STORAGE_TANK_PHOTOGRAPHS,_LEAD_BASED_PAINT_TEST_RESULTS_&_WASTE.pdf

Sault Sainte Marie

A. GENERAL INFORMATION

GENERATOR EPA ID #/REGISTRATION # MI3960020599

GENERATOR CODE (Assigned by Clean Harbors)

St Marys Canal - Soo Area Office 312 W Portage A

GENERATOR NAME:

CITY STATE/PROVINCE

US Army Corp of Engineers

ZIP/POSTAL CODE 49783

PHONE: (906) 632-3311

MIUN40415

ADDRESS

ZIP/POSTAL CODE

CUSTOMER CODE (Assigned by Clean Harbors)

ADDRESS

CUSTOMER NAME:

CITY STATE/PROVINCESault Sainte

Marie

MI 49783

US Army Corp of Engineers St Marys Canal - Soo Area Office 312 W Portage Avenue

UN40415

B. WASTE DESCRIPTION

WASTE DESCRIPTION: Blue Tank water

PROCESS GENERATING WASTE:

IS THIS WASTE CONTAINED IN SMALL PACKAGING CONTAINED WITHIN A LARGER SHIPPING CONTAINER ?

water from Blue storage tank

No

C. PHYSICAL PROPERTIES (at 25C or 77F)

PHYSICAL STATE

SOLID WITHOUT FREE LIQUID

POWDER

MONOLITHIC SOLID

LIQUID WITH NO SOLIDS

LIQUID/SOLID MIXTURE

% FREE LIQUID

% SETTLED SOLID

% TOTAL SUSPENDED SOLID

SLUDGE

GAS/AEROSOL

% BY VOLUME (Approx.)

NUMBER OF PHASES/LAYERS

TOP

MIDDLE

BOTTOM

321 0.00

0.00

0.00

ODOR

NONE

MILD

STRONG

Describe:

BOILING POINT ºF (ºC)

<= 95 (<=35)

95 - 100 (35-38)

101 - 129 (38-54)

>= 130 (>54)

COLOR

clear

VISCOSITY (If liquid present) 1 - 100 (e.g. Water)

101 - 500 (e.g. Motor Oil)

501 - 10,000 (e.g. Molasses)

> 10,000

TOTAL ORGANIC

CARBON

<= 1%

1-9%

>= 10%

< 140 (<60)

140-200 (60-93)

> 200 (>93)

MELTING POINT ºF (ºC)

FLASH POINT ºF (ºC)

< 73 (<23)

73 - 100 (23-38)

101 -140 (38-60)

141 -200 (60-93)

> 200 (>93)

SPECIFIC GRAVITY

< 0.8 (e.g. Gasoline)

0.8-1.0 (e.g. Ethanol)

1.0 (e.g. Water)

> 1.2 (e.g. Methylene Chloride)

1.0-1.2 (e.g. Antifreeze) pH

2.1 - 6.9

<= 2

7 (Neutral)

7.1 - 12.4

>= 12.5

BTU/LB (MJ/kg)

< 2,000 (<4.6)

2,000-5,000 (4.6-11.6)

5,000-10,000 (11.6-23.2)

> 10,000 (>23.2)

Actual:

ASH

< 0.1

0.1 - 1.0

1.1 - 5.0

5.1 - 20.0

> 20

Unknown

D. COMPOSITION

DOES THIS WASTE CONTAIN ANY HEAVY GAUGE METAL DEBRIS OR OTHER LARGE OBJECTS (EX., METAL PLATE OR PIPING >1/4” THICK OR >12” LONG, METAL REINFORCED HOSE >12” LONG, METAL WIRE >12” LONG, METAL VALVES, PIPE FITTINGS, CONCRETE REINFORCING BAR OR

PIECES OF CONCRETE >3”)?

YES NO

If yes, describe, including dimensions:

(List the complete composition of the waste, include any inert components and/or debris. Ranges for individual components are acceptable. If a trade name is used, please supply an MSDS. Please do not use abbreviations.)

CHEMICAL MIN -- MAX UOM

WATER & NON HAZ PROPRIETARY INGREDIENTS 100.0000000 -- 100.0000000 %

DOES THIS WASTE CONTAIN ANY METALS IN POWDERED OR OTHER FINELY DIVIDED FORM? YES NO

DOES THIS WASTE CONTAIN OR HAS IT CONTACTED ANY OF THE FOLLOWING; ANIMAL WASTES, HUMAN BLOOD, BLOOD PRODUCTS, BODY FLUIDS, MICROBIOLOGICAL WASTE, PATHOLOGICAL WASTE, HUMAN OR ANIMAL DERIVED SERUMS OR PROTEINS OR ANY OTHER

POTENTIALLY INFECTIOUS MATERIAL?

YES NO

I acknowledge that this waste material is neither infectious nor does it contain any organism known to be a threat to human health. This certification is based on my knowledge of the material. Select the answer below that applies:

The waste was never exposed to potentially infectious material. YES NO

Chemical disinfection or some other form of sterilization has been applied to the waste. YES NO

I ACKNOWLEDGE THAT THIS PROFILE MEETS THE CLEAN HARBORS BATTERY PACKAGING REQUIREMENTS. YES NO

I ACKNOWLEDGE THAT MY FRIABLE ASBESTOS WASTE IS DOUBLE BAGGED AND WETTED. YES NO

SPECIFY THE SOURCE CODE ASSOCIATED WITH THE

WASTE.

SPECIFY THE FORM CODE ASSOCIATED WITH THE WASTE.G45 W113

Report Printed On : Wednesday, June 19, 2019 /WINWEB/Profile\Waste Profile.rdl Page 1 of 3

Profile No. 1863269

WASTE MATERIAL PROFILE SHEET

If constituent concentrations are based on analytical testing, analysis must be provided. Please attach document(s) using the link on the Submit tab.

TestingKnowledgeAre these values based on testing or knowledge?

E. CONSTITUENTS

OTHER CONSTITUENTS MAX UOM NOT

APPLICABLE

BROMINE

CHLORINE

FLUORINE

IODINE

SULFUR

POTASSIUM

SODIUM

AMMONIA

CYANIDE AMENABLE

CYANIDE REACTIVE

CYANIDE TOTAL

SULFIDE REACTIVE

VOLATILE COMPOUNDS

D018 BENZENE 0.5

D019 CARBON TETRACHLORIDE 0.5

D021 CHLOROBENZENE 100.0

D022 CHLOROFORM 6.0

D028 1,2-DICHLOROETHANE 0.5

D029 1,1-DICHLOROETHYLENE 0.7

D035 METHYL ETHYL KETONE 200.0

D039 TETRACHLOROETHYLENE 0.7

D040 TRICHLOROETHYLENE 0.5

D043 VINYL CHLORIDE 0.2

SEMI-VOLATILE COMPOUNDS

D023 o-CRESOL 200.0

D024 m-CRESOL 200.0

D025 p-CRESOL 200.0

D026 CRESOL (TOTAL) 200.0

D027 1,4-DICHLOROBENZENE 7.5

D030 2,4-DINITROTOLUENE 0.13

D032 HEXACHLOROBENZENE 0.13

D033 HEXACHLOROBUTADIENE 0.5

D034 HEXACHLOROETHANE 3.0

D036 NITROBENZENE 2.0

D037 PENTACHLOROPHENOL 100.0

D038 PYRIDINE 5.0

D041 2,4,5-TRICHLOROPHENOL 400.0

D042 2,4,6-TRICHLOROPHENOL 2.0

PESTICIDES AND HERBICIDES

D012 ENDRIN 0.02

D013 LINDANE 0.4

D014 METHOXYCHLOR 10.0

D015 TOXAPHENE 0.5

D016 2,4-D 10.0

D017 2,4,5-TP (SILVEX) 1.0

D020 CHLORDANE 0.03

D031 HEPTACHLOR (AND ITS EPOXIDE) 0.008

HOCs

NONE

< 1000 PPM

>= 1000 PPM

PCBs

NONE

< 50 PPM

>=50 PPM

IF PCBS ARE PRESENT, IS THE

WASTE REGULATED BY TSCA 40

CFR 761?

