 05:39
Sample Type ID Start- Time
Clean Clean 13:31 Rep
Analysis
Type Run Time (mm:ss)
1 TC 13:30
2 TC 11:59
Sample Type ID µg/g (ppm) ABS Std Dev %RSD Start-
Time Blank
Contrib Sample (TC) 20230150 28 43-012 30354.498 41096.530 262.868 0.866 13:56 1616.271
Rep
Analysis Type
Weight mg (Volume µl) µg µg/g
(ppm)
NDIR
(ABS)
Baseline
(ABS)
Run Time (mm:ss)
1 TC 2.900 87.48900 30168.622 45669.125 6.537 10:44
2 TC 2.270 69.32665 30540.373 36523.934 7.397 06:13
Sample Type ID Start- Time
Clean Clean 14:14 Rep
Analysis
Type Run Time (mm:ss)
1 TC 02:53
2 TC 02:47
Sample Type ID µg/g (ppm) ABS Std Dev %RSD Start-
Time Blank
Contrib Sample (TC) 20230151 29 43-012 33465.320 35919.886 5928.033 17.714 14:20 1616.271
Rep
Analysis Type
Weight mg (Volume µl) µg µg/g
(ppm)
NDIR
(ABS)
Baseline
(ABS)
Run Time (mm:ss)
1 TC 2.460 92.63640 37657.072 48260.964 6.506 10:35
2 TC 1.490 43.61762 29273.567 23578.808 5.749 08:01
created: 3/28/2023 9:24:57 AM Page 4 of 8 printed: 3/28/2023 5:03:18 PM307
Clean Clean 14:39 Rep
Analysis
Type Run Time (mm:ss)
1 TC 02:47
2 TC 02:34
Sample Type ID µg/g (ppm) ABS Std Dev %RSD Start-
Time Blank
Contrib Sample (TC) 20230152 30 43-012 39767.024 38688.746 183.114 0.460 14:44 1616.271
Rep
Analysis Type
Weight mg (Volume µl) µg µg/g
(ppm)
NDIR
(ABS)
Baseline
(ABS)
Run Time (mm:ss)
1 TC 2.290 91.36300 39896.505 47619.775 6.384 09:34
2 TC 1.410 55.88894 39637.543 29757.718 9.510 06:35
Sample Type ID Start- Time
Clean Clean 15:01 Rep
Analysis
Type Run Time (mm:ss)
1 TC 03:07
2 TC 01:58
Sample Type ID µg/g (ppm) ABS Std Dev %RSD Start-
Time Blank
Contrib Sample (TC) 20230153 31 43-012 39193.340 29677.326 1182.404 3.017 15:06 1616.271
Rep
Analysis Type
Weight mg (Volume µl) µg µg/g
(ppm)
NDIR
(ABS)
Baseline
(ABS)
Run Time (mm:ss)
1 TC 1.280 51.23767 40029.426 27415.689 6.869 10:22
2 TC 1.570 60.22089 38357.254 31938.962 33.536 04:33
Sample Type ID Start- Time
Clean Clean 15:22 Rep
Analysis
Type Run Time (mm:ss)
1 TC 03:09
2 TC 02:41
Sample Type ID µg/g (ppm) ABS Std Dev %RSD Start-
Time Blank
Contrib Sample (TC) 20230154 32 43-012 41768.624 32675.034 829.072 1.985 15:28 1616.271
Rep
Analysis Type
Weight mg (Volume µl) µg µg/g
(ppm)
NDIR
(ABS)
Baseline
(ABS)
Run Time (mm:ss)
1 TC 1.710 70.42187 41182.381 37075.407 6.748 10:37
2 TC 1.250 52.94358 42354.866 28274.661 6.898 05:50
Sample Type ID Start- Time
Clean Clean 15:45 created: 3/28/2023 9:24:57 AM Page 5 of 8 printed: 3/28/2023 5:03:18 PM308
Analysis Type
Run Time (mm:ss)
1 TC 03:05
2 TC 02:49
Sample Type ID µg/g (ppm) ABS Std Dev %RSD Start-
Time Blank
Contrib
Sample (TC) 20230169 Composite B 43- 012 29112.819 34141.489 333.279 1.145 15:51 1616.271
