Attachment_A-Sample_Testing_Analysis_Sch.xlsx

XLSX spreadsheet 24 KB Posted

Attached to
Laboratory Analysis of Industrial Hygiene Samples
Solicitation number
SS_463300
Issued by

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The file is an Excel-based Sample Testing/Analysis Schedule for Industrial Hygiene (IH) Airborne Particulate and Vapors Samples, detailing comprehensive analytical methodologies for various compound and element testing. The schedule covers multiple testing profiles including Polynuclear Aromatic Hydrocarbons (PNA/PAHs), Volatile Organic Compounds (VOCs), toxic metals, elemental analyses, silica, asbestos, dust characterization, and fungal testing, with specified turnaround times ranging from 24 hours to 5 days across base and option years.

The related federal contract opportunity is a Pre-Solicitation Request for Information (RFI) from Brookhaven Science Associates on behalf of Brookhaven National Labs, seeking qualified small businesses, with a preference for women-owned small businesses, to perform laboratory analysis of industrial hygiene samples. The solicitation (SS_463300) is issued by the Department of Energy Office of Science and requests interested parties to confirm their capability to meet the attached requirements and provide their SAM UEI number via email. The document emphasizes detailed testing methodologies, including specific analytical techniques like NIOSH methods, ICP-OES, PLM, TEM, and XRD for various environmental and occupational health sample analyses.

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Exhibit_B_Surface_Wipe_Criteria.pdf PDF
IH_SOW_4-14-2025_FINAL.docx DOCX document

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Sheet1

Sample Testing/Analysis ScheduleBase PeriodOption Year 1Option Year 2Option Year 3
TurnaroundTurnaroundTurnaroundTurnaround
Common BNL IH Airborne Particulate and Vapors Samples (metals, VOC, particulates, asbestos)5 Days3 Days24 Hours5 Days3 Days24 Hours5 Days3 Days24 Hours5 Days3 Days24 Hours
AnalyteMethodologySuggested Alternate MethodCompounds in Profile:Unit PriceUnit PriceUnit PriceUnit PriceUnit PriceUnit PriceUnit PriceUnit PriceUnit PriceUnit PriceUnit PriceUnit Price
PNA/PAHsNIOSH# 5506Polynuclear Aromatic Hydrocarbons screen compounds in NIOSH method.
Formaldehyde- AirNIOSH# 2016Formaldehyde
VOC Profile 13M OVMScan: Benzene; Xylene; dimethyl benzene; xylenes; Pentane; Hexane ; Heptane; Octane; Decane; Acetone; 2-Butanone; MIBK; Methanol; Ethanol; Isopropanol; Butanol; Butyl cellosolve; Diethylene glycol ethyl; Phenol; Cresol; Methylphenol; Methylene chloride; Trichloroethane; Perchloroethylene ; Dichlorobenzenes; d-Limonene; Turpentine; Hexanal; Benzaldehyde; Ethyl acetate; Butyl acetate; Amyl acetate; Octamethylcyclotetrasiloxane
VOC Profile 2NIOSH #1550 or

