AMENDMENT 0004

NSN: 7540-01-152-8070

30-105 STANDARD FORM 30 (REV. 10-83

AMENDMENT OF SOLICITATION/MODIFICATION OF CONTRACT

1. CONTRACT ID CODE

PAGE 1 OF PAGES 40

2. AMENDMENT/MODIFICATION NO.

3. EFFECTIVE DATE

28 October 2011

4. REQUISITION/PURCHASE REQ. NO.

5. PROJECT NO. (If applicable)

6. ISSUED BY CODE SP0600 7. ADMINISTERED BY (If other than Item 6) CODE

CODE

DLA ENERGY

8725 JOHN J. KINGMAN RD., SUITE 3938

FT. BELVOIR, VA 22060-6222

BUYER/SYMBOL: IVAN HARGROVE-BXB

PHONE: 703-767-9328 FAX: 703-767-9338

E-MAIL: Ivan.Hargrove@dla.mil

8. NAME AND ADDRESS OF CONTRACTOR (NO., street,city,county,State,and ZIP Code) () 9A. AMENDMENT OF SOLICITATION NO.

X

SP0600-10-R-0527

9B. DATED (SEE ITEM 11)

10A. MODIFICATION OF CONTRACT/ORDER NO.

10B. DATED (SEE ITEM 13)

CODE FACILITY CODE

11. THIS ITEM ONLY APPLIES TO AMENDMENTS OF SOLICITATIONS

[X] The above numbered solicitation is amended as set forth in Item 14. The hour and date specified for receipt of Offers [] is extended, [X] is not extended.

Offers must acknowledge receipt of this amendment prior to the hour and date specified in the solicitation or as amended, by one of the following methods:

(a) By completing Items 8 and 15, and returning 1 copy of the amendment ;(b) By acknowledging receipt of this amendment on each copy of the offer submitted; or(c) By separate letter or telegram which includes a reference to the solicitation and amendment numbers. FAILURE OF YOUR ACKNOWLEDGMENT TO BE RECEIVED AT THE PLACE DESIGNATED FOR THE

RECEIPT OF OFFERS PRIOR TO THE HOUR AND DATE SPECIFIED MAY RESULT IN REJECTION OF YOUR OFFER. If by virtue of this amendment you desire to change an offer already submitted, such change may be made by telegram or letter, provided each telegram or letter makes reference to the solicitation and this amendment, and is received prior to the opening hour and date specified.

12. ACCOUNTING AND APPROPRIATION DATA (If required)

13. THIS ITEM APPLIES ONLY TO MODIFICATIONS OF CONTRACTS/ORDERS,

IT MODIFIES THE CONTRACT/ORDER NO. AS DESCRIBED IN ITEM 14.

A. THIS CHANGE ORDER IS ISSUED PURSUANT TO: (Specify authority) THE CHANGES SET FORTH IN ITEM 14 ARE MADE IN THE CONTRACT ORDER NO. IN ITEM 10A.

B. THE ABOVE NUMBERED CONTRACT/ORDER IS MODIFIED TO REFLECT THE ADMINISTRATIVE CHANGES (such as changes in paying office appropriation date, etc.) SET FORTH

IN ITEM 14, PURSUANT TO THE AUTHORITY OF FAR 43.103(b)

C. THIS SUPPLEMENTAL AGREEMENT IS ENTERED INTO PURSUANT TO AUTHORITY OF:

D. OTHER Specify type of modification and authority)

E. IMPORTANT: Contractor [] is not, [] is required to sign this document and return copies to the issuing office.

14. DESCRIPTION OF AMENDMENT/MODIFICATION (Organized by UCF section headings, including solicitation/contract subject matter where feasible.)

A. DLA Energy requests that all offerors acknowledge receipt of this amendment by completing block 8 above, and signing and dating blocks 15A, 15B, and 15C below, and returning this document with their offer to DLA Energy/BXB e-mail to Ivan.Hargrove@dla.mil or by facsimile to 703-767-9337.

SEE CONTINUATION PAGES

Except as provided herein, all terms and conditions of the document referenced in Items 9A or 10A, as heretofore changed, remain unchanged and in full force and effect.

15A. NAME AND TITLE OF SIGNER (Type or print) 16A. NAME AND TITLE OF CONTRACTING OFFICER (Type or print)

15B. CONTRACTOR/OFFEROR

(Signature of person authorized to sign)

15C.DATE SIGNED 16B. UNITED STATES OF AMERICA

(Signature of Contracting Officer)

16C.DATE SIGNED

mailto:Ivan.Hargrove@dla.mil mailto:Ivan.Hargrove@dla.mil

B. The following line items are hereby added to this solicitation:

CLIN SAMPLE LOCATION

0001 Baton Rouge, LA 0004 Lockhart, MS 0048 Charleston, SC 0049 Pearl Harbor, HI

C. The closing date for submission of offers for line items 0005, 0011, 0012, 0017, 0023, 0024, 0029, 0036, 0046 and 0047 under this solicitation, are hereby extended until Friday, November 11, 2011, 3:00 pm (Local Time, Fort Belvoir, VA).

D. The final date for receipt offers for line items 0001, 0004, 0005, 0011, 0012, 0017, 0023, 0024, 0029, 0036, 0046, 0047, 0048 and 0049 under this solicitation is Friday, November 11, 2011, 3:00 pm (Local Time, Fort Belvoir, VA). All other line items issued under solicitation SP0600-10-R-0527 are closed to new offers.

CLIN SAMPLE LOCATION

0001 Baton Rouge, LA 0004 Lockhart, MS 0005 Montgomery, AL 0011 Salt Lake City, UT 0012 Breman, GA 0017 Tulsa, OK 0023 Columbus, GA 0024 Macon, GA 0029 Alamogordo, NM 0036 Rapid City, SD 0046 Helena, AL 0047 Verona, NY 0048 Charleston, SC 0049 Pearl Harbor, HI

E. Attachment A of this amendment details the Performance Work Statement (PWS). The changes to this document are highlighted in yellow.

F. Attachment B of this amendment details the petroleum products, test methods required for a quality determination.

The changes to this document are highlighted in yellow.

G. Attachment C contains the pricing sheets. Added items are highlighted in yellow. For each CLIN the contractor shall submit pricing on every test, or test group, for each CLIN as shown in the price sheets.

H. All other terms and conditions set forth under solicitation SP0600-10-R-0527 remain in-force and unchanged.

ATTACHMENT A

PERFORMANCE WORK STATEMENT

MULTIPLE CONUS LOCATIONS QUALITY ASSURANCE TESTING AND

SAMPLING OF PETROLEUM PRODUCT

A. INTRODUCTION:

Defense Logistics Agency Energy (DLA Energy) buys petroleum products that are used in support of military operations worldwide. The purpose of this PWS is to provide a description/direction of the services required of a contractor that will represent the United

States Government/ DLA Energy by providing sampling, laboratory testing and transportation of government-owned petroleum products as described herein, and report the information gathered as a result of those services to DLA Energy.