YES NO

Please indicate which constituents below apply. Concentrations must be entered when applicable to assist in accurate review and expedited approval of your waste profile. Please note that the total regulated metals and other constituents sections require answers.

ADDITIONAL HAZARDS

DOES THIS WASTE HAVE ANY UNDISCLOSED HAZARDS OR PRIOR INCIDENTS ASSOCIATED WITH IT, WHICH COULD AFFECT THE WAY IT SHOULD BE HANDLED?

YES NO (If yes, explain)

DEA REGULATED SUBSTANCES EXPLOSIVE FUMING

NONE OF THE ABOVEPOLYMERIZABLE RADIOACTIVE REACTIVE MATERIAL

RCRA REGULATED METALS REGULATORY

LEVEL (mg/l)

TCLP

mg/l

TOTAL UOM NOT APPLICABLE

D004 ARSENIC 5.0

D005 BARIUM 100.0

D006 CADMIUM 1.0

D007 CHROMIUM 5.0

D008 LEAD 5.0

D009 MERCURY 0.2

D010 SELENIUM 1.0

D011 SILVER 5.0

CHOOSE ALL THAT APPLY

OSHA REGULATED CARCINOGENS

Report Printed On : Wednesday, June 19, 2019 /WINWEB/Profile\Waste Profile.rdl Page 2 of 3

G. DOT/TDG INFORMATION

DOT/TDG PROPER SHIPPING NAME:

NON DOT REGULATED MATERIAL

F. REGULATORY STATUS

YES NO IF THIS IS A US EPA HAZARDOUS WASTE, DOES THIS WASTE STREAM CONTAIN BENZENE?

YES NO DO ANY CANADIAN PROVINCIAL WASTE CODES APPLY?

YES NO IS THE GENERATOR OF THE WASTE CLASSIFIED AS VERY SMALL QUANTITY GENERATOR (VSQG) OR A STATE EQUIVALENT DESIGNATION?

YES NO IS THIS WASTE STREAM SUBJECT TO THE INORGANIC METAL BEARING WASTE PROHIBITION FOUND AT 40 CFR 268.3(C)?

Pharmaceuticals production (subpart GGG)Hazardous Organic NESHAP (HON) rule (subpart G)

YES NO IS THE WASTE SUBJECT TO ONE OF THE FOLLOWING NESHAP RULES?

YES NO IS THIS MATERIAL GOING TO BE MANAGED AS A RCRA EXEMPT COMMERCIAL PRODUCT, WHICH IS FUEL (40 CFR 261.2 (C)(2)(II))?

Texas Waste Code

YES NO DO ANY STATE WASTE CODES APPLY?

YES NO USEPA HAZARDOUS WASTE?

NO IS THIS WASTE PROHIBITED FROM LAND DISPOSAL WITHOUT FURTHER TREATMENT PER 40 CFR PART 268?

LDR CATEGORY:

VARIANCE INFO:

YES NO IS THIS A UNIVERSAL WASTE?

YES NO DOES TREATMENT OF THIS WASTE GENERATE A F006 OR F019 SLUDGE?

YES NO

YES NO DOES THE WASTE CONTAIN GREATER THAN 20% OF ORGANIC CONSTITUENTS WITH A VAPOR PRESSURE >= .3KPA (.044 PSIA)?

YES NO DOES THIS WASTE CONTAIN AN ORGANIC CONSTITUENT WHICH IN ITS PURE FORM HAS A VAPOR PRESSURE > 77 KPA (11.2 PSIA)?

NO IS THIS CERCLA REGULATED (SUPERFUND ) WASTE ? YES

YES

DOES THIS WASTE CONTAIN VOC'S IN CONCENTRATIONS >=500 PPM?

Not subject to LDR

Megagram/year (1 Mg = 2,200 lbs)

Describe the knowledge :

Knowledge TestingThe basis for this determination is: Knowledge of the Waste Or Test Data

What is the TAB quantity for your facility?

YES NO Is the generating source of this waste stream a facility with Total Annual Benzene (TAB) >10 Mg/year?

YES NO Does the waste stream come from a facility with one of the SIC codes listed under benzene NESHAP or is this waste regulated under the benzene NESHAP rules because the original source of the waste is from a chemical manufacturing, coke by-product recovery, or petroleum refinery process?

H. TRANSPORTATION REQUIREMENTS

CONTAINER TYPE:

STORAGE CAPACITY:

CONTAINERS/SHIPMENT

CONTAINERIZED

0-0

DRUM

OTHER:

CUBIC YARD BOX

BOX|CARTON|CASEPORTABLE TOTE TANK

DRUM SIZE:

BULK LIQUID

GALLONS/SHIPMENT: GAL.100.00 Min -3500.00 Max

ESTIMATED SHIPMENT FREQUENCY OTHERYEARLYQUARTERLYMONTHLYWEEKLYONE TIME

TONS/YARDS/SHIPMENT:

SHIPMENT UOM: TON YARD

BULK SOLID

0 Min - 0 Max

I. SPECIAL REQUEST

COMMENTS OR REQUESTS:

Please approve for SKVS waste terminating at SGS not MSM

GENERATOR'S CERTIFICATION

I certify that I am authorized to execute this document as an authorized agent. I hereby certify that all information submitted in this and attached documents is correct to the best of my knowledge.I also certify that any samples submitted are representative of the actual waste.If Clean Harbors discovers a discrepancy during the approval process, Generator grants Clean Harbors the authority to amend the profile, as Clean Harbors deems necessary, to reflect the discrepancy.

AUTHORIZED SIGNATURE NAME (PRINT) TITLE DATE

Report Printed On : Wednesday, June 19, 2019 /WINWEB/Profile\Waste Profile.rdl Page 3 of 3

A. GENERAL INFORMATION

GENERATOR EPA ID #/REGISTRATION # MI3960020599

GENERATOR CODE (Assigned by Clean Harbors)

St Marys Canal - Soo Area Office 312 W Portage A

GENERATOR NAME:

CITY STATE/PROVINCE

US Army Corp of Engineers

ZIP/POSTAL CODE 49783

PHONE: (906) 632-3311

MIUN40415

ADDRESS

ZIP/POSTAL CODE

CUSTOMER CODE (Assigned by Clean Harbors)

ADDRESS

CUSTOMER NAME:

CITY STATE/PROVINCESault Sainte

Marie

MI 49783

US Army Corp of Engineers St Marys Canal - Soo Area Office 312 W Portage Avenue

UN40415

B. WASTE DESCRIPTION

WASTE DESCRIPTION: Red Tank water

PROCESS GENERATING WASTE:

IS THIS WASTE CONTAINED IN SMALL PACKAGING CONTAINED WITHIN A LARGER SHIPPING CONTAINER ?

water from Red underground storage tank

No

C. PHYSICAL PROPERTIES (at 25C or 77F)

PHYSICAL STATE

SOLID WITHOUT FREE LIQUID

POWDER

MONOLITHIC SOLID

LIQUID WITH NO SOLIDS

LIQUID/SOLID MIXTURE

% FREE LIQUID

% SETTLED SOLID

% TOTAL SUSPENDED SOLID

SLUDGE

GAS/AEROSOL

% BY VOLUME (Approx.)