LM-GC-8 or

3M OvmScan: Petroleum ether, rubber solvent, petroleum naphtha, VM&P naphtha, mineral spirits, Stoddard solvent, kerosene, coal tar naphtha
VOC Profile 3NIOSH #1550 or LM-GC-8 or 3M OVMScan: Benzene; toluene; ethylbenzene; xylenes; cumene; butyltoluene; methylstyrene; styrene
Elemental & Inorganic MercuryNIOSH 6009, OSHA ID-140OSHA ID 140Hg
Beryllium - Air*NIOSH #7300, NIOSH#7304OSHA 125G, NIOSH 7300Some compounds may require special sample treatment (ICP-AES)
Lead - Air (Atomic Abs is not very sensitive)), If low sensitivity use ICP/MSNIOSH #7105NIOSH 7301Pb by GFAAS. Use ICP/MS for better sensitivity
Lead - AirNIOSH #7301Pb by ICP
Toxic Metals Profile - AirNIOSH #7301Scan: As, Cd, Cr, Fe, Ni, Pb
PerchloratesEPA 314
Metals Profile 20+ Metals - AirNIOSH #7301Ag = 7300, Tungsten = OSHA 213, all others NIOSH 7301Scan: Ag; Al; As; Ba; Be; Ca; Cd; Co; Cr; Cu; Fe; K; La; Li; Mg; Mn; Mo; Ni; P; Pb; Sb; Se, Sn; Sr; Te; Ti; Tl; V; W; Y; Zn; Zr
Welding Fume ProfileNIOSH #7301Scan: Sb, Be, Cd, Cr, Co, Cu, Fe, Pb, Mn, Mo, Ni, V, Zn
SilicaNIOSH #7500Crystalline by XRD ( Includes quartz & cristobalite)
Silica RespirableNIOSH #7501 is the method for amorphous silicaNIOSH 7500Crystalline by XRD (includes quartz & cristobalite)
FiberglassPLMSEM, TEM, EDS
Synthetic Viterous fibers, RockwoolNIOSH 0500, 7400NIOSH 7400
Dust CharecterizationPLM
Dust, Total- AirNIOSH #0500Gravimetric- pre-weighted
Dust, Respirable- AirNIOSH #0600Gravimetric- pre-weighted
Asbestos Bulks PLM analysisEPA600/M4-82/20,600R-93/116 NIOSH 9002
Asbestos Bulks TEM analysisNYS DOH ELAP 198.1, 198.4, 198.6, 198.8Sub-contracted analysis
Asbestos in Air PCM analysisNIOSH #7400
Asbestos in Air TEM analysisNIOSH #7402Sub-contracted analysis
Asbestos in WipesASTM D6480 (Ghost Wipe media)Sub-contracted analysis
VermiculiteNYS 198.8Sub-contracted analysis
Fungal Cultural AirEM-MY-S-1043Sub-contracted analysisThis should be fungi culturable air. 1 day turnaround is not feasible. You have to culture sample
Fungal Cultural BulkEM-MY-S-1040 & EM-MY-S-2584Sub-contracted analysisThis should be fungi culturable bulk. 1 day turnaround is not feasible. You have to culture sample
Fungal Cultural SurfaceEM-MY-S-1040 & EM-MY-S-2584Sub-contracted analysisThis should be fungi culturable surface. 1 day turnaround is not feasible. You have to culture the sample.
Fungal Air Direct ExaminationEM-MY-S-1038Sub-contracted analysisSpore trap analysis(?)
Fungal Bulk Direct ExaminationEM-MY-S-1039 & EM-MY-S-1041Sub-contracted analysisSpore trap analysis(?)
Fungal Surface Direct ExaminationEM-MY-S-1039 & EM-MY-S-1041Sub-contracted analysisSpore trap analysis(?)
Elements on Surface WipesNIOSH 9102, OSHA-ID-121, 6010B ICPOSHA ID 121 PbLead
Elements on Surface WipesNIOSH 9102, OSHA-ID-121, 6010B ICPOSHA ID 121 for CdCadmium
Elements on Surface WipesNIOSH 9102, OSHA-ID-121, 6010B ICPOSHA ID 121 for BeBeryllium
Elements on Surface WipesNIOSH 9102, OSHA-ID-121, 6010B ICPOSHA ID 121 for AsArsenic
Elements on Surface WipesNIOSH 9102, OSHA-ID-121, 6010B ICPOSHA ID 121 for CrHexavalent Chromium
Elements on Surface Wipes (Group)NIOSH 9102, OSHA-ID-121, 6010B ICPOSHA ID 121 for Pb, Cd, Cr, Ar, BePb, Cd, Cr, Ar, Be
Elements on Surface Wipes (Group Mix + Match)NIOSH 9102, OSHA-ID-121, 6010B ICPOSHA ID 121 for Pb, Cd, Cr, Ar, BePb, Cd, Cr, Ar, Be
*BNL may request analysis for Total Beryllium, Beryllium and Beryllium Compounds (as Be) of airborne Beryllium, surface wipe and bulk sampling by inductively coupled plasma optical emission spectrometry (ICP-OES) instrumentation.
Limits of Detection should meet DOE, ACGIH and/or OSHA standards for proper analytical reporting of sample results (i.e. 25% of the standard).
Please view the supplemental document BNL-Adopted Surface Wipe Criteria for BNL Limit of Detection (Non-Operational Areas) for wipe samples.
Where BNL has a lower detection limit, BNL's detection limit must be met.
BNL also may use passive dosimeters and sorbent tubes.
Inhalable sample analysis may also be required.
BNL follows the ACGIH TLV and OSHA PEL standards.

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