B. SERVICES TO BE PROVIDED:

1. The contractor shall provide the following services as part of this Performance Work

Statement:

a. Sampling of vessels and drums containing the petroleum products listed in Attachment A;

b. Transportation of the samples to the contract laboratory via a dedicated laboratory vehicle or commercial carrier (includes packaging);

c. Laboratory testing of the petroleum products listed in Attachment A. Attachment A details the petroleum products, test methods, and groups of test methods required for a quality determination.

d. Attachment B contains the price sheets for the products and locations being solicited. The contractor shall submit pricing on every test or test group listed in Attachment B price sheets. The number of tests listed in Attachment B is for budget planning only. However, at any time the contractor shall be prepared to test any test or test group for a product/location listed in Attachment B.

e. The commercial laboratory must be located within 900 miles of the sample locations listed in the following CONUS locations being solicited in this PWS. However, if all offers generated from the solicitation are not within a 900 mile distance, all remaining offers will be evaluated equally for distance. The exception to this rule is on CLIN

0048 (Charleston, SC). For this location (CLIN 0048) we are requiring a turn-around time of 8 hours for Jet A Full Specification testing of samples.

SAMPLE LOCATION PROPOSED CLIN

Baton Rouge, LA 0001

Lockhart, MS 0004

Montgomery, AL 0005

Salt Lake City, UT 0011

Breman, GA 0012

Tulsa, OK 0017

Columbus, GA 0023

Macon, GA 0024

Alamogordo, NM 0029

Rapid City, SD 0036

Helena, AL 0046

Verona, NY 0047

Charleston, SC 0048

Pearl Harbor, HI 0049

C. LABORATORY TESTING AT MULTIPLE CONUS LOCATIONS

1. DESCRIPTION OF SERVICES:

a. The contractor shall provide one or more laboratories capable of performing the tests associated with the products listed in the Attachments A. The laboratories shall have a system of calibration equivalent to ISO 10012-1 – Quality Assurance Requirements for

Measuring Equipment and meet the equivalent requirements of ISO 17025 – General

Requirements for the Competence of Testing of Calibration Laboratories.

b. The laboratory shall maintain an audit trail that will allow for identification of tests performed and specific equipment and technicians. All testing will be performed in strict accordance with test methods identified in attachments referred to in Attachment A.

c. Testing of U.S. Government-owned fuel products are required 24 hours per day, 7 days per week (including holidays). Under normal circumstances, samples will be received during contractor’s normal working hours as set forth in the contract. Samples shall be processed, tested, and results provided to the DLA Energy Office/QAR (having cognizance over the location from which the samples originate) within the prescribed turn-around times as indicated. Turn-around time is measured from the time the samples are received at the laboratory to the time test results are received by the QAR. Should testing be required at other than normal working hours, and/or neither the CO nor the

QAR are available, the Contractor may perform tests as requested in order to make an adequate analysis of the samples of fuel furnished for testing. No additional tests that are beyond the Contractor’s capability to perform shall be required. The following are general turn-around times for groups of test/ methods:

TESTS REQUIRED and TURN AROUND TIMES

B Series Testing (Attachment A) 24 hours

Individual Testing (as requested) 8 hours

d. The contractor shall maintain records evidencing all analysis performed under this contract.

All samples tested will be documented with a detailed report which reflects standardized

American Petroleum Institute / Institute of Petroleum (API/IP) format when available. The contractor will telephone, fax, or email test results to the DLA Energy office identified below.

Costs for providing test results will not be reimbursed by the U.S. Government and should be included in testing prices.

e. Samples shall be retained, after analysis, for a minimum of 15 days.

f. The Contractor shall be responsible for disposal of excess fuel sample and sample containers.

g. Upon request by DLA Energy, the Contractor may be asked to provide Department of

Transportation (DOT) approved sample containers and packaging/shipping materials. The

Contractor is asked to quote a price under for sample containers and packaging/shipping materials in Attachment B Price Sheets.

E. ORDERING OF SERVICES

Services are considered to be “ordered” when the Contractor’s laboratory personnel receive the sample, along with instructions for which series/tests are to be performed. All orders are subject to the terms and conditions of the contract. Orders may be placed during the performance period of the contract.

1. Ordering of laboratory services shall be authorized by the DLA Energy QAR assigned to

DLA Energy having cognizance over the location from which the samples originate.

2. Additional Services and Testing Outside Normal Working Hours

a. The Contractor shall perform such additional tests as the Contracting Officer (CO) or designated representative may require. The representative of the CO, for purposes detailed below, is hereby designated as the QAR of DLA Energy as having cognizance over the location from which the samples originate.

b. Should testing be required at other than normal working hours, and/or neither the CO nor the QAR are available, the Contractor may perform tests as requested in order to make an adequate analysis of the samples of fuel furnished for testing. No additional tests that are beyond the Contractor’s capability to perform shall be required.

c. Invoices for services performed under this clause shall be submitted in accordance with the Clause XXXXXX-(invoice clause from contract), and this document. However, a separate certification will be required on the invoice citing those additional tests that were requested under this clause, and/or the amount of overtime required, and any resulting overtime charges.

d. Overtime is defined as the time outside the Contractor’s normal working hours when the sample has been placed in the normal queue. Expedite is defined as placing the sample at the front of the queue and performing the test immediately.

F. INVOICES:

The contractor shall submit an invoice to the Quality Assurance Representative (QAR) of

DLA Energy as assigned for certification and authorization for payment. The invoice may be mailed, emailed or faxed to the QAR who will in turn forward a signed copy of the invoice to the contractor and DFAS for payment. The Contractor shall prepare the invoice on the last day of each month. Each invoice shall contain the following information:

1. Contract number, CLIN, and SubCLIN;

2. For each sample submitted:

Sample identification number;

Sample date;

Date testing is performed;

Name and Location of laboratory where testing is performed;

List of tests performed and unit price for each;

3. Total amount due on same line as Contract Line Item Number (CLIN);

4. Invoice shall be made out to:

DFAS-Columbus Center

ATTN: DFAS-FVSFA/CO

3900 East Broad Street, Bldg 21

Columbus, Ohio 43213-1152

G. PERFORMANCE PERIOD:

1. Initial One (1)Year Performance Period from date of Contract Award.

2. Optional First Year of Performance Period

3. Optional Second Year of Performance Period

4. Optional Third Year of Performance Period

5. Optional Fourth Year of Performance Period

H. DELIVERABLES:

1. The Contractor will provide reports within 48 hours to the DLA Energy QAR Email.

2. For Laboratory Testing Support of Petroleum Product, a laboratory report shall be faxed or

Emailed to the DLA Energy QAR responsible for submitting the sample. If the results of any of these tests fall outside that allowable range of reproducibility of the stated test method the DLA Energy assigned QAR will be immediately notified.