NUMBER OF PHASES/LAYERS

TOP

MIDDLE

BOTTOM

321 0.00

0.00

0.00

ODOR

NONE

MILD

STRONG

Describe:

BOILING POINT ºF (ºC)

<= 95 (<=35)

95 - 100 (35-38)

101 - 129 (38-54)

>= 130 (>54)

COLOR

clear

VISCOSITY (If liquid present) 1 - 100 (e.g. Water)

101 - 500 (e.g. Motor Oil)

501 - 10,000 (e.g. Molasses)

> 10,000

TOTAL ORGANIC

CARBON

<= 1%

1-9%

>= 10%

< 140 (<60)

140-200 (60-93)

> 200 (>93)

MELTING POINT ºF (ºC)

FLASH POINT ºF (ºC)

< 73 (<23)

73 - 100 (23-38)

101 -140 (38-60)

141 -200 (60-93)

> 200 (>93)

SPECIFIC GRAVITY

< 0.8 (e.g. Gasoline)

0.8-1.0 (e.g. Ethanol)

1.0 (e.g. Water)

> 1.2 (e.g. Methylene Chloride)

1.0-1.2 (e.g. Antifreeze) pH

2.1 - 6.9

<= 2

7 (Neutral)

7.1 - 12.4

>= 12.5

BTU/LB (MJ/kg)

< 2,000 (<4.6)

2,000-5,000 (4.6-11.6)

5,000-10,000 (11.6-23.2)

> 10,000 (>23.2)

Actual:

ASH

< 0.1

0.1 - 1.0

1.1 - 5.0

5.1 - 20.0

> 20

Unknown

D. COMPOSITION

DOES THIS WASTE CONTAIN ANY HEAVY GAUGE METAL DEBRIS OR OTHER LARGE OBJECTS (EX., METAL PLATE OR PIPING >1/4” THICK OR >12” LONG, METAL REINFORCED HOSE >12” LONG, METAL WIRE >12” LONG, METAL VALVES, PIPE FITTINGS, CONCRETE REINFORCING BAR OR

PIECES OF CONCRETE >3”)?

YES NO

If yes, describe, including dimensions:

(List the complete composition of the waste, include any inert components and/or debris. Ranges for individual components are acceptable. If a trade name is used, please supply an MSDS. Please do not use abbreviations.)

CHEMICAL MIN -- MAX UOM

WATER & NON HAZ PROPRIETARY INGREDIENTS 100.0000000 -- 100.0000000 %

DOES THIS WASTE CONTAIN ANY METALS IN POWDERED OR OTHER FINELY DIVIDED FORM? YES NO

DOES THIS WASTE CONTAIN OR HAS IT CONTACTED ANY OF THE FOLLOWING; ANIMAL WASTES, HUMAN BLOOD, BLOOD PRODUCTS, BODY FLUIDS, MICROBIOLOGICAL WASTE, PATHOLOGICAL WASTE, HUMAN OR ANIMAL DERIVED SERUMS OR PROTEINS OR ANY OTHER

POTENTIALLY INFECTIOUS MATERIAL?

YES NO

I acknowledge that this waste material is neither infectious nor does it contain any organism known to be a threat to human health. This certification is based on my knowledge of the material. Select the answer below that applies:

The waste was never exposed to potentially infectious material. YES NO

Chemical disinfection or some other form of sterilization has been applied to the waste. YES NO

I ACKNOWLEDGE THAT THIS PROFILE MEETS THE CLEAN HARBORS BATTERY PACKAGING REQUIREMENTS. YES NO

I ACKNOWLEDGE THAT MY FRIABLE ASBESTOS WASTE IS DOUBLE BAGGED AND WETTED. YES NO

SPECIFY THE SOURCE CODE ASSOCIATED WITH THE

WASTE.

SPECIFY THE FORM CODE ASSOCIATED WITH THE WASTE.G45 W113

Report Printed On : Wednesday, June 19, 2019 /WINWEB/Profile\Waste Profile.rdl Page 1 of 3

Profile No. 1863291

If constituent concentrations are based on analytical testing, analysis must be provided. Please attach document(s) using the link on the Submit tab.

E. CONSTITUENTS

OTHER CONSTITUENTS MAX UOM NOT

APPLICABLE

BROMINE

CHLORINE

FLUORINE

IODINE

SULFUR

POTASSIUM

SODIUM

AMMONIA

CYANIDE AMENABLE

CYANIDE REACTIVE

CYANIDE TOTAL

SULFIDE REACTIVE

VOLATILE COMPOUNDS

D018 BENZENE 0.5

D019 CARBON TETRACHLORIDE 0.5

D021 CHLOROBENZENE 100.0

D022 CHLOROFORM 6.0

D028 1,2-DICHLOROETHANE 0.5

D029 1,1-DICHLOROETHYLENE 0.7

D035 METHYL ETHYL KETONE 200.0

D039 TETRACHLOROETHYLENE 0.7

D040 TRICHLOROETHYLENE 0.5

D043 VINYL CHLORIDE 0.2

SEMI-VOLATILE COMPOUNDS

D023 o-CRESOL 200.0

D024 m-CRESOL 200.0

D025 p-CRESOL 200.0

D026 CRESOL (TOTAL) 200.0

D027 1,4-DICHLOROBENZENE 7.5

D030 2,4-DINITROTOLUENE 0.13

D032 HEXACHLOROBENZENE 0.13

D033 HEXACHLOROBUTADIENE 0.5

D034 HEXACHLOROETHANE 3.0

D036 NITROBENZENE 2.0

D037 PENTACHLOROPHENOL 100.0

D038 PYRIDINE 5.0

D041 2,4,5-TRICHLOROPHENOL 400.0

D042 2,4,6-TRICHLOROPHENOL 2.0

PESTICIDES AND HERBICIDES

D012 ENDRIN 0.02

D013 LINDANE 0.4

D014 METHOXYCHLOR 10.0

D015 TOXAPHENE 0.5

D016 2,4-D 10.0

D017 2,4,5-TP (SILVEX) 1.0

D020 CHLORDANE 0.03

D031 HEPTACHLOR (AND ITS EPOXIDE) 0.008

HOCs

NONE

< 1000 PPM

>= 1000 PPM

PCBs

NONE

< 50 PPM

>=50 PPM

IF PCBS ARE PRESENT, IS THE

WASTE REGULATED BY TSCA 40

CFR 761?

YES NO

Please indicate which constituents below apply. Concentrations must be entered when applicable to assist in accurate review and expedited approval of your waste profile. Please note that the total regulated metals and other constituents sections require answers.

ADDITIONAL HAZARDS

DOES THIS WASTE HAVE ANY UNDISCLOSED HAZARDS OR PRIOR INCIDENTS ASSOCIATED WITH IT, WHICH COULD AFFECT THE WAY IT SHOULD BE HANDLED?

YES NO (If yes, explain)

DEA REGULATED SUBSTANCES EXPLOSIVE FUMING

NONE OF THE ABOVEPOLYMERIZABLE RADIOACTIVE REACTIVE MATERIAL

RCRA REGULATED METALS REGULATORY

LEVEL (mg/l)

TCLP

mg/l

TOTAL UOM NOT APPLICABLE

D004 ARSENIC 5.0

D005 BARIUM 100.0

D006 CADMIUM 1.0

D007 CHROMIUM 5.0

D008 LEAD 5.0

D009 MERCURY 0.2

D010 SELENIUM 1.0

D011 SILVER 5.0

CHOOSE ALL THAT APPLY

OSHA REGULATED CARCINOGENS

NON DOT REGULATED MATERIAL

F. REGULATORY STATUS

YES NO IF THIS IS A US EPA HAZARDOUS WASTE, DOES THIS WASTE STREAM CONTAIN BENZENE?