Rep
Analysis Type
Weight mg (Volume µl) µg µg/g
(ppm)
NDIR
(ABS)
Baseline
(ABS)
Run Time (mm:ss)
1 TC 2.370 68.43886 28877.155 36076.910 6.094 08:38
2 TC 2.070 60.75136 29348.483 32206.067 6.903 06:04
Sample Type ID Start- Time
Clean Clean 16:07 Rep
Analysis
Type Run Time (mm:ss)
1 TC 02:49
2 TC 02:39
Sample Type ID µg/g (ppm) ABS Std Dev %RSD Start-
Time Blank
Contrib
Sample (TC) 20230170 Composite C 43- 012 28067.854 34165.122 1964.769 7.000 16:12 1616.271
Rep
Analysis Type
Weight mg (Volume µl) µg µg/g
(ppm)
NDIR
(ABS)
Baseline
(ABS)
Run Time (mm:ss)
1 TC 3.130 92.20090 29457.156 48041.679 6.178 08:47
2 TC 1.390 37.08319 26678.553 20288.564 6.925 06:07
Sample Type ID Start- Time
Clean Clean 16:28 Rep
Analysis
Type Run Time (mm:ss)
1 TC 02:55
2 TC 02:33
Sample Type ID µg/g (ppm) ABS Std Dev %RSD Start-
Time Blank
Contrib
Sample (TC) 20230171 Composite D 43- 012 25116.036 27249.837 719.143 2.863 16:33 1616.271
Rep
Analysis Type
Weight mg (Volume µl) µg µg/g
(ppm)
NDIR
(ABS)
Baseline
(ABS)
Run Time (mm:ss)
1 TC 1.930 47.49252 24607.525 25529.919 5.229 06:34
2 TC 2.120 54.32404 25624.548 28969.755 6.334 05:36
Sample Type ID Start- Time
Clean Clean 16:46 created: 3/28/2023 9:24:57 AM Page 6 of 8 printed: 3/28/2023 5:03:18 PM309
Analysis Type
Run Time (mm:ss)
1 TC 02:07
Sample Type ID µg/g (ppm) ABS Std Dev %RSD Start-
Time Min/Max
Chk Std (TC) 1000.0000 ppmC 949.335 Passed 20384.922 4.999 0.527 16:48 900.000 /
1100.000 Rep
Analysis
Type Weight mg (Volume µl) µg µg/g
(ppm)
NDIR
(ABS)
Baseline
(ABS)
Run Time (mm:ss)
1 TC 40.000 37.79581 944.895 20295.500 7.206 04:17
2 TC 40.000 38.18996 954.749 20493.966 11.610 04:25
3 TC 40.000 37.93443 948.361 20365.300 9.908 04:22
created: 3/28/2023 9:24:57 AM Page 7 of 8 printed: 3/28/2023 5:03:18 PM310
Date: 3/28/2023 9:16:18 AM Instrument Name: Lotix - 1 Method: Solids TC Schedule: from schedule 032823 STD Sample ppm Calculation Uses: Latest Method Blank Software Ver: 3.3.7431.18150 Sample Source: Solids Module
TC
Linear Curve: y = 503.524x + 1264.387 Coefficient of Determination (r²): 0.99992
Standard Results
Actual µgC/g (ppmC)
Weight mg (Volume µl) µg ABS Measured µgC When
500.00 40.000 20.00000 11239.537 19.81066 3/28/2023 8:39:04
AM
1000.00 40.000 40.00000 21382.671 39.95493 3/28/2023 8:49:47
AM
2000.00 40.000 80.00000 41830.085 80.56351 3/28/2023 9:01:50
AM
3000.00 40.000 120.00000 61521.618 119.67091 3/28/2023 9:15:04
AM
created: 3/28/2023 9:24:57 AM Page 8 of 8 printed: 3/28/2023 5:03:18 PM311
Schedule: 033023 43-012 Controls samples Report Date: 3/30/2023 9:11:06 AM Instrument: Lotix - 1 Method: Solids TC Sample Source: Solids Module Calibration: 3/30/2023 8:59:24 AM Software Ver: 3.3.7431.18150 Comment: 1. Disregard first run of 20230179. LH