Attachment B

TEST METHOD AND GROUPS BY PRODUCT

TURBINE FUELS, AVIATION, KEROSENE TYPES,

NATO F-34 (JP-8)

TESTING REQUIREMENTS, MIL-DTL-83133 (LATEST VERSION)

A. Full Specification Testing (A Series), includes all tests listed below (one price for all). Testing shall be performed in accordance with the specified test method.

B. Individual tests are any one, or combination, of tests below (individual prices).

CHARACTERISTIC TEST METHOD, ASTM

1) Workmanship 1/

2) Color, Saybolt 2/ D156 R/, D6045

3) Total Acid Number D3242

4) Aromatics D1319

5) Sulfur, Total Percent D129, D1266, D2622, D3120, D4294 R/, or D5453

6) Sulfur, Mercaptan D3227

7) Doctor Test D4952

8) Distillation 3/ D86 R/, D2887

9) Flash Point D93 R/, D3828 4/, D56

10) Density, or API Gravity D1298, D4052 R/

11) Freezing Point D2386 R/, D5972, D7153, or D7154

12) Viscosity at -20 o C D445

13) Net Heat of Combustion, MJ/kg BTU/lb D3338, D4809 R/, D4529

14) Hydrogen Content D3701 R/, D3343

15) Naphthalenes D1840

16) Smoke Point D1322 /

17) Cetane Index, Calculated 2/ D976 6/, or D4737

18) Copper Strip Corrosion D130

19) Thermal Stability D3241 7/

20) Existent Gum D381

21) Particulate Matter (Solids) 8/ D2276 8/, D5452 R/

22) Filtration Time D2276 8/

OR Combined Test for Particulate

Matter and Filtration Time 12/

23) Water Reaction, Interface Rating D1094

24) Water Separation Index 9/ D3948, or D7224 R/

25) Fuel Systems Icing Inhibitor D5006 10/

26) Fuel Electrical Conductivity 11/ D2624

27) Color, Visual D4176

28) Sulfides in Bottom Water See Statement of Work

C. B-1 Series Testing (one price for the following 15 tests):

CHARACTERISTIC

1) Workmanship

2) Color (Visual)

3) Density or API Gravity

4) Particulate Matter

5) Distillation

6) Copper Strip Corrosion

7) Freezing Point

8) Existent Gum

9) Flash Point

10) Water Reaction

11) Fuel Systems Icing Inhibitor

12) Filtration Time

13) Water Separation Index

14) Fuel Electrical Conductivity

15) Thermal Stability

D. B-2 Series Testing (one price for the following 17 tests):

2) Color (Visual)

3) Density or API Gravity

4) Particulate Matter

5) Distillation

6) Copper Strip Corrosion

7) Freezing Point

8) Existent Gum

9) Flash Point

10) Water Reaction

11) Fuel Systems Icing Inhibitor

12) Filtration Time

13) Water Separation Index

14) Fuel Electrical Conductivity

15) Thermal Stability

16) Color, Saybolt

17) Acid Number

E. Type C Testing (one price for the following 4 tests):

2) Color (Visual)

3) Density or API Gravity

4) Flash Point

F. Series for Secure Fuels Testing: (one price for the following 12 tests):

1 Density or API Gravity

2 Distillation

3 Freezing Point

4 Flash Point

5 Particulate Matter

6 Conductivity

7 Copper Corrosion

8 Water Reaction

9 Existent Gum

10 Fuel System Icing Inhibitor

11 Workmanship

12 Thermal Stability

NOTES:

R/ Referee Test Method

1/ Workmanship. At the time of Government acceptance, the finished fuel shall be visually free from undissolved water, sediment, or suspended matter and shall be clear and bright. In case of dispute, the fuel shall be clear and bright at 21°C (70°F) and shall contain no more than 1.0 mg/L of particulate matter as required in table I.

2/ To be reported - not limited.

3/ A condenser temperature of 0 o C to 4 o C (32 o F to 40 o F) shall be used for distillation by

ASTM D86.

4/ ASTM D93 is the referee method, Method IP170 is also permitted. The minimum

Flash Point shall be 40 o C by ASTM D56, as it can be 1 o to 2 o C above those obtained by other methods.

5/ When the fuel distillation test is performed using ASTM D2887, the average distillation temperature, for use in ASTM D3338 shall be calculated as follows: V =

(10% + 50% + 95%)/3.

6/ Mid-boiling temperature may be obtained by either ASTM D86 or ASTM D2887 to perform the cetane index calculation. ASTM D86 values should be corrected to standard barometric pressure.

7/ See MIL-DTL-83133, paragraph 4.5.2.1 for ASTM D3241 test conditions and test limits.

8/ A minimum sample size of 3.79 liters (one gallon) shall be filtered. Filtration time will be determined in accordance with the procedures in MIL-DTL-83133, Appendix

A. This procedures may also be used for the determination of particulate matter as an alternate to ASTM D2276.

9/ A minimum water separation index rating for JP-8 shall be 85 with all additives except for the corrosion inhibitor/lubricity improver additive and the static dissipator additive, or 70 with all additives except the static dissipator additive.

10/ Test shall be performed in accordance with ASTM D5006 or method 5327 or 5340 of Fed-STD-791. Use the appropriate scale of the refractometer.

11/ The conductivity must be between 150 and 600pS/m for F-34 and between 50 and

450 pS/m for F-3 5.

12/ Filtration Time Test Procedure.

a. Membrane filters shall be removed from the package and placed in an oven for a minimum of 15 minutes to 90º C. After preheating, but prior to weighing, the membrane filters shall be stored in a desiccator.

b. Each membrane filter shall be weighed. A filter weighing in excess of 90 mg will not be used in the test.

c. The membrane filter shall be placed directly over the insert ring. The top funnel shall be locked into place.

d. Immediately prior to filtering the fuel, shake the sample to obtain a homogeneous mix and assure that fuel temperature does not exceed 30º C (86º F). Clean the exterior or top portion of the sample container to ensure that no contaminants are introduced. Any free water present in the fuel sample will invalidate the filtration time results by giving an excessive filtration time rating.

e. With the vacuum off, pour approximately 200 ml of fuel into the funnel.

f. Turn vacuum on and record starting time. Continue filtration of the 3.79 liters (1 gallon) sample, periodically shaking the sample container to maintain a homogenous mix.