YES NO DO ANY CANADIAN PROVINCIAL WASTE CODES APPLY?

YES NO IS THE GENERATOR OF THE WASTE CLASSIFIED AS VERY SMALL QUANTITY GENERATOR (VSQG) OR A STATE EQUIVALENT DESIGNATION?

YES NO IS THIS WASTE STREAM SUBJECT TO THE INORGANIC METAL BEARING WASTE PROHIBITION FOUND AT 40 CFR 268.3(C)?

Pharmaceuticals production (subpart GGG)Hazardous Organic NESHAP (HON) rule (subpart G)

YES NO IS THE WASTE SUBJECT TO ONE OF THE FOLLOWING NESHAP RULES?

YES NO IS THIS MATERIAL GOING TO BE MANAGED AS A RCRA EXEMPT COMMERCIAL PRODUCT, WHICH IS FUEL (40 CFR 261.2 (C)(2)(II))?

Texas Waste Code

YES NO DO ANY STATE WASTE CODES APPLY?

YES NO USEPA HAZARDOUS WASTE?

NO IS THIS WASTE PROHIBITED FROM LAND DISPOSAL WITHOUT FURTHER TREATMENT PER 40 CFR PART 268?

LDR CATEGORY:

VARIANCE INFO:

YES NO IS THIS A UNIVERSAL WASTE?

YES NO DOES TREATMENT OF THIS WASTE GENERATE A F006 OR F019 SLUDGE?

YES NO

YES NO DOES THE WASTE CONTAIN GREATER THAN 20% OF ORGANIC CONSTITUENTS WITH A VAPOR PRESSURE >= .3KPA (.044 PSIA)?

YES NO DOES THIS WASTE CONTAIN AN ORGANIC CONSTITUENT WHICH IN ITS PURE FORM HAS A VAPOR PRESSURE > 77 KPA (11.2 PSIA)?

NO IS THIS CERCLA REGULATED (SUPERFUND ) WASTE ? YES

YES

DOES THIS WASTE CONTAIN VOC'S IN CONCENTRATIONS >=500 PPM?

Not subject to LDR

Megagram/year (1 Mg = 2,200 lbs)

Describe the knowledge :

Knowledge TestingThe basis for this determination is: Knowledge of the Waste Or Test Data

What is the TAB quantity for your facility?

YES NO Is the generating source of this waste stream a facility with Total Annual Benzene (TAB) >10 Mg/year?

YES NO Does the waste stream come from a facility with one of the SIC codes listed under benzene NESHAP or is this waste regulated under the benzene NESHAP rules because the original source of the waste is from a chemical manufacturing, coke by-product recovery, or petroleum refinery process?

H. TRANSPORTATION REQUIREMENTS

CONTAINER TYPE:

STORAGE CAPACITY:

CONTAINERS/SHIPMENT

CONTAINERIZED

0-0

DRUM

OTHER:

CUBIC YARD BOX

BOX|CARTON|CASEPORTABLE TOTE TANK

DRUM SIZE:

BULK LIQUID

GALLONS/SHIPMENT: GAL.100.00 Min -3500.00 Max

ESTIMATED SHIPMENT FREQUENCY OTHERYEARLYQUARTERLYMONTHLYWEEKLYONE TIME

TONS/YARDS/SHIPMENT:

SHIPMENT UOM: TON YARD

BULK SOLID

0 Min - 0 Max

I. SPECIAL REQUEST

COMMENTS OR REQUESTS:

Please approve for SKVS waste terminating at SGS not MSM

GENERATOR'S CERTIFICATION

I certify that I am authorized to execute this document as an authorized agent. I hereby certify that all information submitted in this and attached documents is correct to the best of my knowledge.I also certify that any samples submitted are representative of the actual waste.If Clean Harbors discovers a discrepancy during the approval process, Generator grants Clean Harbors the authority to amend the profile, as Clean Harbors deems necessary, to reflect the discrepancy.

AUTHORIZED SIGNATURE NAME (PRINT) TITLE DATE

A. GENERAL INFORMATION

GENERATOR EPA ID #/REGISTRATION # MI3960020599

GENERATOR CODE (Assigned by Clean Harbors)

St Marys Canal - Soo Area Office 312 W Portage A

GENERATOR NAME:

CITY STATE/PROVINCE

US Army Corp of Engineers

ZIP/POSTAL CODE 49783

PHONE: (906) 632-3311

MIUN40415

ADDRESS

ZIP/POSTAL CODE

CUSTOMER CODE (Assigned by Clean Harbors)

ADDRESS

CUSTOMER NAME:

CITY STATE/PROVINCESault Sainte

Marie

MI 49783

US Army Corp of Engineers St Marys Canal - Soo Area Office 312 W Portage Avenue

UN40415

B. WASTE DESCRIPTION

WASTE DESCRIPTION: West Tank oil and water mixed

PROCESS GENERATING WASTE:

IS THIS WASTE CONTAINED IN SMALL PACKAGING CONTAINED WITHIN A LARGER SHIPPING CONTAINER ?

West tank oil storage cap was left off and water gathered over the years

No

C. PHYSICAL PROPERTIES (at 25C or 77F)

PHYSICAL STATE

SOLID WITHOUT FREE LIQUID

POWDER

MONOLITHIC SOLID

LIQUID WITH NO SOLIDS

LIQUID/SOLID MIXTURE

% FREE LIQUID

% SETTLED SOLID

% TOTAL SUSPENDED SOLID

SLUDGE

GAS/AEROSOL

% BY VOLUME (Approx.)

NUMBER OF PHASES/LAYERS

TOP

MIDDLE

BOTTOM

321 20.00

0.00

80.00

ODOR

NONE

MILD

STRONG

Describe:

BOILING POINT ºF (ºC)

<= 95 (<=35)

95 - 100 (35-38)

101 - 129 (38-54)

>= 130 (>54)

COLOR

veries

VISCOSITY (If liquid present) 1 - 100 (e.g. Water)

101 - 500 (e.g. Motor Oil)

501 - 10,000 (e.g. Molasses)

> 10,000

TOTAL ORGANIC

CARBON

<= 1%

1-9%

>= 10%

< 140 (<60)

140-200 (60-93)

> 200 (>93)

MELTING POINT ºF (ºC)

FLASH POINT ºF (ºC)

< 73 (<23)

73 - 100 (23-38)

101 -140 (38-60)

141 -200 (60-93)

> 200 (>93)

SPECIFIC GRAVITY

< 0.8 (e.g. Gasoline)

0.8-1.0 (e.g. Ethanol)

1.0 (e.g. Water)

> 1.2 (e.g. Methylene Chloride)

1.0-1.2 (e.g. Antifreeze) pH

2.1 - 6.9

<= 2

7 (Neutral)

7.1 - 12.4

>= 12.5

BTU/LB (MJ/kg)

< 2,000 (<4.6)

2,000-5,000 (4.6-11.6)

5,000-10,000 (11.6-23.2)

> 10,000 (>23.2)

Actual:

ASH

< 0.1

0.1 - 1.0

1.1 - 5.0

5.1 - 20.0

> 20

Unknown

D. COMPOSITION

DOES THIS WASTE CONTAIN ANY HEAVY GAUGE METAL DEBRIS OR OTHER LARGE OBJECTS (EX., METAL PLATE OR PIPING >1/4” THICK OR >12” LONG, METAL REINFORCED HOSE >12” LONG, METAL WIRE >12” LONG, METAL VALVES, PIPE FITTINGS, CONCRETE REINFORCING BAR OR

PIECES OF CONCRETE >3”)?