Schedule Summary
Sample Type ID µg/g (ppm) Std Dev %RSD Clean Clean
Sample (TC) USGS 92577.589 1144.501 1.236 Clean Clean
Chk Std (TC) 1000.0000 ppmC 977.118 Passed 0.000 0.000
Clean Clean
Blank (TC) Blank 1425.478
(ABS) 49.321 3.460
Sample (TC) 20230172 Composite E 43-012 28488.453 540.509 1.897 Clean Clean
Sample (TC) 20230172 SPK 43-012 45214.934 517.671 1.145 Clean Clean
Sample (TC) 20230173 Composite G 43-012 22808.863 2002.623 8.780 Clean Clean
Sample (TC) 20230174 Composite H 43-012 34359.404 1045.322 3.042 Clean Clean
Sample (TC) 20230175 Composite I 43-012 32242.174 277.598 0.861 Clean Clean
Chk Std (TC) 1000.0000 ppmC 972.594 Passed 0.000 0.000
Clean Clean Sample (TC) 20230176 Composite J 43-012 30481.214 1899.209 6.231
Clean Clean Sample (TC) 20230177 Composite K 43-012 30973.056 1952.064 6.302
Clean Clean Sample (TC) 20230178 Composite L 43-012 31712.240 2036.877 6.423
Clean Clean Sample (TC) 20230179 Composite M 43-012 60798.179 85981.609 141.421
Clean Clean Sample (TC) 20230179 Composite M 43-012 40367.194 2118.621 5.248
Clean Clean Sample (TC) 20230164 Solid Phase Control 29537.234 3235.909 10.955
Clean Clean Sample (TC) 20230165 Clam Control 904.239 22.653 2.505
Clean Clean Sample (TC) 20230166 Worm Control 13347.147 349.765 2.621
Clean Clean
Chk Std (TC) 1000.0000 ppmC 981.137 Passed 6.408 0.653
Lotix Report: Samples Schedule created: 3/30/2023 9:11:06 AM Page 1 of 8 printed: 3/30/2023 4:35:58 PM312
CHall Highlight
CHall Highlight
CHall Highlight
CHall Highlight
CHall Highlight
CHall Highlight
CHall Highlight
CHall Highlight
CHall Highlight
CHall Highlight
CHall Highlight
Sample Details
Time
Clean Clean 09:12 Rep
Analysis
Type Run Time (mm:ss)
1 TC 02:23
2 TC 02:33
3 TC 03:03
4 TC 03:07
Sample Type ID µg/g (ppm) ABS Std Dev %RSD Start-
Time Blank
Contrib Sample (TC) USGS 92577.589 30101.070 1144.501 1.236 09:23 1616.271
Rep
Analysis Type
Weight mg (Volume µl) µg µg/g
(ppm)
NDIR
(ABS)
Baseline
(ABS)
Run Time (mm:ss)
1 TC 0.720 67.32132 93501.838 35152.608 3.365 04:42
2 TC 0.570 53.31375 93532.893 28174.689 5.191 05:33
3 TC 0.640 58.36326 91192.591 30690.119 4.789 05:18
4 TC 0.540 49.72484 92083.036 26386.862 5.283 05:39
Sample Type ID Start- Time
Clean Clean 09:45 Rep
Analysis
Type Run Time (mm:ss)
1 TC 02:39
Sample Type ID µg/g (ppm) ABS Std Dev %RSD Start-
Time Min/Max
Chk Std (TC) 1000.0000 ppmC 977.118 Passed 20739.456 0.000 0.000 09:48 900.000 /
1100.000 Rep
Analysis
Type Weight mg (Volume µl) µg µg/g
(ppm)
NDIR
(ABS)
Baseline
(ABS)
Run Time (mm:ss)