Record the vacuum in kPa (inches of mercury) 1 minute after start and again immediately prior to completion of filtration. Throughout filtration, maintain a sufficient quantity of fuel in the funnel so that the membrane filter is always covered.

g. Report the filtration time in minutes expressed to the nearest whole number. If filtration of the 3.79 liters (1 gallon) is not completed within 30 minutes, the test will be stopped and the volume of the fuel filtered will be measured. In these cases, report filtration time as “>30 minutes” and the total volume of fuel filtered.

h. Report the vacuum in kPa (inches of mercury) as determined from the average of the two readings taken in f.

i. After recording the filtration time, shut off the vacuum and rinse the sample container with approximately 100 ml of filtered petroleum ether and dispense into the filtration funnel. Turn the vacuum on and filter the 100 ml. Rinse. Turn vacuum off and wash the inside of the funnel with approximately 50 ml of filtered petroleum ether. Turn vacuum on and filter. Repeat the funnel rinse with another 50 ml of petroleum ether but allow the rinse to soak the filter for approximately 30 seconds before turning the vacuum on to filter the rinse. With vacuum on, carefully remove the top funnel and rinse the periphery of the membrane filter by directing a gentle stream of petroleum ether from the solvent dispenser from the edge of the membrane toward the center, taking care not to wash contaminants off the filter.

Maintain vacuum after final rinse for a few seconds to remove the excess petroleum ether from the filter.

j. Using forceps, carefully remove the membrane filter from the filter and place in a clean petri dish. Dry in the oven at 90º C (194º F) for 15 minutes with the cover on the petri dish slightly ajar. Place dish in a desiccator and allow to cool for a minimum of 15 minutes. If more than one sample is processed, cooling time will have to be increased.

Reweigh the filter.

k. Report the total solids content in mg/liter by using the following formula:

Weight gain of filter in mgs = mg/liter

3.785

l. Should the sample exceed the 30-minute filtration time and a portion of the fuel is not filtered, the solids content in mg/liter will be filtered as follows: Determine the volume of fuel filtered by subtracting the ml of fuel remaining from 3.785.

ml of fuel filtered X 0.001

TURBINE FUEL, AVIATION, GRADES JP-5 NATO F-44

TESTING REQUIREMENTS, MIL-DTL-5624 (Latest Version)

A. Full Specification Testing (A Series), includes all tests listed below (one price for all). Testing shall be performed in accordance with the specified test method.

CHARACTERISTIC TEST METHOD, ASTM,

1 Workmanship (2)

2 Color, Saybolt D156 (1), D6045

3 Total Acid Number D3242

4 Aromatics D1319

5 Sulfur, Mercaptan, mass percent D3227 (3)

OR Doctor Test D4952 (3)

6 Sulfur, Total Mass Percent D1266, D2622, D3120, D4294 (1), or

D5453

7 Distillation (4) D86 (1), D2887

8 Flash Point (5) D56, D93 (1), D3828

9 Density, or API Gravity D1298, D4052 (1)

10 Freezing Point D2386 (1), D5972

11 Viscosity at -20 o C D445

12 Heating Value, Net Heat of Combustion D3338, D4809 (1), D4529

13 Cetane Index, Calculated (6) D976, D4737

14 Hydrogen Content, Mass Percent D3701

15 Smoke Point D1322

16 Copper Strip Corrosion D130

17 Thermal Stability D3241 (7)

18 Existent Gum D381 (8)

19 Particulate Matter (Solids) D2276 or D5452 9/10/

Filtration Time D2276 9/ 10/

OR Combined Test for Particulate

Matter and Filtration Time

12/

20 Micro-separometer Rating D3948

21 Fuel Systems Icing Inhibitor D5006 (11)

22 Visual (Color) NPA, Common Descriptive Terms (13)

23 Sulfides in Bottom Water See Statement of Work

C. B-1 Series Testing (one price for the following 13 tests):

1 Workmanship

2 Color (Visual)

3 Distillation

4 Flash Point

5 Density or API Gravity

6 Freezing Point

7 Copper Strip Corrosion

8 Existent Gum

9 Particulate Matter (Solids)

10 Water Reaction Interface Rating

11 Fuel Systems Icing Inhibitor

12 Micro Separometer rating

13 Thermal Stability

D. B-2 Series Testing (one price for the following 15 tests):

1 Workmanship

2 Color (Visual)

3 Distillation

4 Flash Point

5 Density or API Gravity

6 Freezing Point

7 Copper Strip Corrosion

8 Existent Gum

9 Particulate Matter (Solids)

10 Water Reaction Interface Rating

11 Fuel Systems Icing Inhibitor

12 Micro Separometer rating

13 Thermal Stability

14 Total Acid Number

15 Saybolt Color

E. Type C Series Testing (one price for the following 4 tests):

CHARACTERISTIC

1 Workmanship

2 Color (Visual)

3 Density or API Gravity

4 Flash Point

1 Density or API Gravity

2 Distillation

3 Freezing Point

4 Flash Point

5 Particulate Matter

6 Conductivity

7 Copper Corrosion

8 Water Reaction

9 Existent Gum

10 Fuel System Icing Inhibitor

1. Referee Test Method.

2. Workmanship; the fuel shall be clear and bright and visually free from undissolved water, sediment, or suspended matter. In case of dispute, the fuel shall be clear and bright at 21 °C and shall contain no more than 1.0 mg/L. Use particulate matter test methods listed herein to determine foreign matter content.

3. Perform Sulfur, Mercaptan test or Doctor test.

4. A condenser temperature of 0 to 4 °C (32 to 40 °F) shall be used for the distillation of JP-5 fuel.

5. ASTM D3828 may give results up to 1.7 °C below the ASTM D93 results. ASTM D56 may give results up to 1 °C below the ASTM D93 results.

6. Mid-boiling temperatures shall be obtained by either ASTM D86 or ASTM D2887 to perform the Cetane Index calculation. If ASTM D86 values are used, they shall be corrected to standard barometric pressure.

7. Thermal Stability test conditions and procedures for ASTM D3241

a. Minimum heater tube temperature at maximum point: 260 °C

b. Fuel system pressure: 3.45 MPa (500 psig)

c. Fuel flow rate: 3.0 Ml/minute

d. Test duration: 150 minutes

8. If air is used instead of steam while performing ASTM D381, it shall be recorded. In case of a failure with air, the sample shall be retested using steam.