YES NO

If yes, describe, including dimensions:

(List the complete composition of the waste, include any inert components and/or debris. Ranges for individual components are acceptable. If a trade name is used, please supply an MSDS. Please do not use abbreviations.)

CHEMICAL MIN -- MAX UOM

MOTOR OIL 1.0000000 -- 20.0000000 %

WATER 20.0000000 -- 80.0000000 %

DOES THIS WASTE CONTAIN ANY METALS IN POWDERED OR OTHER FINELY DIVIDED FORM? YES NO

DOES THIS WASTE CONTAIN OR HAS IT CONTACTED ANY OF THE FOLLOWING; ANIMAL WASTES, HUMAN BLOOD, BLOOD PRODUCTS, BODY FLUIDS, MICROBIOLOGICAL WASTE, PATHOLOGICAL WASTE, HUMAN OR ANIMAL DERIVED SERUMS OR PROTEINS OR ANY OTHER

POTENTIALLY INFECTIOUS MATERIAL?

YES NO

I acknowledge that this waste material is neither infectious nor does it contain any organism known to be a threat to human health. This certification is based on my knowledge of the material. Select the answer below that applies:

The waste was never exposed to potentially infectious material. YES NO

Chemical disinfection or some other form of sterilization has been applied to the waste. YES NO

I ACKNOWLEDGE THAT THIS PROFILE MEETS THE CLEAN HARBORS BATTERY PACKAGING REQUIREMENTS. YES NO

I ACKNOWLEDGE THAT MY FRIABLE ASBESTOS WASTE IS DOUBLE BAGGED AND WETTED. YES NO

SPECIFY THE SOURCE CODE ASSOCIATED WITH THE

WASTE.

SPECIFY THE FORM CODE ASSOCIATED WITH THE WASTE.G11 W119

Report Printed On : Wednesday, June 19, 2019 /WINWEB/Profile\Waste Profile.rdl Page 1 of 3

Profile No. 1863311

If constituent concentrations are based on analytical testing, analysis must be provided. Please attach document(s) using the link on the Submit tab.

E. CONSTITUENTS

OTHER CONSTITUENTS MAX UOM NOT

APPLICABLE

BROMINE

CHLORINE

FLUORINE

IODINE

SULFUR

POTASSIUM

SODIUM

AMMONIA

CYANIDE AMENABLE

CYANIDE REACTIVE

CYANIDE TOTAL

SULFIDE REACTIVE

VOLATILE COMPOUNDS

D018 BENZENE 0.5

D019 CARBON TETRACHLORIDE 0.5

D021 CHLOROBENZENE 100.0

D022 CHLOROFORM 6.0

D028 1,2-DICHLOROETHANE 0.5

D029 1,1-DICHLOROETHYLENE 0.7

D035 METHYL ETHYL KETONE 200.0

D039 TETRACHLOROETHYLENE 0.7

D040 TRICHLOROETHYLENE 0.5

D043 VINYL CHLORIDE 0.2

SEMI-VOLATILE COMPOUNDS

D023 o-CRESOL 200.0

D024 m-CRESOL 200.0

D025 p-CRESOL 200.0

D026 CRESOL (TOTAL) 200.0

D027 1,4-DICHLOROBENZENE 7.5

D030 2,4-DINITROTOLUENE 0.13

D032 HEXACHLOROBENZENE 0.13

D033 HEXACHLOROBUTADIENE 0.5

D034 HEXACHLOROETHANE 3.0

D036 NITROBENZENE 2.0

D037 PENTACHLOROPHENOL 100.0

D038 PYRIDINE 5.0

D041 2,4,5-TRICHLOROPHENOL 400.0

D042 2,4,6-TRICHLOROPHENOL 2.0

PESTICIDES AND HERBICIDES

D012 ENDRIN 0.02

D013 LINDANE 0.4

D014 METHOXYCHLOR 10.0

D015 TOXAPHENE 0.5

D016 2,4-D 10.0

D017 2,4,5-TP (SILVEX) 1.0

D020 CHLORDANE 0.03

D031 HEPTACHLOR (AND ITS EPOXIDE) 0.008

HOCs

NONE

< 1000 PPM

>= 1000 PPM

PCBs

NONE

< 50 PPM

>=50 PPM

IF PCBS ARE PRESENT, IS THE

WASTE REGULATED BY TSCA 40

CFR 761?

YES NO

Please indicate which constituents below apply. Concentrations must be entered when applicable to assist in accurate review and expedited approval of your waste profile. Please note that the total regulated metals and other constituents sections require answers.

ADDITIONAL HAZARDS

DOES THIS WASTE HAVE ANY UNDISCLOSED HAZARDS OR PRIOR INCIDENTS ASSOCIATED WITH IT, WHICH COULD AFFECT THE WAY IT SHOULD BE HANDLED?

YES NO (If yes, explain)

DEA REGULATED SUBSTANCES EXPLOSIVE FUMING

NONE OF THE ABOVEPOLYMERIZABLE RADIOACTIVE REACTIVE MATERIAL

RCRA REGULATED METALS REGULATORY

LEVEL (mg/l)

TCLP

mg/l

TOTAL UOM NOT APPLICABLE

D004 ARSENIC 5.0

D005 BARIUM 100.0

D006 CADMIUM 1.0

D007 CHROMIUM 5.0

D008 LEAD 5.0

D009 MERCURY 0.2

D010 SELENIUM 1.0

D011 SILVER 5.0

CHOOSE ALL THAT APPLY

OSHA REGULATED CARCINOGENS

NON DOT REGULATED MATERIAL

F. REGULATORY STATUS

YES NO IF THIS IS A US EPA HAZARDOUS WASTE, DOES THIS WASTE STREAM CONTAIN BENZENE?

YES NO DO ANY CANADIAN PROVINCIAL WASTE CODES APPLY?

YES NO IS THE GENERATOR OF THE WASTE CLASSIFIED AS VERY SMALL QUANTITY GENERATOR (VSQG) OR A STATE EQUIVALENT DESIGNATION?

YES NO IS THIS WASTE STREAM SUBJECT TO THE INORGANIC METAL BEARING WASTE PROHIBITION FOUND AT 40 CFR 268.3(C)?

Pharmaceuticals production (subpart GGG)Hazardous Organic NESHAP (HON) rule (subpart G)

YES NO IS THE WASTE SUBJECT TO ONE OF THE FOLLOWING NESHAP RULES?

YES NO IS THIS MATERIAL GOING TO BE MANAGED AS A RCRA EXEMPT COMMERCIAL PRODUCT, WHICH IS FUEL (40 CFR 261.2 (C)(2)(II))?

Texas Waste Code

YES NO DO ANY STATE WASTE CODES APPLY?

YES NO USEPA HAZARDOUS WASTE?

NO IS THIS WASTE PROHIBITED FROM LAND DISPOSAL WITHOUT FURTHER TREATMENT PER 40 CFR PART 268?

LDR CATEGORY:

VARIANCE INFO:

YES NO IS THIS A UNIVERSAL WASTE?

YES NO DOES TREATMENT OF THIS WASTE GENERATE A F006 OR F019 SLUDGE?

YES NO

YES NO DOES THE WASTE CONTAIN GREATER THAN 20% OF ORGANIC CONSTITUENTS WITH A VAPOR PRESSURE >= .3KPA (.044 PSIA)?