1 TC 40.000 39.08473 977.118 20739.456 6.603 04:35
Sample Type ID Start- Time
Clean Clean 09:53 Rep
Analysis
Type Run Time (mm:ss)
1 TC 02:31
2 TC 02:49
Sample Type ID ABS Std Dev %RSD Start- Time
Blank (TC) Blank 1425.478 49.321 3.460 09:58
Rep
Analysis Type
Weight mg (Volume µl) NDIR (ABS) Baseline
(ABS)
Run Time (mm:
ss)
1 TC 50.000 1460.353 3.654 04:49
2 TC 50.000 1390.602 3.411 04:11
created: 3/30/2023 9:11:06 AM Page 2 of 8 printed: 3/30/2023 4:35:58 PM313
Time Blank
Contrib
Sample (TC) 20230172 Composite E 43- 012 28488.453 23799.168 540.509 1.897 10:08 1425.478
Rep
Analysis Type
Weight mg (Volume µl) µg µg/g
(ppm)
NDIR
(ABS)
Baseline
(ABS)
Run Time (mm:ss)
1 TC 1.690 48.79140 28870.651 25731.073 4.766 09:15
2 TC 1.460 41.03513 28106.256 21867.263 6.534 05:32
Sample Type ID Start- Time
Clean Clean 10:24 Rep
Analysis
Type Run Time (mm:ss)
1 TC 02:51
2 TC 02:10
Sample Type ID µg/g (ppm) ABS Std Dev %RSD Start-
Time Blank
Contrib Sample (TC) 20230172 SPK 43-012 45214.934 34751.831 517.671 1.145 10:29 1425.478
Rep
Analysis Type
Weight mg (Volume µl) µg µg/g
(ppm)
NDIR
(ABS)
Baseline
(ABS)
Run Time (mm:ss)
1 TC 1.430 65.18080 45580.982 33895.508 5.243 11:10
2 TC 1.530 68.61880 44848.886 35608.154 5.416 05:51
Sample Type ID Start- Time
Clean Clean 10:46 Rep
Analysis
Type Run Time (mm:ss)
1 TC 03:07
2 TC 01:41
Sample Type ID µg/g (ppm) ABS Std Dev %RSD Start-
Time Blank
Contrib
Sample (TC) 20230173 Composite G 43- 012 22808.863 28171.498 2002.623 8.780 10:51 1425.478
Rep
Analysis Type
Weight mg (Volume µl) µg µg/g
(ppm)
NDIR
(ABS)
Baseline
(ABS)
Run Time (mm:ss)
1 TC 1.960 47.48086 24224.931 25078.225 5.865 12:14
2 TC 2.800 59.89983 21392.795 31264.772 6.316 06:10
Sample Type ID Start- Time
Clean Clean 11:10 Rep
Analysis
Type Run Time (mm:ss)
1 TC 03:12
2 TC 02:58
Sample Type ID µg/g (ppm) ABS Std Dev %RSD Start-
Time Blank
Contrib
Sample (TC) 20230174 Composite H 43- 012 34359.404 36283.712 1045.322 3.042 11:17 1425.478 created: 3/30/2023 9:11:06 AM Page 3 of 8 printed: 3/30/2023 4:35:58 PM314
Analysis Type
Weight mg (Volume µl) µg µg/g
(ppm)
NDIR
(ABS)
Baseline
(ABS)
Run Time (mm:ss)
1 TC 1.880 65.98529 35098.558 34296.265 4.897 09:22
2 TC 2.200 73.96455 33620.249 38271.159 5.139 06:00
Sample Type ID Start- Time
Clean Clean 11:33 Rep
Analysis
Type Run Time (mm:ss)
1 TC 02:33
2 TC 03:00
Sample Type ID µg/g (ppm) ABS Std Dev %RSD Start-
Time Blank
Contrib
Sample (TC) 20230175 Composite I 43- 012 32242.174 27906.491 277.598 0.861 11:38 1425.478
Rep
Analysis Type
Weight mg (Volume µl) µg µg/g
(ppm)
NDIR
(ABS)
Baseline
(ABS)
Run Time (mm:ss)
1 TC 1.860 59.60534 32045.882 31118.073 5.548 10:07