9. A minimum sample size of 3.79 liters (1 gallon) shall be filtered.

10. The flow reducer ring of Appendix paragraph A.3.c of MIL-DTL-5624, is not required.

11. Tests shall be performed with ASTM D5006 using the DiEGME scale of the refractometer.

12. The following procedure shall be used for the determination of Filtration Time and may be used to determine particulate matter as an alternate to ASTM D2276 or ASTM 5452.

a. Membrane filters shall be removed from the package and placed in an oven for a minimum of

15 minutes at 90 °C. After preheating, but prior to weighing, the membrane filters shall be stored in a desiccator.

b. Each membrane filter shall be weighed. A filter weighing in excess of 90 mg shall not be used in the test.

c. The insert ring shall be centered on the filter base. One membrane filter shall be placed directly over the insert ring. The top funnel shall be locked into place.

d. Immediately prior to filtering the fuel, shake the sample to obtain a homogenous mix and ensure that fuel temperature does not exceed 30 °C. Clean the exterior or top portion of the sample container to ensure no contaminants are introduced. Any free water present in the fuel sample will invalidate the filtration time results by giving an excessive filtration time rating.

e. With the vacuum off, pour approximately 200 mL of fuel into the funnel.

f. Turn vacuum on and record starting time. Continue filtration of the 3.79 liter sample, periodically shaking the sample container to maintain a homogenous mix. Record the vacuum in kPa (in. of mercury) 1 minute after start and again immediately prior to completion of filtration. Throughout filtration, maintain a sufficient quantity of fuel in the funnel so the membrane filter is always covered.

g. Record the filtration time in minutes expressed to the nearest whole number. If filtration of the

3.79 liters is not completed within 30 minutes, the test will be stopped and the volume of the fuel filtered will be measured. In these cases, record filtration time as “greater than 30 minutes” and the total volume of fuel filtered.

h. Record the vacuum in kPa (in. of mercury) as determined from the average of the two readings taken in A.6.1.f.

i. After recording the filtration time, shut off the vacuum and rinse the sample container with approximately 100 mL of filtered petroleum ether and dispense into the filtration funnel.

Turn on the vacuum and filter the 100 mL rinse. Turn off the vacuum and wash the inside of the funnel with approximately 50 mL of filtered petroleum ether. Turn on vacuum and filter. Repeat the funnel rinse with another 50 mL of petroleum ether but allow the rinse to soak the filter for approximately 30 seconds before turning on the vacuum to filter the rinse. With the vacuum on, carefully remove the top funnel and rinse the periphery of the membrane filter by directing a gentle stream of petroleum ether from the solvent dispenser from the edge of the membrane toward the center, taking care not to wash contaminants off the filter. Maintain vacuum after final rinse for a few seconds to remove the excess petroleum ether from the filter.

j. Using forceps, carefully remove the membrane filter from the filter base and place in a clean

Petri dish. Dry in the oven at 90 °C for 15 minutes with the cover on the Petri dish slightly ajar. Place dish in a dessicator and allow to cool for a minimum of 15 minutes. If more than one sample is processed, cooling time will have to be increased. Reweigh the filter.

k. Record the total solids content in mg/liter by using the following formula:

l. Should the sample exceed the 30-minute filtration time and a portion of the fuel is not filtered, the solids content in mg/liter will be reported as follows: Determine the volume of fuel filtered by subtracting the ml of fuel remaining from 3.785.

m. Vacuum shall exceed 67.5 kPa (20 in. of mercury) throughout the test and fuel temperature shall be between 18 and 30 °C.

13. Common Descriptive Terms; Water White, Light Straw, Straw, Prime White, Standard White, Lily White, Cream White.

AVIATION TURBINE FUEL, GRADE JET A/A1

TESTING REQUIREMENTS, ASTM D1655 (Latest Version)

A. Individual tests are any one, or combination, of tests below (individual prices).

CHARACTERISTIC TEST METHOD, ASTM 1/

1) Workmanship Section 7, ASTM D1655

2) Color, Visual D4176

3) Total Acid Number D3242

4) Aromatics D1319, D6379

5) Sulfur, Mercaptan D3227

6) Sulfur, Total Percent D1266, D2622, D4294, or D5453

7) Distillation/Simulated Distillation D86, D2887

8) Flash Point D56, D3828

9) Density, or API Gravity D1298, D4052

10) Freezing Point D5972, D7153, D7154, or D2386

11) Viscosity at –20 o C D445

12) Net Heat of Combustion D4529, D3338, D4809

13) Smoke Point, mm D1322,

14) Naphthalenes D1840

15) Copper Strip Corrosion, 2 hrs at 100 o C D130

16) JFTOT (2.5 h at 260 o C) D3241

17) Existent Gum, mg/100 ml D381, IP540

18) Water Separation Index D3948

19) Electrical Conductivity D2624

20) Particulate Matter (Solids) D2276, D5452

21) Filtration Time 2/

OR Combined Test for Particulate

Matter and Filtration Time 2/

22) Water Reaction Interface Rating D1094

23) Fuel Systems Icing Inhibitor (FSII) D5006 3/

24) Sulfides in Bottom Water See Statement of Work

B. Full Specification Testing (A Series), includes all tests listed below (one price for all 17).

Testing shall be performed in accordance with the specified test method.

CHARACTERISTIC TEST METHOD, ASTM 1/

1) Total Acid Number mg KOH/g D3242

2) Aromatics, volume % D1319, D6379

3) Sulfur, Mercaptan, mass % D3227

4) Sulfur, Total Mass % D1266, D2622, D4294, or D5453

5) Distillation/Simulated Distillation, °C D86, D2887

6) Flash Point °C D56, D3828

7) Density at 15°C, kg/m3 D1298, D4052

8) Freezing Point, °C D5972, D7153, D7154, or D2386

9) Viscosity at –20 o C, mm²/s D445

10) Net Heat of Combustion D4529, D3338, D4809

11) Smoke Point, mm D1322

12) Naphthalenes, vol % D1840

13) Copper Strip Corrosion, 2 hrs at 100 o C D130

14) JFTOT (2.5 h at 260 o C) D3241

15) Existent Gum, mg/100 ml D381, IP540

16) Microseparometer, Rating D3948

17) Electrical Conductivity, pS/m D2624

C. B-1 Series Testing (one price for the following 15 tests):

2) Color (Visual)

3) Density or API Gravity

4) Particulate Matter (Solids)

5) Distillation/Simulated Distillation

6) Copper Strip Corrosion

7) Freezing Point

8) Existent Gum

9) Flash Point

10) Water Reaction Interface Rating

11) Filtration Time

12) Electrical Conductivity

13) JFTOT

14) Fuel Systems Icing Inhibitor (FSII)

15) Water Separation Index

D. B-2 Series Testing (one price for the following 16 tests):

1) Workmanship

2) Color (Visual)

3) Density or API Gravity

4) Particulate Matter (Solids)

5) Distillation/Simulated Distillation

6) Copper Strip Corrosion

7) Freezing Point

8) Existent Gum

9) Flash Point

10) Water Reaction

11) Filtration Time

12) Electrical Conductivity

13) JFTOT

14) Acid Number

15) Fuel Systems Icing Inhibitor (FSII)

16) Water Separation Index

E. Type C Testing (one price for the following 4 tests):

CHARACTERISTIC

1) Workmanship

3) Color (Visual)

3) Density or API Gravity

4) Flash Point

1 Density, or API Gravity

2 Distillation

3 Freezing Point

4 Flash Point

5 Particulate Content

6 Conductivity

7 Copper Corrosion

8 Water Reaction

9 Existent Gum

10 Fuel System Icing Inhibitor

1/ The test methods indicated in this table are referred to in ASTM D1655, Section 10. Refer to

ASTM D1655, Table I, for test limits/ranges, and additional information on testing conditions for individual characteristics.