YES NO DOES THIS WASTE CONTAIN AN ORGANIC CONSTITUENT WHICH IN ITS PURE FORM HAS A VAPOR PRESSURE > 77 KPA (11.2 PSIA)?

NO IS THIS CERCLA REGULATED (SUPERFUND ) WASTE ? YES

YES

DOES THIS WASTE CONTAIN VOC'S IN CONCENTRATIONS >=500 PPM?

Not subject to LDR

Megagram/year (1 Mg = 2,200 lbs)

Describe the knowledge :

Knowledge TestingThe basis for this determination is: Knowledge of the Waste Or Test Data

What is the TAB quantity for your facility?

YES NO Is the generating source of this waste stream a facility with Total Annual Benzene (TAB) >10 Mg/year?

YES NO Does the waste stream come from a facility with one of the SIC codes listed under benzene NESHAP or is this waste regulated under the benzene NESHAP rules because the original source of the waste is from a chemical manufacturing, coke by-product recovery, or petroleum refinery process?

H. TRANSPORTATION REQUIREMENTS

CONTAINER TYPE:

STORAGE CAPACITY:

CONTAINERS/SHIPMENT

CONTAINERIZED

0-0

DRUM

OTHER:

CUBIC YARD BOX

BOX|CARTON|CASEPORTABLE TOTE TANK

DRUM SIZE:

BULK LIQUID

GALLONS/SHIPMENT: GAL.100.00 Min -3000.00 Max

ESTIMATED SHIPMENT FREQUENCY OTHERYEARLYQUARTERLYMONTHLYWEEKLYONE TIME

TONS/YARDS/SHIPMENT:

SHIPMENT UOM: TON YARD

BULK SOLID

0 Min - 0 Max

I. SPECIAL REQUEST

COMMENTS OR REQUESTS:

Please approve for SKOS_SKVS waste terminating at SGS not MSM

GENERATOR'S CERTIFICATION

I certify that I am authorized to execute this document as an authorized agent. I hereby certify that all information submitted in this and attached documents is correct to the best of my knowledge.I also certify that any samples submitted are representative of the actual waste.If Clean Harbors discovers a discrepancy during the approval process, Generator grants Clean Harbors the authority to amend the profile, as Clean Harbors deems necessary, to reflect the discrepancy.

AUTHORIZED SIGNATURE NAME (PRINT) TITLE DATE

A. GENERAL INFORMATION

GENERATOR EPA ID #/REGISTRATION # MI3960020599

GENERATOR CODE (Assigned by Clean Harbors)

St Marys Canal - Soo Area Office 312 W Portage A

GENERATOR NAME:

CITY STATE/PROVINCE

US Army Corp of Engineers

ZIP/POSTAL CODE 49783

PHONE: (906) 632-3311

MIUN40415

ADDRESS

ZIP/POSTAL CODE

CUSTOMER CODE (Assigned by Clean Harbors)

ADDRESS

CUSTOMER NAME:

CITY STATE/PROVINCESault Sainte

Marie

MI 49783

US Army Corp of Engineers St Marys Canal - Soo Area Office 312 W Portage Avenue

UN40415

B. WASTE DESCRIPTION

WASTE DESCRIPTION: West Tank oil and water mixed

PROCESS GENERATING WASTE:

IS THIS WASTE CONTAINED IN SMALL PACKAGING CONTAINED WITHIN A LARGER SHIPPING CONTAINER ?

West tank oil storage cap was left off and water gathered over the years

No

C. PHYSICAL PROPERTIES (at 25C or 77F)

PHYSICAL STATE

SOLID WITHOUT FREE LIQUID

POWDER

MONOLITHIC SOLID

LIQUID WITH NO SOLIDS

LIQUID/SOLID MIXTURE

% FREE LIQUID

% SETTLED SOLID

% TOTAL SUSPENDED SOLID

SLUDGE

GAS/AEROSOL

% BY VOLUME (Approx.)

NUMBER OF PHASES/LAYERS

TOP

MIDDLE

BOTTOM

321 20.00

0.00

80.00

ODOR

NONE

MILD

STRONG

Describe:

BOILING POINT ºF (ºC)

<= 95 (<=35)

95 - 100 (35-38)

101 - 129 (38-54)

>= 130 (>54)

COLOR

veries

VISCOSITY (If liquid present) 1 - 100 (e.g. Water)

101 - 500 (e.g. Motor Oil)

501 - 10,000 (e.g. Molasses)

> 10,000

TOTAL ORGANIC

CARBON

<= 1%

1-9%

>= 10%

< 140 (<60)

140-200 (60-93)

> 200 (>93)

MELTING POINT ºF (ºC)

FLASH POINT ºF (ºC)

< 73 (<23)

73 - 100 (23-38)

101 -140 (38-60)

141 -200 (60-93)

> 200 (>93)

SPECIFIC GRAVITY

< 0.8 (e.g. Gasoline)

0.8-1.0 (e.g. Ethanol)

1.0 (e.g. Water)

> 1.2 (e.g. Methylene Chloride)

1.0-1.2 (e.g. Antifreeze) pH

2.1 - 6.9

<= 2

7 (Neutral)

7.1 - 12.4

>= 12.5

BTU/LB (MJ/kg)

< 2,000 (<4.6)

2,000-5,000 (4.6-11.6)

5,000-10,000 (11.6-23.2)

> 10,000 (>23.2)

Actual:

ASH

< 0.1

0.1 - 1.0

1.1 - 5.0

5.1 - 20.0

> 20

Unknown

D. COMPOSITION

DOES THIS WASTE CONTAIN ANY HEAVY GAUGE METAL DEBRIS OR OTHER LARGE OBJECTS (EX., METAL PLATE OR PIPING >1/4” THICK OR >12” LONG, METAL REINFORCED HOSE >12” LONG, METAL WIRE >12” LONG, METAL VALVES, PIPE FITTINGS, CONCRETE REINFORCING BAR OR

PIECES OF CONCRETE >3”)?

YES NO

If yes, describe, including dimensions:

(List the complete composition of the waste, include any inert components and/or debris. Ranges for individual components are acceptable. If a trade name is used, please supply an MSDS. Please do not use abbreviations.)

CHEMICAL MIN -- MAX UOM

MOTOR OIL 1.0000000 -- 20.0000000 %

WATER 20.0000000 -- 80.0000000 %

DOES THIS WASTE CONTAIN ANY METALS IN POWDERED OR OTHER FINELY DIVIDED FORM? YES NO

DOES THIS WASTE CONTAIN OR HAS IT CONTACTED ANY OF THE FOLLOWING; ANIMAL WASTES, HUMAN BLOOD, BLOOD PRODUCTS, BODY FLUIDS, MICROBIOLOGICAL WASTE, PATHOLOGICAL WASTE, HUMAN OR ANIMAL DERIVED SERUMS OR PROTEINS OR ANY OTHER

POTENTIALLY INFECTIOUS MATERIAL?

YES NO

I acknowledge that this waste material is neither infectious nor does it contain any organism known to be a threat to human health. This certification is based on my knowledge of the material. Select the answer below that applies:

The waste was never exposed to potentially infectious material. YES NO

Chemical disinfection or some other form of sterilization has been applied to the waste. YES NO

I ACKNOWLEDGE THAT THIS PROFILE MEETS THE CLEAN HARBORS BATTERY PACKAGING REQUIREMENTS. YES NO

I ACKNOWLEDGE THAT MY FRIABLE ASBESTOS WASTE IS DOUBLE BAGGED AND WETTED. YES NO

SPECIFY THE SOURCE CODE ASSOCIATED WITH THE

WASTE.