2 TC 1.440 46.71139 32438.465 24694.909 5.101 05:47
Sample Type ID Start- Time
Clean Clean 11:55 Rep
Analysis
Type Run Time (mm:ss)
1 TC 06:53
Sample Type ID µg/g (ppm) ABS Std Dev %RSD Start-
Time Min/Max
Chk Std (TC) 1000.0000 ppmC 972.594 Passed 20649.304 0.000 0.000 13:02 900.000 /
1100.000 Rep
Analysis
Type Weight mg (Volume µl) µg µg/g
(ppm)
NDIR
(ABS)
Baseline
(ABS)
Run Time (mm:ss)
1 TC 40.000 38.90376 972.594 20649.304 5.458 04:50
Sample Type ID Start- Time
Clean Clean 13:07 Rep
Analysis
Type Run Time (mm:ss)
1 TC 03:45
2 TC 02:39
Sample Type ID µg/g (ppm) ABS Std Dev %RSD Start-
Time Blank
Contrib
Sample (TC) 20230176 Composite J 43- 012 30481.214 33379.441 1899.209 6.231 13:14 1425.478
Rep
Analysis Type
Weight mg (Volume µl) µg µg/g
(ppm)
NDIR
(ABS)
Baseline
(ABS)
Run Time (mm:ss)
1 TC 2.200 70.01315 31824.158 36302.756 4.823 10:08
2 TC 2.000 58.27654 29138.270 30456.127 5.294 06:07
created: 3/30/2023 9:11:06 AM Page 4 of 8 printed: 3/30/2023 4:35:58 PM315
Clean Clean 13:31 Rep
Analysis
Type Run Time (mm:ss)
1 TC 03:19
2 TC 02:55
Sample Type ID µg/g (ppm) ABS Std Dev %RSD Start-
Time Blank
Contrib
Sample (TC) 20230177 Composite K 43- 012 30973.056 33274.799 1952.064 6.302 13:37 1425.478
Rep
Analysis Type
Weight mg (Volume µl) µg µg/g
(ppm)
NDIR
(ABS)
Baseline
(ABS)
Run Time (mm:ss)
1 TC 1.940 62.76554 32353.374 32692.339 5.468 10:27
2 TC 2.200 65.10402 29592.739 33857.260 8.218 05:40
Sample Type ID Start- Time
Clean Clean 13:54 Rep
Analysis
Type Run Time (mm:ss)
1 TC 03:03
2 TC 02:51
Sample Type ID µg/g (ppm) ABS Std Dev %RSD Start-
Time Blank
Contrib
Sample (TC) 20230178 Composite L 43- 012 31712.240 36804.699 2036.877 6.423 14:00 1425.478
Rep
Analysis Type
Weight mg (Volume µl) µg µg/g
(ppm)
NDIR
(ABS)
Baseline
(ABS)
Run Time (mm:ss)
1 TC 2.020 61.14934 30271.950 31887.221 5.575 10:19
2 TC 2.440 80.89217 33152.529 41722.177 4.975 05:43
Sample Type ID Start- Time
Clean Clean 14:16 Rep
Analysis
Type Run Time (mm:ss)
1 TC 04:39
2 TC 03:02
Sample Type ID µg/g (ppm) ABS Std Dev %RSD Start-
Time Blank
Contrib
Sample (TC) 20230179 Composite M 43- 012 60798.179 51394.026 85981.609 141.421 14:24 1425.478
Rep
Analysis Type
Weight mg (Volume µl) µg µg/g
(ppm)
NDIR
(ABS)
Baseline
(ABS)
Run Time (mm:ss)
1 TC 1.650 200.63399 121596.358 101371.955 5.151 11:54
2 TC 2.030 0.00000 0.000 1416.097 6.321 05:23
created: 3/30/2023 9:11:06 AM Page 5 of 8 printed: 3/30/2023 4:35:58 PM316
Clean Clean 14:42 Rep
Analysis
Type Run Time (mm:ss)
1 TC 02:13
Sample Type ID µg/g (ppm) ABS Std Dev %RSD Start-
Time Blank
Contrib
Sample (TC) 20230179 Composite…
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