2/ Filtration Time Test Procedure.

a. Membrane filters shall be removed from the package and placed in an oven for a minimum of

15 minutes to 90º C. After preheating, but prior to weighing, the membrane filters shall be stored in a desiccator.

b. Each membrane filter shall be weighed. A filter weighing in excess of 90 mg will not be used in the test.

c. The membrane filter shall be placed directly over the insert ring. The top funnel shall be locked into place.

d. Immediately prior to filtering the fuel, shake the sample to obtain a homogeneous mix and assure that fuel temperature does not exceed 30º C (86º F). Clean the exterior or top portion of the sample container to ensure that no contaminants are introduced. Any free water present in the fuel sample will invalidate the filtration time results by giving an excessive filtration time rating.

e. With the vacuum off, pour approximately 200 ml of fuel into the funnel.

f. Turn vacuum on and record starting time. Continue filtration of the 3.79 liters (1 gallon) sample, periodically shaking the sample container to maintain a homogenous mix. Record the vacuum in kPa (inches of mercury) 1 minute after start and again immediately prior to completion of filtration. Throughout filtration, maintain a sufficient quantity of fuel in the funnel so that the membrane filter is always covered.

g. Report the filtration time in minutes expressed to the nearest whole number. If filtration of the

3.79 liters (1 gallon) is not completed within 30 minutes, the test will be stopped and the volume of the fuel filtered will be measured. In these cases, report filtration time as “>30 minutes” and the total volume of fuel filtered.

h. Report the vacuum in kPa (inches of mercury) as determined from the average of the two readings taken in f.

i. After recording the filtration time, shut off the vacuum and rinse the sample container with approximately 100 ml of filtered petroleum ether and dispense into the filtration funnel. Turn the vacuum on and filter the 100 ml. Rinse. Turn vacuum off and wash the inside of the funnel with approximately 50 ml of filtered petroleum ether. Turn vacuum on and filter. Repeat the funnel rinse with another 50 ml of petroleum ether but allow the rinse to soak the filter for approximately 30 seconds before turning the vacuum on to filter the rinse. With vacuum on, carefully remove the top funnel and rinse the periphery of the membrane filter by directing a gentle stream of petroleum ether from the solvent dispenser from the edge of the membrane toward the center, taking care not to wash contaminants off the filter. Maintain vacuum after final rinse for a few seconds to remove the excess petroleum ether from the filter.

j. Using forceps, carefully remove the membrane filter from the filter and place in a clean petri dish. Dry in the oven at 90º C (194º F) for 15 minutes with the cover on the petri dish slightly ajar. Place dish in a desiccator and allow to cool for a minimum of 15 minutes. If more than one sample is processed, cooling time will have to be increased. Reweigh the filter.

k. Report the total solids content in mg/liter by using the following formula:

l. Should the sample exceed the 30-minute filtration time and a portion of the fuel is not filtered, the solids content in mg/liter will be filtered as follows: Determine the volume of fuel filtered by subtracting the ml of fuel remaining from 3.785.

3/ Test shall be performed in accordance with ASTM D5006 or method 5327 or 5340 of Fed-

STD-791. Use the appropriate scale of the refractometer.

TESTING FOR SULFIDES IN BOTTOM WATER

(a) SCOPE. This method describes a procedure for determining the presence of hydrogen sulfide, which is sometimes formed as a result of bacterial action on the sulfates contained in water bottoms in fuel storage tanks.

(b) APPARATUS:

(1) 250 ml conical flask.

(c) MATERIALS:

(1) Dilute (10%) American Chemical Society (ACS) grade, sulfuric or hydrochloric acid.

(2) Lead acetate paper.

(d) SAMPLES. Representative water samples from storage tank bottoms must be taken in a glass bottle. In some cases it will be necessary to take the water sample in a Bacon bomb sampler.

Samples so taken will always be transferred to a glass bottle. To preclude oxidation by air, the filled bottle must be capped immediately. The sample should be tested as soon as possible after sampling to minimize possible changes in the composition of materials in the water.

(e) PROCEDURE.

(1) The sample must be shaken thoroughly just prior to performing the test to make certain that any sediment present is included in the portion of the sample to be tested.

(2) Transfer 100 ml of the shaken sample into a conical flask. Add 20 ml of dilute (10%) chemically pure sulfuric or hydrochloric acid to the flask. Immediately place a piece of lead acetate paper folded in a "V" shape in the neck of the flask. Bring the water to a boil and continue to gently boil for three or four minutes.

(f) REPORT. The presence of sulfides in the sample will be reported if the lead acetate paper shows a light brown to black discoloration.

FUEL ETHANOL (E85) FOR AUTOMOTIVE SPARK-IGNITION ENGINES

TESTING REQUIREMENTS, ASTM D 5798 (Latest Version)

A. Full Specification Testing (A Series), includes all tests listed below (one price for all).

Testing will be performed in accordance with the specified method.

CHARACTERISTIC TEST METHOD, ASTM,

1) Ethanol and Methanol, Volume % D5501

2) Hydrocarbon/Aliphatic Ether Blend Content, Volume %

D4815

3) Vapor Pressure, kPa/PSI D4953, D5190, or D5191

4) Sulfur Content, mg/kg D1266, D2622, D3120, or D5453

5) Higher Alcohols (C3 – C8), Volume % D4815

6) Acidity, Mass % (mg/L) D1613

7) pH D6423

8) Gum Content, Solvent Washed and Unwashed, mg/100mL

D381

9) Inorganic Chloride, mg/kg D512, D2988, or Annex A1

10) Copper, mg/L Modification of D1688 as indicated in D4806

11 ) Water, Mass % E203, or E1064

12 ) Appearance 1)

C. B-2 Series Testing (one price for the following 10 tests):

1) Appearance

2) Water, Mass %

3) Ethanol, Volume %

4) Vapor Pressure, kPa/PSI

5) Higher Alcohols (C3 – C8), Volume %

6) Sulfur Content, mg/kg

7) Acidity, Mass % (mg/L)

8) pH

9) Gum Content, Solvent Washed and Unwashed, mg/100mL

10) Copper, mg/L

NOTES: 1) Visibly free of suspended or precipitated contaminants (clear and bright) determined at ambient temperature or 21 deg C, whichever is higher.