SPECIFY THE FORM CODE ASSOCIATED WITH THE WASTE.G11 W119

Report Printed On : Wednesday, June 19, 2019 /WINWEB/Profile\Waste Profile.rdl Page 1 of 3

Profile No. 1863325

If constituent concentrations are based on analytical testing, analysis must be provided. Please attach document(s) using the link on the Submit tab.

E. CONSTITUENTS

OTHER CONSTITUENTS MAX UOM NOT

APPLICABLE

BROMINE

CHLORINE

FLUORINE

IODINE

SULFUR

POTASSIUM

SODIUM

AMMONIA

CYANIDE AMENABLE

CYANIDE REACTIVE

CYANIDE TOTAL

SULFIDE REACTIVE

VOLATILE COMPOUNDS

D018 BENZENE 0.5

D019 CARBON TETRACHLORIDE 0.5

D021 CHLOROBENZENE 100.0

D022 CHLOROFORM 6.0

D028 1,2-DICHLOROETHANE 0.5

D029 1,1-DICHLOROETHYLENE 0.7

D035 METHYL ETHYL KETONE 200.0

D039 TETRACHLOROETHYLENE 0.7

D040 TRICHLOROETHYLENE 0.5

D043 VINYL CHLORIDE 0.2

SEMI-VOLATILE COMPOUNDS

D023 o-CRESOL 200.0

D024 m-CRESOL 200.0

D025 p-CRESOL 200.0

D026 CRESOL (TOTAL) 200.0

D027 1,4-DICHLOROBENZENE 7.5

D030 2,4-DINITROTOLUENE 0.13

D032 HEXACHLOROBENZENE 0.13

D033 HEXACHLOROBUTADIENE 0.5

D034 HEXACHLOROETHANE 3.0

D036 NITROBENZENE 2.0

D037 PENTACHLOROPHENOL 100.0

D038 PYRIDINE 5.0

D041 2,4,5-TRICHLOROPHENOL 400.0

D042 2,4,6-TRICHLOROPHENOL 2.0

PESTICIDES AND HERBICIDES

D012 ENDRIN 0.02

D013 LINDANE 0.4

D014 METHOXYCHLOR 10.0

D015 TOXAPHENE 0.5

D016 2,4-D 10.0

D017 2,4,5-TP (SILVEX) 1.0

D020 CHLORDANE 0.03

D031 HEPTACHLOR (AND ITS EPOXIDE) 0.008

HOCs

NONE

< 1000 PPM

>= 1000 PPM

PCBs

NONE

< 50 PPM

>=50 PPM

IF PCBS ARE PRESENT, IS THE

WASTE REGULATED BY TSCA 40

CFR 761?

YES NO

Please indicate which constituents below apply. Concentrations must be entered when applicable to assist in accurate review and expedited approval of your waste profile. Please note that the total regulated metals and other constituents sections require answers.

ADDITIONAL HAZARDS

DOES THIS WASTE HAVE ANY UNDISCLOSED HAZARDS OR PRIOR INCIDENTS ASSOCIATED WITH IT, WHICH COULD AFFECT THE WAY IT SHOULD BE HANDLED?

YES NO (If yes, explain)

DEA REGULATED SUBSTANCES EXPLOSIVE FUMING

NONE OF THE ABOVEPOLYMERIZABLE RADIOACTIVE REACTIVE MATERIAL

RCRA REGULATED METALS REGULATORY

LEVEL (mg/l)

TCLP

mg/l

TOTAL UOM NOT APPLICABLE

D004 ARSENIC 5.0

D005 BARIUM 100.0

D006 CADMIUM 1.0

D007 CHROMIUM 5.0

D008 LEAD 5.0

D009 MERCURY 0.2

D010 SELENIUM 1.0

D011 SILVER 5.0

CHOOSE ALL THAT APPLY

OSHA REGULATED CARCINOGENS

NON DOT REGULATED MATERIAL

F. REGULATORY STATUS

YES NO IF THIS IS A US EPA HAZARDOUS WASTE, DOES THIS WASTE STREAM CONTAIN BENZENE?

YES NO DO ANY CANADIAN PROVINCIAL WASTE CODES APPLY?

YES NO IS THE GENERATOR OF THE WASTE CLASSIFIED AS VERY SMALL QUANTITY GENERATOR (VSQG) OR A STATE EQUIVALENT DESIGNATION?

YES NO IS THIS WASTE STREAM SUBJECT TO THE INORGANIC METAL BEARING WASTE PROHIBITION FOUND AT 40 CFR 268.3(C)?

Pharmaceuticals production (subpart GGG)Hazardous Organic NESHAP (HON) rule (subpart G)

YES NO IS THE WASTE SUBJECT TO ONE OF THE FOLLOWING NESHAP RULES?

YES NO IS THIS MATERIAL GOING TO BE MANAGED AS A RCRA EXEMPT COMMERCIAL PRODUCT, WHICH IS FUEL (40 CFR 261.2 (C)(2)(II))?

Texas Waste Code

YES NO DO ANY STATE WASTE CODES APPLY?

YES NO USEPA HAZARDOUS WASTE?

NO IS THIS WASTE PROHIBITED FROM LAND DISPOSAL WITHOUT FURTHER TREATMENT PER 40 CFR PART 268?

LDR CATEGORY:

VARIANCE INFO:

YES NO IS THIS A UNIVERSAL WASTE?

YES NO DOES TREATMENT OF THIS WASTE GENERATE A F006 OR F019 SLUDGE?

YES NO

YES NO DOES THE WASTE CONTAIN GREATER THAN 20% OF ORGANIC CONSTITUENTS WITH A VAPOR PRESSURE >= .3KPA (.044 PSIA)?

YES NO DOES THIS WASTE CONTAIN AN ORGANIC CONSTITUENT WHICH IN ITS PURE FORM HAS A VAPOR PRESSURE > 77 KPA (11.2 PSIA)?

NO IS THIS CERCLA REGULATED (SUPERFUND ) WASTE ? YES

YES

DOES THIS WASTE CONTAIN VOC'S IN CONCENTRATIONS >=500 PPM?

Not subject to LDR

Megagram/year (1 Mg = 2,200 lbs)

Describe the knowledge :

Knowledge TestingThe basis for this determination is: Knowledge of the Waste Or Test Data

What is the TAB quantity for your facility?

YES NO Is the generating source of this waste stream a facility with Total Annual Benzene (TAB) >10 Mg/year?

YES NO Does the waste stream come from a facility with one of the SIC codes listed under benzene NESHAP or is this waste regulated under the benzene NESHAP rules because the original source of the waste is from a chemical manufacturing, coke by-product recovery, or petroleum refinery process?

H. TRANSPORTATION REQUIREMENTS

CONTAINER TYPE:

STORAGE CAPACITY:

CONTAINERS/SHIPMENT

CONTAINERIZED

0-0

DRUM

OTHER:

CUBIC YARD BOX

BOX|CARTON|CASEPORTABLE TOTE TANK

DRUM SIZE:

BULK LIQUID

GALLONS/SHIPMENT: GAL.100.00 Min -3000.00 Max

ESTIMATED SHIPMENT FREQUENCY OTHERYEARLYQUARTERLYMONTHLYWEEKLYONE TIME

TONS/YARDS/SHIPMENT:

SHIPMENT UOM: TON YARD

BULK SOLID

0 Min - 0 Max

I. SPECIAL REQUEST

COMMENTS OR REQUESTS:

Please approve for SKOS_SKVS waste terminating at SGS not MSM

GENERATOR'S CERTIFICATION

I certify that I am authorized to execute this document as an authorized agent. I hereby certify that all information submitted in this and attached documents is correct to the best of my knowledge.I also certify that any samples submitted are representative of the actual waste.If Clean Harbors discovers a discrepancy during the approval process, Generator grants Clean Harbors the authority to amend the profile, as Clean Harbors deems necessary, to reflect the discrepancy.