Attachment C

PRICE SHEETS BY LOCATION

CLIN 0001 Baton Rouge, LA

Lab name and address: Name of Lab Manager

Lab Phone Number

Lab Fax Number

SubCLIN: Product Type of Test Est.Sample Price per tests/Series

JP8 A

JP8 B-1 50 $ __________

JP8 B-2 0 $ __________

JP8 C 0 $ __________

JP8 Secure Fuels 0 $ __________

JP8 Individual: UTE

Workmanship $ __________

Color, Saybolt $ __________

Total Acid Number $ __________

Aromatics $ __________

Sulfur, Total Percent $ __________

Sulfur, Mercaptan $ __________

Doctor Test $ __________

Distillation $ __________

Flash Point $ __________

Density, or API Gravity $ __________

Freezing Point $ __________

Viscosity at -20 o C $ __________

Net Heat of Combustion, MJ/kg BTU/lb $ __________

Hydrogen Content $ __________

Naphthalenes $ __________

Smoke Point $ __________

Cetane Index, Calculated $ __________

Copper Strip Corrosion $ __________

Thermal Stability $ __________

Existent Gum $ __________

Particulate Matter $ __________

Filtration Time $ __________

OR Combined Test for Particulate

Matter and Filtration Time

Water Reaction, Interface Rating $ __________

Water Separation Index 9/ $ __________

Fuel Systems Icing Inhibitor $ __________

Fuel Electrical Conductivity $ __________

Color, Visual $ __________

Sulfides in Bottom Water $ __________

SubCLIN Product Task Est. Sample Price per task

JP8 Transportation 50 $

JP8 Vessel Sampling $

JP8 Tank Sampling $

Charge for working outside normal working hours (overtime): $_________ per hour

Normal working hours __________ am - _________ pm Mon. - Fri. Except Holidays

CLIN 0001 Baton Rouge, LA

SubCLIN Product Type of Test Est.Sample Price per tests/Series

JP5 A $ __________

JP5 B-1 4 $ __________

JP5 C $ __________

JP5 Individual:

Workmanship $ __________

Color, Saybolt $ __________

Total Acid Number $ __________

Aromatics $ __________

Sulfur, Mercaptan, mass percent $ __________

OR Doctor Test $ __________

Sulfur, Total Mass Percent $ __________

Distillation (4) $ __________

Flash Point (5) $ __________

Density, or API Gravity $ __________

Freezing Point $ __________

Viscosity at -20 o C $ __________

Heating Value, Net Heat of Combustion $ __________

Cetane Index, Calculated (6) $ __________

Hydrogen Content, Mass Percent $ __________

Smoke Point $ __________

Copper Strip Corrosion $ __________

Thermal Stability $ __________

Existent Gum $ __________

Particulate Matter (Solids) $ __________

Filtration Time $ __________

OR Combined Test for Particulate

Matter and Filtration Time

Micro-separometer Rating $ __________

Fuel Systems Icing Inhibitor $ __________

Visual (Color) $ __________

Sulfides in Bottom Water $_________

JP5 Transportation 4 $

JP5 Vessel Sampling $

JP5 Tank Sampling $

CLIN 0004 Lockhart, MS

JP8 A 0

JP8 B-1 15 $ __________

JP8 B-2 0 $ __________

JP8 C 0 $ __________

JP8 Secure Fuels 0 $ __________

JP8 Individual:

Workmanship 0 $ __________

Color, Saybolt 0 $ __________

Total Acid Number 0 $ __________

Aromatics 0 $ __________

Sulfur, Total Percent $ __________

Sulfur, Mercaptan 0 $ __________

Doctor Test 0 $ __________

Distillation 0 $ __________

Flash Point 0 $ __________

Density, or API Gravity 0 $ __________

Freezing Point 0 $ __________

Viscosity at -20 o C 0 $ __________

Net Heat of Combustion, MJ/kg BTU/lb 0 $ __________

Hydrogen Content 0 $ __________

Naphthalenes 0 $ __________

Smoke Point 0 $ __________

Cetane Index, Calculated 0 $ __________

Copper Strip Corrosion 0 $ __________

Thermal Stability $ __________

Existent Gum 0 $ __________

Particulate Matter 0 $ __________

Filtration Time 0 $ __________

OR Combined Test for Particulate

Matter and Filtration Time

0 $ __________

Water Reaction, Interface Rating 0 $ __________

Water Separation Index 9/ 0 $ __________

Fuel Systems Icing Inhibitor 0 $ __________

Fuel Electrical Conductivity 0 $ __________

Color, Visual 0 $ __________

Sulfides in Bottom Water 0 $ __________

JP8 Transportation 15 $

JP8 Vessel Sampling $

JP8 Tank Sampling $

CLIN 0005 Montgomery, AL

JP8 B-1 25 $ __________

JP8 B-2 0 $ __________

JP8 C 0 $ __________

JP8 Secure Fuels 0 $ __________

JP8 Individual:

Workmanship 0 $ __________

Color, Saybolt 0 $ __________

Total Acid Number 0 $ __________

Aromatics 0 $ __________

Sulfur, Total Percent $ __________

Sulfur, Mercaptan 0 $ __________

Doctor Test 0 $ __________

Distillation 0 $ __________

Flash Point 0 $ __________

Density, or API Gravity 0 $ __________

Freezing Point 0 $ __________

Viscosity at -20 o C 0 $ __________

Net Heat of Combustion, MJ/kg BTU/lb 0 $ __________

Hydrogen Content 0 $ __________

Naphthalenes 0 $ __________

Smoke Point 0 $ __________

Cetane Index, Calculated 0 $ __________

Copper Strip Corrosion 0 $ __________

Thermal Stability $ __________

Existent Gum 0 $ __________

Particulate Matter 0 $ __________

Filtration Time 0 $ __________

OR Combined Test for Particulate

Matter and Filtration Time

0 $ __________

Water Reaction, Interface Rating 0 $ __________

Water Separation Index 9/ 0 $ __________

Fuel Systems Icing Inhibitor 0 $ __________

Fuel Electrical Conductivity 0 $ __________

Color, Visual 0 $ __________

Sulfides in Bottom Water 0 $ __________

JP8 Transportation 25 $ __________

JP8 Vessel Sampling $ __________

JP8 Tank Sampling $ __________

CLIN 0011 Salt Lake City, UT

JP8 B-1 18 $ __________

JP8 B-2 0 $ __________

JP8 C 0 $ __________

JP8 Secure Fuels 0 $ __________

JP8 Individual:

Workmanship $ __________

Color, Saybolt $ __________

Total Acid Number $ __________

Aromatics $ __________

Sulfur, Total Percent $ __________

Sulfur, Mercaptan $ __________

Doctor Test $ __________

Distillation $ __________

Flash Point $ __________

Density, or API Gravity $ __________

Freezing Point $ __________

Viscosity at -20 o C $ __________

Net Heat of Combustion, MJ/kg BTU/lb $ __________

Hydrogen Content $ __________

Naphthalenes $ __________

Smoke Point $ __________

Cetane Index, Calculated $ __________

Copper Strip Corrosion $ __________

Thermal Stability $ __________

Existent Gum $ __________

Particulate Matter $ __________

Filtration Time $ __________

OR Combined Test for Particulate

Matter and Filtration Time

Water Reaction, Interface Rating $ __________

Water Separation Index 9/ $ __________

Fuel Systems Icing Inhibitor $ __________

Fuel Electrical Conductivity $ __________

Color, Visual $ __________

JP8 Transportation 18 $ __________

CLIN 0012 Breman, GA

JP8 B-1 25 $ __________

JP8 B-2 0 $ __________

JP8 C 0 $ __________

JP8 Secure Fuels 0 $ __________

JP8 Individual:

Workmanship $ __________

Color, Saybolt $ __________

Total Acid Number $ __________

Aromatics $ __________

Sulfur, Total Percent $ __________

Sulfur, Mercaptan $ __________

Doctor Test $ __________

Distillation $ __________

Flash Point $ __________

Density, or API Gravity $ __________

Freezing Point $ __________

Viscosity at -20 o C $ __________

Net Heat of Combustion, MJ/kg BTU/lb $ __________

Hydrogen Content $ __________

Naphthalenes $ __________

Smoke Point $ __________

Cetane Index, Calculated $ __________

Copper Strip Corrosion $ __________

Thermal Stability $ __________

Existent Gum $ __________

Particulate Matter $ __________

Filtration Time $ __________

OR Combined Test for Particulate

Matter and Filtration Time

Water Reaction, Interface Rating $ __________

Water Separation Index 9/ $ __________

Fuel Systems Icing Inhibitor $ __________

Fuel Electrical Conductivity $ __________

Color, Visual $ __________

JP8 Transportation 25 $ __________

JP8 Vessel Sampling $ __________

CLIN 0017 Tulsa, OK

JP8 B-1 4 $ __________

JP8 B-2 0 $ __________

JP8 C 0 $ __________

JP8 Secure Fuels 0 $ __________

JP8 Individual: 4

Workmanship 4 $ __________

Color, Saybolt 4 $ __________

Total Acid Number 4 $ __________

Aromatics 4 $ __________

Sulfur, Total Percent 4 $ __________

Sulfur, Mercaptan 4 $ __________

Doctor Test 4 $ __________

Distillation 4 $ __________

Flash Point 4 $ __________

Density, or API Gravity 4 $ __________

Freezing Point 4 $ __________

Viscosity at -20 o C 4 $ __________

Net Heat of Combustion, MJ/kg BTU/lb 4 $ __________

Hydrogen Content 4 $ __________

Naphthalenes 4 $ __________

Smoke Point 4 $ __________

Cetane Index, Calculated 4 $ __________

Copper Strip Corrosion 4 $ __________

Thermal Stability 4 $ __________

Existent Gum 4 $ __________

Particulate Matter 4 $ __________

Filtration Time 4 $ __________

OR Combined Test for Particulate

Matter and Filtration Time

4 $ __________

Water Reaction, Interface Rating 4 $ __________

Water Separation Index 9/ 4 $ __________

Fuel Systems Icing Inhibitor 4 $ __________

Fuel Electrical Conductivity 4 $ __________

Color, Visual 4 $ __________

Sulfides in Bottom Water 4 $ __________

JP8 Transportation 10 $ __________

CLIN 0023 Columbus, GA

JP8 B-1 12 $ __________

JP8 B-2 0 $ __________

JP8 C 0 $ __________

JP8 Secure Fuels 0 $ __________

JP8 Individual: 4

Workmanship $ __________

Color, Saybolt $ __________

Total Acid Number $ __________

Aromatics $ __________

Sulfur, Total Percent $ __________

Sulfur, Mercaptan $ __________

Doctor Test $ __________

Distillation $ __________

Flash Point $ __________

Density, or API Gravity $ __________

Freezing Point $ __________

Viscosity at -20 o C $ __________

Net Heat of Combustion, MJ/kg BTU/lb $ __________

Hydrogen Content $ __________

Naphthalenes $ __________

Smoke Point $ __________

Cetane Index, Calculated $ __________

Copper Strip Corrosion $ __________

Thermal Stability $ __________

Existent Gum $ __________

Particulate Matter $ __________

Filtration Time $ __________

OR Combined Test for Particulate

Matter and Filtration Time

Water Reaction, Interface Rating $ __________

Water Separation Index 9/ $ __________

Fuel Systems Icing Inhibitor $ __________

Fuel Electrical Conductivity $ __________

Color, Visual $ __________

CLIN 0024 Macon, GA

JP8 B-1 10 $ __________

JP8 B-2 10 $ __________

JP8 C 0 $ __________

JP8 Secure Fuels 0 $ __________

JP8 Individual: 36

Workmanship $ __________

Color, Saybolt $ __________

Total Acid Number $ __________

Aromatics $ __________

Sulfur, Total Percent $ __________

Sulfur, Mercaptan $ __________

Doctor Test $ __________

Distillation $ __________

Flash Point $ __________

Density, or API Gravity $ __________

Freezing Point $ __________

Viscosity at -20 o C $ __________

Net Heat of Combustion, MJ/kg BTU/lb $ __________

Hydrogen Content $ __________

Naphthalenes $ __________

Smoke Point $ __________

Cetane Index, Calculated $ __________

Copper Strip Corrosion $ __________

Thermal Stability $ __________

Existent Gum $ __________

Particulate Matter $ __________

Filtration Time $ __________

OR Combined Test for Particulate

Matter and Filtration Time

Water Reaction, Interface Rating $ __________

Water Separation Index 9/ $ __________

Fuel Systems Icing Inhibitor $ __________

Fuel Electrical Conductivity $ __________

Color, Visual $ __________

JP8 Transportation 20 $ __________

JP8 Vessel Sampling $ __________

JP8 Tank Sampling $ __________

CLIN 0029 Alamogordo, NM

JP8 B-1 25 $ __________

JP8 B-2 0 $ __________

JP8 C 0 $ __________

JP8 Secure Fuels 0 $ __________

JP8 Individual: 20

Workmanship $ __________

Color, Saybolt $ __________

Total Acid Number $ __________

Aromatics $ __________

Sulfur, Total Percent $ __________

Sulfur, Mercaptan $ __________

Doctor Test $ __________

Distillation $ __________

Flash Point $ __________

Density, or API Gravity $ __________

Freezing Point $…