AUTHORIZED SIGNATURE NAME (PRINT) TITLE DATE

PSC-FOH ENVIRONMENTAL LABORATORY

536 S. CLARK STREET CHICAGO, IL 60605 PHONE: (312) 886-0413 FAX: (312) 886-0434

Project 19736

ANALYTICAL REPORT

Submitted To: U.S. Army Corps of Engineers 312 Portage Avenue Sault Ste Marie, MI 49783

Attention: Mr. Michael Krzycki

Submitted By: Ms. Michelle C. Stemmons

Reference Data: Lead Sampling Site: ACOE: Sault Ste Marie, MI Sample Type: Paint chip(s) Method Reference: OSHA ID-121 Project ID: Project 19736 DFOH Lab Nos.: TM-19-194386 through TM-19-194389 Date Received: 07/02/19 Data Analyzed: 07/08/19 – 07/09/19 Date Issued: 07/15/19

The paint chip samples were digested using the CEM MARS-Xpress. The samples were run on a Perkin Elmer 200/400 flame atomic absorption spectrophotometer (AA).

General Lab Comments:

All quality control criteria have been met.

* All samples received in condition acceptable for analysis unless otherwise noted.

** Sample results have not been corrected for contamination based on the field blank or other analytical blank unless otherwise noted.

The FOH Environmental Laboratory is an EPA Recognized Testing Lab.

Analytical results are given in the enclosed table. Results relate only to items tested. If you have any questions about these results, feel free to phone the Laboratory at (312) 886-0413.

Ms. Edna A. Bautista Ms. Michelle C. Stemmons Technical Manager Laboratory Director

Project 19736

LEAD in PAINT RESULTS

SAMPLE

NUMBER*

LABORATORY

NUMBER

CONCENTRATION

(%weight)

CONCENTRATION

(mg/g)

NWPB-1 TM-19-194386 7.9** 79

NWPB-2 TM-19-194387 0.02 0.17

NWPB-3 TM-19-194388 <0.006 <0.06

NWPB-4 TM-19-194389 <0.006 <0.06

**NOTE: The Department of Housing and Urban Development classifies paint containing more than 0.5% lead by weight as being lead-based.

Lead in Paint Limits

ANALYTICAL METHOD METHOD DETECTION LIMIT

REPORTING LIMIT

OSHA-ID 121 0.003 @ 0.10 gram sample 0.006 @ 0.10 gram sample

Ms. Edna A. Bautista Technical Manager

Project 19737

312 Portage Avenue Sault Ste Marie, MI 49783

Attention: Mr. Michael Krzycki

Submitted By: Ms. Michelle C. Stemmons

Reference Data: Lead Sampling Site: ACOE: Sault Ste Marie, MI Sample Type: Paint chip(s) Method Reference: OSHA ID-121 Project ID: Project 19737 DFOH Lab Nos.: TM-19-194390 through TM-19-194393 Date Received: 07/02/19

The paint chip samples were digested using the CEM MARS-Xpress. The samples were run on a Perkin Elmer

General Lab Comments:

All quality control criteria have been met.

* All samples received in condition acceptable for analysis unless otherwise noted.

** Sample results have not been corrected for contamination based on the field blank or other analytical blank unless otherwise noted.

The FOH Environmental Laboratory is an EPA Recognized Testing Lab.

Analytical results are given in the enclosed table. Results relate only to items tested. If you have any questions about

Project 19737

LABORATORY

NUMBER

CONCENTRATION

(%weight)

CONCENTRATION

(mg/g) Poe Boom #13 1A TM-19-194390 <0.006 <0.06 Poe Boom #13 1B TM-19-194391 <0.006 <0.06 Poe Boom #11 1A TM-19-194392 <0.006 <0.06 Poe Boom #11 1B TM-19-194393 <0.006 <0.06

**NOTE: The Department of Housing and Urban Development classifies paint containing more than 0.5% lead

Project 19738

312 Portage Avenue Sault Ste Marie, MI 49783

Attention: Mr. Michael Krzycki

Submitted By: Ms. Michelle C. Stemmons

Reference Data: Lead Sampling Site: ACOE: Sault Ste Marie, MI Sample Type: Paint chip(s) Method Reference: OSHA ID-121 Project ID: Project 19738 DFOH Lab Nos.: TM-19-194394 through TM-19-194397 Date Received: 07/02/19

The paint chip samples were digested using the CEM MARS-Xpress. The samples were run on a Perkin Elmer

General Lab Comments:

All quality control criteria have been met.

* All samples received in condition acceptable for analysis unless otherwise noted.

** Sample results have not been corrected for contamination based on the field blank or other analytical blank unless otherwise noted.

The FOH Environmental Laboratory is an EPA Recognized Testing Lab.

Analytical results are given in the enclosed table. Results relate only to items tested. If you have any questions about

Project 19738

LABORATORY

NUMBER

CONCENTRATION

(%weight)

CONCENTRATION

(mg/g) Mac Ship Arrestor 7-1A TM-19-194394 0.02 0.24 Mac Ship Arrestor 7-1B TM-19-194395 0.02 0.23

Mac Boom 8 #1 TM-19-194396 0.02 0.24 Mac Boom 8 #1 TM-19-194397 0.03 0.25

**NOTE: The Department of Housing and Urban Development classifies paint containing more than 0.5% lead

Project 19740

312 Portage Avenue Sault Ste Marie, MI 49783

Attention: Mr. Michael Krzycki

Submitted By: Ms. Michelle C. Stemmons

Reference Data: Lead Sampling Site: ACOE: Sault Ste Marie, MI Sample Type: Paint chip(s) Method Reference: OSHA ID-121 Project ID: Project 19740 DFOH Lab Nos.: TM-19-194399 through TM-19-19414 Date Received: 07/02/19

The paint chip samples were digested using the CEM MARS-Xpress. The samples were run on a Perkin Elmer

General Lab Comments:

All quality control criteria have been met.

* All samples received in condition acceptable for analysis unless otherwise noted.

** Sample results have not been corrected for contamination based on the field blank or other analytical blank unless otherwise noted.

The FOH Environmental Laboratory is an EPA Recognized Testing Lab.

Analytical results are given in the enclosed table. Results relate only to items tested. If you have any questions about

Project 19740

LABORATORY

NUMBER

CONCENTRATION

(%weight)

CONCENTRATION

(mg/g) Tainter valve 1A TM-19-194399 8.3** 83 Tainter valve 1B TM-19-194400 1.4** 14 Tainter valve 1C TM-19-194401 1.6** 16 Tainter valve 1D TM-19-194402 7.0** 70 Tainter valve 2A TM-19-194403 3.4** 34 Tainter valve 2B TM-19-194404 3.2** 32 Tainter valve 2C TM-19-194405 3.8** 38 Tainter valve 2D TM-19-194406 8.2** 82 Tainter valve 3A TM-19-194407 7.2** 72 Tainter valve 3B TM-19-194408 7.1** 71 Tainter valve 3C TM-19-194409 5.9** 59 Tainter valve 3D TM-19-194410 4.6** 46 Tainter valve 4A TM-19-194411 4.7** 47 Tainter valve 4B TM-19-194412 4.0** 40 Tainter valve 4C TM-19-194413 4.0** 40 Tainter valve 4D TM-19-194414 10** 101

**NOTE: The Department of Housing and Urban Development classifies paint containing more than 0.5% lead